1. 49-0028
NaVO3
Groupa 31,59
Dexp. Dcal. d(D) h k l
6.3000 6.3495 -.0495 3 0 0
4.3800 4.3901 -.0101 1 0 2
4.2200 4.2116 .0084 4 0 1
3.1900 3.1904 -.0004 1 1 0
2.9700 2.9709 -.0009 1 0 3
2.9000 2.9013 -.0013 2 1 1
2.7200 2.7212 -.0012 7 0 0
2.6100 2.6053 .0047 7 0 1
2.6000 2.5964 .0036 6 0 2
2.5400 2.5430 -.0030 4 0 3
2.3800 2.3791 .0009 5 1 1
1.7970 1.7966 .0004 1 0 5
1.7540 1.7549 -.0009 10 0 2
a=19.05 b= 3.2361 c= 9.023
da= .01 db= .0001 dc= .006
V= 556.2
2. 49-0029
Rb2Cu{VO3}4
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
5.4500 5.4101 .0399 0 1 3
4.0900 4.0916 -.0016 0 2 1
3.8800 3.8829 -.0029 0 2 2
3.8000 3.7977 .0023 0 1 5
3.5900 3.5964 -.0064 0 2 3
3.3300 3.3313 -.0013 1 1 0
3.2800 3.2844 -.0044 0 2 4
3.1800 3.1798 .0002 1 1 2
3.0500 3.0471 .0029 0 0 7
2.7600 2.7561 .0039 0 3 1
2.7400 2.7394 .0006 1 2 0
2.4400 2.4367 .0033 1 2 4
1.9320 1.9311 .0009 1 1 9
1.7380 1.7384 -.0004 0 1 12
1.6390 1.6391 -.0001 2 1 5
a= 3.6340 b= 8.338 c=21.33
da= .0003 db= .005 dc= .01
V= 646.3
3. 49-0030
Cs2Cu{VO3}4
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.6100 5.6190 -.0090 -1 1 1
4.1100 4.1067 .0033 1 2 1
3.5900 3.5973 -.0073 -1 1 2
3.4100 3.4115 -.0015 -3 0 1
3.2300 3.2279 .0021 2 0 2
3.0500 3.0492 .0008 3 2 0
2.8300 2.8322 -.0022 3 2 1
2.7700 2.7694 .0006 -3 0 2
2.6000 2.6004 -.0004 -1 3 2
2.4200 2.4195 .0005 -2 3 2
1.9610 1.9608 .0002 -4 0 3
1.7810 1.7809 .0001 2 4 3
1.6980 1.6980 -.0000 -3 4 3
a= 11.16 b= 10.6447 c= 8.063 beta= 91.47
da=.01 db=.0004 dc= .005 dbeta=.04
V= 957.9
4. 49-0030
Cs2Cu{VO3}4
Triklin
Dexp Dcal d(D) h k l
5.6100 5.6095 .0005 -1 1 0
4.1100 4.1102 -.0002 -1 1 1
3.5900 3.5890 .0010 -1 -1 1
3.4100 3.4080 .0020 0 2 0
3.2300 3.2315 -.0015 -2 1 0
3.0500 3.0506 -.0006 2 0 0
2.8300 2.8306 -.0006 -2 1 1
2.7700 2.7723 -.0023 0 -2 2
2.6000 2.5992 .0008 2 -1 2
2.4200 2.4200 .0000 -1 3 0
1.9610 1.9612 -.0002 2 2 0
1.7810 1.7807 .0003 -2 -1 3
1.6980 1.6981 -.0001 -2 2 3
A= 6.5405 DA= .0004
B= 7.4310 DB= .0003
C= 7.54950 DC= .00008
GAMMA=111.025 DGAMMA= .05
BETA = 83.73 DBETA = .01
ALPHA=102.22 DALPHA= .02
V= 334.5
5. 49-0031
Ag2Cu{VO3}4
Triklin
Dexp Dcal d(D) h k l
3.7500 3.7507 -.0007 0 1 1
3.6700 3.6678 .0022 0 -1 1
3.2800 3.2801 -.0001 -1 1 1
3.1700 3.1675 .0025 2 0 0
3.0900 3.0882 .0018 -1 -1 1
3.0700 3.0718 -.0018 1 -2 1
2.9000 2.9014 -.0014 -2 3 0
2.4300 2.4297 .0003 -2 2 1
2.4200 2.4201 -.0001 2 3 0
2.1500 2.1503 -.0003 -3 1 0
1.8930 1.8930 -.0000 0 -1 2
1.8330 1.8327 .0003 -1 7 1
1.8170 1.8167 .0003 2 -6 1
1.7930 1.7930 -.0000 1 -2 2
A= 6.4575 DA= .0005
B= 14.413 DB= .001
C= 3.847 DC= .001
GAMMA=101.15 DGAMMA= .05
BETA = 89.60 DBETA = .01
ALPHA= 87.61 DALPHA= .02
V= 351.0
6. 49-0171
NaGaV6O17*H2O
Triklin
Dexp Dcal d(D) h k l
7.9000 7.8979 .0021 1 0 0
5.1000 5.0941 .0059 0 1 1
3.5100 3.5094 .0006 -2 -1 1
3.3300 3.3307 -.0007 1 1 2
3.2100 3.2103 -.0003 2 0 1
3.0400 3.0409 -.0009 -1 0 3
2.8140 2.8159 -.0019 -2 1 0
2.6110 2.6102 .0008 0 2 0
2.5260 2.5247 .0013 2 0 2
2.2460 2.2459 .0001 0 2 3
2.0320 2.0322 -.0002 2 -1 2
1.8360 1.8359 .0001 -4 1 2
1.5750 1.5751 -.0001 3 3 2
1.5570 1.5571 -.0001 -1 -3 2
1.5220 1.5220 .0000 0 -1 5
A= 8.5258 DA= .0004
B= 5.5105 DB= .0005
C= 9.3021 DC= .0002
GAMMA= 78.9750 DGAMMA= .0003
BETA =106.361 DBETA = .002
ALPHA= 78.909 DALPHA= .003
V=397.3
7. 49-0172
NaGaV6O17
Triklin
Dexp Dcal d(D) h k l
7.9000 7.8990 .0010 1 0 0
5.0000 4.9998 .0002 0 1 0
3.5000 3.5005 -.0005 0 -1 2
3.3000 3.3005 -.0005 2 1 0
3.1700 3.1703 -.0003 -2 -1 1
3.0200 3.0187 .0013 2 1 1
2.6330 2.6330 .0000 3 0 0
2.5260 2.5269 -.0009 -3 0 1
2.3800 2.3786 .0014 -2 1 2
2.2090 2.2084 .0006 0 0 4
2.1320 2.1325 -.0005 -3 1 1
1.9410 1.9415 -.0005 -3 -1 3
A= 7.959 DA= .001
B= 5.067 DB= .001
C= 8.8856 DC= .0008
GAMMA= 82.952 DGAMMA= .003
BETA = 91.06 DBETA = .02
ALPHA= 96.21 DALPHA= .02
V= 353.5
8. 49-0173
NaGaV6O17*4H2O
Triklin
Dexp Dcal d(D) h k l
9.6000 9.6004 -.0004 1 0 0
5.7000 5.6879 .0121 0 1 1
4.4000 4.3914 .0086 -2 -1 1
3.8700 3.8674 .0026 -1 -2 1
3.6500 3.6458 .0042 -2 -2 1
3.5300 3.5316 -.0016 0 -2 1
3.3800 3.3809 -.0009 2 0 1
3.2500 3.2572 -.0072 -1 0 2
3.0800 3.0815 -.0015 -3 -2 1
2.8810 2.8813 -.0003 -2 -3 1
2.7640 2.7642 -.0002 -3 1 0
2.5220 2.5230 -.0010 -4 -2 1
A= 10.525 DA= .001
B= 10.214 DB= .003
C= 6.542 DC= .002
GAMMA= 71.816 DGAMMA= .02
BETA =103.93 DBETA = .03
ALPHA= 85.588 DALPHA= .007
V= 639.6
9. 49-0674
Na10.42Si2.5VO5.08*xH2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
14.4300 14.4134 .0166 -1 0 1
11.9800 11.9854 -.0054 1 1 0
10.9700 10.9498 .0202 1 0 1
6.0700 6.0672 .0028 -1 0 3
4.7900 4.7896 .0004 0 2 3
4.2000 4.2002 -.0002 2 1 3
3.9600 3.9602 -.0002 4 0 1
3.5800 3.5797 .0003 2 4 1
2.8800 2.8800 -.0000 3 5 0
a= 17.955 b= 16.622 c= 18.250 beta= 105.549
da=.008 db= .002 dc=.009 dbeta=.007
V= 5247
10. 49-0685
{VO}3{HAsO4}2*5H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
6.8900 6.9069 -.0169 1 0 1
4.4400 4.4441 -.0041 2 1 0
4.0400 4.0437 -.0037 1 1 2
3.4500 3.4535 -.0035 2 0 2
3.2700 3.2712 -.0012 2 1 2
3.1800 3.1768 .0032 0 1 3
3.0700 3.0731 -.0031 -1 3 1
3.0200 3.0210 -.0010 -3 1 1
2.7700 2.7657 .0043 3 2 0
2.7200 2.7208 -.0008 2 0 3
2.7000 2.7007 -.0007 -3 1 2
2.4000 2.3993 .0007 4 1 0
a=9.881 b= 10.203 c= 10.036 beta=92.16
da=.003 db=.007 dc=.007 dbeta=.09
V= 1011
11. 49-0686
{VO}3{As2O7}2
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
9.0600 9.0652 -.0052 0 0 1
6.0500 6.0314 .0186 1 1 0
4.6400 4.6419 -.0019 1 1 1
4.1600 4.1581 .0019 0 1 2
3.6800 3.6787 .0013 1 2 1
3.2600 3.2509 .0091 0 3 1
3.1500 3.1500 .0000 1 3 0
3.0400 3.0409 -.0009 2 1 1
2.9300 2.9266 .0034 -1 1 3
2.7100 2.7121 -.0021 -1 3 2
2.6000 2.5985 .0015 1 0 3
2.2800 2.2823 -.0023 0 3 3
a= 7.583 b= 10.45 c= 9.306 beta= 103.057
da=.009 db= .02 dc=.004 dbeta=.008
V= 718
Triklin
Dexp Dcal d(D) h k l
9.0600 9.0609 -.0009 1 0 0
6.0500 6.0520 -.0020 -1 1 0
4.6400 4.6420 -.0020 2 0 1
4.1600 4.1598 .0002 2 1 0
3.6800 3.6799 .0001 0 1 2
3.2600 3.2601 -.0001 1 -2 3
3.1500 3.1507 -.0007 3 0 1
3.0400 3.0403 -.0003 2 2 1
2.9300 2.9297 .0003 3 1 1
2.7100 2.7099 .0001 -1 3 0
2.6000 2.5999 .0001 3 0 3
2.2800 2.2800 -.0000 -3 0 2
A= 9.460 DA= .005
B= 9.389 DB= .003
C= 10.746 DC= .009
GAMMA= 91.601 DGAMMA= .001
BETA = 73.93 DBETA = .07
ALPHA=111.05 DALPHA= .07
V= 853.2
12. 49-0689
Cu3V2O8
Rombik
Groupa 50
Dexp. Dcal. d(D) h k l
5.9000 5.8983 .0017 4 0 0
4.2300 4.2323 -.0023 0 2 0
3.9700 3.9837 -.0137 2 2 0
3.1200 3.1314 -.0114 7 1 0
3.1000 3.1050 -.0050 1 1 1
2.8900 2.8808 .0092 6 2 0
2.8000 2.8016 -.0016 1 3 0
2.6200 2.6208 -.0008 1 2 1
2.5600 2.5595 .0005 6 0 1
2.4500 2.4500 .0000 6 1 1
2.4200 2.4197 .0003 8 2 0
2.4100 2.4074 .0026 4 2 1
a=23.59 b= 8.465 c= 3.372
da= .01 db= .003 dc= .004
V= 673
Triklin
Dexp. Dcal. d(D) h k l
5.9000 5.9000 .0000 -1 -2 0
4.2300 4.2300 .0000 3 0 0
3.9700 3.9697 .0003 3 -1 0
3.1200 3.1169 .0031 1 -4 0
3.1000 3.1000 .0000 -3 -3 0
2.8900 2.8901 -.0001 -2 -1 1
2.8000 2.8015 -.0015 4 -2 0
2.6200 2.6183 .0017 -4 -3 0
2.5600 2.5602 -.0002 -1 -3 1
2.4500 2.4500 .0000 0 4 1
2.4200 2.4206 -.0006 -3 -2 1
2.4100 2.4102 -.0002 2 -3 1
A= 12.71007 DA= .00005
B= 13.0573 DB= .0002
C= 3.4534 DC= .0004
GAMMA= 87.2604 DGAMMA= .0009
BETA = 88.138 DBETA = .006
ALPHA= 85.99 DALPHA= .01
V= 570.8
13. 49-0690
beta-Cu3V2O8
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
4.2300 4.2167 .0133 3 0 2
3.9000 3.8927 .0073 0 0 4
3.5500 3.5586 -.0086 -2 0 3
3.2400 3.2370 .0030 1 0 5
3.1300 3.1318 -.0018 1 1 0
3.1000 3.1000 -.0000 4 0 3
2.9000 2.9023 -.0023 -3 0 3
2.8200 2.8199 .0001 2 1 2
2.6900 2.6917 -.0017 1 0 6
2.6200 2.6216 -.0016 5 0 2
2.5700 2.5694 .0006 3 1 2
2.4600 2.4635 -.0035 -3 1 1
A= 13.126 DA= .003
B= 3.234 DB= .002
C= 16.1916 DC= .0007
BETA = 74.09 DBETA = .02
V=661.7
14. 49-0754
K3V2{O2}4OH*H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.4400 5.4509 -.0109 1 1 0
5.1700 5.1473 .0227 -1 0 2
4.8600 4.8630 -.0030 -2 0 1
3.5600 3.5649 -.0049 1 1 2
3.4600 3.4592 .0008 -2 1 2
3.2900 3.2888 .0012 0 2 0
3.2200 3.2160 .0040 -2 0 3
3.0800 3.0835 -.0035 1 0 3
2.9700 2.9662 .0038 -3 1 1
2.7700 2.7714 -.0014 -1 2 2
2.6000 2.5991 .0009 1 2 2
2.5200 2.5178 .0022 3 0 2
2.4300 2.4315 -.0015 -4 0 2
2.2800 2.2807 -.0007 -4 1 2
2.1500 2.1503 -.0003 3 0 3
a= 10.0036 b= 6.58 c=10.81 beta= 103.2
da=.0008 db=,01 dc=.02 dbeta=.1
V= 692
Triklin
Dexp Dcal d(D) h k l
5.4400 5.4433 -.0033 0 1 1
5.1700 5.1688 .0012 1 1 0
4.8600 4.8617 -.0017 0 -1 1
3.5600 3.5618 -.0018 1 0 2
3.4600 3.4614 -.0014 1 1 2
3.2900 3.2909 -.0009 -1 2 0
3.2200 3.2223 -.0023 0 1 2
3.0800 3.0761 .0039 1 -1 2
2.9700 2.9692 .0008 0 -1 2
2.7700 2.7710 -.0010 -1 -2 1
2.6000 2.6004 -.0004 -1 0 2
2.5200 2.5188 .0012 -1 1 2
2.4300 2.4308 -.0008 0 -2 2
2.2800 2.2798 .0002 3 1 1
2.1500 2.1504 -.0004 3 -1 1
A= 6.9668 DA= .0005
B= 8.0760 DB= .0006
C= 7.298 DC= .005
GAMMA= 83.30 DGAMMA= .02
BETA = 67.53 DBETA = .01
ALPHA= 81.41 DALPHA= .01
V= 374.4
15. 49-0755
{NH4}2KVO2F4*H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.1000 5.0871 .0129 1 1 0
4.4900 4.4881 .0019 -1 0 2
4.4000 4.3981 .0019 0 1 2
4.1700 4.1786 -.0086 1 1 1
3.4500 3.4466 .0034 1 0 2
3.1400 3.1361 .0039 0 1 3
3.1200 3.1204 -.0004 -1 1 3
2.8300 2.8298 .0002 -2 1 2
2.5600 2.5622 -.0022 -1 0 4
2.3100 2.3100 -.0000 0 4 0
2.2500 2.2508 -.0008 0 4 1
2.2000 2.1991 .0009 0 2 4
a= 6.316432 b= 9.240047 c= 10.367250 beta= 105.25
da=.001 db=.005 dc=.001 dbeta=.04
V= 583.7
Triklin
Dexp Dcal d(D) h k l
5.1000 5.1056 -.0056 1 0 1
4.4900 4.4901 -.0001 1 1 1
4.4000 4.3999 .0001 -1 -1 1
4.1700 4.1700 -.0000 2 1 0
3.4500 3.4501 -.0001 -2 -1 1
3.1400 3.1410 -.0010 -1 2 0
3.1200 3.1214 -.0014 0 -2 1
2.8300 2.8299 .0001 -1 2 1
2.5600 2.5613 -.0013 3 2 0
2.3100 2.3101 -.0001 2 -1 2
2.2500 2.2493 .0007 0 -3 1
2.2000 2.1981 .0019 1 -2 2
A= 8.984 DA= .002
B= 7.461 DB= .002
C= 6.2716 DC= .0001
GAMMA= 77.833 DGAMMA= .005
BETA = 89.66 DBETA = .01
ALPHA= 88.67 DALPHA= .01
V= 410.8
16. 49-0756
{NH4}K2VO2F4*H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.8600 5.8584 .0016 1 1 1
4.9800 4.9851 -.0051 2 0 0
4.6900 4.6800 .0100 1 1 2
3.4500 3.4471 .0029 -2 1 2
3.2900 3.2907 -.0007 3 0 1
3.1400 3.1402 -.0002 2 2 1
2.9900 2.9921 -.0021 0 2 3
2.8800 2.8797 .0003 3 1 2
2.7700 2.7687 .0013 0 3 0
2.4900 2.4897 .0003 -2 1 4
2.2100 2.2096 .0004 -2 2 4
2.0500 2.0503 -.0003 0 4 1
1.9000 1.9002 -.0002 3 2 5
a= 10.010 b= 8.3062 c= 12.996 beta= 84.86
da=.004 db=.0004 dc=.007 dbeta=.07
V= 1076
Triklin
Dexp Dcal d(D) h k l
5.8600 5.8604 -.0004 0 1 1
4.9800 4.9799 .0001 0 -1 1
4.6900 4.6898 .0002 -1 0 1
3.4500 3.4508 -.0008 1 0 1
3.2900 3.2904 -.0004 -1 3 0
3.1400 3.1395 .0005 -1 1 2
2.9900 2.9883 .0017 1 3 0
2.8800 2.8800 .0000 0 4 1
2.7700 2.7691 .0009 -1 -1 2
2.4900 2.4899 .0001 0 -2 2
2.2100 2.2099 .0001 -2 4 1
2.0500 2.0501 -.0001 0 1 3
A= 5.5165 DA= .0003
B= 12.1899 DB= .0002
C= 6.5154 DC= .0003
GAMMA= 99.840 DGAMMA= .006
BETA =109.21 DBETA = .01
ALPHA= 76.0472 DALPHA= .0008
V= 399.53
17. 49-0821
KPbVO4
Rombik
Groupa 46,74
Dexp. Dcal. d(D) h k l
5.0000 4.9951 .0049 1 1 0
3.3900 3.3949 -.0049 2 1 1
3.0800 3.0771 .0029 3 0 1
3.0400 3.0404 -.0004 2 0 2
2.9000 2.9032 -.0032 3 1 0
2.3100 2.3091 .0009 3 1 2
2.2100 2.2107 -.0007 4 1 1
2.1100 2.1103 -.0003 2 1 3
2.1000 2.1005 -.0005 3 2 1
1.7820 1.7821 -.0001 2 0 4
1.6980 1.6974 .0006 4 2 2
a=10.091 b= 5.749 c= 7.620
da= .003 db= .009 dc= .002
V= 442
Triklin
Dexp Dcal d(D) h k l
5.0000 4.9995 .0005 1 0 0
3.3900 3.3916 -.0016 -1 0 1
3.0800 3.0809 -.0009 1 -2 1
3.0400 3.0394 .0006 1 -2 0
2.9000 2.9004 -.0004 -1 1 1
2.3100 2.3107 -.0007 0 0 2
2.2100 2.2098 .0002 -1 2 1
2.1100 2.1095 .0005 -1 -1 2
2.1000 2.1002 -.0002 2 1 0
1.7820 1.7820 -.0000 -1 -3 1
1.6980 1.6979 .0001 2 0 2
A= 5.2822 DA= .0001
B= 6.8633 DB= .0004
C= 4.9670 DC= .0004
GAMMA=108.84 DGAMMA= .03
BETA = 83.153 DBETA = .004
ALPHA=111.50 DALPHA= .01
V= 158.57
18. 49-0822
KPb4{VO4}3
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
4.3400 4.3413 -.0013 2 1 0
4.1100 4.1113 -.0013 0 1 2
3.7000 3.7006 -.0006 -1 0 2
3.4100 3.4128 -.0028 1 2 2
3.2900 3.2909 -.0009 3 0 1
3.0100 3.0098 .0002 -1 2 2
2.9800 2.9874 -.0074 0 0 3
2.9100 2.9100 .0000 -2 0 2
2.2200 2.2201 -.0001 2 3 3
2.0800 2.0798 .0002 2 2 4
1.9810 1.9809 .0001 5 0 1
1.9330 1.9330 .0000 -2 4 2
1.8780 1.8779 .0001 0 5 2
A= 9.91787 DA= .00001
B= 10.34329 DB= .00006
C= 9.29069 DC= .00003
BETA = 74.7240 DBETA = .0002
V=919.3
Triklin
Dexp Dcal d(D) h k l
4.3400 4.3394 .0006 -1 1 1
4.1100 4.1092 .0008 0 -1 1
3.7000 3.7001 -.0001 1 -1 1
3.4100 3.4084 .0016 -2 1 0
3.2900 3.2884 .0016 0 0 2
3.0100 3.0105 -.0005 -1 0 2
2.9800 2.9815 -.0015 -1 1 2
2.9100 2.9108 -.0008 2 -1 1
2.2200 2.2202 -.0002 2 -2 1
2.0800 2.0801 -.0001 1 3 1
1.9810 1.9809 .0001 1 2 3
1.9330 1.9329 .0001 -2 1 3
1.8780 1.8780 .0000 -2 3 0
A= 8.01 DA= .01
B= 6.501 DB= .002
C= 6.7621 DC= .0005
GAMMA= 90.54 DGAMMA= .08
BETA = 88.46 DBETA = .07
ALPHA= 76.67 DALPHA= .03
V= 342.6
19. 49-0830
H2GeMoW10VO40*21*H2O
Triklin
Dexp Dcal d(D) h k l
10.9200 10.9374 -.0174 0 1 0
10.0700 10.0689 .0011 1 1 0
8.9200 8.9255 -.0055 1 0 1
5.4700 5.4687 .0013 0 2 0
4.8900 4.8913 -.0013 0 -1 2
4.4200 4.4192 .0008 -1 2 1
3.7200 3.7213 -.0013 3 2 3
3.1900 3.1891 .0009 3 4 3
3.1500 3.1451 .0049 4 2 1
2.9900 2.9905 -.0005 2 0 4
2.9400 2.9394 .0006 -1 -2 3
2.6000 2.5993 .0007 3 0 4
2.5100 2.5103 -.0003 -3 -4 1
2.3600 2.3603 -.0003 2 1 6
A= 12.670 DA= .003
B= 13.76 DB= .01
C= 15.45 DC= .01
GAMMA= 60.43 DGAMMA= .04
BETA = 71.48 DBETA = .06
ALPHA= 60.53 DALPHA= .04
V=2030
20. 49-0855
NaV3O8*xH2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
10.8740 10.8746 -.0006 0 0 1
9.9356 9.9350 .0006 1 1 0
7.8233 7.8236 -.0003 1 1 1
3.4478 3.4478 -.0000 1 4 0
3.1523 3.1523 .0000 -4 0 1
1.7995 1.7995 .0000 3 7 2
a= 14.07 b= 14.238 c= 11.03 beta= 80.2
da=.042 db=.004 dc= .08 dbeta=.2
V= 2179
21. 49-0860
Cs2B{OH}V6*O17*3.5H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.6000 5.5891 .0109 1 0 1
4.8000 4.8079 -.0079 1 1 0
4.5000 4.4897 .0103 1 1 1
3.5300 3.5252 .0048 0 0 2
3.2400 3.2405 -.0005 2 0 1
3.1200 3.1212 -.0012 2 0 0
2.3680 2.3669 .0011 0 3 1
2.1410 2.1421 -.0011 -1 3 1
1.9850 1.9857 -.0007 2 3 1
1.9180 1.9192 -.0012 2 2 3
1.4350 1.4348 .0002 -4 0 1
1.4150 1.4149 .0001 -1 5 1
1.3660 1.3660 .0000 -3 0 3
a= 6.550 b= 7.5383 c=7.398 beta= 72.3
da=.007 db=.0006 dc=.002 dbeta=.09
V= 348.1
22. 49-0861
Cs2B{OH}V6O17*0.5H2O
Triklin
Dexp Dcal d(D) h k l
9.7000 9.6955 .0045 1 0 0
5.7000 5.6985 .0015 0 1 1
4.8000 4.8024 -.0024 0 -1 1
4.5000 4.5007 -.0007 1 1 1
3.5700 3.5695 .0005 -1 1 2
3.5300 3.5312 -.0012 0 1 2
3.3000 3.3016 -.0016 1 2 0
3.1200 3.1199 .0001 -3 1 1
2.9730 2.9722 .0008 1 -2 1
2.6220 2.6215 .0005 2 2 1
2.1510 2.1511 -.0001 -4 2 0
1.9250 1.9250 .0000 -4 1 3
1.8060 1.8060 -.0000 5 0 1
A= 9.9394 DA= .0001
B= 7.549 DB= .003
C= 7.5747 DC= .0002
GAMMA= 98.99 DGAMMA= .01
BETA =100.518 DBETA = .005
ALPHA= 78.876 DALPHA= .002
V= 544.0
23. 49-0862
Cs4B2V12O35
Triklin
Dexp Dcal d(D) h k l
3.6900 3.6906 -.0006 1 1 0
3.5700 3.5723 -.0023 1 1 1
2.8540 2.8546 -.0006 1 -1 1
2.8140 2.8152 -.0012 2 0 1
2.5880 2.5873 .0007 0 2 0
2.4680 2.4693 -.0013 -1 -1 1
2.2900 2.2892 .0008 -2 2 1
2.2220 2.2220 .0000 0 2 2
1.9030 1.9018 .0012 3 1 1
1.7690 1.7690 .0000 -2 0 2
1.7590 1.7595 -.0005 -1 3 0
1.7570 1.7571 -.0001 -1 3 2
1.6470 1.6471 -.0001 -4 1 0
1.5350 1.5350 -.0000 3 -1 2
A= 6.6343 DA= .0002
B= 5.7538 DB= .0003
C= 5.017 DC= .001
GAMMA= 99.91 DGAMMA= .01
BETA = 87.46 DBETA = .01
ALPHA= 66.7989 DALPHA= .0007
V= 172.06
24. 49-2042
C3H10NO3V
Triklin
Dexp Dcal d(D) h k l
11.2000 11.1510 .0490 1 0 0
7.8300 7.8079 .0221 0 1 1
6.6900 6.7057 -.0157 0 -1 1
6.6300 6.6329 -.0029 -1 2 0
5.7600 5.7547 .0053 -1 2 1
5.5700 5.5755 -.0055 2 0 0
5.0400 5.0389 .0011 -2 1 1
4.6760 4.6743 .0017 2 0 1
4.3360 4.3326 .0034 0 3 0
4.1520 4.1551 -.0031 0 3 1
4.0880 4.0877 .0003 -1 -2 1
3.9860 3.9865 -.0005 -2 3 1
A= 11.817 DA= .002
B= 13.963 DB= .002
C= 8.773 DC= .002
GAMMA=109.335 DGAMMA= .009
BETA = 93.580 DBETA = .001
ALPHA= 79.933 DALPHA= .002
V=1343
25. 49-2043
C3H10NO3V
Triklin
Dexp Dcal d(D) h k l
10.4000 10.3988 .0012 0 1 0
7.7400 7.7623 -.0223 1 -1 1
6.7300 6.7274 .0026 0 -1 2
6.4100 6.4189 -.0089 1 -1 2
5.8300 5.8326 -.0026 1 1 0
5.6800 5.6795 .0005 1 0 2
4.4390 4.4372 .0018 -1 0 2
4.1830 4.1871 -.0041 1 0 3
4.0400 4.0430 -.0030 1 2 0
3.8830 3.8838 -.0008 1 -3 2
3.7230 3.7216 .0014 0 -3 2
3.6070 3.6085 -.0015 1 -1 4
A= 8.512 DA= .003
B= 11.844 DB= .001
C= 14.728 DC= .002
GAMMA=107.19 DGAMMA= .02
BETA = 69.81 DBETA = .01
ALPHA=117.11 DALPHA= .03
V= 1224
26. 49-2249
C42H60N6O28V10*3H2O
Rombik
Groupa 26,28,51
Dexp. Dcal. d(D) h k l
9.4500 9.4969 -.0469 2 0 1
8.5400 8.5279 .0121 3 0 0
8.0700 8.1220 -.0520 0 1 0
6.7900 6.7942 -.0042 1 1 1
5.8750 5.8814 -.0064 3 1 0
4.7390 4.7362 .0028 4 1 1
4.5290 4.5261 .0029 3 1 2
4.0620 4.0610 .0010 0 2 0
3.1490 3.1483 .0007 2 1 4
3.0990 3.0999 -.0009 4 0 4
a=25.58 b= 8.12 c=14.17
da= .01 db= .02 dc= .01
V=2946
27. 49-2255
C10H12N2O16V6*H2O
Rombik
Groupa 30,53
Dexp. Dcal. d(D) h k l
10.6500 10.6869 -.0369 1 1 0
5.4300 5.4320 -.0020 1 1 1
4.0220 4.0231 -.0011 3 1 1
3.3860 3.3871 -.0011 5 0 0
3.2900 3.2891 .0009 5 1 0
3.1120 3.1127 -.0007 4 3 0
2.9780 2.9758 .0022 1 4 1
2.7010 2.6999 .0011 3 1 2
2.3250 2.3259 -.0009 0 4 2
1.7950 1.7950 .0000 6 4 2
a=16.935 b=13.776 c= 6.308
da= .004 db= .004 dc= .001
V=1472
Triklin
Dexp Dcal d(D) h k l
10.6500 10.6493 .0007 1 0 0
5.4300 5.4300 -.0000 -1 1 0
4.0220 4.0214 .0006 -1 1 1
3.3860 3.3860 .0000 -2 0 1
3.2900 3.2900 -.0000 0 2 1
3.1120 3.1120 .0000 -1 2 0
2.9780 2.9780 .0000 -1 2 1
2.7010 2.7010 -.0000 3 2 1
2.3250 2.3250 -.0000 3 1 2
1.7950 1.7950 .0000 6 1 1
A= 10.9109 DA= .0001
B= 7.1577 DB= .0001
C= 5.3035 DC= .0001
GAMMA= 80.720 DGAMMA= .008
BETA = 79.000 DBETA = .006
ALPHA= 70.856 DALPHA= .006
V= 381.89
28. 50-0533
VMoO
Groupa 31,59
Dexp. Dcal. d(D) h k l
6.0300 6.0323 -.0023 2 0 0
5.5400 5.5173 .0227 0 0 2
4.1200 4.1197 .0003 1 1 0
3.5100 3.5183 -.0083 1 0 3
3.3800 3.3759 .0041 2 1 1
3.2500 3.2498 .0002 3 0 2
2.9800 2.9830 -.0030 2 1 2
2.6900 2.6892 .0008 1 0 4
2.4100 2.4129 -.0029 5 0 0
1.9800 1.9782 .0018 6 0 1
1.8400 1.8391 .0009 0 0 6
1.7800 1.7811 -.0011 4 0 5
a=12.065 b= 4.383 c=11.035
da= .006 db= .001 dc= .001
V= 583.5
29. 50-0534
Mo6V4O25
Monoklin
GRUPA 4,11
Dexp. Dcal. d(D) h k l
5.9970 5.9880 .0090 0 1 1
4.0920 4.0948 -.0028 -1 0 2
3.5200 3.5161 .0039 1 2 0
3.3580 3.3601 -.0021 1 1 2
2.9940 2.9940 .0000 0 2 2
2.7060 2.7053 .0007 1 0 3
2.6730 2.6751 -.0021 -2 2 1
2.4290 2.4290 .0000 -2 2 2
2.2490 2.2490 .0000 3 1 1
2.0440 2.0440 .0000 -3 0 3
1.9960 1.9960 .0000 0 3 3
1.8230 1.8230 .0000 0 4 2
a= 7.54871 b= 7.96096 c= 9.1444 beta= 96.429
da=.000004 db=.00008 dc=.0007 dbet=.002
V=546.0
30. 50-0535
V0.95Mo0.97O5
Rombik
Groupa 17
Dexp. Dcal. d(D) h k l
6.0400 5.9953 .0447 0 3 0
4.0500 4.0360 .0140 1 4 0
3.5400 3.5368 .0032 0 0 1
3.3400 3.3480 -.0080 1 5 0
3.0100 3.0089 .0011 3 1 0
2.7200 2.7198 .0002 3 3 0
2.6700 2.6724 -.0024 2 2 1
2.4330 2.4314 .0016 1 5 1
2.3110 2.3106 .0004 3 0 1
2.2080 2.2090 -.0010 2 5 1
2.0180 2.0180 .0000 2 8 0
2.0180 2.0180 .0000 2 8 0
a= 9.15571 b=17.9858 c= 3.53683
da= .00001 db= .0004 dc= .00003
V= 582.42
31. 50-1359
K{NH4}VO2F3*H2O
Triklin
Dexp Dcal d(D) h k l
5.1550 5.1414 .0136 1 0 1
4.5520 4.5576 -.0056 0 1 1
4.4390 4.4394 -.0004 -1 1 1
4.2000 4.2012 -.0012 0 -1 1
3.5200 3.5205 -.0005 -2 1 1
3.1640 3.1653 -.0013 -1 0 2
3.1150 3.1107 .0043 2 1 0
2.9880 2.9886 -.0006 -1 1 2
2.9540 2.9491 .0049 -1 2 0
2.8450 2.8506 -.0056 3 0 0
2.4110 2.4129 -.0019 2 -2 1
2.2670 2.2675 -.0005 -2 -1 2
A= 8.8103 DA= .0001
B= 5.96159 DB= .00006
C= 6.71992 DC= .00001
GAMMA=103.630 DGAMMA= .001
BETA = 94.078 DBETA = .001
ALPHA= 84.480 DALPHA= .001
V=340.8
32. 50-1360
{NH4}RbVO2F3*H2O
Triklin
Dexp Dcal d(D) h k l
5.1850 5.1711 .0139 0 1 1
4.5620 4.5561 .0059 1 1 1
4.4500 4.4418 .0082 -1 1 0
4.2400 4.2372 .0028 0 0 2
3.5610 3.5556 .0054 -1 0 2
3.1800 3.1787 .0013 2 1 1
3.1260 3.1261 -.0001 1 -1 2
3.0070 3.0091 -.0021 -1 1 2
2.6030 2.6040 -.0010 0 -1 3
2.5850 2.5856 -.0006 0 2 2
2.4260 2.4259 .0001 1 -1 3
2.2950 2.2955 -.0005 3 1 1
A= 7.189 DA= .002
B= 6.6767 DB= .0007
C= 8.485 DC= .002
GAMMA= 79.94 DGAMMA= .04
BETA = 87.14 DBETA = .01
ALPHA= 90.02 DALPHA= .02
V=402.2
33. 50-1361
KRbVO2F3*H2O
Triklin
Dexp. Dcal. d(D) h k l
3.5610 3.5610 .0000 -2 -2 0
3.2080 3.2080 .0000 -3 -2 0
3.1470 3.1467 .0003 0 0 1
3.0420 3.0417 .0003 1 1 1
2.8750 2.8750 .0000 -4 -2 0
2.7630 2.7634 -.0004 3 0 1
2.7030 2.7022 .0008 -3 2 1
2.4480 2.4482 -.0002 5 -3 0
2.3030 2.3040 -.0010 1 -2 1
2.2920 2.2925 -.0005 6 -3 0
2.2370 2.2366 .0004 -4 3 1
2.2110 2.2099 .0011 3 -2 1
A= 19.452 DA= .001
B= 8.5582 DB= .0003
C= 3.2153 DC= .0001
GAMMA=101.094 DGAMMA= .008
BETA = 95.07 DBETA = .04
ALPHA= 78.52 DALPHA= .01
V= 514.1
34. 50-2145
C14H14N2O10S2V
Triklin
Dexp Dcal d(D) h k l
6.2300 6.2170 .0130 -1 -1 1
5.9800 5.9732 .0068 0 1 1
5.8000 5.8063 -.0063 0 -1 1
5.5900 5.5808 .0092 -1 1 1
4.7000 4.6934 .0066 0 2 0
4.4560 4.4568 -.0008 2 0 0
4.1670 4.1635 .0035 -1 0 2
3.9330 3.9367 -.0037 0 -2 1
3.7600 3.7645 -.0045 -2 0 2
3.5690 3.5711 -.0021 1 2 1
3.4730 3.4717 .0013 0 -1 2
3.2660 3.2649 .0011 -3 -1 1
A= 9.959 DA= .001
B= 9.5261 DB= .0005
C= 8.335 DC= .001
GAMMA= 80.335 DGAMMA= .002
BETA =114.863 DBETA = .006
ALPHA= 92.567 DALPHA= .001
V=707.1