1. 47-0145
MnV10O26*10H2O
Triklin
Dexp Dcal d(D) h k l
7.2190 7.2130 .0060 1 0 0
6.6769 6.6697 .0072 -1 1 0
5.5391 5.5416 -.0025 -1 0 1
5.1375 5.1356 .0019 1 0 1
4.8217 4.8201 .0016 -1 -1 1
4.6083 4.6021 .0062 -1 1 1
3.5815 3.5819 -.0004 -1 0 2
3.3585 3.3587 -.0002 1 0 2
3.3338 3.3349 -.0011 -2 2 0
3.1710 3.1714 -.0004 0 1 2
3.0522 3.0524 -.0002 -2 -1 1
2.8975 2.8973 .0002 2 -2 2
A= 7.56944 DA= .00003
B= 10.1923 DB= .0002
C= 8.63796 DC= .00007
GAMMA=107.1261 DGAMMA= .0003
BETA = 87.12263 DBETA = .00003
ALPHA=113.4649 DALPHA= .0009
V=582.5
2. 47-0146
MnV12O31*10H2O
Monoklin
GRUPA 4,11
Dexp. Dcal. d(D) h k l
3.4452 3.4486 -.0034 2 1 0
3.3192 3.3196 -.0004 1 1 1
3.2856 3.2865 -.0009 0 2 0
2.5822 2.5819 .0003 0 0 2
1.9233 1.9231 .0002 2 0 2
1.9050 1.9038 .0012 1 3 1
1.7972 1.7981 -.0009 -2 0 3
1.7909 1.7909 .0000 3 2 1
1.5248 1.5248 .0000 0 2 3
a= 8.524 b= 6.573 c= 5.433 beta= 108.11
da=.007 db=.001 dc=.005 dbet=.07
V=289.0
3. 47-0147
MnV2O6*4H2O
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
7.8027 7.8171 -.0144 1 1 0
5.0390 5.0442 -.0052 1 0 2
3.8760 3.8770 -.0010 2 1 2
3.2364 3.2382 -.0018 4 0 1
3.0319 3.0308 .0011 2 1 3
2.6070 2.6057 .0013 3 3 0
2.0403 2.0399 .0004 6 1 2
1.9951 1.9954 -.0003 0 4 3
1.9787 1.9787 .0000 0 2 5
a=13.569 b= 9.564 c=10.867
da= .001 db= .004 dc= .001
V=1410
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
7.8027 7.8223 -.0196 0 0 1
5.0390 5.0356 .0034 1 1 0
3.8760 3.8754 .0006 3 0 1
3.2364 3.2360 .0004 3 1 0
3.0319 3.0326 -.0007 2 1 2
2.6070 2.6074 -.0004 0 0 3
2.0403 2.0403 -.0000 -2 2 2
1.9951 1.9944 .0007 1 0 4
1.9787 1.9790 -.0003 2 0 4
1.8712 1.8712 -.0000 -1 0 4
1.8712 1.8712 -.0000 -1 0 4
a= 12.19 b= 5.5530 c= 7.983 beta=78.47
da=.01 db=.0005 dc=.001 dbeta=.01
V= 529.6
4. 47-0147
Mn2V2O7*3H2O
Rombik
Groupa 26,28,51
Dexp. Dcal. d(D) h k l
10.0480 10.0790 -.0310 1 0 0
7.7618 7.7266 .0352 0 0 2
4.2302 4.2210 .0092 2 0 2
3.5339 3.5329 .0010 0 1 0
3.0789 3.0810 -.0021 3 0 2
3.0583 3.0612 -.0029 1 1 2
2.8455 2.8435 .0020 2 1 1
2.8139 2.8140 -.0001 3 0 3
2.6070 2.6071 -.0001 0 1 4
a=10.079 b= 3.5329 c=15.45
da= .001 db= .0001 dc= .01
V= 550.3
5. 47-0154
CaCdV2O7
Rombik
Groupa 31,59
Dexp. Dcal. d(D) h k l
5.6000 5.5873 .0127 1 0 2
3.3400 3.3404 -.0004 5 0 0
3.2200 3.2230 -.0030 3 0 3
3.1200 3.1172 .0028 1 1 0
2.9610 2.9645 -.0035 0 0 4
2.7970 2.7937 .0033 2 0 4
2.7530 2.7567 -.0037 3 1 0
2.5490 2.5513 -.0023 5 0 3
2.5040 2.4997 .0043 3 1 2
2.3840 2.3860 -.0020 7 0 0
2.3410 2.3391 .0019 7 0 1
2.2800 2.2814 -.0014 2 0 5
a=16.702 b= 3.1729 c=11.86
da= .004 db= .0004 dc= .01
V=628.4
6. 47-0155
Na2CdV2O7
Rombik
Groupa 20
Dexp. Dcal. d(D) h k l
4.9000 4.9075 -.0075 0 1 1
4.5800 4.5823 -.0023 0 0 2
4.0300 4.0229 .0071 1 1 1
3.8400 3.8378 .0022 1 0 2
2.9060 2.9054 .0006 0 2 0
2.8550 2.8560 -.0010 2 1 1
2.7870 2.7874 -.0004 2 0 2
2.7030 2.7040 -.0010 0 1 3
2.2380 2.2386 -.0006 2 2 0
2.0120 2.0114 .0006 2 2 2
1.9190 1.9189 .0001 2 0 4
1.8950 1.8951 -.0001 0 3 1
a= 7.024 b= 5.8108 c= 9.165
da= .002 db= .0004 dc= .001
V= 374.0
Triklin
Dexp Dcal d(D) h k l
4.9000 4.9014 -.0014 0 1 1
4.5800 4.5810 -.0010 -1 0 1
4.0300 4.0315 -.0015 0 -1 1
3.8400 3.8382 .0018 1 0 1
2.9060 2.9039 .0021 1 2 1
2.8550 2.8557 -.0007 0 1 2
2.7870 2.7898 -.0028 -1 0 2
2.7030 2.7011 .0019 -1 1 2
2.2380 2.2375 .0005 1 2 2
2.0120 2.0120 -.0000 -3 0 1
1.9190 1.9191 -.0001 2 0 2
1.8950 1.8948 .0002 2 3 1
A= 6.175 DA= .002
B= 7.0442 DB= .0009
C= 5.9244 DC= .0001
GAMMA= 83.17 DGAMMA= .02
BETA = 98.67 DBETA = .02
ALPHA= 79.960 DALPHA= .007
V= 248.0
7. 47-0198
Na12V24O59*39H2O
Tetragon
Groupa 105,112,131
Dexp. Dcal. d(D) h k l
10.9690 11.1008 -.1318 0 0 1
9.6120 9.5430 .0690 1 1 0
9.3490 9.5430 -.1940 1 1 0
7.3000 7.2365 .0635 1 1 1
5.5980 5.5504 .0476 0 0 2
4.5110 4.4986 .0124 3 0 0
4.3710 4.3837 -.0127 2 2 1
3.2290 3.2281 .0009 4 0 1
2.8520 2.8577 -.0057 3 0 3
2.8000 2.7958 .0042 3 1 3
2.7780 2.7752 .0028 0 0 4
2.7150 2.7183 -.0033 1 0 4
a= 13.496 c= 11.10
da= .007 dc= .01
v=2021
Triklin
Dexp. Dcal. d(D) h k l
10.9690 10.9690 .0000 1 -1 0
9.6120 9.6140 -.0020 0 0 1
9.3490 9.3490 .0000 2 0 0
7.3000 7.3003 -.0003 1 -1 1
5.5980 5.5980 .0000 0 2 0
4.5110 4.5115 -.0005 -1 0 2
4.3710 4.3718 -.0008 -1 1 2
3.2290 3.2306 -.0016 -3 -1 2
2.8520 2.8532 -.0012 -5 1 2
2.8000 2.7990 .0010 0 4 0
2.7780 2.7779 .0001 -3 -2 2
2.7150 2.7145 .0005 -4 3 2
A= 19.53679 DA= .00005
B= 11.61342 DB= .00007
C= 9.706 DC= .002
GAMMA=105.026 DGAMMA= .001
BETA = 82.939 DBETA = .001
ALPHA= 88.49 DALPHA= .01
V= 2106.8
8. 47-0206
FeVW2O10
Rombik
Grupa 16
Dexp. Dcal. d(D) h k l
6.9700 6.9741 .0041 2 0 0
4.6600 4.6494 -.0106 3 0 0
3.6500 3.6518 .0018 1 1 2
3.4900 3.4870 -.0030 4 0 0
3.4200 3.4151 -.0049 3 0 2
3.2900 3.2949 .0049 4 0 1
3.0200 3.0235 .0035 2 0 3
2.7900 2.7896 -.0004 5 0 0
2.7600 2.7593 -.0007 0 2 1
2.7100 2.7068 -.0032 1 2 1
2.4600 2.4584 -.0016 3 1 3
2.3700 2.3670 -.0030 2 0 4
a=13.948 b= 5.7383 c=10.066
da=.004 db=.0007 dc=.007
V= 805.6
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
6.9700 6.9674 .0026 1 1 0
4.6600 4.6626 -.0026 -1 0 2
3.6500 3.6496 .0004 1 3 0
3.4900 3.4871 .0029 1 0 3
3.4200 3.4208 -.0008 -1 0 3
3.2900 3.2893 .0007 0 3 2
3.0200 3.0223 -.0023 1 2 3
2.7900 2.7904 -.0004 -2 0 3
2.7600 2.7592 .0008 0 3 3
2.7100 2.7097 .0003 1 0 4
2.4600 2.4598 .0002 -3 1 2
2.3700 2.3700 -.0000 0 5 1
a= 8.519 b=12.1179 c= 11.338 beta= 88.51
da=.002 db=.0004 dc=.001 dbeta=.06
V= 1170.0
9. 47-0450
K2Cd{VO3}4
Triklin
Dexp Dcal d(D) h k l
6.1400 6.1365 .0035 -2 1 0
5.8100 5.8159 -.0059 -1 0 1
5.4900 5.4898 .0002 0 2 0
4.0500 4.0492 .0008 1 -3 0
3.9600 3.9607 -.0007 -2 3 0
3.8900 3.8902 -.0002 1 1 1
3.7700 3.7707 -.0007 -3 1 1
3.6600 3.6599 .0001 0 3 0
3.3400 3.3399 .0001 0 -3 1
3.1800 3.1804 -.0004 -2 -2 1
3.1000 3.0997 .0003 3 1 0
3.0200 3.0191 .0009 -1 0 2
A= 12.5988 DA= .0007
B= 12.2513 DB= .0004
C= 6.045 DC= .001
GAMMA=114.916 DGAMMA= .001
BETA =102.49 DBETA = .07
ALPHA= 92.60 DALPHA= .03
V=816.9
10. 47-0451
Rb2Cd{VO3}4
Triklin
Dexp Dcal d(D) h k l
6.2000 6.1965 .0035 0 2 0
5.8200 5.8233 -.0033 0 -1 1
4.3800 4.3822 -.0022 -1 -1 1
4.1200 4.1220 -.0020 1 3 0
3.9400 3.9394 .0006 1 3 1
3.6600 3.6577 .0023 0 3 1
3.3700 3.3676 .0024 0 1 2
3.2000 3.1998 .0002 1 -1 2
3.0100 3.0088 .0012 -2 -1 1
2.9600 2.9617 -.0017 -2 0 1
2.8400 2.8386 .0014 -1 0 2
2.8000 2.8006 -.0006 2 3 2
A= 8.1499 DA= .0003
B= 13.0439 DB= .0003
C= 7.21308 DC= .00002
GAMMA= 72.296 DGAMMA= .004
BETA = 72.389 DBETA = .002
ALPHA= 80.917 DALPHA= .004
V=694.4
11. 47-0772
K2BaV4O12
Triklin
Dexp Dcal d(D) h k l
7.3200 7.3039 .0161 0 1 1
6.9900 7.0146 -.0246 1 0 0
5.5800 5.5783 .0017 0 -1 1
4.5800 4.5838 -.0038 -1 1 1
3.9000 3.8951 .0049 0 1 2
3.6500 3.6514 -.0014 1 1 2
3.5100 3.5073 .0027 2 0 0
3.4700 3.4713 -.0013 2 1 1
3.3700 3.3719 -.0019 2 2 0
3.3200 3.3230 -.0030 1 -2 1
3.2700 3.2644 .0056 2 0 1
3.2200 3.2195 .0005 1 3 2
A= 7.30037 DA= .00007
B= 12.5313 DB= .0003
C= 7.88360 DC= .00009
GAMMA= 74.4289 DGAMMA= .0008
BETA = 81.420 DBETA = .001
ALPHA= 71.6379 DALPHA= .0003
V=657.6
12. 47-0790
YV18O48H3*22H2O
Tetragon
Groupa 85,118,129
Dexp. Dcal. d(D) h k l
13.1200 13.1706 -.0506 0 0 1
4.4000 4.3902 .0098 0 0 3
3.4500 3.4481 .0019 1 0 3
2.9300 2.9319 -.0019 1 1 3
2.5600 2.5653 -.0053 2 0 2
1.9170 1.9175 -.0005 1 1 6
1.7980 1.7970 .0010 2 2 3
1.5190 1.5190 .0000 1 1 8
1.5190 1.5177 .0013 3 0 5
1.5190 1.5190 .0000 1 1 8
a= 5.57 c= 13.171
da= .01 dc= .005
V=409
13. 47-0966
H4V3P3O16.5
geksag
Grupa 143
Dexp. Dcal. d(D) h k l
4.3000 4.2821 .0179 1 0 2
4.1700 4.1700 .0000 2 0 0
3.0900 3.0900 .0000 1 0 3
a= 9.630 c= 9.980
da= .001 dc= .001
v= 926
14. 47-0967
H4V3P3O16.5*xH2O
Rombik
Groupa 32,55
Dexp. Dcal. d(D) h k l
7.1700 7.1550 .0150 2 0 0
6.9600 6.9161 .0439 1 1 0
3.0400 3.0423 -.0023 3 2 0
2.3700 2.3700 .0000 0 0 1
a=14.310 b= 7.900 c= 2.370
da= .001 db= .001 dc= .001
V= 267.9
15. 47-1182
LiVO2
Tetragon
Grupa 75
Dexp. Dcal. d(D) h k l
15.1720 15.0339 .1381 0 0 1
4.9210 4.9256 -.0046 1 1 1
2.4224 2.4254 -.0030 3 0 1
2.0624 2.0620 .0004 1 0 7
2.0570 2.0569 .0001 3 0 4
2.0455 2.0449 .0006 3 2 0
1.8922 1.8933 -.0011 3 2 3
1.3664 1.3667 -.0003 0 0 11
1.2210 1.2207 .0003 4 1 9
a= 7.373 c= 15.034
da= .005 dc= .003
V= 817
16. 47-1683
K2VO3F*0.5H2O
Triklin
Dexp Dcal d(D) h k l
4.1300 4.1297 .0003 -1 1 0
3.5900 3.5900 .0000 1 -1 1
3.4700 3.4691 .0009 -1 -1 2
2.9800 2.9794 .0006 -2 1 1
2.9000 2.8998 .0002 1 -1 2
2.8900 2.8900 -.0000 -2 1 0
2.3800 2.3801 -.0001 -1 2 0
2.2000 2.2000 -.0000 -1 1 4
2.1900 2.1904 -.0004 0 -1 4
2.1400 2.1399 .0001 -3 -1 2
2.0400 2.0408 -.0008 -3 -1 3
1.7100 1.7095 .0005 -4 1 1
1.6600 1.6600 .0000 0 3 0
1.6400 1.6400 .0000 2 -1 4
A= 7.272 DA= .009
B= 4.993 DB= .002
C= 10.062 DC= .008
GAMMA= 91.87 DGAMMA= .09
BETA =109.70 DBETA = .03
ALPHA= 92.84 DALPHA= .01
V= 343.1
17. 47-1684
{NH4}2VO3F*H2O
Triklin
Dexp Dcal d(D) h k l
5.8300 5.8410 -.0110 -1 -1 1
5.1300 5.1215 .0085 0 1 1
4.8500 4.8451 .0049 0 -1 1
4.5100 4.5027 .0073 1 0 1
4.3800 4.3812 -.0012 1 1 1
4.0800 4.0834 -.0034 -1 -1 2
3.6900 3.6897 .0003 -2 0 1
2.9500 2.9499 .0001 0 2 1
2.8700 2.8692 .0008 -2 -1 3
2.7100 2.7098 .0002 -3 -1 2
2.6700 2.6705 -.0005 -2 1 1
2.6000 2.6001 -.0001 -1 1 3
A= 8.316 DA= .007
B= 6.9550 DB= .0006
C= 9.269 DC= .009
GAMMA= 62.55 DGAMMA= .01
BETA =114.12 DBETA = .06
ALPHA= 98.13 DALPHA= .05
V=433.1
18. 47-1685
NaVO2S*H2O
Triklin
Dexp Dcal d(D) h k l
10.6900 10.8194 -.1294 0 0 1
10.3700 10.3710 -.0010 1 0 0
7.6700 7.6733 -.0033 -1 1 1
5.7200 5.7170 .0030 1 -1 1
4.0500 4.0503 -.0003 1 1 2
3.9200 3.9226 -.0026 0 -3 1
3.8500 3.8487 .0013 -1 0 3
3.4300 3.4293 .0007 -3 1 2
3.3300 3.3308 -.0008 3 1 0
3.2100 3.2102 -.0002 -2 2 3
3.1100 3.1089 .0011 0 4 1
3.0800 3.0798 .0002 -2 -3 2
A= 11.0709 DA= .0004
B= 12.84 DB= .01
C= 11.558 DC= .002
GAMMA= 91.39 DGAMMA= .03
BETA =110.48 DBETA = .01
ALPHA= 87.35 DALPHA= .04
V= 1537.6
19. 47-1686
KVO2S*H2O
Triklin
Dexp Dcal d(D) h k l
10.2600 10.2301 .0299 0 0 1
9.5900 9.6007 -.0107 0 1 1
7.6700 7.6883 -.0182 0 -1 1
5.7200 5.7108 .0092 1 0 0
5.2000 5.2003 -.0003 1 0 1
4.0200 4.0229 -.0029 1 -2 1
3.8900 3.8880 .0020 1 2 2
3.8000 3.8000 .0000 0 4 0
3.4100 3.4100 -.0000 0 0 3
3.3100 3.3107 -.0007 1 4 1
3.1900 3.1903 -.0003 -1 3 2
3.1400 3.1395 .0005 1 1 3
A= 5.745 DA= .001
B= 15.665 DB= .002
C= 10.586 DC= .001
GAMMA= 86.846 DGAMMA= .007
BETA = 83.983 DBETA = .008
ALPHA= 76.12 DALPHA= .01
V= 919.3
20. 47-1687
NaVOS2*2H2O
Triklin
Dexp Dcal d(D) h k l
10.1600 10.1711 -.0111 -1 0 1
9.7800 9.7879 -.0079 1 1 0
9.2300 9.2187 .0113 1 0 1
9.0100 9.0469 -.0369 0 1 1
5.6600 5.6487 .0113 -2 1 0
4.9300 4.9347 -.0047 2 -1 1
4.0100 4.0120 -.0020 0 -2 2
3.8000 3.7998 .0002 1 3 0
3.3900 3.3904 -.0004 -3 0 3
3.2900 3.2890 .0010 -1 -2 3
3.1700 3.1698 .0002 -1 1 4
3.0700 3.0704 -.0004 -2 0 4
A= 14.801 DA= .004
B= 11.4981 DB= .0006
C= 13.0807 DC= .0004
GAMMA= 80.15 DGAMMA= .02
BETA = 94.52 DBETA = .01
ALPHA= 83.979 DALPHA= .004
V=2169
21. 47-1705
Mo0.03VP1.1O4.85
Rombik
Groupa 31,39
Dexp. Dcal. d(D) h k l
5.7200 5.7211 -.0011 1 0 0
4.8100 4.8098 .0002 0 0 2
4.5300 4.5333 -.0033 1 1 0
3.6800 3.6816 -.0016 1 0 2
3.3000 3.2989 .0011 1 1 2
3.1200 3.1162 .0038 1 2 0
2.9400 2.9405 -.0005 0 2 2
2.8000 2.7971 .0029 1 0 3
2.6700 2.6696 .0004 2 1 0
2.6100 2.6153 -.0053 1 2 2
2.4000 2.3989 .0011 0 3 1
a= 5.721 b= 7.431 c= 9.6196
da= .003 db= .003 dc= .0005
v= 409.0
22. 47-1706
Mo*V*P*O
Rombik
Groupa 31,59
Dexp. Dcal. d(D) h k l
5.7100 5.6762 .0338 1 0 0
4.8000 4.8052 -.0052 0 0 2
4.5200 4.5117 .0083 1 1 0
3.6700 3.6675 .0025 1 0 2
3.2900 3.2891 .0009 1 1 2
3.1100 3.1098 .0002 1 2 0
2.9400 2.9402 -.0002 0 2 2
2.7900 2.7898 .0002 1 0 3
2.6500 2.6515 -.0015 2 1 0
2.6100 2.6108 -.0008 1 2 2
2.4000 2.3998 .0002 0 3 1
a= 5.68 b= 7.43481 c= 9.610
da= .02 db= .00001 dc= .003
V=406.0
23. 47-1914
C4H3BrN2O3V*2H2O
Triklin
Dexp Dcal d(D) h k l
8.0285 8.0323 -.0038 -1 1 0
6.2431 6.2484 -.0053 0 1 1
5.3774 5.3661 .0113 0 -1 1
4.7003 4.7001 .0002 -1 2 0
4.1591 4.1565 .0026 0 2 0
3.7887 3.7898 -.0011 2 -1 2
3.6447 3.6493 -.0046 -1 -1 1
3.3746 3.3803 -.0057 2 1 1
3.2581 3.2549 .0032 1 2 1
3.0823 3.0821 .0002 3 -1 2
3.0418 3.0418 .0000 -3 2 0
2.9942 2.9929 .0013 3 0 1
A= 10.06943 DA= .00008
B= 9.416 DB= .005
C= 8.702 DC= .006
GAMMA=116.74 DGAMMA= .01
BETA = 68.10 DBETA = .02
ALPHA= 92.446 DALPHA= .006
V= 675.8
24. 47-2117
C189H147N21O21*Ca3V10O28
Triklin
Dexp Dcal d(D) h k l
8.3386 8.3742 -.0356 1 0 0
7.7552 7.7625 -.0073 0 1 0
6.9641 6.9649 -.0008 0 0 1
6.4114 6.4061 .0053 -1 1 0
5.5690 5.5675 .0015 0 1 1
4.8701 4.8703 -.0002 0 -1 1
4.1872 4.1871 .0001 2 0 0
3.9831 3.9831 .0000 -2 0 1
3.7509 3.7510 -.0001 -1 2 1
3.6012 3.6014 -.0002 0 2 1
3.3983 3.3979 .0004 2 1 0
A= 8.84591 DA= .00004
B= 8.0838 DB= .0003
C= 7.25699 DC= .00003
GAMMA=104.3219 DGAMMA= .0003
BETA =104.4370 DBETA = .0002
ALPHA= 79.220 DALPHA= .002
V=488.5