1. 48-0131
Rb2Ni{VO3}4
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.2600 5.2503 .0097 1 1 0
4.3300 4.3300 -.0000 -1 0 1
3.3700 3.3675 .0025 2 0 1
3.1900 3.1887 .0013 0 2 1
3.0700 3.0738 -.0038 2 1 1
2.8400 2.8401 -.0001 -1 2 1
2.6400 2.6400 .0000 -1 0 2
2.5100 2.5093 .0007 2 2 1
2.2500 2.2459 .0041 1 3 1
2.1700 2.1705 -.0005 -1 3 1
2.0800 2.0806 -.0006 -2 1 2
2.0500 2.0489 .0011 3 2 0
a= 7.417 b= 7.525 c= 6.079 beta= 81.1
da=.005 db= .003 dc=.002 dbeta=.1
V= 335.3
Triklin
Dexp Dcal d(D) h k l
5.2600 5.2581 .0019 0 1 1
4.3300 4.3290 .0010 -1 0 1
3.3700 3.3706 -.0006 0 -1 1
3.1900 3.1913 -.0013 1 -1 1
3.0700 3.0713 -.0013 -1 2 0
2.8400 2.8415 -.0015 -1 1 2
2.6400 2.6420 -.0020 -2 2 0
2.5100 2.5097 .0003 -1 0 2
2.2500 2.2509 -.0009 0 3 1
2.1700 2.1680 .0020 -2 3 1
2.0800 2.0801 -.0001 -1 -2 1
2.0500 2.0492 .0008 3 1 1
A= 7.5123 DA= .0002
B= 6.9752 DB= .0002
C= 5.9026 DC= .0001
GAMMA=104.33 DGAMMA= .07
BETA = 97.16 DBETA = .03
ALPHA= 64.14 DALPHA= .01
V= 269.6
2. 48-0485
K3VO2F4
Rombik
Groupa 26,28,51
Dexp. Dcal. d(D) h k l
4.8800 4.8803 -.0003 1 0 1
4.2600 4.2588 .0012 0 3 0
3.0000 2.9969 .0031 1 4 0
2.7300 2.7308 -.0008 1 1 2
2.5700 2.5707 -.0007 2 4 0
2.4500 2.4509 -.0009 1 5 0
2.3900 2.3900 -.0000 3 3 0
2.2800 2.2795 .0005 2 2 2
a= 8.66 b=12.78 c= 5.907
da= .02 db= .01 dc= .006
V= 654
3. 48-0608
VO2*AlO2*PO2
Triklin
Dexp Dcal d(D) h k l
16.5780 16.5785 -.0005 2 0 0
16.3510 16.3492 .0018 -2 1 0
14.1030 14.1100 -.0070 -2 0 1
8.2476 8.2483 -.0007 -4 0 1
6.1698 6.1700 -.0002 -2 -2 2
5.7073 5.7076 -.0003 6 -2 1
5.4925 5.4923 .0002 4 -3 2
5.1374 5.1378 -.0004 -4 3 2
4.8374 4.8375 -.0001 2 3 0
4.6337 4.6334 .0003 -6 2 3
4.4848 4.4847 .0001 -2 4 1
4.4421 4.4421 .0000 6 0 2
A= 37.621 DA= .001
B= 19.832 DB= .002
C= 20.105 DC= .002
GAMMA=115.898 DGAMMA= .004
BETA = 96.946 DBETA = .003
ALPHA= 97.647 DALPHA= .001
V=13104
4. 48-0611
H2VAs2O8
Triklin
Dexp Dcal d(D) h k l
7.3800 7.3776 .0024 0 1 0
6.4600 6.4668 -.0068 1 0 0
4.5900 4.5924 -.0024 0 -1 2
4.1300 4.1331 -.0031 1 -1 1
3.9600 3.9603 -.0003 -1 -1 2
3.9100 3.9112 -.0012 1 2 0
3.8000 3.7999 .0001 1 1 2
3.7200 3.7176 .0024 0 -2 1
3.2500 3.2488 .0012 0 2 1
2.9300 2.9295 .0005 2 1 2
2.4700 2.4705 -.0005 1 3 1
2.4500 2.4499 .0001 -2 -3 1
A= 7.012 DA= .002
B= 8.098 DB= .001
C= 10.20910 DC= .00005
GAMMA= 68.585 DGAMMA= .005
BETA = 86.36 DBETA = .04
ALPHA= 99.68 DALPHA= .01858
V=526.7
5. 48-0612
V2As4O17
Rombik
Groupa 33,49,62
Dexp. Dcal. d(D) h k l
6.0000 5.9991 .0009 1 1 0
4.1400 4.1334 .0066 0 0 2
3.1500 3.1560 -.0060 4 0 0
3.0500 3.0577 -.0077 1 2 1
3.0000 2.9995 .0005 2 2 0
2.9500 2.9485 .0015 4 0 1
2.8700 2.8641 .0059 4 1 0
2.5200 2.5225 -.0025 3 2 1
2.2300 2.2301 -.0001 4 2 1
2.1600 2.1591 .0009 1 3 1
1.5800 1.5798 .0002 3 4 0
1.5500 1.5500 -.0000 8 0 1
a=12.624 b= 6.818 c= 8.267
da= .003 db= .004 dc= .006
v= 712
6. 48-0615
NaIn2V5O15{OH}2*7H2O
Triklin
Dexp Dcal d(D) h k l
8.5000 8.4957 .0043 1 0 0
7.9000 7.9010 -.0010 0 1 0
7.2000 7.2112 -.0112 0 1 1
5.8000 5.8061 -.0061 -1 -1 1
3.9700 3.9690 .0010 1 2 1
3.6300 3.6305 -.0005 2 0 1
3.3800 3.3803 -.0003 -1 2 1
3.3300 3.3298 .0002 -2 1 2
3.2100 3.2094 .0006 1 -1 2
3.1600 3.1593 .0007 -1 -1 3
2.9790 2.9796 -.0006 0 -1 3
2.9030 2.9030 -.0000 -2 -2 2
A= 9.09803 DA= .00002
B= 8.405 DB= .001
C= 11.178 DC= .002
GAMMA= 75.367 DGAMMA= .002
BETA =101.89 DBETA = .01
ALPHA= 80.09 DALPHA= .02
V=786.4
7. 48-0616
NaIn2V5O15{OH}2*4H2O
Triklin
Dexp Dcal d(D) h k l
9.7000 9.6964 .0036 -1 0 1
9.4000 9.4090 -.0090 0 1 0
8.3000 8.2989 .0011 1 0 1
7.1000 7.1054 -.0054 1 1 1
4.5000 4.4984 .0016 -2 1 0
3.7100 3.7098 .0002 0 -2 2
3.6000 3.6002 -.0002 3 0 1
2.8020 2.8028 -.0008 2 -2 2
2.6070 2.6066 .0004 -2 2 4
2.6000 2.6002 -.0002 1 0 5
2.3960 2.3961 -.0001 -3 -1 5
2.2150 2.2146 .0004 1 4 3
A= 12.133 DA= .001
B= 9.7174 DB= .0004
C= 14.031 DC= .001
GAMMA= 76.855 DGAMMA= .002
BETA = 97.812 DBETA = .003
ALPHA= 85.896 DALPHA= .001
V=1587
8. 48-0617
NaIn2V5O15{OH}2
Rombik
Groupa 30,53
Dexp. Dcal. d(D) h k l
3.6100 3.6115 -.0015 1 3 0
3.1900 3.1876 .0024 4 1 0
2.8140 2.8145 -.0005 0 4 0
2.7800 2.7805 -.0005 2 1 2
2.6070 2.6100 -.0030 4 2 1
2.2980 2.2981 -.0001 4 0 2
2.2150 2.2157 -.0007 6 0 0
1.9080 1.9080 .0000 6 3 0
1.7280 1.7278 .0002 3 6 0
1.6310 1.6307 .0003 7 0 2
a=13.294 b=11.258 c= 6.3622
da= .002 db= .002 dc= .0008
v= 952.2
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
3.6100 3.6184 -.0084 0 1 2
3.1900 3.1906 -.0006 2 1 0
2.8140 2.8146 -.0006 -2 0 2
2.7800 2.7813 -.0013 0 2 0
2.6070 2.6070 .0000 3 0 1
2.2980 2.2976 .0004 -2 0 3
2.2150 2.2149 .0001 -3 1 1
1.9080 1.9081 -.0001 -2 0 4
1.7280 1.7279 .0001 0 3 2
1.6310 1.6310 .0000 -2 3 1
a= 7.880 b= 5.5625 c= 9.638 beta= 81.32
da= .002 db= .0009 dc= .001 dbeta=.01
V= 417.7
9. 48-0618
NaIn2V5O16
Triklin
Dexp Dcal d(D) h k l
9.4000 9.3878 .0122 1 0 0
8.2000 8.1994 .0006 -1 1 0
7.3000 7.2958 .0042 0 -1 1
4.3000 4.2993 .0007 2 0 1
4.1000 4.0997 .0003 -2 2 0
4.0000 3.9961 .0039 1 2 0
3.7600 3.7663 -.0063 -2 0 2
3.6700 3.6702 -.0002 2 1 1
3.5500 3.5476 .0024 0 -1 3
3.5300 3.5298 .0002 -1 3 0
3.3800 3.3807 -.0007 0 3 0
3.3600 3.3584 .0016 0 3 1
A= 9.860 DA= .002
B= 10.718 DB= .001
C= 12.004 DC= .00357
GAMMA=107.63 DGAMMA= .02
BETA = 94.86 DBETA = .05
ALPHA= 82.039 DALPHA= .00927
V= 1196.1
10. 48-0619
NaIn2V5O16
Rombik
Groupa 27
Dexp. Dcal. d(D) h k l
3.5900 3.5907 -.0007 1 1 1
2.8310 2.8336 -.0026 3 1 0
2.6070 2.6067 .0003 4 0 0
2.2980 2.2991 -.0011 3 0 2
2.2150 2.2149 .0001 2 2 0
1.9130 1.9123 .0007 0 2 2
1.7380 1.7378 .0002 6 0 0
1.6310 1.6311 -.0001 0 3 0
a=10.4267 b= 4.8934 c= 6.1314
da= .0002 db= .0009 dc= .0006
V= 312.8
11. 48-0620
NaIn2V5O16
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
6.7000 6.7144 -.0144 1 1 0
4.8000 4.8043 -.0043 2 0 1
4.2000 4.2018 -.0018 2 1 1
3.9400 3.9477 -.0077 1 0 2
3.6000 3.5925 .0075 1 1 2
3.4900 3.4940 -.0040 -1 2 1
3.2100 3.2109 -.0009 3 1 1
2.9790 2.9816 -.0026 -2 2 1
2.8790 2.8767 .0023 -3 1 1
2.3320 2.3312 .0008 1 3 2
2.1440 2.1438 .0002 5 0 1
1.9880 1.9881 -.0001 0 0 4
1.9750 1.9750 .0000 2 4 1
a=10.7733 b=8.666 c= 8.067 beta=80.33
da=.0003 db=.003 dc=.003 dbeta=.02
V= 742.4
12. 48-0621
Cs2InV6O17{OH}*3H2O
Triklin
Dexp Dcal d(D) h k l
11.4000 11.4018 -.0018 0 0 1
10.7000 10.7973 -.0973 1 1 0
10.1000 10.1019 -.0019 0 1 1
9.6000 9.6002 -.0002 0 -1 1
7.8000 7.7982 .0018 1 -2 0
4.8000 4.8001 -.0001 0 -2 2
4.2000 4.1975 .0025 -2 3 2
4.0000 3.9987 .0013 -1 1 3
3.6000 3.5991 .0009 3 3 0
3.4000 3.4004 -.0004 -4 1 1
3.3400 3.3397 .0003 2 5 0
3.2600 3.2597 .0003 -2 -3 3
A= 13.79 DA= .02
B= 19.53 DB= .01
C= 12.135 DC= .00454
GAMMA= 91.3 DGAMMA= .1
BETA =109.76 DBETA = .02
ALPHA= 86.42 DALPHA= .02
V= 3070
13. 48-0622
Cs2InV6O17{OH}*H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.5000 5.5068 -.0068 2 1 0
4.3000 4.2986 .0014 0 0 2
3.8800 3.8804 -.0004 2 1 2
3.4200 3.4207 -.0007 3 1 2
3.3100 3.3076 .0024 -3 1 1
3.1900 3.1893 .0007 -2 0 2
3.1100 3.1082 .0018 4 1 0
2.9920 2.9896 .0024 2 3 1
2.7520 2.7534 -.0014 4 2 0
2.4460 2.4461 -.0001 -3 3 1
2.2430 2.2438 -.0008 2 0 4
2.1740 2.1739 .0001 6 0 0
2.0820 2.0821 -.0001 -3 1 3
a= 13.629 b= 10.279 c= 8.983 beta=73.14
da= .003 db=.005 dc=.005 dbeta=.04
V= 1204.3
14. 48-0623
Cs2InV6O17{OH}
TRiklin
Dexp Dcal d(D) h k l
3.5800 3.5782 .0018 -1 -1 1
3.2400 3.2429 -.0029 1 -1 3
2.8670 2.8668 .0002 -1 -1 3
2.8260 2.8258 .0002 -2 -1 1
2.8020 2.7998 .0022 1 -1 4
2.7700 2.7695 .0005 -3 0 1
2.6070 2.6078 -.0008 0 1 4
2.4620 2.4610 .0010 -1 1 4
2.3130 2.3135 -.0005 3 1 1
2.3020 2.3029 -.0009 -3 0 3
2.2360 2.2365 -.0005 3 -1 4
2.2190 2.2183 .0007 4 0 1
A= 8.9316 DA= .0006
B= 4.3482 DB= .0007
C= 13.9399 DC= .0001
GAMMA= 96.554 DGAMMA= .001
BETA = 80.513 DBETA = .001
ALPHA= 94.534 DALPHA= .006
V=529.7
15. 48-0624
Cs2InV6O17.5
Triklin
Dexp Dcal d(D) h k l
3.5300 3.5329 -.0029 0 2 0
3.2300 3.2297 .0003 -1 -2 2
3.0800 3.0800 .0000 0 -2 2
2.9980 2.9970 .0010 -1 2 0
2.9210 2.9207 .0003 -2 -1 3
2.8360 2.8390 -.0030 -2 -2 2
2.7530 2.7510 .0020 -1 -2 3
2.5360 2.5356 .0004 -1 0 4
2.4550 2.4547 .0003 2 1 2
2.2790 2.2794 -.0004 -3 0 3
2.2120 2.2114 .0006 3 0 1
2.1810 2.1810 .0000 3 1 1
1.8950 1.8950 -.0000 1 -2 4
1.7500 1.7500 .0000 -1 3 3
1.7340 1.7338 .0002 4 2 0
1.7220 1.7223 -.0003 3 0 3
A= 7.7690 DA= .0006
B= 7.3062 DB= .0003
C= 10.3684 DC= .0009
GAMMA= 77.826 DGAMMA= .006
BETA =108.376 DBETA = .001
ALPHA=101.624 DALPHA= .001
V=540.2
16. 48-0625
Cs2InV6O17.5
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
4.1000 4.1054 -.0054 2 1 0
3.8000 3.7945 .0055 0 0 3
3.6900 3.6895 .0005 2 1 1
3.5800 3.5792 .0008 0 1 3
3.3300 3.3308 -.0008 1 3 0
3.2500 3.2504 -.0004 -1 3 1
3.1000 3.1027 -.0027 0 2 3
3.0200 3.0214 -.0014 -2 1 3
2.9590 2.9600 -.0010 3 0 0
2.8540 2.8544 -.0004 3 1 0
2.8140 2.8152 -.0012 1 2 3
2.7300 2.7281 .0019 -3 1 2
a= 8.999 b= 10.78 c= 11.536 beta= 99.32
da=.005 db= .01 dc=.006 dbeta=.05
V= 1104
Triklin
Dexp Dcal d(D) h k l
4.1000 4.1024 -.0024 1 -1 1
3.8000 3.7981 .0019 3 1 1
3.6900 3.6940 -.0040 2 -1 1
3.5800 3.5837 -.0037 -3 1 0
3.3300 3.3295 .0005 0 0 2
3.2500 3.2505 -.0005 4 0 1
3.1000 3.0998 .0002 -1 0 2
3.0200 3.0206 -.0006 -1 2 1
2.9590 2.9591 -.0001 3 1 2
2.8540 2.8525 .0015 -2 2 0
2.8140 2.8144 -.0004 3 2 1
2.7300 2.7289 .0011 4 -1 1
A= 13.744 DA= .006
B= 6.687 DB= .002
C= 6.978 DC= .002
GAMMA= 83.91 DGAMMA= .07
BETA = 78.19 DBETA = .06
ALPHA= 76.23 DALPHA= .03
V=608.9
17. 48-0626
Cs2InV6O17.5
Monoklin
GRUPA 3
Dexp. Dcal. d(D) h k l
6.9000 6.8963 .0037 1 1 0
3.5600 3.5588 .0012 1 0 2
2.8490 2.8495 -.0005 2 3 0
2.8090 2.8090 .0000 2 1 2
2.6070 2.6064 .0006 0 0 3
2.5820 2.5805 .0015 2 2 2
2.3060 2.3066 -.0006 -2 3 2
2.2980 2.2988 -.0008 3 3 0
2.2900 2.2918 -.0018 0 4 2
2.2870 2.2870 .0000 -1 2 3
2.2150 2.2144 .0006 1 4 2
2.1910 2.1901 .0009 1 5 0
a= 8.699 b= 11.31 c= 7.819 beta= 90.3
da=.002 db=.001 dc=.004 dbet=.1
V=769.7
18. 48-0627
Cs2InV6O17.5
Triklin
Dexp Dcal d(D) h k l
7.0000 6.9980 .0020 1 0 0
3.5700 3.5721 -.0021 0 1 1
3.4900 3.4905 -.0005 -2 -1 1
3.2300 3.2316 -.0016 -2 -2 1
3.0100 3.0070 .0030 -1 -1 2
2.9400 2.9392 .0008 -2 0 1
2.9210 2.9214 -.0004 -1 1 1
2.9030 2.9034 -.0004 -1 -2 2
2.6030 2.6022 .0008 -2 -2 2
2.5820 2.5827 -.0007 -1 0 2
2.4640 2.4655 -.0015 -3 -2 1
2.2870 2.2859 .0011 2 3 0
A= 7.718 DA= .005
B= 7.882 DB= .008
C= 6.259 DC= .002
GAMMA= 65.10 DGAMMA= .05
BETA = 99.72 DBETA = .01
ALPHA=116.353 DALPHA= .006
V= 309.4
19. 48-0629
Cs2InV6O17.5
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
6.9000 6.8960 .0040 1 1 0
3.5600 3.5623 -.0023 1 0 2
2.8490 2.8486 .0004 2 3 0
2.8090 2.8099 -.0009 3 1 0
2.6070 2.6078 -.0008 0 0 3
2.5820 2.5824 -.0004 2 2 2
2.3060 2.3058 .0002 -2 3 2
2.2980 2.2987 -.0007 3 3 0
2.2900 2.2909 -.0009 0 4 2
2.2870 2.2871 -.0001 -1 2 3
2.2150 2.2141 .0009 1 4 2
2.1910 2.1904 .0006 2 1 3
a= 8.703 b= 11.305 c=7.824 beta= 90.23
da=.003 db=.004 dc=.001 dbeta=.01
V= 769.7
Triklin
Dexp Dcal d(D) h k l
6.9000 6.9032 -.0032 -1 1 0
3.5600 3.5591 .0009 0 -1 1
2.8490 2.8491 -.0001 0 -3 1
2.8090 2.8095 -.0005 -2 -1 1
2.6070 2.6081 -.0011 -2 -2 1
2.5820 2.5825 -.0005 1 -3 1
2.3060 2.3065 -.0005 -3 1 1
2.2980 2.3011 -.0031 -3 3 0
2.2900 2.2908 -.0008 1 6 0
2.2870 2.2858 .0012 -3 0 1
2.2150 2.2143 .0007 -3 -1 1
2.1910 2.1910 .0000 -1 6 1
A= 7.665 DA= .003
B= 14.953 DB= .002
C= 3.8612 DC= .0002
GAMMA= 95.670 DGAMMA= .001
BETA =101.241 DBETA = .009
ALPHA= 82.89 DALPHA= .01
V= 429.5
20. 48- 0631
Na7V13BO36{OH}3{H2O}6*29.5H2O
Triklin
Dexp Dcal d(D) h k l
9.9000 9.9004 -.0004 0 1 0
9.8000 9.8710 -.0710 0 0 1
8.5000 8.4974 .0026 1 0 0
7.8000 7.7889 .0111 -1 1 1
7.3000 7.2976 .0024 -1 0 1
5.0000 4.9988 .0012 0 2 1
4.4000 4.3997 .0003 -2 1 0
3.4100 3.4101 -.0001 0 1 3
3.0800 3.0803 -.0003 -2 3 0
2.9550 2.9547 .0003 1 -2 2
2.7350 2.7350 .0000 -3 0 2
2.6370 2.6369 .0001 1 2 3
A= 9.412 DA= .001
B= 11.101 DB= .003
C= 10.856 DC= .003
GAMMA=112.144 DGAMMA= .004
BETA =109.220 DBETA = .002
ALPHA= 68.89 DALPHA= .03
V==956.4
21. 48-0632
Na7V13BO36{OH}3{OH}6*25.5
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
7.9000 7.8869 .0131 1 1 0
7.8000 7.8067 -.0067 0 1 1
5.0000 4.9988 .0012 -1 2 1
3.4300 3.4292 .0008 2 2 1
3.2300 3.2312 -.0012 -2 3 1
3.1300 3.1302 -.0002 -2 1 3
3.1100 3.1096 .0004 0 4 0
2.9160 2.9163 -.0003 -1 4 1
2.3210 2.3208 .0002 -3 3 3
2.2510 2.2510 -.0000 -3 4 2
1.7950 1.7950 -.0000 3 0 4
1.7800 1.7800 .0000 -1 6 3
a= 10.61 b= 12.438 c= 10.43 beta= 106.0
da=.01 db=.003 dc= .01 dbeta=.1
V= 1323
22. 48-0633
Na7V13BO36{OH}3{H2O}6*1.5H2O
Triklin
Dexp Dcal d(D) h k l
7.5000 7.4946 .0054 1 0 0
7.4000 7.3990 .0010 -1 1 0
7.3000 7.3027 -.0027 -1 0 1
7.1000 7.0974 .0026 -1 1 1
6.8000 6.7914 .0086 0 1 1
4.9000 4.8968 .0032 -1 2 0
3.5000 3.5002 -.0002 0 -2 2
3.4100 3.4099 .0001 0 0 3
3.2200 3.2199 .0001 -2 -1 1
3.2100 3.2103 -.0003 1 1 2
3.1200 3.1203 -.0003 -2 3 1
3.1100 3.1101 -.0001 0 3 0
A= 8.65370 DA= .00000
B= 10.1745 DB= .0002
C= 10.9040 DC= .0002
GAMMA=113.453 DGAMMA= .001
BETA =110.193 DBETA = .002
ALPHA= 83.62852 DALPHA= .00002
V=826.4
Triklin
Dexp Dcal d(D) h k l
7.5000 7.5068 -.0068 1 0 1
7.4000 7.4116 -.0116 0 1 1
7.3000 7.2997 .0003 0 -1 1
7.2000 7.2016 -.0016 -1 0 1
7.1000 7.1125 -.0125 1 1 1
6.8000 6.7626 .0374 -1 -1 1
4.9000 4.9032 -.0032 1 0 2
3.5000 3.4952 .0048 1 0 3
3.4100 3.4093 .0007 3 2 0
3.2200 3.2195 .0005 -2 -3 1
3.2100 3.2091 .0009 -3 -2 1
3.1200 3.1190 .0010 -2 1 2
A= 10.698 DA= .002
B= 10.705 DB= .001
C= 11.0553 DC= .0005
GAMMA= 67.147 DGAMMA= .007
BETA = 87.04 DBETA = .02
ALPHA= 88.05 DALPHA= .04
V=1164
23. 48-0634
7Na2O*B2O3*13V2O5*15H2O
Triklin
Dexp Dcal d(D) h k l
7.0000 7.0166 -.0166 1 0 0
5.1000 5.0952 .0048 1 1 1
5.0000 5.0180 -.0180 0 -1 1
4.9000 4.9084 -.0084 -1 1 0
3.8800 3.8773 .0027 1 2 0
3.5700 3.5692 .0008 2 0 1
3.5400 3.5447 -.0047 2 1 1
3.4700 3.4678 .0022 2 1 0
3.2200 3.2189 .0011 0 0 2
3.0600 3.0580 .0020 2 -1 1
3.0300 3.0307 -.0007 -2 1 0
3.0200 3.0200 -.0000 0 1 2
A= 7.5186 DA= .0002
B= 8.4041 DB= .0007
C= 6.7802 DC= .0001
GAMMA= 78.366 DGAMMA= .003
BETA = 71.760 DBETA = .007
ALPHA= 85.226 DALPHA= .004
V=398.3
24. 48-0635
Na14V26B2O75
Triklin
Dexp Dcal d(D) h k l
6.9000 6.9041 -.0041 1 0 0
6.8000 6.7973 .0027 0 1 0
5.0000 5.0109 -.0109 1 1 0
3.8600 3.8630 -.0030 0 0 4
3.8300 3.8326 -.0026 -1 1 2
3.5300 3.5281 .0019 2 0 1
3.4300 3.4313 -.0013 0 1 4
3.2300 3.2297 .0003 -2 0 1
3.1900 3.1894 .0006 2 0 3
3.1700 3.1685 .0015 0 2 2
3.1100 3.1080 .0020 -1 0 4
3.0900 3.0904 -.0004 0 0 5
A= 7.078 DA= .003
B= 6.826 DB= .001
C= 15.827 DC= .005
GAMMA= 85.56 DGAMMA= .01
BETA = 77.82 DBETA = .02
ALPHA= 86.34 DALPHA= .01
V= 744.4
25. 48-0636
Na14V26B2O75
Triklin
Dexp Dcal d(D) h k l
7.0000 7.0033 -.0033 2 0 0
3.8800 3.8778 .0022 0 1 1
3.6600 3.6616 -.0016 0 -1 1
3.6400 3.6434 -.0034 2 -1 1
3.6300 3.6279 .0021 4 0 1
3.5000 3.5017 -.0017 4 0 0
3.2700 3.2682 .0018 -3 0 2
3.2100 3.2101 -.0001 2 1 0
3.1600 3.1605 -.0005 0 -1 2
3.1400 3.1395 .0005 -4 0 1
3.0200 3.0220 -.0020 2 0 4
2.7970 2.7954 .0016 2 -1 3
A= 14.7247 DA= .0007
B= 4.0463 DB= .0003
C= 12.264 DC= .002
GAMMA= 99.57 DGAMMA= .02
BETA = 75.442 DBETA = .006
ALPHA= 87.21 DALPHA= .01
V=694.2
Triklin
Dexp Dcal d(D) h k l
7.0000 7.0041 -.0041 1 0 0
3.8800 3.8783 .0017 0 1 1
3.6600 3.6623 -.0023 0 -1 1
3.6400 3.6433 -.0033 1 -1 1
3.6300 3.6296 .0004 2 0 1
3.5000 3.5020 -.0020 2 0 0
3.2700 3.2674 .0026 1 1 1
3.2100 3.2119 -.0019 1 1 0
3.1600 3.1605 -.0005 0 -1 2
3.1400 3.1386 .0014 -2 0 1
3.0200 3.0213 -.0013 1 0 4
2.7970 2.7952 .0018 1 -1 3
1.9080 n.i
A= 7.3644 DA= .0002
B= 4.04669 DB= .00009
C= 12.258 DC= .002
GAMMA= 99.52 DGAMMA= .01
BETA = 75.366 DBETA = .007
ALPHA= 87.22 DALPHA= .01
V=346.8
26. 48-0712
NH4TiVO5
Triklin
Dexp Dcal d(D) h k l
5.6700 5.6714 -.0014 1 0 0
4.3200 4.3217 -.0017 -1 1 0
4.0500 4.0495 .0005 -1 1 1
3.4800 3.4793 .0007 1 1 2
3.3800 3.3802 -.0002 -1 1 2
2.8500 2.8495 .0005 0 2 2
2.7400 2.7404 -.0004 -1 1 3
2.6600 2.6568 .0032 1 2 1
2.5900 2.5894 .0006 2 0 2
2.3600 2.3598 .0002 1 1 4
1.9800 1.9796 .0004 -1 3 1
1.9100 1.9105 -.0005 1 3 1
A= 5.7081 DA= .0004
B= 6.2217 DB= .0006
C= 10.4250 DC= .0006
GAMMA= 93.35 DGAMMA= .01
BETA = 85.06 DBETA = .01
ALPHA= 80.50 DALPHA= .01
V= 362.8
27. 48-0713
K6TiV10O30
Rombik
Groupa 17
Dexp. Dcal. d(D) h k l
5.0000 5.0050 -.0050 0 1 0
4.3000 4.2967 .0033 0 0 1
4.1800 4.1881 -.0081 1 0 1
3.0000 3.0005 -.0005 5 1 0
2.8200 2.8248 -.0048 5 0 1
2.0700 2.0693 .0007 7 1 1
1.7100 1.7104 -.0004 8 2 0
1.6300 1.6301 -.0001 0 2 2
1.5500 1.5499 .0001 1 3 1
1.2900 1.2900 .0000 11 1 2
a=18.745 b= 5.0050 c= 4.297
da= .004 db= .0001 dc= .003
V= 403.10
28. 48-0884
gamma-Cu3V2O8
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.8600 5.8502 .0098 0 0 2
4.0000 4.0017 -.0017 0 1 0
3.5200 3.5192 .0008 4 0 1
3.2400 3.2429 -.0029 2 0 3
3.1500 3.1463 .0037 5 0 0
3.1000 3.1005 -.0005 -4 0 3
2.8200 2.8212 -.0012 -1 1 3
2.6400 2.6426 -.0026 4 1 1
2.5700 2.5767 -.0067 2 0 4
2.4200 2.4203 -.0003 -5 1 2
2.3200 2.3185 .0015 -3 0 5
2.2400 2.2376 .0024 5 0 3
a= 16.1 b= 4.002 c= 11.947 beta= 101.66
.001 db=.001 dc=.001 dbeta=.04
V= 752.1
Triklin
Dexp Dcal d(D) h k l
5.8600 5.8436 .0164 -1 0 1
4.0000 4.0003 -.0003 -2 -1 1
3.5200 3.5174 .0026 -1 -2 1
3.2400 3.2378 .0022 2 2 0
3.1500 3.1475 .0025 0 -2 1
3.1000 3.1016 -.0016 2 0 1
2.8200 2.8211 -.0011 -3 -1 1
2.6400 2.6381 .0019 1 -1 2
2.5700 2.5686 .0014 3 2 0
2.4200 2.4226 -.0026 -2 -3 1
2.3200 2.3191 .0009 -2 -1 3
2.2400 2.2386 .0014 3 2 1
A= 8.5526 DA= .0002
B= 7.484 DB= .004
C= 7.336 DC= .001
GAMMA= 66.02 DGAMMA= .01
BETA =104.61 DBETA = .05
ALPHA= 98.86 DALPHA= .05
V=414.9
29. 48-1052
C6Cu2O13V*H2O
Rombik
Groupa 31,59
Dexp. Dcal. d(D) h k l
9.1900 9.1623 .0277 1 0 0
4.7600 4.7634 -.0034 1 0 3
3.8000 3.8046 -.0046 1 0 4
2.4500 2.4479 .0021 1 1 1
2.2900 2.2906 -.0006 4 0 0
2.1200 2.1188 .0012 4 0 3
1.8500 1.8508 -.0008 1 1 6
1.7700 1.7699 .0001 4 0 6
1.7500 1.7501 -.0001 0 1 7
a= 9.162 b= 2.570 c=16.729
da= .005 db= .001 dc= .009
v= 393.9
30. 48-1053
C6Cu2O15V
Rombik
Groupa 29,57
Dexp. Dcal. d(D) h k l
8.3800 8.3867 -.0067 2 0 0
7.8800 7.8418 .0382 0 1 0
3.8200 3.8180 .0020 1 2 0
2.4000 2.3971 .0029 4 2 1
2.1900 2.1904 -.0004 0 0 2
2.0300 2.0306 -.0006 7 1 1
1.9600 1.9604 -.0004 0 4 0
1.8500 1.8500 -.0000 3 4 0
a=16.77 b= 7.8418 c= 4.3807
da= .01 db= .0007 dc= .0007
V= 576.2