1. 36-0248
Et2V1.6Ti0.4O7
Triklin
Dexp Dcal d(D) h k l
6.4000 6.3974 .0026 1 1 0
5.7800 5.7835 -.0035 -1 0 1
3.3300 3.3301 -.0001 -1 -2 1
3.1900 3.1928 -.0028 0 1 2
3.0300 3.0302 -.0002 0 -2 1
2.9000 2.8937 .0063 -2 1 0
2.7700 2.7708 -.0008 -2 -1 2
2.5400 2.5374 .0026 1 2 2
2.5100 2.5107 -.0007 -3 0 1
2.3000 2.3003 -.0003 -3 0 2
2.1300 2.1301 -.0001 2 2 2
1.9600 1.9600 .0000 -4 -1 1
A= 7.84710 DA= .00004
B= 8.299 DB= .001
C= 6.778 DC= .001
GAMMA= 73.901 DGAMMA= .003
BETA =106.40 DBETA = .02
ALPHA= 82.82 DALPHA= .01
V= 396.8
2. 36-256
NaCrV2O7
Rombik
Groupa 30,53
Dexp. Dcal. d(D) h k l
8.3400 8.3379 .0021 0 0 2
6.9200 6.8632 .0568 0 1 1
6.1000 6.1010 -.0010 1 1 0
4.1700 4.1689 .0011 0 0 4
3.8100 3.8084 .0016 2 1 2
3.4700 3.4692 .0008 3 0 0
3.3900 3.3917 -.0017 2 1 3
2.9800 2.9863 -.0063 1 2 3
2.9500 2.9474 .0026 3 1 2
2.7800 2.7793 .0007 0 0 6
a=10.407 b= 7.531 c=16.68
da= .003 db= .003 dc= .01
v=1307
3. 36-0257
NaAlV2O7
Rombik
Groupa 30,53
Dexp. Dcal. d(D) h k l
8.3000 8.2811 .0189 1 0 0
6.9400 6.8792 .0608 1 1 0
6.1800 6.1785 .0015 0 2 0
4.1400 4.1405 -.0005 2 0 0
3.7400 3.7430 -.0030 1 2 1
3.4400 3.4396 .0004 2 2 0
3.3400 3.3419 -.0019 0 3 1
2.9500 2.9472 .0028 2 2 1
2.7600 2.7604 -.0004 3 0 0
a= 8.281 b=12.357 c= 5.717
da= .002 db= .006 dc= .004
V= 585.0
4. 38-0264
KCrV2O7
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
7.7800 7.8032 -.0232 0 1 0
5.2300 5.2400 -.0100 2 1 0
4.8600 4.8580 .0020 -1 0 1
4.1000 4.1016 -.0016 1 1 1
3.0400 3.0420 -.0020 -1 2 1
2.9000 2.8992 .0008 4 0 1
2.8400 2.8395 .0005 2 2 1
2.7500 2.7439 .0061 -4 1 1
2.5900 2.5876 .0024 3 2 1
2.4300 2.4290 .0010 -2 0 2
2.3200 2.3192 .0008 -2 1 2
2.2900 2.2901 -.0001 5 2 0
a= 14.14 b= 7.8032 c= 5.1509 beta= 90.67
da=.05 db=.0001 dc=.0005 dbeta=.01
V= 568.5
Triklin
Dexp Dcal d(D) h k l
7.7800 7.7701 .0099 1 0 0
5.2300 5.2357 -.0057 0 1 1
4.8600 4.8595 .0005 0 -1 1
4.1000 4.1008 -.0008 0 2 0
3.0400 3.0397 .0003 1 2 1
2.9000 2.8998 .0002 0 -1 2
2.8400 2.8397 .0003 2 0 2
2.7500 2.7509 -.0009 -1 1 2
2.5900 2.5900 -.0000 3 0 0
2.4300 2.4297 .0003 0 -2 2
2.3200 2.3199 .0001 1 3 0
2.2900 2.2901 -.0001 3 1 1
A= 8.6397 DA= .0006
B= 8.8545 DB= .0002
C= 6.594 DC= .001
GAMMA=111.728 DGAMMA= .009
BETA = 76.1159 DBETA = .0006
ALPHA= 91.129 DALPHA= .008
V= 453.6
5. 36-0309
alfa-Mg{VO3}2
Triklin
Dexp Dcal d(D) h k l
6.1500 6.1442 .0058 1 2 0
4.7000 4.6972 .0028 2 2 0
4.2600 4.2606 -.0006 1 3 0
3.4000 3.3999 .0001 3 0 0
3.2500 3.2547 -.0047 1 0 1
3.1200 3.1162 .0038 0 -1 1
3.0500 3.0497 .0003 0 4 0
2.7000 2.7004 -.0004 -1 4 0
2.6400 2.6408 -.0008 -3 2 0
2.4800 2.4815 -.0015 0 -3 1
2.4200 2.4198 .0002 2 4 1
2.1800 2.1795 .0005 -1 -4 1
A= 10.8919 DA= .0008
B= 12.9112 DB= .0003
C= 3.3254 DC= .0002
GAMMA= 71.150 DGAMMA= .006
BETA = 80.193 DBETA = .005
ALPHA= 83.82 DALPHA= .01
V=435.9
6. 36-0310
beta-Mg{VO3}2
Triklin
Dexp Dcal d(D) h k l
4.6500 4.6509 -.0009 -1 1 1
4.2300 4.2304 -.0004 0 -1 1
4.0800 4.0773 .0027 1 -1 1
3.7100 3.7124 -.0024 -1 -1 1
3.4900 3.4895 .0005 -2 1 1
3.2900 3.2935 -.0035 3 0 1
3.0300 3.0330 -.0030 1 -1 2
3.0200 3.0184 .0016 0 -1 2
2.8700 2.8698 .0002 -3 1 0
2.7900 2.7885 .0015 2 -1 2
2.6300 2.6301 -.0001 -1 2 2
2.3500 2.3495 .0005 4 1 1
A= 10.0266 DA= .0007
B= 6.092 DB= .001
C= 9.144 DC= .008
GAMMA= 87.406 DGAMMA= .004
BETA = 77.051 DBETA = .002
ALPHA= 72.252 DALPHA= .006
V=518.1
7. 36-0313
K1.11V3O8
Triklin
Dexp Dcal d(D) h k l
8.2000 8.1984 .0016 0 0 1
6.1100 6.1088 .0012 1 -1 1
4.0800 4.0843 -.0043 0 -2 1
3.4700 3.4694 .0006 -1 2 0
3.3900 3.3889 .0011 2 0 2
3.2600 3.2565 .0035 -2 1 0
3.2000 3.2006 -.0006 2 1 1
3.1100 3.1130 -.0030 -1 -1 2
2.9300 2.9285 .0015 1 -2 3
2.8900 2.8888 .0012 0 -1 3
2.7200 2.7208 -.0008 2 0 3
2.5500 2.5513 -.0013 3 -1 2
A= 7.760 DA= .009
B= 8.409 DB= .002
C= 9.53 DC= .01
GAMMA=100.31 DGAMMA= .03
BETA = 65.50 DBETA = .06
ALPHA=111.43 DALPHA= .06
V= 526.4
8. 36-0442
C2H10N2O14P2V2*5H2O
Triklin
Dexp Dcal d(D) h k l
8.7600 8.7593 .0007 1 0 0
7.4700 7.4603 .0097 0 1 0
6.2940 6.2937 .0003 0 -1 1
5.7180 5.7188 -.0008 1 -1 1
5.4640 5.4585 .0055 -1 1 0
5.2000 5.1921 .0079 0 1 1
4.3510 4.3515 -.0005 0 0 2
4.1160 4.1194 -.0034 0 -1 2
3.9640 3.9660 -.0020 2 1 1
3.7250 3.7301 -.0051 0 2 0
3.6930 3.6955 -.0025 0 -2 1
3.5160 3.5111 .0049 1 -2 1
A= 9.518 DA= .005
B= 7.603 DB= .007
C= 9.6032 DC= .0003
GAMMA= 89.47 DGAMMA= .03
BETA = 67.45 DBETA = .06
ALPHA=100.03 DALPHA= .09
V= 629.7
9. 36-0541
K6V2O8{SO3}4
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
6.5590 6.5555 .0035 -1 0 1
5.7680 5.7772 -.0092 1 1 0
5.1390 5.1531 -.0141 1 0 1
5.0460 5.0506 -.0046 0 1 1
4.8440 4.8439 .0001 -1 1 1
4.1870 4.1882 -.0012 1 1 1
4.0190 4.0227 -.0037 2 1 0
3.5960 3.5944 .0016 0 2 0
3.2060 3.2067 -.0007 0 2 1
3.0970 3.0948 .0022 1 0 2
2.9470 2.9481 -.0011 1 2 1
2.8410 2.8426 -.0016 1 1 2
a= 10.020 b= 7.189 c=7.326 beta= 104.34
da=.005 db= .003 dc=.002 dbeta=.01
V= 511.2
10. 36-0659
Na{NH4}2VO2F4
Rombik
Groupa 16
Dexp. Dcal. d(D) h k l
4.8700 4.8777 -.0077 1 0 0
4.3400 4.3225 .0175 0 2 0
2.9400 2.9437 -.0037 0 2 1
2.4400 2.4388 .0012 2 0 0
2.1100 2.1113 -.0013 1 3 1
1.8800 1.8780 .0020 2 2 1
1.7300 1.7290 .0010 0 5 0
1.6300 1.6296 .0004 1 5 0
1.5000 1.5006 -.0006 2 4 1
1.4100 1.4105 -.0005 2 5 0
1.3400 1.3400 .0000 0 0 3
a= 4.878 b= 8.645 c= 4.020
da= .002 db= .003 dc= .003
V= 169.5
11. 36-0694
K2V2S2O12
Monoklin
GRUPA 4,11
Dexp. Dcal. d(D) h k l
5.9300 5.9227 .0073 1 2 0
4.3660 4.3650 .0010 2 0 0
4.2180 4.2133 .0047 2 1 0
3.8440 3.8385 .0055 2 2 0
3.6630 3.6596 .0034 1 4 0
3.3830 3.3883 -.0053 2 3 0
3.9800 3.9819 -.0019 0 2 1
3.1360 3.1371 -.0011 1 3 1
3.0240 3.0249 -.0009 1 5 0
2.8580 2.8581 -.0001 -2 3 1
2.7880 2.7893 -.0013 1 4 1
2.5590 2.5590 .0000 3 3 0
2.4770 2.4757 .0013 1 5 1
a= 8.797 b= 16.124 c= 4.615 beta= 97.1
da=.002 db=.0013 dc=.008 dbet=.1
V=649.5
12. 36-0703
RbVO2SO4
Triklin
Dexp Dcal d(D) h k l
5.3360 5.3376 -.0016 -1 -1 1
4.5620 4.5578 .0042 1 1 1
4.3920 4.3903 .0017 -1 1 1
3.5230 3.5218 .0012 1 -1 1
3.4450 3.4396 .0054 0 2 2
3.2800 3.2770 .0030 -1 0 3
2.8410 2.8398 .0012 2 2 0
2.7610 2.7613 -.0003 1 3 1
2.5790 2.5820 -.0030 -2 -1 3
2.4860 2.4870 -.0010 1 3 2
2.3300 2.3302 -.0002 -1 3 1
2.2910 2.2921 -.0011 1 -2 2
A= 6.403 DA= .002
B= 8.754 DB= .001
C= 10.20 DC= .01
GAMMA= 74.35 DGAMMA= .05
BETA =105.44 DBETA = .03
ALPHA= 85.682 DALPHA= .001
V= 523.7
13. 36-0704
cSvo2so4
tRIKLIN
Dexp Dcal d(D) h k l
4.3000 4.2955 .0045 0 -1 1
4.1760 4.1729 .0031 1 1 0
3.6960 3.6960 -.0000 0 -3 1
3.5870 3.5866 .0004 -1 3 0
3.3190 3.3201 -.0011 0 -4 1
3.2060 3.2039 .0021 1 0 1
3.1360 3.1382 -.0022 1 1 1
3.0830 3.0831 -.0001 1 -2 1
3.0010 3.0014 -.0004 1 2 1
2.9250 2.9237 .0013 -1 0 1
2.8790 2.8799 -.0009 -1 1 1
2.8240 2.8235 .0005 0 5 1
A= 4.3024 DA= .0006
B= 19.3724 DB= .0002
C= 4.3796 DC= .0001
GAMMA= 90.9055 DGAMMA= .0004
BETA = 84.731 DBETA = .008
ALPHA= 92.939 DALPHA= .001
V=363.6
14. 36-0705
K3VO2{SO4}2
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
6.5590 6.5558 .0032 -1 0 1
5.7680 5.7757 -.0077 1 1 0
5.1390 5.1532 -.0142 1 0 1
5.0460 5.0499 -.0039 0 1 1
4.8440 4.8433 .0007 -1 1 1
4.1870 4.1878 -.0008 1 1 1
4.0190 4.0221 -.0031 2 1 0
3.5960 3.5932 .0028 0 2 0
3.2060 3.2058 .0002 0 2 1
3.0970 3.0949 .0021 1 0 2
2.9470 2.9474 -.0004 1 2 1
2.8410 2.8425 -.0015 1 1 2
a= 10.019 b=7.186 c= 7.327 beta= 104.34
da=.003 db=.004 dc=.003 dbeta=.03
V=511.1
15. 36-0706
Rb3VO2{SO4}2
Triklin
Dexp Dcal d(D) h k l
3.9240 3.9204 .0036 -1 3 0
3.8700 3.8695 .0005 0 4 0
3.5590 3.5610 -.0020 2 1 0
3.4850 3.4814 .0036 0 0 1
3.4060 3.4032 .0028 2 2 0
3.3530 3.3531 -.0001 -2 1 0
3.3290 3.3266 .0024 0 1 1
3.1400 3.1405 -.0005 -1 -2 1
3.0970 3.0956 .0014 0 5 0
3.0500 3.0504 -.0004 -1 1 1
3.0310 3.0285 .0025 0 -3 1
2.9700 2.9733 -.0033 1 1 1
A= 7.1751 DA= .0002
B= 15.7225 DB= .0009
C= 3.5101 DC= .0008
GAMMA= 81.625 DGAMMA= .003
BETA = 94.64 DBETA = .03
ALPHA= 96.297 DALPHA= .006
V=389.0
16. 36-0707
Cs3VO2{SO4)2
Triklin
Dexp Dcal d(D) h k l
4.0810 4.0904 -.0094 0 1 1
3.9830 3.9871 -.0041 0 -1 1
3.6900 3.6890 .0010 1 1 0
3.6100 3.6100 -.0000 0 -1 2
3.5590 3.5669 -.0079 2 0 1
3.4850 3.4824 .0026 -1 -1 1
3.4450 3.4459 -.0009 2 0 2
3.2520 3.2541 -.0021 1 -1 2
3.1290 3.1286 .0004 0 0 5
2.8150 2.8153 -.0003 2 1 1
2.7730 2.7704 .0026 2 1 0
2.6240 2.6213 .0027 2 -1 1
A= 7.158 DA= .004
B= 4.195 DB= .002
C= 15.94 DC= .01
GAMMA= 86.0 DGAMMA= .1
BETA = 79.3 DBETA = .1
ALPHA= 86.4 DALPHA= .1
V=469.6
17. 36-0708
Rb4V2O4{SO4}2S2O7
Triklin
Dexp Dcal d(D) h k l
5.2600 5.2601 -.0001 0 1 1
4.9620 4.9535 .0085 0 -1 1
4.1760 4.1841 -.0081 -1 -1 1
4.1110 4.1146 -.0036 1 0 1
3.8800 3.8820 -.0020 0 2 0
3.7450 3.7445 .0005 -1 2 1
3.6660 3.6588 .0072 -2 1 1
3.5590 3.5566 .0024 -1 0 2
3.4210 3.4191 .0019 -2 1 0
3.3810 3.3819 -.0009 0 0 2
3.1140 3.1149 -.0009 -2 2 1
3.0520 3.0504 .0016 1 2 0
A= 7.506 DA= .004
B= 8.1256 DB= .0008
C= 7.3066 DC= .0006
GAMMA=106.82 DGAMMA= .02
BETA =111.973 DBETA = .003
ALPHA= 80.69 DALPHA= .02
V=395.6
18. 36-0709
Cs4V2O4{SO4}2S2O7
Triklin
Dexp Dcal d(D) h k l
4.2470 4.2511 -.0041 1 2 0
4.0920 4.0915 .0005 -1 1 1
3.8700 3.8739 -.0039 2 0 0
3.8240 3.8248 -.0008 0 3 0
3.6750 3.6776 -.0026 -1 -2 1
3.5310 3.5261 .0049 -2 2 0
3.4820 3.4810 .0010 2 1 0
3.4290 3.4269 .0021 1 -2 1
3.3040 3.3029 .0011 -2 1 1
3.2290 3.2303 -.0013 1 1 1
3.2060 3.2033 .0027 1 3 0
3.0110 3.0136 -.0026 -2 3 0
A= 8.0865 DA= .0001
B= 11.80365 DB= .00006
C= 4.84082 DC= .00001
GAMMA= 98.3352 DGAMMA= .0003
BETA =102.8915 DBETA = .0001
ALPHA= 98.49020 DALPHA= .00002
V=437.8
19. 36-0835
V6Ga2O13
Rombik
Groupa 29,57
Dexp. Dcal. d(D) h k l
4.7000 4.6995 .0005 2 0 0
3.4000 3.4008 -.0008 2 1 0
2.8440 2.8447 -.0007 0 0 2
2.6410 2.6439 -.0029 3 1 0
2.4640 2.4638 .0002 0 2 0
2.4330 2.4336 -.0006 2 0 2
2.3830 2.3833 -.0003 1 2 0
2.1820 2.1821 -.0001 2 2 0
1.9350 1.9367 -.0017 3 2 0
1.8630 1.8624 .0006 0 2 2
1.7020 1.7004 .0016 4 2 0
1.6000 1.6009 -.0009 3 2 2
1.5500 1.5506 -.0006 2 3 0
1.4930 1.4929 .0001 6 1 0
1.4230 1.4224 .0006 0 3 2
a= 9.399 b= 4.928 c= 5.6893
da= .001 db= .001 dc= .0002
v= 263.50
20. 36-838
V6GeO12
Rombik
Groupa 33,49,62
Dexp. Dcal. d(D) h k l
4.2300 4.2269 .0031 2 0 1
3.2200 3.2175 .0025 1 1 1
3.0400 3.0392 .0008 0 1 3
2.9870 2.9885 -.0015 0 0 6
2.8610 2.8691 -.0081 1 1 3
2.7640 2.7670 -.0030 2 0 5
2.6470 2.6421 .0049 1 1 4
2.6220 2.6210 .0010 2 1 2
2.4900 2.4913 -.0013 2 1 3
2.4650 2.4631 .0019 2 0 6
a= 8.699 b= 3.530 c=17.931
da= .007 db= .002 dc= .005
V= 551
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
4.2300 4.2300 .0000 -1 1 1
3.2200 3.2245 -.0045 0 2 0
3.0400 3.0424 -.0024 -1 0 2
2.9870 2.9875 -.0005 1 2 0
2.8610 2.8650 -.0040 2 0 1
2.7640 2.7680 -.0040 -3 0 1
2.6470 2.6463 .0007 3 0 0
2.6220 2.6182 .0038 2 1 1
2.4900 2.4885 .0015 -2 2 1
2.4650 2.4651 -.0001 1 0 2
a= 8.39 b= 6.449 c= 6.090 beta= 108.85
da=.01 db=.004 dc=.002 dbeta=.05
V= 311.8
21. 36-1150
Tl3ScV2O8
Triklin
Dexp Dcal d(D) h k l
4.2300 4.2288 .0012 2 0 1
4.0400 4.0411 -.0011 2 1 1
3.8700 3.8687 .0013 0 -1 1
3.6300 3.6281 .0019 -1 -1 1
3.1900 3.1893 .0007 3 1 1
3.1400 3.1406 -.0006 3 0 1
3.0700 3.0696 .0004 -2 -1 1
2.8900 2.8894 .0006 1 2 1
2.7700 2.7706 -.0006 2 2 0
2.5900 2.5897 .0003 -1 2 0
2.5100 2.5101 -.0001 -1 1 2
2.4500 2.4504 -.0004 0 -2 1
A= 10.3629 DA= .0004
B= 6.01752 DB= .00002
C= 6.2339 DC= .0006
GAMMA= 74.1894 DGAMMA= .0008
BETA = 75.624 DBETA = .002
ALPHA= 78.405 DALPHA= .001
V=358.7
22. 36-1151
TlYV2O8
Triklin
Dexp Dcal d(D) h k l
5.1500 5.1488 .0012 -1 0 1
3.5700 3.5703 -.0003 -1 0 2
3.4100 3.4110 -.0010 -1 2 0
3.3500 3.3529 -.0029 0 2 0
3.2900 3.2887 .0013 0 -2 1
3.0900 3.0892 .0008 1 1 2
3.0400 3.0403 -.0003 -2 1 1
2.9000 2.9007 -.0007 0 -1 3
2.6700 2.6712 -.0012 2 1 1
2.6400 2.6395 .0005 -1 0 3
2.3600 2.3574 .0026 1 -3 1
2.1400 2.1397 .0003 2 -3 2
A= 7.239 DA= .003
B= 7.095 DB= .001
C= 9.284 DC= .009
GAMMA=107.57 DGAMMA= .03
BETA = 79.92 DBETA = .05
ALPHA=100.17 DALPHA= .08
V=443.0
23. 36-1152
Tl3V2O8
Triklin
Dexp. Dcal. d(D) h k l
3.6600 3.6603 -.0003 4 0 0
3.4800 3.4821 -.0021 -3 -2 0
3.1400 3.1397 .0003 -2 -3 0
2.9900 2.9899 .0001 1 0 1
2.9200 2.9192 .0008 -4 -2 0
2.7200 2.7204 -.0004 -2 1 1
2.6100 2.6096 .0004 1 -2 1
2.5300 2.5307 -.0007 3 1 1
2.3800 2.3797 .0003 3 -2 1
2.1500 2.1493 .0007 4 2 1
2.0600 2.0595 .0005 -4 -2 1
1.9100 1.9099 .0001 -5 -4 0
A= 14.706 DA= .001
B= 10.919 DB= .002
C= 3.03493 DC= .00009
GAMMA= 95.020 DGAMMA= .005
BETA = 88.14 DBETA = .03
ALPHA= 88.588 DALPHA= .003
V= 485.0
24. 36-1153
Tl3NdV2O8
Triklin
Dexp Dcal d(D) h k l
5.2700 5.2776 -.0076 0 1 1
4.8300 4.8367 -.0067 0 -1 1
4.2900 4.2903 -.0003 -2 -1 1
4.0300 4.0269 .0031 2 1 1
3.6600 3.6598 .0002 0 2 0
3.4100 3.4091 .0009 -4 1 0
3.3500 3.3501 -.0002 -4 1 1
3.2600 3.2600 -.0000 1 0 2
3.0900 3.0911 -.0011 4 0 1
3.0400 3.0408 -.0008 0 -1 2
2.9800 2.9796 .0004 -2 -1 2
2.9000 2.8990 .0010 1 -1 2
A= 15.429 DA= .001
B= 7.357 DB= .001
C= 7.114 DC= .002
GAMMA= 92.94 DGAMMA= .02
BETA =100.989 DBETA = .003
ALPHA= 84.546 DALPHA= .007
V=786.6
25. 36-1154
TlEuV2O8
Triklin
Dexp Dcal d(D) h k l
3.8700 3.8680 .0020 0 2 1
3.6500 3.6511 -.0011 0 -2 1
3.4000 3.4003 -.0003 1 2 1
3.3300 3.3281 .0019 1 -2 1
3.2600 3.2614 -.0014 -1 -2 1
3.0800 3.0771 .0029 -1 0 3
3.0300 3.0299 .0001 0 -2 2
2.9800 2.9808 -.0008 1 2 2
2.7700 2.7700 .0000 -2 2 1
2.7300 2.7327 -.0027 2 2 0
2.6900 2.6902 -.0002 0 2 3
2.4500 2.4485 .0015 2 2 2
A= 7.6450 DA= .0001
B= 8.1317 DB= .0004
C= 10.066 DC= .001
GAMMA= 92.017 DGAMMA= .001
BETA = 90.890 DBETA = .008
ALPHA= 85.215 DALPHA= .007
V=623.2
26. 36-1155
Tl3TbV2O8
Triklin
Dexp Dcal d(D) h k l
3.6300 3.6267 .0033 0 1 0
3.2900 3.2899 .0001 1 0 2
3.0300 3.0273 .0027 0 -1 2
2.9500 2.9506 -.0006 -1 -1 1
2.6700 2.6689 .0011 1 1 1
2.6200 2.6200 .0000 2 0 1
2.2300 2.2294 .0006 1 1 2
2.1300 2.1284 .0016 -2 -1 1
1.8600 1.8597 .0003 0 -2 1
1.8300 1.8292 .0008 2 1 2
1.7900 1.7907 -.0007 3 0 1
1.7300 1.7296 .0004 -1 2 0
1.7100 1.7113 -.0013 1 2 0
1.6100 1.6101 -.0001 1 2 1
1.5800 1.5802 -.0002 0 0 5
A= 5.453 DA= .005
B= 3.721 DB= .001
C= 8.1199 DC= .0006
GAMMA= 91.82 DGAMMA= .01
BETA = 86.32 DBETA = .04
ALPHA=102.92 DALPHA= .04
V= 160.2
27. 36-1156
Tl3HoV2O8
Triklin
Dexp Dcal d(D) h k l
5.2600 5.2419 .0181 1 0 0
3.9700 3.9648 .0052 0 1 1
3.8200 3.8279 -.0079 0 -1 1
3.4200 3.4165 .0035 -1 1 0
3.3100 3.3050 .0050 1 1 0
3.1200 3.1244 -.0044 0 1 2
3.0600 3.0547 .0053 -1 1 1
2.9900 2.9920 -.0020 0 -1 2
2.8500 2.8464 .0036 0 0 3
2.6800 2.6814 -.0014 2 0 1
2.5300 2.5311 -.0011 -1 1 2
2.3600 2.3604 -.0004 -2 0 1
A= 5.3828 DA= .0002
B= 4.3816 DB= .0002
C= 8.772 DC= .001
GAMMA= 91.42 DGAMMA= .01
BETA = 77.01 DBETA = .01
ALPHA= 87.91 DALPHA= .01
V=201.4
28. 36-1157
TlErV2O8
Rombik
Grupa 16
Dexp. Dcal. d(D) h k l
3.9200 3.9250 -.0050 1 1 1
3.5600 3.5650 -.0050 2 1 1
3.4000 3.4025 -.0025 0 0 3
3.2900 3.2962 -.0062 3 1 0
3.0900 3.0898 .0002 2 0 3
3.0500 3.0503 -.0003 2 1 2
2.9500 2.9517 -.0017 5 0 0
2.6600 2.6566 .0034 1 1 3
2.5100 2.5145 -.0045 1 0 4
2.3700 2.3674 .0026 3 1 3
2.2100 2.2125 -.0025 0 1 4
2.1500 2.1516 -.0016 6 1 0
a=14.758 b= 4.440 c=10.207
da= .005 db= .002 dc= .001
V= 668.
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
3.9200 3.9156 .0044 3 0 1
3.5600 3.5575 .0025 0 1 0
3.4000 3.4061 -.0061 1 1 0
3.2900 3.2900 .0000 0 0 5
3.0900 3.0895 .0005 1 0 5
3.0500 3.0534 -.0034 3 0 3
2.9500 2.9498 .0002 4 0 0
2.6600 2.6589 .0011 -3 0 5
2.5100 2.5113 -.0013 -2 1 4
2.3700 2.3697 .0003 -5 0 1
2.2100 2.2100 .0000 5 0 2
2.1500 2.1497 .0003 3 0 6
a= 11.86 b= 3.5575 c=16.534 beta=95.78
da=.01 db=.0006 dc=.004 dbeta=.04
V= 694.0
Triklin
Dexp Dcal d(D) h k l
3.9200 3.9157 .0043 -1 1 1
3.5600 3.5598 .0002 1 1 0
3.4000 3.4016 -.0016 -1 -1 1
3.2900 3.2870 .0030 1 0 1
3.0900 3.0916 -.0016 1 2 0
3.0500 3.0542 -.0042 -1 3 2
2.9500 2.9505 -.0005 1 2 1
2.6600 2.6596 .0004 -1 4 2
2.5100 2.5093 .0007 -1 -2 2
2.3700 2.3699 .0001 0 1 4
2.2100 2.2094 .0006 -1 5 3
2.1500 2.1502 -.0002 1 0 3
A= 3.9769 DA= .0006
B= 12.692 DB= .008
C= 9.9834 DC= .0003
GAMMA= 99.781 DGAMMA= .005
BETA =104.78 DBETA = .01
ALPHA= 66.60 DALPHA= .02
V=445.8
29. 36-1158
TlYbV2O8
Triklin
Dexp Dcal d(D) h k l
5.0400 5.0378 .0022 0 -1 1
4.2300 4.2313 -.0013 -1 1 1
3.8200 3.8201 -.0001 1 -1 1
3.5000 3.4995 .0005 -2 1 0
3.3000 3.3011 -.0011 -1 2 0
3.2500 3.2497 .0003 0 -2 1
3.0800 3.0818 -.0018 -1 -1 2
2.9200 2.9203 -.0003 2 1 0
2.4000 2.4003 -.0003 2 -2 1
2.3400 2.3399 .0001 -3 -1 1
2.2600 2.2599 .0001 -1 3 0
2.1300 2.1299 .0001 -1 -1 3
A= 7.9265 DA= .0008
B= 6.919 DB= .002
C= 6.466 DC= .001
GAMMA= 97.5887 DGAMMA= .0001
BETA =111.33 DBETA = .04
ALPHA=100.138 DALPHA= .006
V= 317.7
30. 36-1214
Rb3V5O14
Rombik
Groupa 32,55
Dexp. Dcal. d(D) h k l
5.2500 5.2573 -.0073 0 0 1
4.3000 4.3018 -.0018 2 0 1
3.3500 3.3495 .0005 0 2 1
3.0500 3.0484 .0016 4 0 1
2.8440 2.8443 -.0003 1 3 0
2.6290 2.6287 .0003 0 0 2
2.5040 2.5053 -.0013 3 3 0
2.2490 2.2492 -.0002 0 2 2
2.1730 2.1728 .0002 0 4 0
2.0870 2.0866 .0004 2 4 0
1.9920 1.9921 -.0001 3 4 0
1.9310 1.9310 -.0000 7 1 1
a=14.966 b= 8.691 c= 5.257
da= .003 db= .001 dc= .002
V= 683.8
31. 36-1215
Rb2V6O16
Triklin
Dexp Dcal d(D) h k l
7.7600 7.7503 .0097 1 0 0
6.8900 6.8918 -.0018 -1 1 0
5.7000 5.7080 -.0080 -1 0 1
3.9600 3.9594 .0006 -2 1 0
3.5200 3.5213 -.0013 -2 2 1
3.2020 3.2008 .0012 -1 1 2
2.0140 2.0139 .0001 1 -3 2
2.9080 2.9075 .0005 2 -1 1
2.8540 2.8540 .0000 -2 0 2
2.5970 2.5973 -.0003 -2 -2 1
2.4750 2.4754 -.0004 0 -2 2
2.3920 2.3920 .0000 1 3 1
2.1930 2.1927 .0003 -2 -2 2
2.1190 2.1189 .0001 -4 1 1
2.0190 2.0191 -.0001 3 1 1
A= 8.503 DA= .001
B= 9.73308 DB= .00006
C= 6.4997 DC= .0004
GAMMA=107.14 DGAMMA= .01
BETA =109.310 DBETA = .005
ALPHA= 80.754 DALPHA= .003
V= 483.9
32. 36-1265
K3V{SO4}3
Triklin
Dexp Dcal d(D) h k l
7.2550 7.2551 -.0001 1 0 1
6.3710 6.3792 -.0082 0 1 0
4.4970 4.5016 -.0046 0 -1 2
4.2910 4.2906 .0004 1 0 3
4.2180 4.2232 -.0052 -1 -1 1
3.5560 3.5560 -.0000 0 -1 3
3.2710 3.2703 .0007 2 -1 1
3.0320 3.0359 -.0039 -1 1 3
2.8050 2.8022 .0028 1 2 2
2.7630 2.7630 -.0000 1 -2 2
2.5190 2.5195 -.0005 3 0 1
2.4620 2.4617 .0003 0 1 5
A= 7.5831 DA= .0007
B= 6.383 DB= .003
C= 13.637 DC= .002
GAMMA= 90.49 DGAMMA= .02
BETA = 74.778 DBETA = .002
ALPHA= 88.23 DALPHA= .04
V= 636.5
33. 36-1713
C20H40Cl5O5VZn
Triklin
Dexp Dcal d(D) h k l
10.7000 10.7057 -.0057 1 0 0
9.3000 9.3221 -.0221 0 1 1
8.3400 8.3442 -.0042 0 -1 1
7.4300 7.4528 -.0228 -1 1 0
7.0200 7.0227 -.0027 1 1 1
6.2700 6.2578 .0122 1 -1 1
5.4000 5.3988 .0012 0 2 1
5.1800 5.1801 -.0001 -2 0 1
5.0900 5.0882 .0018 1 2 0
4.5000 4.5015 -.0015 -2 0 2
4.3700 4.3687 .0013 1 -2 1
4.2700 4.2701 -.0001 1 2 2
4.1700 4.1721 -.0021 0 -2 2
4.0400 4.0397 .0003 -1 -2 2
3.7500 3.7490 .0010 -2 0 3
A= 10.775 DA= .006
B= 11.222 DB= .009
C= 14.497 DC= .004
GAMMA= 86.49 DGAMMA= .06
BETA = 95.08 DBETA = .01
ALPHA= 83.814 DALPHA= .004
V= 1731.4