1. 45-088
CdNbVO9
Triklin
Dexp Dcal d(D) h k l
7.8000 7.7788 .0212 -1 0 1
5.3800 5.3874 -.0074 1 1 0
4.9300 4.9214 .0086 -1 -1 2
4.7300 4.7315 -.0015 1 -1 1
4.6000 4.5895 .0105 0 0 2
4.3400 4.3409 -.0009 -2 0 1
3.9600 3.9599 .0001 2 0 0
3.8900 3.8894 .0006 -2 0 2
3.6900 3.6880 .0020 -1 1 2
3.5900 3.5906 -.0006 0 -2 2
3.4900 3.4899 .0001 0 1 2
3.3500 3.3538 -.0038 -1 0 3
A= 8.71452 DA= .00002
B= 8.238 DB= .001
C= 10.6498 DC= .0002
GAMMA= 85.217 DGAMMA= .001
BETA =114.441 DBETA = .004
ALPHA=109.088 DALPHA= .002
V=656.6
2. 45-0089
TbNb2VO9
Triklin
Dexp Dcal d(D) h k l
7.7900 7.7718 .0182 1 0 0
5.4900 5.4977 -.0077 1 1 1
4.9300 4.9366 -.0066 -1 -1 1
4.6900 4.6919 -.0019 -1 1 0
4.5800 4.5807 -.0007 1 -1 1
3.9400 3.9381 .0019 2 0 1
3.8900 3.8859 .0041 2 0 0
3.7000 3.6998 .0002 1 2 0
3.5600 3.5602 -.0002 -1 -1 2
3.4900 3.4845 .0055 0 -2 1
3.3400 3.3371 .0029 2 1 2
3.1800 3.1837 -.0037 1 0 3
A= 8.299 DA= .008
B= 7.54 DB= .01
C= 9.691 DC= .007
GAMMA= 74.65 DGAMMA= .07
BETA = 77.07 DBETA = .02
ALPHA= 91.28 DALPHA= .03
V= 568.0
3. 45-0090
DyNb2VO9
Triklin
Dexp Dcal d(D) h k l
7.7600 7.7559 .0041 0 1 1
6.1500 6.1725 -.0225 1 1 0
5.4700 5.4691 .0009 0 -1 1
4.9300 4.9430 -.0130 1 1 1
4.6900 4.6909 -.0009 0 2 0
4.5700 4.5629 .0071 -1 1 2
4.3800 4.3812 -.0012 -1 0 2
3.9400 3.9382 .0018 -1 2 0
3.9000 3.9038 -.0038 -2 1 1
3.6900 3.6844 .0056 2 1 0
3.5600 3.5604 -.0004 -1 -1 2
3.4900 3.4909 -.0009 -2 0 2
A= 8.2796 DA= .0002
B= 9.985 DB= .001
C= 9.583 DC= .002
GAMMA= 93.58 DGAMMA= .03
BETA =108.53 DBETA = .03
ALPHA= 70.192 DALPHA= .004
V=705.7
4. 45-0091
HoNb2VO9
Triklin
Dexp Dcal d(D) h k l
7.7300 7.7218 .0082 1 1 0
5.4500 5.4508 -.0008 0 1 1
4.9300 4.9260 .0040 0 -1 1
4.6700 4.6682 .0018 1 -1 1
4.5300 4.5312 -.0012 2 1 1
3.9000 3.9081 -.0081 -2 -1 1
3.7000 3.7002 -.0002 3 1 1
3.5400 3.5397 .0003 2 2 1
3.4900 3.4873 .0027 -3 0 1
3.3400 3.3399 .0001 4 0 0
3.1000 3.0989 .0011 -2 -2 1
3.0300 3.0306 -.0006 -3 2 0
A= 13.4827 DA= .0001
B= 9.01883 DB= .00005
C= 6.4123 DC= .0001
GAMMA= 84.6370 DGAMMA= .0006
BETA = 83.8458 DBETA = .0003
ALPHA= 83.3548 DALPHA= .0003
V=767.6
5. 45-0093
Ba2CeV3O11
Triklin
Dexp Dcal d(D) h k l
4.5380 4.5406 -.0026 0 0 1
3.9650 3.9688 -.0038 0 -2 1
3.9140 3.9126 .0014 -1 -1 1
3.6480 3.6463 .0017 -1 -2 1
3.6250 3.6297 -.0047 1 -2 1
3.5340 3.5390 -.0050 0 5 0
3.2780 3.2788 -.0008 2 4 0
3.1360 3.1360 -.0000 2 2 1
2.9920 2.9924 -.0004 -1 4 1
2.9500 2.9492 .0008 0 6 0
2.9120 2.9108 .0012 1 -4 1
2.7780 2.7770 .0010 1 5 1
A= 9.1244 DA= .0003
B= 17.7504 DB= .0007
C= 4.5470 DC= .0002
GAMMA= 86.26 DGAMMA= .01
BETA = 88.36 DBETA = .01
ALPHA= 87.36 DALPHA= .01
V=734.7
Kvazi-monokl
Dexp Dcal d(D) h k l
4.5380 4.5356 .0024 2 1 0
3.9650 3.9627 .0023 -2 0 2
3.9140 3.9120 .0020 1 0 2
3.6480 3.6474 .0006 -1 2 1
3.6250 3.6244 .0006 3 0 0
3.5340 3.5374 -.0034 1 1 2
3.2780 3.2775 .0005 2 2 0
3.1360 3.1371 -.0011 3 0 1
2.9920 2.9922 -.0002 -3 1 2
2.9500 2.9501 -.0001 2 -1 2
2.9120 2.9132 -.0012 -1 -1 3
2.7780 2.7772 .0008 -2 -1 3
A= 11.15646 DA= .00004
B= 8.2053 DB= .0001
C= 9.37898 DC= .00002
GAMMA= 89.9669 DGAMMA= .0003
BETA =102.94700 DBETA = .00003
ALPHA= 89.7619 DALPHA= .0002
V=837.6
6. 45-0094
Ba2PrV3O11
Triklin
Dexp Dcal d(D) h k l
4.5020 4.5023 -.0003 1 1 0
3.9650 3.9673 -.0023 -1 1 1
3.9070 3.9060 .0010 -1 -1 1
3.6160 3.6180 -.0020 2 1 0
3.5340 3.5389 -.0049 -1 1 2
3.2760 3.2766 -.0006 -2 -1 1
3.1360 3.1372 -.0012 3 0 0
2.9920 2.9896 .0024 -1 1 3
2.9100 2.9085 .0015 2 -1 1
2.7750 2.7755 -.0005 3 0 2
2.6430 2.6414 .0016 -3 -1 1
2.3980 2.3986 -.0006 -2 -1 3
A= 9.5396 DA= .0002
B= 4.89110 DB= .00005
C= 11.5527 DC= .0006
GAMMA= 80.755 DGAMMA= .003
BETA = 86.445 DBETA = .003
ALPHA= 77.599 DALPHA= .001
V=518.8
7. 45-0095
Ba2SmV3O11
Triklin
Dexp Dcal d(D) h k l
4.4930 4.4991 -.0061 -1 1 1
3.9480 3.9495 -.0015 -1 -1 1
3.8800 3.8792 .0008 1 1 0
3.6630 3.6653 -.0023 -1 1 2
3.5960 3.5938 .0022 0 1 2
3.5170 3.5199 -.0029 -2 0 1
3.2480 3.2463 .0017 -2 0 2
3.1100 3.1099 .0001 2 0 1
2.9730 2.9719 .0011 -2 1 2
2.8940 2.8938 .0002 1 -1 3
2.7550 2.7549 .0001 1 -2 1
2.7100 2.7104 -.0004 0 0 4
A= 7.2479 DA= .0001
B= 5.70003 DB= .00003
C= 11.16252 DC= .00006
GAMMA=102.313 DGAMMA= .001
BETA =100.5679 DBETA = .0003
ALPHA= 96.288 DALPHA= .001
V=437.1
8. 45-0096
Ba2EuV3O4
Triklin
Dexp Dcal d(D) h k l
3.9450 3.9450 .0000 -1 2 0
3.8800 3.8798 .0002 0 -1 3
3.5870 3.5866 .0004 1 -2 2
3.5070 3.5069 .0001 -1 0 3
2.2480 2.2480 -.0000 -1 0 5
3.1090 3.1090 .0000 0 3 0
2.9730 2.9729 .0001 0 -1 4
2.8920 2.8925 -.0005 0 3 1
2.7800 2.7802 -.0002 -1 -1 4
2.6200 2.6201 -.0001 3 1 2
2.2690 2.2689 .0001 0 3 3
2.2430 2.2429 .0001 -3 -3 1
A= 8.8523 DA= .0007
B= 9.50278 DB= .00009
C= 12.0553 DC= .0002
GAMMA= 84.400 DGAMMA= .004
BETA = 86.543 DBETA = .002
ALPHA= 99.1233 DALPHA= .0008
V=993.5
9. 45-0097
Ba2GdV3O11
Triklin
Dexp Dcal d(D) h k l
3.9340 3.9245 .0095 -2 3 0
3.8630 3.8640 -.0010 -1 0 1
3.5730 3.5718 .0012 3 0 0
3.4980 3.4979 .0001 0 3 0
3.2410 3.2404 .0006 -2 0 1
3.1000 3.1001 -.0001 -1 -2 1
2.9670 2.9670 -.0000 -2 2 1
2.9120 2.9136 -.0016 -4 3 0
2.8850 2.8819 .0031 -3 4 0
2.7450 2.7449 .0001 1 2 1
2.3800 2.3815 -.0015 -3 5 0
2.2170 2.2170 .0000 5 -4 1
A= 12.401 DA= .002
B= 12.337 DB= .002
C= 4.3474 DC= .0001
GAMMA=120.118 DGAMMA= .007
BETA = 80.888 DBETA = .001
ALPHA=103.610 DALPHA= .001
V=558.9
10. 45-0098
Ba2TbV3O11
Triklin
Dexp Dcal d(D) h k l
4.6660 4.6668 -.0008 1 0 2
4.5060 4.5041 .0019 2 1 0
4.3700 4.3702 -.0002 -1 -2 2
3.9580 3.9588 -.0008 0 -2 2
3.8800 3.8782 .0018 -2 -2 2
3.5900 3.5879 .0021 -2 1 0
3.5120 3.5135 -.0015 0 2 2
3.2550 3.2560 -.0010 2 0 2
3.2140 3.2144 -.0004 -1 -3 1
3.1100 3.1112 -.0012 -2 0 4
2.9730 2.9714 .0016 0 1 4
2.8920 2.8921 -.0001 2 3 0
A= 9.8216 DA= .0001
B= 9.6439 DB= .0004
C= 14.1410 DC= .0001
GAMMA= 70.300 DGAMMA= .001
BETA =110.19460 DBETA = .00003
ALPHA=103.2429 DALPHA= .0003
V=1173.6
11. 45-099
Ba2DyV3O4
Triklin
Dexp Dcal d(D) h k l
4.4790 4.4788 .0002 1 1 0
3.9140 3.9130 .0010 -1 1 1
3.8570 3.8609 -.0039 -1 -1 1
3.8470 3.8445 .0025 1 0 1
3.5760 3.5790 -.0030 1 3 0
3.4900 3.4908 -.0008 1 2 1
3.2360 3.2326 .0034 -1 -3 1
3.0940 3.0964 -.0024 0 -5 1
2.8740 2.8743 -.0003 -1 1 2
2.7420 2.7417 .0003 0 -4 2
2.4670 2.4665 .0005 0 7 0
2.3760 2.3783 -.0023 -1 -4 2
A= 4.678 DA= .001
B= 17.2738 DB= .0006
C= 7.1778 DC= .0009
GAMMA= 91.63 DGAMMA= .05
BETA = 92.34 DBETA = .03
ALPHA= 89.24 DALPHA= .02
V=579.6
12. 45-0101
Ba2ErV3O4
Triklin
Dexp Dcal d(D) h k l
4.6320 4.6331 -.0011 -2 1 0
4.5020 4.5022 -.0002 3 1 0
3.9340 3.9323 .0017 2 0 1
3.8830 3.8838 -.0008 2 2 0
3.6010 3.6005 .0005 -3 0 1
3.5620 3.5617 .0003 -1 2 0
3.5040 3.5019 .0021 4 1 0
3.2430 3.2439 -.0009 3 1 1
3.1000 3.0992 .0008 -2 2 0
2.9590 2.9595 -.0005 -3 -2 1
2.8940 2.8945 -.0005 -4 1 0
2.8760 2.8759 .0001 1 -2 1
A= 14.314 DA= .001
B= 8.1749 DB= .0001
C= 5.1554 DC= .0003
GAMMA= 75.113 DGAMMA= .004
BETA = 95.641 DBETA = .001
ALPHA= 90.727 DALPHA= .003
V=579.9
13. 45-0102
Ba2TmV3O11
Triklin
Dexp Dcal d(D) h k l
4.5990 4.6009 -.0019 -1 2 0
4.4840 4.4831 .0009 0 2 0
3.9070 3.9072 -.0002 0 0 1
3.8570 3.8594 -.0024 3 1 0
3.5870 3.5898 -.0028 4 0 0
3.4770 3.4767 .0003 -2 1 1
3.2320 3.2313 .0007 -1 -1 1
3.0870 3.0895 -.0025 4 1 0
2.9440 2.9454 -.0014 -5 1 0
2.8740 2.8719 .0021 5 0 0
2.8670 2.8673 -.0003 -3 2 1
2.7470 2.7474 -.0004 0 -2 1
A= 14.7829 DA= .0007
B= 9.33577 DB= .00009
C= 3.9530 DC= .0007
GAMMA=103.713 DGAMMA= .007
BETA = 90.99 DBETA = .02
ALPHA= 81.342 DALPHA= .008
V=523.4
14. 45-0103
Ba2YbV3O11
Triklin
Dexp Dcal d(D) h k l
4.0040 4.0043 -.0003 1 1 0
3.9340 3.9335 .0005 0 1 1
3.8670 3.8654 .0016 0 -1 1
3.5900 3.5896 .0004 1 -1 1
3.4930 3.4928 .0002 -2 1 1
3.2880 3.2831 .0049 2 0 1
3.2480 3.2484 -.0004 1 1 1
3.1000 3.0961 .0039 0 0 2
2.9590 2.9597 -.0007 2 -1 1
2.8850 2.8857 -.0007 -3 0 1
2.8490 2.8492 -.0002 -2 -1 1
2.7470 2.7503 -.0033 1 0 2
A= 9.2119 DA= .0002
B= 5.14936 DB= .00005
C= 6.3376 DC= .0001
GAMMA=102.8926 DGAMMA= .0007
BETA =102.262 DBETA = .001
ALPHA= 86.317 DALPHA= .0002
V=286.4
15. 45-0104
Ba2InV3O11
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
4.6200 4.6155 .0045 -2 0 1
4.4900 4.4906 -.0006 2 1 1
3.9170 3.9176 -.0006 2 1 2
3.8670 3.8654 .0016 0 1 3
3.6360 3.6327 .0033 2 2 0
3.5620 3.5664 -.0044 2 2 1
3.4610 3.4628 -.0018 3 0 0
3.2480 3.2439 .0041 -3 0 1
3.2200 3.2213 -.0013 1 3 0
3.1640 3.1630 .0010 1 2 3
3.1020 3.1006 .0014 1 0 4
2.9530 2.9547 -.0017 -2 1 3
a= 10.457 b= 10.165 c=12.62 beta= 83.42
da=.003 db=.002 dc=.01 dbeta=.07
V= 1333
16. 45-0105
Ba2SeV3O11
Monoklin
Grupa 4,11
Dexp Dcal d(D) h k l
4.6080 4.6066 .0014 1 1 2
3.8730 3.8707 .0023 2 1 2
3.5500 3.5458 .0042 1 0 4
3.4530 3.4501 .0029 0 0 4
3.2300 3.2246 .0054 0 2 0
3.1210 3.1197 .0013 3 1 0
2.9160 2.9119 .0041 -3 1 1
2.8490 2.8501 -.0011 3 0 4
2.7720 2.7726 -.0006 -1 1 4
2.7260 2.7257 .0003 4 0 2
2.6730 2.6721 .0009 4 0 0
2.5100 2.5115 -.0015 -4 0 1
A= 11.0211 DA= .0003
B= 6.449 DB= .002
C= 14.2300 DC= .0008
BETA = 75.888 DBETA = .007
V=980
17. 45-106
Ba2YV3O11
Triklin
Dexp Dcal d(D) h k l
3.9170 3.9175 -.0005 -1 0 3
3.8470 3.8460 .0010 2 1 1
3.5870 3.5869 .0001 -2 -1 1
3.4900 3.4904 -.0004 0 1 4
3.2480 3.2472 .0008 1 1 4
3.0940 3.0942 -.0002 -1 0 4
2.9500 2.9498 .0002 -2 -2 1
2.8970 2.8966 .0004 0 -1 4
2.8760 2.8772 -.0012 2 2 3
2.8650 2.8642 .0008 1 3 3
2.7450 2.7450 -.0000 2 -1 3
2.7370 2.7367 .0003 3 0 1
A= 8.372 DA= .001
B= 9.836 DB= .004
C= 13.996 DC= .007
GAMMA= 88.188 DGAMMA= .09
BETA = 88.83 DBETA = .05
ALPHA= 73.01 DALPHA= .05
V=1100
18. 45-0107
Ba2NdV3O11
Triklin
Dexp Dcal d(D) h k l
4.5100 4.5097 .0003 0 0 1
3.9580 3.9574 .0006 -1 0 1
3.8900 3.8892 .0008 0 -2 1
3.6040 3.6027 .0013 -1 2 1
3.5170 3.5169 .0001 -1 -2 1
3.2550 3.2557 -.0007 0 5 0
3.1210 3.1236 -.0026 1 -3 1
2.9790 2.9789 .0001 -2 1 1
2.9030 2.9047 -.0017 2 -1 1
2.7630 2.7660 -.0030 2 -2 1
2.7140 2.7131 .0009 0 6 0
2.6290 2.6279 .0011 3 -1 0
2.3920 2.3917 .0003 -3 3 0
A= 7.9874 DA= .0009
B= 16.28805 DB= .00001
C= 4.513 DC= .001
GAMMA= 90.151 DGAMMA= .004
BETA = 91.04 DBETA = .02
ALPHA= 88.06 DALPHA= .01
V=586.6
19. 45-0108
Ba2LuV3O11
Triklin
Dexp Dcal d(D) h k l
4.5990 4.6046 -.0056 1 1 2
4.4700 4.4737 -.0037 1 3 0
3.8960 3.8954 .0006 1 -3 1
3.8310 3.8323 -.0013 1 -1 3
3.5810 3.5784 .0026 2 -2 2
3.4800 3.4817 -.0017 2 2 2
3.2480 3.2472 .0008 3 1 1
3.1250 3.1239 .0011 3 2 1
3.0830 3.0821 .0009 3 1 2
3.0620 3.0619 .0001 2 -3 2
2.9440 2.9466 -.0026 3 -1 1
2.8740 2.8752 -.0012 -2 0 2
A= 9.748 DA= .005
B= 14.384 DB= .002
C= 11.581 DC= .005
GAMMA= 78.8 DGAMMA= .1
BETA = 73.74 DBETA = .01
ALPHA=108.4 DALPHA= .1
V=1406
20. 45-0222
Ba-V
Triklin
Dexp Dcal d(D) h k l
6.7400 6.7224 .0176 -1 -1 1
6.2000 6.2177 -.0177 1 -1 1
4.9000 4.8906 .0094 1 1 3
4.5900 4.5893 .0007 2 0 0
4.2400 4.2469 -.0069 2 0 2
4.0900 4.0904 -.0004 -1 1 3
4.0700 4.0720 -.0020 0 0 4
3.8200 3.8225 -.0025 2 1 3
3.5900 3.5875 .0025 0 3 2
3.3600 3.3612 -.0012 -2 -2 2
3.2100 3.2073 .0027 1 0 5
3.0000 2.9983 .0017 3 0 2
A= 9.464 DA= .004
B= 11.82 DB= .01
C= 16.530 DC= .005
GAMMA= 78.12 DGAMMA= .08
BETA = 81.30 DBETA = .03
ALPHA= 83.83 DALPHA= .08
V=1780
21. 45-0475
NaVO{SO4}2
Triklin
Dexp Dcal d(D) h k l
6.1900 6.1853 .0047 0 0 1
5.4800 5.4854 -.0054 0 -2 1
5.1600 5.1505 .0095 1 0 0
4.9800 4.9751 .0049 1 -1 0
4.5600 4.5598 .0002 1 -2 0
4.4500 4.4549 -.0049 1 0 1
4.4000 4.3999 .0001 1 -1 1
4.3000 4.2990 .0010 1 1 1
4.0100 4.0051 .0049 0 5 0
3.5800 3.5778 .0022 -1 -1 1
3.5000 3.5044 -.0044 -1 1 1
2.8600 2.8608 -.0008 0 7 0
A= 5.2731 DA= .0001
B= 20.1062 DB= .0005
C= 6.35741 DC= .00002
GAMMA= 90.48516 DGAMMA= .00005
BETA = 77.644 DBETA = .002
ALPHA= 95.1051 DALPHA= .0001
V=655.7
22. 45-0525
V{H2PO4}3*2H2O
Triklin
Dexp Dcal d(D) h k l
9.8100 9.8174 -.0074 1 0 0
8.8300 8.8256 .0044 0 1 1
8.1500 8.1538 -.0038 0 -1 1
7.9100 7.9166 -.0066 1 1 1
7.5700 7.5862 -.0162 1 0 2
6.0300 6.0098 .0202 1 0 3
5.8500 5.8530 -.0030 -1 -1 2
4.6700 4.6700 .0000 -2 0 1
4.4300 4.4342 -.0042 -1 0 4
4.2200 4.2190 .0010 -2 -1 2
3.9400 3.9426 -.0026 2 1 4
3.8300 3.8299 .0001 -2 0 3
A= 10.342 DA= .001
B= 9.752 DB= .003
C= 21.33 DC= .03
GAMMA= 72.70 DGAMMA= .02
BETA = 81.72 DBETA = .09
ALPHA= 81.73 DALPHA= .09
V= 2020.9
23. 45-0684
K3V5Cu2O16
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
9.8000 9.8462 -.0462 0 1 0
8.4000 8.4022 -.0022 0 1 1
4.7000 4.7083 -.0083 0 2 1
4.1500 4.1572 -.0072 1 1 0
3.6000 3.5972 .0028 1 1 2
3.2500 3.2501 -.0001 1 2 1
2.9200 2.9212 -.0012 1 0 4
2.6500 2.6503 -.0003 -1 2 4
2.5500 2.5495 .0005 1 0 5
2.5000 2.5016 -.0016 1 3 2
2.3500 2.3501 -.0001 1 3 3
2.1600 2.1596 .0004 -1 4 1
1.8800 1.8797 .0003 2 3 0
1.7000 1.6998 .0002 1 5 3
a= 4.599 b= 9.846 c= 16.16 beta= 94.2
da=.003 db=.007 dc=.05 dbeta=.3
V= 730
Triklin
Dexp Dcal d(D) h k l
9.8000 9.7964 .0036 0 1 0
8.4000 8.4025 -.0025 0 0 1
4.7000 4.7006 -.0006 0 -2 1
4.1500 4.1514 -.0014 1 0 0
3.6000 3.5999 .0001 0 -2 2
3.2500 3.2530 -.0030 1 -1 1
2.9200 2.9197 .0003 -1 2 1
2.6500 2.6504 -.0004 1 0 2
2.5500 2.5501 -.0001 0 1 3
2.5000 2.4999 .0001 1 1 2
2.3500 2.3503 -.0003 0 -4 2
2.1600 2.1596 .0004 1 -3 2
1.8800 1.8799 .0001 2 1 1
1.7000 1.7000 .0000 1 -2 4
A= 4.31294 DA= .00001
B= 10.120 DB= .002
C= 8.924 DC= .003
GAMMA= 82.69 DGAMMA= .01
BETA =105.26 DBETA = .03
ALPHA=104.01 DALPHA= .01
V= 363.7
24. 45-0686
K3VCuO5
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
6.1000 6.0895 .0105 1 1 0
5.6000 5.5996 .0004 -1 1 1
4.9600 4.9602 -.0002 2 0 1
4.8200 4.8233 -.0033 2 0 0
4.4600 4.4574 .0026 -2 0 1
3.8800 3.8763 .0037 -2 1 1
3.5400 3.5381 .0019 2 1 4
3.3800 3.3823 -.0023 0 2 3
3.2000 3.2014 -.0014 2 1 5
2.8700 2.8718 -.0018 -3 0 2
2.6800 2.6804 -.0004 3 1 5
2.1400 2.1400 .0000 2 1 9
2.0500 2.0500 -.0000 3 3 1
2.0000 1.9999 .0001 2 3 6
1.7700 1.7699 .0001 4 3 4
1.4800 1.4800 -.0000 2 5 3
a= 9.9207 b= 7.85154 c= 20.56 beta= 76.5
da=.0003 db=.00004 dc= 9.39 dbeta=.1
V= 1557
Triklin
Dexp Dcal d(D) h k l
6.1000 6.0964 .0036 0 1 1
5.6000 5.6065 -.0065 0 -1 1
4.9600 4.9561 .0039 1 0 0
4.8200 4.8109 .0091 0 0 2
4.4600 4.4510 .0090 1 0 1
3.8800 3.8729 .0071 0 -1 2
3.5400 3.5327 .0073 0 2 1
3.3800 3.3784 .0016 -1 1 2
3.2000 3.1972 .0028 -1 2 1
2.8700 2.8691 .0009 -1 -1 2
2.6800 2.6823 -.0023 1 2 0
2.1400 2.1399 .0001 1 2 3
2.0500 2.0504 -.0004 2 -2 2
2.0000 2.0004 -.0004 -1 3 3
1.7700 1.7700 .0000 -1 3 4
1.4800 1.4800 -.0000 -1 2 6
A= 5.079 DA= .003
B= 7.55 DB= .01
C= 9.658 DC= .006
GAMMA=102.567 DGAMMA= .006
BETA = 89.67 DBETA = .01
ALPHA= 85.23 DALPHA= .07
V= 360.1
25. 45-1051
MnV2O6
Triklin
Dexp Dcal d(D) h k l
4.4200 4.4178 .0022 0 3 0
4.3730 4.3671 .0059 3 0 0
3.4040 3.4050 -.0010 3 2 0
3.2700 3.2708 -.0008 -1 1 1
3.2370 3.2358 .0012 1 1 1
3.1670 3.1676 -.0006 -2 4 0
3.0870 3.0846 .0024 2 0 1
3.0540 3.0546 -.0006 0 -2 1
3.0370 3.0369 .0001 -2 0 1
2.8840 2.8839 .0001 3 3 0
2.7370 2.7379 -.0009 3 0 1
2.6110 2.6107 .0003 2 -3 1
A= 13.274 DA= .001
B= 13.4264 DB= .0005
C= 3.4624 DC= .00012
GAMMA= 99.194 DGAMMA= .006
BETA = 89.02 DBETA = .02
ALPHA= 89.546 DALPHA= .004
V=608.7
26. 45-1052
CoV2O6
Triklin
Dexp Dcal d(D) h k l
6.9870 6.9837 .0033 -1 1 0
4.3660 4.3638 .0022 2 1 1
4.1620 4.1630 -.0010 2 -1 1
4.0810 4.0851 -.0041 0 2 0
3.8350 3.8319 .0031 3 0 1
3.6920 3.6897 .0023 0 2 1
3.3470 3.3433 .0037 0 -2 1
3.2460 3.2468 -.0008 2 2 1
3.1860 3.1876 -.0016 2 0 2
3.0810 3.0826 -.0016 2 -2 1
3.0360 3.0354 .0006 4 0 1
2.9170 2.9182 -.0012 4 1 0
A= 12.795 DA= .005
B= 8.2233 DB= .0002
C= 6.919 DC= .006
GAMMA= 91.24 DGAMMA= .03
BETA = 82.35 DBETA = .06
ALPHA= 83.83 DALPHA= .02
V=717.4
27. 45- 1053
NiV2O6
Triklin
Dexp Dcal d(D) h k l
4.9300 4.9463 -.0163 -1 1 0
4.1450 4.1515 -.0065 2 1 0
3.8060 3.8049 .0011 -2 0 1
3.6640 3.6668 -.0028 1 0 2
3.3580 3.3640 -.0060 2 2 0
3.2330 3.2345 -.0015 -2 1 0
3.1680 3.1720 -.0040 -1 2 0
3.0870 3.0877 -.0007 -2 0 2
3.0380 3.0360 .0020 -1 2 1
2.9170 2.9178 -.0008 1 -2 1
2.8840 2.8842 -.0002 2 1 2
2.7310 2.7286 .0024 1 3 0
A= 8.552 DA= .001
B= 8.1883 DB= .0006
C= 8.613 DC= .003
GAMMA= 72.73 DGAMMA= .02
BETA = 94.58 DBETA = .01
ALPHA= 89.52 DALPHA= .02516
V=572.4
28. 45-1529
C2.7H8.1O1.35S1.35V2O5
Geksagon
Groupa 186,190,194
Dexp. Dcal. d(D) h k l
16.6500 16.8000 -.1500 0 0 1
8.3000 8.2664 .0336 1 0 1
4.2000 4.2000 .0000 0 0 4
3.3000 3.3003 -.0003 2 1 2
2.8000 2.8000 .0000 0 0 6
2.4000 2.4000 .0000 0 0 7
2.1000 2.1000 .0000 0 0 8
a=10.96 c= 16.800
da=.07 dc=.004
V=1749
29. 45-1530
C18H36O9S4.5V2O5
Geksagon
Groupa 143
Dexp. Dcal. d(D) h k l
17.6000 17.4997 .1003 0 0 1
8.8000 8.7499 .0501 0 0 2
4.4000 4.4007 -.0007 1 0 2
3.5000 3.4999 .0001 0 0 5
2.9000 2.8989 .0011 1 1 1
2.5000 2.5000 .0000 0 0 7
2.2000 2.2003 -.0003 2 0 4
a= 5.879 c=17.5
da=.001 dc=.02
V= 523.8
30. 45-1999
C16H28O12V2O5
Tetragon
Groupa 90,113
Dexp. Dcal. d(D) h k l
21.5000 21.6002 -.1002 0 0 1
10.7000 10.8001 -.1001 0 0 2
7.2000 7.2001 -.0001 0 0 3
4.3000 4.3015 -.0015 1 0 1
3.6000 3.6000 -.0000 0 0 6
3.1000 3.1038 -.0038 1 1 0
2.7000 2.7000 -.0000 0 0 8
2.4000 2.4000 -.0000 0 0 9
2.1000 2.0994 .0006 2 0 3
a= 4.389 c= 21.600
da= .003 dc= .005
V=416.2