1. 40-0044
RbV5O13*2.3H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
9.4700 9.4868 -.0168 -1 0 1
6.6400 6.6527 -.0127 3 0 0
4.0000 4.0013 -.0013 2 2 0
3.6300 3.6306 -.0006 5 1 0
3.2900 3.2865 .0035 4 2 0
3.2700 3.2669 .0031 0 2 2
3.0400 3.0384 .0016 4 1 2
2.9140 2.9119 .0021 0 3 0
2.7300 2.7308 -.0008 5 2 1
2.5540 2.5539 .0001 -7 1 2
2.4950 2.4948 .0002 8 0 0
2.3520 2.3525 -.0005 5 3 0
a= 20.249 b= 8.7357 c= 9.987 beta= 99.72
da=.002 db=.0006 dc=.005 dbeta=.07
V= 1741
Triklin
Dexp Dcal d(D) h k l
9.4700 9.4751 -.0051 1 0 0
6.6400 6.6479 -.0079 -1 1 1
4.0000 3.9988 .0012 -1 -1 1
3.6300 3.6263 .0037 0 2 0
3.2900 3.2909 -.0009 1 2 1
3.2700 3.2709 -.0009 -3 1 1
3.0400 3.0396 .0004 -1 1 3
2.9140 2.9147 -.0007 2 1 2
2.7300 2.7288 .0012 1 1 3
2.5540 2.5549 -.0009 -2 -1 2
2.4950 2.4947 .0003 -1 3 0
2.3520 2.3522 -.0002 2 1 3
A= 9.965 DA= .0002
B= 8.244 DB= .001
C= 9.213 DC= .002
GAMMA=107.508 DGAMMA= .004
BETA =101.122 DBETA = .002
ALPHA= 65.210 DALPHA= .006
V= 653.3
2. 40-0186
beta-VPO4.75
Rombik
Groupa 31,59
Dexp. Dcal. d(D) h k l
4.8700 4.8563 .0137 1 0 0
4.2300 4.2313 -.0013 0 2 0
3.1900 3.1902 -.0002 1 2 0
2.6400 2.6400 .0000 1 0 1
2.4400 2.4392 .0008 1 3 0
2.1000 2.1000 -.0000 0 3 1
1.8400 1.8403 -.0003 2 3 0
a= 4.856 b= 8.4626 c= 3.1453
da= .001 db= .0004 dc= .0003
v= 129.26
3. 40-0189
Ca6Sc2V8O29
Triklin
Dexp Dcal d(D) h k l
4.8000 4.8019 -.0019 2 1 0
4.4700 4.4721 -.0021 0 1 1
3.8900 3.8925 -.0025 2 2 0
3.5600 3.5586 .0014 3 0 0
3.2900 3.2898 .0002 -2 0 1
3.2300 3.2315 -.0015 -2 1 1
3.1500 3.1484 .0016 2 -2 1
3.0940 3.0948 -.0008 -3 2 0
3.0580 3.0588 -.0008 3 0 1
3.0020 3.0020 .0000 3 2 0
2.9480 2.9488 -.0008 -1 3 1
2.9090 2.9067 .0023 0 -3 1
A= 10.7962 DA= .0003
B= 11.838 DB= .001
C= 4.7491 DC= .0003
GAMMA= 91.36 DGAMMA= .01
BETA = 81.673 DBETA = .004
ALPHA= 85.924 DALPHA= .009
V=598.3
4. 40-0308
Ag7I4VO4
Rombik
Groupa 33,49,62
Dexp. Dcal. d(D) h k l
3.9400 3.9377 .0023 2 1 0
3.7200 3.7393 -.0193 0 1 1
2.9100 2.9106 -.0006 3 1 0
2.7800 2.7793 .0007 2 2 0
2.4400 2.4404 -.0004 3 1 1
2.2800 2.2762 .0038 4 1 0
2.0300 2.0291 .0009 4 1 1
1.9500 1.9464 .0036 2 1 2
1.4300 1.4302 -.0002 5 1 2
1.2200 1.2202 -.0002 6 2 2
a= 9.66 b= 6.80 c= 4.478
da= .015 db= .01 dc= .004
V= 294
Monoklin
GRUPA 4
Dexp. Dcal. d(D) h k l
3.9400 3.9432 -.0032 1 1 0
3.7200 3.7288 -.0088 -1 0 1
2.9100 2.9129 -.0029 1 0 2
2.7800 2.7794 .0006 2 1 1
2.4400 2.4400 .0000 0 2 0
2.2800 2.2790 .0010 2 1 2
2.0300 2.0290 .0010 3 1 0
1.9500 1.9500 .0000 1 0 3
1.4300 1.4300 .0000 4 2 1
1.2200 1.2200 .0000 0 4 0
a=7.061 b= 4.880 c= 5.8557 beta=71.4
da=.006 db=.005 dc=.0008 dbet=.1
V=191.2
5. 40-0421
KVO{SeO4}2
Triklin
Dexp Dcal d(D) h k l
7.8000 7.7991 .0009 1 0 0
5.9600 5.9642 -.0042 -1 1 1
4.6100 4.6106 -.0006 1 -1 1
4.5200 4.5222 -.0022 -1 -1 1
4.3500 4.3553 -.0053 -1 1 2
3.9600 3.9590 .0010 -1 2 0
3.5300 3.5292 .0008 1 2 0
3.4600 3.4605 -.0005 2 0 1
3.3200 3.3227 -.0027 1 -1 2
3.1700 3.1721 -.0021 2 1 1
3.1300 3.1278 .0022 0 0 3
3.0300 3.0279 .0021 -1 0 3
A= 7.9718 DA= .0003
B= 8.8913 DB= .0006
C= 9.812 DC= .003
GAMMA= 99.92 DGAMMA= .02
BETA = 99.06 DBETA = .02
ALPHA= 74.350 DALPHA= .003
V= 655.1
6. 40-0422
RbVO{SeO4}2
Triklin
Dexp Dcal d(D) h k l
7.9400 7.9513 -.0113 0 1 1
6.1100 6.1135 -.0035 0 -1 1
4.5500 4.5461 .0039 -1 -1 1
4.4200 4.4219 -.0019 0 -1 2
4.0100 4.0047 .0053 -1 1 2
3.7900 3.7944 -.0044 1 2 1
3.5500 3.5442 .0058 1 -1 2
3.3400 3.3414 -.0014 -1 1 3
3.2300 3.2300 .0000 -1 2 0
3.1500 3.1483 .0017 0 0 4
2.8700 2.8716 -.0016 -2 -1 1
2.7800 2.7800 .0000 -1 1 4
A= 6.325 DA= .005
B= 8.612 DB= .001
C= 13.173 DC= .001
GAMMA= 81.35 DGAMMA= .03
BETA = 85.03 DBETA = .02
ALPHA= 73.139 DALPHA= .008
V= 678.2
7. 40-0423
CsVO{SeO4}2
Triklin
Dexp Dcal d(D) h k l
7.9300 7.9188 .0112 1 0 0
6.1500 6.1587 -.0087 1 1 1
4.5500 4.5590 -.0090 -1 -1 1
4.4300 4.4351 -.0051 1 -1 1
4.0300 4.0273 .0027 0 1 2
3.8300 3.8273 .0027 2 1 2
3.5600 3.5624 -.0024 -1 0 2
3.3400 3.3371 .0029 0 2 1
3.2500 3.2514 -.0014 -2 -1 1
3.1600 3.1616 -.0016 2 -1 1
2.9200 2.9208 -.0008 2 -1 2
2.8900 2.8901 -.0001 0 2 2
A= 8.9149 DA= .0002
B= 7.3980 DB= .0004
C= 10.2158 DC= .0003
GAMMA= 70.8254 DGAMMA= .0009
BETA = 68.074 DBETA = .001
ALPHA= 79.944 DALPHA= .001
V=589.2
8. 40-0427
LaVTa2O9
Triklin
Dexp Dcal d(D) h k l
5.3300 5.3389 -.0089 0 1 1
4.9300 4.9240 .0060 -1 -1 1
4.7000 4.7030 -.0030 0 -1 1
3.6100 3.6126 -.0026 1 -1 1
3.3700 3.3716 -.0016 2 1 1
3.3000 3.2974 .0026 -2 1 1
3.1900 3.1861 .0039 -1 0 3
3.0600 3.0598 .0002 1 2 0
2.9500 2.9534 -.0034 -2 0 3
2.8100 2.8101 -.0001 1 -1 2
2.7500 2.7495 .0005 -3 -1 2
2.7100 2.7097 .0003 2 1 2
A= 9.219 DA= .002
B= 6.1732 DB= .0002
C= 9.5839 DC= .0004
GAMMA= 78.040 DGAMMA= .007
BETA =107.534 DBETA = .003
ALPHA= 86.2524 DALPHA= .0003
V=504.0
9. 40-0428
ScVTa2O9
Triklin
Dexp Dcal d(D) h k l
7.7500 7.7528 -.0028 0 0 1
5.5900 5.5950 -.0050 1 1 0
4.9300 4.9309 -.0009 0 -2 1
4.7500 4.7508 -.0008 1 0 1
3.7800 3.7806 -.0006 0 3 1
3.7000 3.7005 -.0005 0 -1 2
3.6400 3.6375 .0025 -1 3 0
3.4900 3.4883 .0017 1 3 0
3.3400 3.3404 -.0004 0 2 2
2.9900 2.9913 -.0013 0 4 1
2.9300 2.9297 .0003 -1 4 0
2.8600 2.8593 .0007 1 2 2
A= 6.3671 DA= .0008
B= 12.920 DB= .003
C= 7.7725 DC= .0004
GAMMA= 92.6426 DGAMMA= .0007
BETA = 94.033 DBETA = .007
ALPHA= 89.144 DALPHA= .003
V= 637.1
10. 40-0429
alfa-YVTa2O9
Triklin
Dexp Dcal d(D) h k l
5.2900 5.2935 -.0035 0 1 0
4.9100 4.9131 -.0031 -1 0 1
3.2900 3.2888 .0012 0 -1 1
3.0400 3.0411 -.0011 -1 -1 1
2.9400 2.9389 .0011 1 -1 1
2.8000 2.7977 .0023 1 1 2
2.6800 2.6787 .0013 -2 1 2
2.6200 2.6193 .0007 1 2 1
2.4300 2.4337 -.0037 -2 2 1
2.0800 2.0790 .0010 2 2 0
1.9750 1.9747 .0003 -3 -1 1
1.7860 1.7857 .0003 -2 3 1
A= 7.2887 DA= .0002
B= 5.959 DB= .001
C= 6.734 DC= .001
GAMMA= 97.2452 DGAMMA= .0006
BETA =100.327 DBETA = .001
ALPHA= 62.80 DALPHA= .01
V=255.6
11. 40-0430
beta-YVTa2O9
Triklin
Dexp Dcal d(D) h k l
4.9100 4.9064 .0036 0 1 1
4.6700 4.6790 -.0090 0 -1 1
3.8700 3.8664 .0036 1 0 1
3.6800 3.6768 .0032 1 1 1
3.6200 3.6200 .0000 -1 -1 1
3.4800 3.4800 -.0000 1 0 2
3.3500 3.3478 .0022 0 -1 3
3.1200 3.1203 -.0003 -1 0 3
3.0400 3.0414 -.0014 1 0 3
3.0000 3.0009 -.0009 1 1 3
2.9100 2.9104 -.0004 -1 -1 3
2.8500 2.8495 .0005 0 0 5
A= 4.2474 DA= .0003
B= 5.350 DB= .001
C= 14.2877 DC= .0004
GAMMA= 72.376 DGAMMA= .005
BETA = 90.197 DBETA = .009
ALPHA= 85.970 DALPHA= .007
V=309.0
12. 40-0433
Na2Sc2V2O9
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
4.4180 4.4142 .0038 2 1 0
4.4090 4.4142 -.0052 2 1 0
4.1140 4.1150 -.0010 -2 1 1
3.3440 3.3455 -.0015 0 1 3
3.1870 3.1875 -.0005 1 1 3
3.1300 3.1313 -.0013 2 2 0
2.8000 2.8005 -.0005 3 1 2
2.6718 2.6725 -.0007 0 2 3
2.5580 2.5599 -.0019 -3 2 1
2.4590 2.4589 .0001 -3 1 3
2.0877 2.0876 .0001 3 3 0
2.0377 2.0373 .0004 5 1 1
a= 10.77878 b= 7.695 c=11.1456 beta= 90.54
da=.0005 db=.007 dc=.0001 dbeta=.03
V= 924.4
Triklin
Dexp Dcal d(D) h k l
4.4180 4.4211 -.0031 -1 1 1
4.4090 4.4068 .0022 -1 1 0
4.1140 4.1105 .0035 -1 -1 1
3.3440 3.3419 .0021 1 -1 1
3.1870 3.1844 .0026 -2 1 0
3.1300 3.1255 .0045 0 2 1
2.8000 2.8013 -.0013 -2 1 2
2.6718 2.6727 -.0009 2 0 2
2.5580 2.5573 .0007 0 1 3
2.4590 2.4596 -.0006 1 -1 2
2.0877 2.0881 -.0004 0 3 1
2.0377 2.0377 .0000 -3 0 3
A= 9.567 DA= .001
B= 6.520 DB= .001
C= 7.7090 DC= .0002
GAMMA= 74.23 DGAMMA= .01
BETA = 92.509 DBETA = .007
ALPHA= 72.481 DALPHA= .003
V=437.7
13. 40-0437
NaCa4{VO4}3
Triklin
Dexp Dcal d(D) h k l
8.6900 8.6915 -.0015 0 1 1
6.7200 6.7212 -.0012 1 0 0
5.7100 5.7026 .0074 -1 1 1
5.3700 5.3710 -.0010 -1 0 2
4.7900 4.7922 -.0022 0 2 1
4.6600 4.6547 .0053 0 2 0
4.0100 4.0101 -.0001 -1 2 1
3.9000 3.8972 .0028 -1 2 2
3.6700 3.6668 .0032 0 2 3
3.5700 3.5681 .0019 0 -1 3
3.5000 3.5026 -.0026 -1 2 3
3.3200 3.3162 .0038 1 -2 1
A= 6.944 DA= .001
B= 9.64 DB= .01
C= 13.79 DC= .01
GAMMA= 91.80 DGAMMA= .08
BETA =104.42 DBETA = .03
ALPHA= 75.04 DALPHA= .04
V= 863.3
14. 40-0563
V2Se2O11
Triklin
Dexp Dcal d(D) h k l
7.0800 7.0767 .0033 1 2 0
4.7700 4.7659 .0041 3 2 0
4.2300 4.2263 .0037 0 2 1
3.7300 3.7311 -.0011 -3 0 1
3.6500 3.6519 -.0019 -2 -2 1
3.5600 3.5543 .0057 -3 1 1
3.2900 3.2908 -.0008 3 0 1
2.7600 2.7597 .0003 -5 0 1
2.7100 2.7098 .0002 -2 -4 1
2.6800 2.6781 .0019 -4 3 0
2.6500 2.6512 -.0012 6 2 0
2.6100 2.6108 -.0008 -5 2 0
A= 16.101 DA= .003
B= 14.578 DB= .001
C= 4.801 DC= .001
GAMMA= 76.536 DGAMMA= .007
BETA = 95.27 DBETA = .03
ALPHA= 82.78 DALPHA= .02
V=1079
15. 40-0711
Cs2{HBV6O18}*0.65
Rombik
Groupa 16
Dexp. Dcal. d(D) h k l
7.8000 7.8735 -.0735 0 1 0
7.1000 7.0902 .0098 1 0 0
3.9700 3.9664 .0036 1 1 2
3.5800 3.5783 .0017 0 1 3
3.4000 3.4010 -.0010 2 0 1
3.3100 3.3095 .0005 1 2 1
2.4100 2.4115 -.0015 1 3 1
a= 7.09 b= 7.87 c=12.052
da= .01 db= .01 dc= .001
V= 673
16. 40-0712
Cs2HBV6O18
Rombik
Groupa 17
Dexp. Dcal. d(D) h k l
8.0000 8.0370 -.0370 0 1 0
4.0600 4.0667 -.0067 2 1 0
3.6600 3.6697 -.0097 2 0 2
3.5200 3.5248 -.0048 1 2 1
2.8000 2.7974 .0026 0 2 3
2.7880 2.7914 -.0034 1 0 4
2.7060 2.7098 -.0038 2 2 2
2.5780 2.5770 .0010 1 3 0
2.4490 2.4465 .0025 3 0 3
2.2810 2.2797 .0013 3 2 2
2.2700 2.2692 .0008 1 0 5
2.2100 2.2076 .0024 0 3 3
a= 9.43 b= 8.037 c=11.690
da= .01 db= .003 dc= .003
V= 886
Triklin
Dexp Dcal d(D) h k l
8.0000 8.0056 -.0056 1 0 0
4.0600 4.0548 .0052 -1 1 1
3.6600 3.6591 .0009 1 -1 1
3.5200 3.5242 -.0042 -1 -1 2
2.8000 2.7998 .0002 0 2 0
2.7880 2.7879 .0001 1 2 2
2.7060 2.7055 .0005 3 1 0
2.5780 2.5770 .0010 3 0 1
2.4490 2.4500 -.0010 2 -1 2
2.2810 2.2803 .0007 -1 -1 4
2.2700 2.2699 .0001 3 2 1
2.2100 2.2095 .0005 1 2 4
A= 8.310 DA= .001
B= 5.923 DB= .004
C= 11.153 DC= .004
GAMMA= 74.53 DGAMMA= .01
BETA = 88.45 DBETA = .02
ALPHA= 78.81 DALPHA= .03
V= 518.8
17. 40-0739
H2VPO3O10*3H2O
Triklin
Dexp Dcal d(D) h k l
10.1500 10.1368 .0132 1 0 0
9.8100 9.8160 -.0060 -1 1 0
7.5100 7.5181 -.0081 1 0 1
7.0900 7.0989 -.0089 0 -1 1
5.9500 5.9492 .0008 -1 2 0
5.1100 5.1092 .0008 0 2 1
5.0300 5.0294 .0006 -2 1 1
4.8700 4.8705 -.0005 -1 1 2
4.5300 4.5287 .0013 1 -1 2
3.6700 3.6702 -.0002 -3 2 0
3.0500 3.0501 -.0001 2 2 1
2.8800 2.8800 .0000 -2 -2 1
2.8400 2.8399 .0001 3 1 1
A= 11.261 DA= .001
B= 12.0787 DB= .0008
C= 10.789 DC= .008
GAMMA=115.71 DGAMMA= .02
BETA = 91.150 DBETA = .01
ALPHA= 82.18 DALPHA= .02
V= 1308.7
18. 40-0740
H2VP3O10*1.5H2O
Triklin
Dexp Dcal d(D) h k l
8.9800 8.9844 -.0044 1 0 0
8.0300 8.0290 .0010 0 1 1
7.1100 7.1010 .0090 0 -1 1
5.7800 5.7843 -.0043 -1 2 0
5.3600 5.3596 .0004 0 2 1
4.7200 4.7188 .0012 0 1 2
4.4000 4.3994 .0006 -2 1 1
3.7000 3.6996 .0004 2 -2 1
3.5500 3.5505 -.0005 0 -2 2
3.2700 3.2704 -.0004 0 3 2
2.9100 2.9101 -.0001 3 -1 1
2.6300 2.6300 -.0000 -3 -1 1
A= 9.443 DA= .001
B= 12.5086 DB= .0004
C= 9.868 DC= .002
GAMMA=107.71 DGAMMA= .01
BETA = 95.26 DBETA = .01
ALPHA= 81.614 DALPHA= .001
V= 1097.15
19. 40-0868
Cu0.8V1.1S2
Triklin
Dexp Dcal d(D) h k l
4.8900 4.8916 -.0016 -1 0 1
3.6100 3.6097 .0003 -2 -1 1
3.0800 3.0802 -.0002 -1 -2 1
2.8640 2.8633 .0007 -3 -1 1
2.4640 2.4639 .0001 -2 -1 2
2.2040 2.2041 -.0001 -3 -1 2
2.1640 2.1635 .0005 -2 1 2
2.0700 2.0701 -.0001 2 3 0
2.0330 2.0326 .0004 4 2 0
1.9670 1.9669 .0001 3 0 2
1.8230 1.8231 -.0001 3 1 2
1.6930 1.6931 -.0001 4 3 0
A= 10.056 DA= .009
B= 6.892 DB= .001
C= 5.42893 DC= .00004
GAMMA= 87.09 DGAMMA= .02
BETA = 96.70 DBETA = .02
ALPHA=101.970 DALPHA= .001
V= 365.4
20. 40-1114
H1.43V205
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
6.2140 6.2120 .0020 1 1 0
4.3790 4.3825 -.0035 1 0 1
4.1910 4.1994 -.0084 3 1 0
3.3670 3.3660 .0010 0 2 0
2.6870 2.6865 .0005 6 0 0
1.8600 1.8599 .0001 5 0 2
a=16.119 b= 6.732 c= 4.554
da= .001 db= .001 dc= .001
V=494.2
21. 40-1115
H1.87V2O5
Rombik
Groupa 26,28,51
Dexp. Dcal. d(D) h k l
6.2290 6.2335 -.0045 1 0 2
4.3790 4.3820 -.0030 3 0 0
4.1870 4.1861 .0009 3 0 1
2.9970 2.9990 -.0020 0 1 0
2.6790 2.6791 -.0001 2 1 1
a=13.146 b= 2.999 c=14.160
da= .001 db= .001 dc= .001
V=558.26
22. 40-1229
Al80V12.5Fe7.5
Rombik
Groupa 30,53
Dexp. Dcal. d(D) h k l
3.9226 3.9211 .0015 1 0 0
3.3882 3.3879 .0003 1 1 1
2.5540 2.5535 .0005 1 2 2
2.2018 2.2019 -.0001 1 1 3
2.0948 2.0951 -.0003 1 2 3
1.7948 1.7947 .0001 1 1 4
1.5166 1.5166 .0000 2 4 2
1.4761 1.4762 -.0001 2 3 3
1.2938 1.2938 .0000 0 9 1
a= 3.9211 b=11.792 c= 8.19486
da= .0003 db= .001 dc= .00005
V= 378.91
23. 40-1239
Al80V11.5Co8.5
Rombik
Groupa 30,53
Dexp. Dcal. d(D) h k l
3.9206 3.9237 -.0031 2 1 0
3.3929 3.3873 .0056 1 2 0
2.5656 2.5655 .0001 2 0 2
2.2055 2.2048 .0007 3 2 1
2.0955 2.0962 -.0007 2 2 2
1.7843 1.7843 -.0000 1 4 0
1.5161 1.5160 .0001 1 0 4
1.4832 1.4833 -.0001 2 4 2
1.2954 1.2954 -.0000 6 2 2
a= 9.321 b= 7.2718 c= 6.1460
da= .001 db= .0001 dc= .0009
V= 416.6
24. 40-1240
Al86V14
Rombik
Groupa 30,53
Dexp. Dcal. d(D) h k l
4.0112 4.0170 -.0058 3 0 0
2.6013 2.5995 .0018 3 2 0
2.2347 2.2338 .0009 1 3 0
2.1257 2.1269 -.0012 2 3 0
1.5395 1.5395 .0000 0 0 2
1.3139 1.3139 .0000 9 1 0
a=12.050900 b= 6.819600 c= 3.079000
da= .001000 db= .001000 dc= .001000
V= 253.0
25. 40-1297
V2O5*0.5H2O
Rombik
Groupa 39,67
Dexp. Dcal. d(D) h k l
8.7500 8.7570 -.0070 1 0 0
4.3700 4.3785 -.0085 2 0 0
2.9200 2.9190 .0010 3 0 0
2.1900 2.1892 .0008 4 0 0
1.7500 1.7500 .0000 0 0 2
1.4600 1.4600 .0000 0 2 0
1.4600 1.4595 .0005 6 0 0
a= 8.757 b= 2.9200 c= 3.500
da= .001 db= .0005 dc= .001
V= 89.50