1. 28-0024
AlInV2O8
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
4.7900 4.7872 .0028 1 1 0
4.2900 4.2879 .0021 0 1 2
3.9000 3.9051 -.0051 1 0 2
3.6100 3.6111 -.0011 1 2 1
3.3300 3.3313 -.0013 1 2 1
2.8900 2.8894 .0006 1 3 0
2.7300 2.7282 .0018 2 0 1
2.5700 2.5701 -.0001 1 3 2
2.5400 2.5379 .0021 -1 0 3
2.3600 2.3604 -.0004 0 0 4
2.1900 2.1910 -.0010 -2 0 2
2.1300 2.1306 -.0006 2 3 1
A= 5.49349 DA= .00003
B= 10.245 DB= .001
C= 9.5840 DC= .0004
BETA = 80.12 DBETA = .02
V=530.8
Triklin
Dexp Dcal d(D) h k l
4.7900 4.7888 .0012 -1 2 0
4.2900 4.2914 -.0014 0 0 1
3.9000 3.9019 -.0019 0 -2 1
3.6100 3.6097 .0003 -1 4 0
3.3300 3.3322 -.0022 -1 2 1
2.8900 2.8891 .0009 1 -3 1
2.7300 2.7318 -.0018 0 7 0
2.5700 2.5698 .0002 0 6 1
2.5400 2.5404 -.0004 -2 3 0
2.3600 2.3596 .0004 -2 -2 1
2.1900 2.1892 .0008 -1 8 0
2.1300 2.1302 -.0002 0 -1 2
A= 5.5824 DA= .0006
B= 19.124 DB= .008
C= 4.3083 DC= .0008
GAMMA= 89.56 DGAMMA= .03
BETA = 95.070 DBETA = .002
ALPHA= 89.53 DALPHA= .03
V= 458.1
2. 28-0087
{NH4}2VCl5*H2O
Triklin
Dexp Dcal d(D) h k l
6.2800 6.2886 -.0086 1 1 0
5.7100 5.7072 .0028 1 1 1
5.3000 5.3071 -.0071 1 -1 1
4.9300 4.9331 -.0031 1 2 0
3.8500 3.8475 .0025 1 3 1
3.5700 3.5681 .0019 0 -3 1
3.4100 3.4076 .0024 -1 -2 1
3.0700 3.0701 -.0001 0 -1 2
2.9880 2.9882 -.0002 2 1 2
2.8760 2.8770 -.0010 1 -4 1
2.8080 2.8073 .0007 0 -2 2
2.7510 2.7526 -.0016 -1 4 1
A= 7.620 DA= .009
B= 13.961 DB= .002
C= 6.995 DC= .004
GAMMA= 87.95 DGAMMA= .01
BETA = 68.51 DBETA = .06
ALPHA= 83.06 DALPHA= .01
V= 687.3
3. 28-0088
{NH4}3VO2F4
Triklin
Dexp Dcal d(D) h k l
4.6100 4.6105 -.0005 0 1 1
4.4900 4.4926 -.0026 0 -1 1
3.9500 3.9506 -.0006 1 1 0
2.8400 2.8410 -.0010 1 -2 1
2.8000 2.8001 -.0001 0 2 1
2.7500 2.7467 .0033 0 -2 1
2.4900 2.4891 .0009 2 -1 2
2.4000 2.4000 -.0000 1 2 1
2.3700 2.3679 .0021 -2 -1 1
2.3100 2.3095 .0005 -1 -2 1
2.1900 2.1911 -.0011 3 0 0
2.1300 2.1300 .0000 0 -1 3
A= 6.864 DA= .005
B= 6.2959 DB= .0005
C= 6.9282 DC= .0004
GAMMA=105.74 DGAMMA= .03
BETA = 84.435 DBETA = .005
ALPHA= 90.08 DALPHA= .01363
V= 286.7
4. 28-0088
{NH4}3VO2F4
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
4.6100 4.6093 .0007 2 1 0
4.4900 4.4918 -.0018 0 2 0
3.9500 3.9499 .0001 2 1 1
2.8400 2.8396 .0004 0 0 3
2.8000 2.7996 .0004 3 2 0
2.7500 2.7489 .0011 -1 3 1
2.4900 2.4895 .0005 -2 1 3
2.4000 2.4002 -.0002 0 2 3
2.3700 2.3665 .0035 1 3 2
2.3100 2.3098 .0002 -3 0 3
2.1900 2.1898 .0002 4 2 1
2.1300 2.1297 .0003 0 0 4
a= 10.76972 b= 8.9837 c= 8.542 beta= 94.254
da= .00007 db=.0004 dc=.002 dbeta=.009
V= 824.2
Triklin
Dexp Dcal d(D) h k l
4.6100 4.6105 -.0005 0 1 1
4.4900 4.4926 -.0026 0 -1 1
3.9500 3.9506 -.0006 1 1 0
2.8400 2.8410 -.0010 1 -2 1
2.8000 2.8001 -.0001 0 2 1
2.7500 2.7467 .0033 0 -2 1
2.4900 2.4891 .0009 2 -1 2
2.4000 2.4000 -.0000 1 2 1
2.3700 2.3679 .0021 -2 -1 1
2.3100 2.3095 .0005 -1 -2 1
2.1900 2.1911 -.0011 3 0 0
2.1300 2.1300 .0000 0 -1 3
A= 6.864 DA= .005
B= 6.2959 DB= .0005
C= 6.9282 DC= .0004
GAMMA=105.74 DGAMMA= .03
BETA = 84.435 DBETA = .005
ALPHA= 90.08 DALPHA= .01363
V= 286.7
5. 28-0089
{NH4}4V2O3{SO4}4
Triklin
Dexp Dcal d(D) h k l
9.5000 9.5102 -.0102 1 1 0
7.8200 7.8251 -.0051 0 1 1
7.5400 7.5077 .0323 0 -1 1
6.8200 6.8258 -.0058 1 1 1
6.5000 6.4995 .0005 -1 0 1
6.1000 6.1185 -.0185 0 -2 1
5.8600 5.8597 .0003 -1 2 1
5.0600 5.0612 -.0012 2 1 1
4.9300 4.9271 .0029 0 -3 1
4.8000 4.8002 -.0002 -2 1 1
4.6000 4.5998 .0002 2 -3 1
4.4400 4.4386 .0014 2 2 1
A= 13.267 DA= .002
B= 19.684 DB= .007
C= 8.490 DC= .002
GAMMA=104.222 DGAMMA= .005
BETA = 80.84 DBETA = .01
ALPHA= 89.167 DALPHA= .001
v=2118
6. 28-0091
alfa-{NH4}3V{SO4}3
Triklin
Dexp Dcal d(D) h k l
7.6000 7.6051 -.0051 1 1 0
4.3400 4.3402 -.0002 -1 2 0
4.2200 4.2246 -.0046 2 1 0
4.1600 4.1631 -.0031 2 0 0
3.9900 3.9921 -.0021 1 2 1
3.7000 3.6987 .0013 -1 2 1
3.3800 3.3775 .0025 2 1 1
3.3300 3.3289 .0011 0 -3 1
3.2100 3.2094 .0006 2 3 0
2.9530 2.9531 -.0001 1 4 0
2.8610 2.8612 -.0002 1 -3 1
2.8280 2.8283 -.0003 0 2 2
A= 8.584 DA= .006
B= 11.920 DB= .003
C= 6.520 DC= .004
GAMMA= 77.248 DGAMMA= .002
BETA = 96.21 DBETA = .09
ALPHA= 91.48 DALPHA= .09
V=646.1
7. 28-0091
alfa-{NH4}3V{SO4}3
Triklin
Dexp Dcal d(D) h k l
7.6000 7.6051 -.0051 1 1 0
4.3400 4.3402 -.0002 -1 2 0
4.2200 4.2246 -.0046 2 1 0
4.1600 4.1631 -.0031 2 0 0
3.9900 3.9921 -.0021 1 2 1
3.7000 3.6987 .0013 -1 2 1
3.3800 3.3775 .0025 2 1 1
3.3300 3.3289 .0011 0 -3 1
3.2100 3.2094 .0006 2 3 0
2.9530 2.9531 -.0001 1 4 0
2.8610 2.8612 -.0002 1 -3 1
2.8280 2.8283 -.0003 0 2 2
A= 8.584 DA= .006
B= 11.920 DB= .003
C= 6.520 DC= .004
GAMMA= 77.248 DGAMMA= .002
BETA = 96.21 DBETA = .09
ALPHA= 91.48 DALPHA= .09
V=646.1
8. 28-0092
beta-{NH4}3V{SO4}3
Monoklin
GRUPA 3
Dexp. Dcal. d(D) h k l
7.6700 7.6526 .0174 0 1 0
4.4200 4.4219 -.0019 0 1 1
4.3700 4.3774 -.0074 1 1 1
4.2500 4.2536 -.0036 2 0 1
4.2500 4.2522 -.0022 2 1 0
3.4100 3.4096 .0004 3 0 0
3.3500 3.3459 .0041 -2 0 1
2.9940 2.9931 .0009 3 1 1
2.8810 2.8815 -.0005 -1 2 1
2.8450 2.8447 .0003 2 2 1
2.7880 2.7864 .0016 1 0 2
2.6670 2.6684 -.0014 2 0 2
a= 10.528 b=7.653 c= 5.575 beta= 76.35
da=.009 db=.004 dc=.002 dbet=.03
V=436.8
9. 28-0093
{NH4}2{VO}2{SO4}3
Triklin
Dexp Dcal d(D) h k l
7.6200 7.6184 .0016 0 1 1
5.8600 5.8640 -.0040 -1 1 1
5.6900 5.6848 .0052 0 -1 1
4.9400 4.9386 .0014 -1 -1 1
4.4900 4.4903 -.0003 -1 0 2
3.9700 3.9741 -.0041 -2 1 1
3.8700 3.8672 .0028 1 2 0
3.8100 3.8092 .0008 0 2 2
3.5100 3.5077 .0023 0 1 3
3.5000 3.5044 -.0044 -1 2 2
3.4300 3.4271 .0029 -2 1 2
3.3300 3.3322 -.0022 -1 -2 1
A= 9.458 DA= .001
B= 8.72295 DB= .00009
C= 10.59891 DC= .00001
GAMMA= 88.088 DGAMMA= .008
BETA = 90.077 DBETA = .007
ALPHA= 73.152 DALPHA= .003
V=836.5
10. 28-0094
{NH4}2VO{SO4}2
Triklin
Dexp Dcal d(D) h k l
10.1000 10.1191 -.0191 -1 1 0
7.0800 7.0826 -.0026 0 1 1
6.8300 6.8374 -.0074 0 -1 1
6.2300 6.2249 .0051 1 1 0
6.1200 6.1281 -.0081 -2 1 0
4.8000 4.7954 .0046 1 -1 2
4.3400 4.3427 -.0027 2 0 2
4.2400 4.2398 .0002 0 -1 2
4.0200 4.0219 -.0019 2 -2 2
3.9100 3.9100 .0000 -1 1 2
3.8100 3.8079 .0021 3 -1 2
3.7900 3.7888 .0012 1 -3 0
A= 13.1084 DA= .0004
B= 11.6059 DB= .0004
C= 10.08222 DC= .00001
GAMMA=117.766 DGAMMA= .001
BETA = 69.8933 DBETA = .0001
ALPHA= 97.522 DALPHA= .001
V=1273.7
11. 28-0095
{NH4}2VO{SO4}2*0.25H2O
Rombik
Groupa 26,28,51
Dexp. Dcal. d(D) h k l
7.0500 7.0310 .0190 1 1 0
5.5400 5.5583 -.0183 1 0 1
4.1300 4.1318 -.0018 1 3 0
3.5600 3.5652 -.0052 2 0 1
3.4700 3.4676 .0024 1 0 2
3.3900 3.3922 -.0022 0 2 2
3.2900 3.2946 -.0046 1 4 0
3.0900 3.0878 .0022 2 3 0
2.8910 2.8887 .0023 0 5 0
2.7820 2.7791 .0029 2 0 2
2.2020 2.2024 -.0004 2 4 2
2.1370 2.1372 -.0002 2 1 3
a= 8.049 b=14.44 c= 7.6848
da= .001 db= .01 dc= .0001
V= 893.4
12. 28-0203
Cd3V2O8
Triklin
Dexp Dcal d(D) h k l
6.1900 6.1967 -.0067 -1 0 2
5.2800 5.2788 .0012 -1 1 1
5.0700 5.0687 .0013 1 -1 1
4.4600 4.4599 .0001 0 -1 3
4.1500 4.1504 -.0004 -1 0 4
4.0000 3.9996 .0004 -2 0 1
3.8500 3.8500 -.0000 2 0 2
3.7700 3.7693 .0007 0 -1 4
3.4800 3.4785 .0015 0 2 1
3.4000 3.4014 -.0014 0 2 2
3.2300 3.2278 .0022 -1 2 1
3.2100 3.2125 -.0025 -1 2 0
A= 8.2428 DA= .0002
B= 6.9646 DB= .0004
C= 19.846 DC= .001
GAMMA= 91.254 DGAMMA= .005
BETA = 88.016 DBETA = .004
ALPHA= 82.310 DALPHA= .006
V-1127
13. 28-0250
Ca2V6O17
Triklin
Dexp Dcal d(D) h k l
4.8800 4.8770 .0030 -1 1 0
4.5500 4.5478 .0022 1 -1 1
4.3800 4.3827 -.0027 0 -1 1
3.5600 3.5585 .0015 -1 1 1
3.4000 3.4007 -.0007 0 0 2
3.2000 3.1962 .0038 1 -1 2
2.9600 2.9602 -.0002 0 2 0
2.8800 2.8811 -.0011 2 0 2
2.6100 2.6114 -.0014 -1 0 2
2.4390 2.4385 .0005 -2 2 0
2.2720 2.2739 -.0019 2 -2 2
1.9220 1.9214 .0006 2 -2 3
1.8360 1.8359 .0001 3 1 0
A= 6.877 DA= .002
B= 6.084 DB= .001
C= 7.315 DC= .004
GAMMA=103.14 DGAMMA= .08
BETA = 68.52 DBETA = .01
ALPHA= 92.77 DALPHA= .03
V= 277.1
14. 28-0251
Ca7V4O17
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
8.4900 8.4609 .0291 1 0 0
5.4000 5.4026 -.0026 -1 0 1
5.4000 5.3975 .0025 1 1 0
4.8900 4.8854 .0046 1 0 2
4.2300 4.2304 -.0004 2 0 0
4.0100 4.0078 .0022 1 1 2
3.6200 3.6218 -.0018 2 1 0
3.5000 3.5044 -.0044 0 2 0
3.4300 3.4292 .0008 -2 0 1
3.2400 3.2377 .0023 1 2 0
3.2000 3.1985 .0015 -1 1 2
3.2000 3.1953 .0047 1 2 1
a= 9.037 b=7.009 c= 9.995 beta= 69.43
da=.004 db=.002 dc=.01 dbeta=.05
V= 592.7
Triklin
Dexp Dcal d(D) h k l
8.4900 8.4819 .0081 1 0 0
5.4000 5.3917 .0083 1 1 1
4.8900 4.8941 -.0041 -1 -1 1
4.2300 4.2332 -.0032 1 -1 1
4.0100 4.0052 .0048 2 1 1
3.6200 3.6187 .0013 0 1 2
3.5000 3.4979 .0021 0 2 0
3.4300 3.4301 -.0001 1 2 1
3.2400 3.2401 -.0001 0 2 1
3.2000 3.1992 .0008 2 1 2
2.9090 2.9102 -.0012 3 1 1
2.8450 2.8464 -.0014 1 2 2
A= 8.992 DA= .006
B= 7.3632 DB= .0004
C= 8.482 DC= .001
GAMMA= 71.84 DGAMMA= .01
BETA = 82.58 DBETA = .05
ALPHA= 87.21 DALPHA= .04
V=529.4
15. 28-0252
Ca2V2O7
Triklin
Dexp Dcal d(D) h k l
6.8900 6.8970 -.0070 1 0 0
6.3100 6.3027 .0073 -1 0 1
4.6600 4.6600 .0000 -1 -2 1
4.6100 4.6113 -.0013 0 -1 2
4.3100 4.3092 .0008 1 -1 1
3.4800 3.4797 .0003 -2 -1 2
3.3100 3.3109 -.0009 1 -2 1
3.2000 3.1997 .0003 1 2 1
3.1500 3.1514 -.0014 -2 0 2
3.1000 3.1008 -.0008 0 -3 1
3.0400 3.0402 -.0002 2 2 0
2.9770 2.9787 -.0017 1 1 2
A= 7.5691 DA= .0009
B= 9.8478 DB= .0001
C= 10.055 DC= .001
GAMMA= 70.8473 DGAMMA= .0001
BETA =111.24 DBETA = .01
ALPHA=114.326 DALPHA= .002
V=622.3
16. 28-0253
Ca2V6O17*13H2O
Groupa 29, 57
Dexp. Dcal. d(D) h k l
2.9900 2.9904 -.0004 2 1 1
2.8200 2.8203 -.0003 2 0 2
2.7300 2.7306 -.0006 0 1 2
2.6500 2.6527 -.0027 3 1 0
2.3900 2.3887 .0013 2 1 2
2.1620 2.1611 .0009 4 1 0
1.9600 1.9595 .0005 2 2 1
1.6320 1.6323 -.0003 3 2 2
a= 9.8603 b= 4.4928 c= 6.8770
da= .0003 db= .0001 dc= .0002
V= 304.65
17. 28-0254
Ca3V2O8*10H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
7.0000 7.0019 -.0019 0 1 1
6.1300 6.1283 .0017 1 1 1
3.9900 3.9883 .0017 2 1 1
3.8200 3.8178 .0022 2 1 0
3.2400 3.2386 .0014 1 3 1
2.9500 2.9506 -.0006 0 1 3
2.7200 2.7212 -.0012 3 0 0
2.0100 2.0096 .0004 -1 1 4
1.8910 1.8906 .0004 -2 4 2
1.8200 1.8202 -.0002 2 2 5
a= 8.647 b=10.790 c=9.747 beta= 70.75
da=.009 db=.006 dc=.006 dbeta=.07
V= 858.6
18. 28-0255
Ca2V2O7*5H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
3.9600 3.9581 .0019 2 1 0
3.8100 3.8052 .0048 -1 1 2
3.4700 3.4684 .0016 -2 1 1
3.2200 3.2189 .0011 -1 2 2
2.9200 2.9180 .0020 0 2 3
2.7500 2.7505 -.0005 3 1 0
2.7000 2.7000 .0000 3 1 2
2.6100 2.6119 -.0019 -1 2 3
2.0000 2.0000 .0000 4 2 2
1.8900 1.8900 .0000 4 0 4
1.8150 1.8150 -.0000 2 4 4
a= 8.794 b= 10.455 c= 10.85 beta= 76.54
da=.001 db= .008 dc=.01 dbeta=.07
V= 970.0
Triklin
Dexp Dcal d(D) h k l
3.9600 3.9610 -.0010 0 1 1
3.8100 3.8124 -.0024 0 -1 1
3.4700 3.4683 .0017 -1 -1 1
3.2200 3.2185 .0015 -1 1 0
2.9200 2.9219 -.0019 1 1 1
2.7500 2.7497 .0003 0 1 2
2.7000 2.6999 .0001 -1 -1 2
2.6100 2.6069 .0031 -1 1 2
2.0000 2.0006 -.0006 -2 1 2
1.8900 1.8902 -.0002 -1 2 2
1.8150 1.8149 .0001 2 -1 1
A= 5.038 DA= .002
B= 4.8789 DB= .0006
C= 6.8182 DC= .0007
GAMMA= 83.732 DGAMMA= .004
BETA =107.49 DBETA = .03
ALPHA= 89.72 DALPHA= .02
V= 158.75
19. 28-0352
Cs2VCl5*H2O
Triklin
Dexp Dcal d(D) h k l
6.0300 6.0387 -.0087 0 1 1
4.6000 4.5976 .0024 2 1 0
3.9700 3.9719 -.0019 -2 -1 1
3.7500 3.7522 -.0022 1 2 1
3.4500 3.4518 -.0018 0 1 2
3.0200 3.0194 .0006 0 2 2
2.9380 2.9369 .0011 -2 2 1
2.8240 2.8249 -.0009 1 2 2
2.7400 2.7373 .0027 3 1 1
2.5350 2.5343 .0007 2 3 1
2.4770 2.4771 -.0001 2 2 2
2.3130 2.3113 .0017 -1 0 3
A= 10.05530 DA= .00007
B= 8.43687 DB= .00008
C= 7.14410 DC= .00003
GAMMA= 80.0497 DGAMMA= .0008
BETA =102.701 DBETA = .001
ALPHA= 76.2682 DALPHA= .0002
V=558.0
20. 28-0353
Cs2VCl5*4H2O
Triklin
Dexp Dcal d(D) h k l
8.5300 8.5311 -.0011 1 0 0
6.7700 6.7882 -.0182 0 1 1
6.2200 6.2202 -.0002 -1 0 1
5.2400 5.2375 .0025 0 0 2
5.1100 5.1243 -.0143 -1 1 0
4.2600 4.2656 -.0056 2 0 0
4.1800 4.1776 .0024 2 1 0
3.9400 3.9410 -.0010 1 2 1
3.4900 3.4917 -.0017 0 0 3
3.3700 3.3700 -.0000 -1 -2 1
3.2600 3.2584 .0016 2 -1 1
3.2200 3.2201 -.0001 -1 2 0
A= 8.941 DA= .003
B= 8.093 DB= .004
C= 10.830 DC= .008
GAMMA= 74.32 DGAMMA= .06
BETA = 79.37 DBETA = .09
ALPHA= 77.42 DALPHA= .07
V=729.7
21. 28-0354
Cs2V5F17
Triklin
Dexp Dcal d(D) h k l
7.4300 7.4312 -.0012 1 0 0
7.2200 7.2041 .0159 -1 1 0
6.5000 6.5043 -.0043 1 0 1
6.2700 6.2980 -.0280 0 -1 1
4.1400 4.1415 -.0015 0 2 1
4.0300 4.0295 .0005 0 3 0
3.8600 3.8616 -.0016 1 -1 2
3.7600 3.7595 .0005 1 2 1
3.6900 3.6877 .0023 1 -2 2
3.6300 3.6307 -.0007 2 -3 1
3.3700 3.3699 .0001 -1 -2 1
3.3300 3.3293 .0007 0 0 2
A= 8.80062 DA= .00002
B= 13.172 DB= .001
C= 7.7349 DC= .0006
GAMMA=111.41 DGAMMA= .01
BETA = 60.8522 DBETA = .0006
ALPHA=108.357 DALPHA= .009
V=720.0
22. 28-0355
Cs4Mo2V6O23
Triklin
Dexp Dcal d(D) h k l
3.5300 3.5297 .0003 -1 1 1
3.0900 3.0901 -.0001 -1 1 2
3.0300 3.0310 -.0010 1 1 0
2.9510 2.9499 .0011 -1 2 0
2.9280 2.9284 -.0004 -1 -1 1
2.8370 2.8373 -.0003 0 -1 4
2.8020 2.8022 -.0002 -1 2 1
2.5200 2.5197 .0003 0 2 3
2.4550 2.4548 .0002 1 0 4
2.2720 2.2713 .0007 1 2 0
2.2140 2.2143 -.0003 -1 3 0
2.1210 2.1214 -.0004 1 2 2
A= 3.9999 DA= .0002
B= 7.0408 DB= .0003
C= 12.1952 DC= .0002
GAMMA=105.228 DGAMMA= .001
BETA = 85.5109 DBETA = .0005
ALPHA= 94.7234 DALPHA= .0005
V=329.7
23. 28-0542
{NH4}3V2O4F5
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.9000 5.8999 .0001 1 1 0
4.1700 4.1703 -.0003 -1 0 2
2.7700 2.7706 -.0006 1 0 2
2.7300 2.7294 .0006 2 0 1
2.6500 2.6497 .0003 -3 0 1
2.6200 2.6199 .0001 -2 1 3
2.1500 2.1498 .0002 0 4 2
2.1200 2.1201 -.0001 -3 3 1
a= 8.068 b=10.603 c=8.350 beta=118.34
da=.001 db=.003 dc= .002 dbeta=.01
V= 628.7
24. 28-0544
alfa-Pb4VF11
Rombik
Groupa 31,59
Dexp. Dcal. d(D) h k l
12.1000 12.1293 -.0293 1 0 0
3.3500 3.3555 -.0055 1 1 2
3.1300 3.1262 .0038 2 1 1
3.0000 3.0008 -.0008 4 0 1
2.6420 2.6426 -.0006 3 1 2
2.1660 2.1694 -.0034 2 1 7
2.0470 2.0457 .0013 4 1 5
2.0130 2.0125 .0005 2 1 8
1.9830 1.9847 -.0017 6 0 2
1.8430 1.8442 -.0012 4 1 7
1.7960 1.7986 -.0026 1 1 10
1.7470 1.7468 .0002 2 2 2
1.6910 1.6891 .0019 0 1 11
1.6740 1.6733 .0007 6 0 7
1.6310 1.6310 .0000 2 2 5
a=12.129 b= 3.7052 c=20.87
da= .004 db= .0001 dc= .01
V= 938.2
Triklin
Dexp. Dcal. d(D) h k l
12.1000 12.0850 .0150 1 0 0
3.3500 3.3483 .0017 -1 0 1
3.1300 3.1311 -.0011 -3 -1 0
3.0000 2.9982 .0018 -2 0 1
2.6420 2.6420 -.0000 -1 -2 0
2.1660 2.1649 .0011 -2 -2 1
2.0470 2.0460 .0010 -4 1 1
2.0130 2.0125 .0005 4 1 1
1.9830 1.9837 -.0007 -3 -2 1
1.8430 1.8413 .0017 1 -3 0
1.7960 1.7960 -.0000 -1 -3 0
1.7470 1.7469 .0001 -5 -2 0
A= 12.142 DA= .004
B= 5.644 DB= .003
C= 3.5872 DC= .0008
GAMMA= 95.26 DGAMMA= .05
BETA = 87.19 DBETA = .01
ALPHA=101.20 DALPHA= .06
V= 240.04
25. 28-0556
NH4VO2F2
Triklin
Dexp Dcal d(D) h k l
5.7800 5.7747 .0053 1 1 0
5.6300 5.6232 .0068 -1 2 0
4.4800 4.4756 .0044 0 -1 1
4.2700 4.2655 .0045 1 2 0
4.1600 4.1635 -.0035 1 -3 0
3.4900 3.4900 .0000 1 -2 1
3.3500 3.3493 .0007 2 1 0
3.2700 3.2702 -.0002 -2 3 0
3.2400 3.2362 .0038 -2 1 1
3.2100 3.2142 -.0042 -2 0 1
3.1300 3.1300 .0000 0 4 0
2.8700 2.8707 -.0007 1 2 1
A= 7.906 DA= .001
B= 13.0467 DB= .0008
C= 4.681 DC= .001
GAMMA=105.004 DGAMMA= .009
BETA = 99.43 DBETA = .09
ALPHA= 93.82 DALPHA= .01
V=457.9
26. 28-0563
{NH4}2VO2F3
Monoklin
GRUPA 4,11
Dexp. Dcal. d(D) h k l
13.7000 13.7708 -.0708 1 0 0
8.1600 8.1750 -.0150 0 2 0
5.0700 5.0676 .0024 1 3 0
4.7000 4.6982 .0018 -2 1 1
4.0300 4.0307 -.0007 0 3 1
3.4000 3.4009 -.0009 3 0 1
3.3300 3.3296 .0004 3 1 1
3.1400 3.1400 .0000 3 2 1
a= 13.934 b= 16.350 c= 6.05984 beta= 98.784
da=.003 db=.001 dc=.00002 dbet=.003
V=1365
27. 28-0573
{NH4}8V2O2{SO4}6
Triklin
Dexp Dcal d(D) h k l
9.3000 9.2918 .0082 1 1 1
8.3400 8.3584 -.0184 0 1 1
7.8600 7.8424 .0176 0 -1 1
7.1900 7.1980 -.0080 1 2 0
6.9600 6.9828 -.0228 0 2 0
6.3000 6.2968 .0032 2 1 1
5.2400 5.2427 -.0027 1 0 2
4.9900 4.9850 .0050 1 3 0
4.9200 4.9230 -.0030 1 3 1
4.7900 4.7887 .0013 1 2 2
4.4400 4.4409 -.0009 2 3 0
4.3300 4.3280 .0020 0 3 1
A= 12.898 DA= .003
B= 15.354 DB= .009
C= 10.814 DC= .005
GAMMA= 65.74 DGAMMA= .03
BETA = 66.86 DBETA = .03
ALPHA= 77.41 DALPHA= .04
V=1791.3
28. 28-0578
VO{NH4}2{SO4}2*3H2O
Triklin
Dexp Dcal d(D) h k l
10.3000 10.2925 .0075 -1 0 1
7.6900 7.6816 .0084 0 1 1
6.4300 6.4305 -.0005 0 -1 1
5.8600 5.8634 -.0034 -2 0 1
5.1500 5.1463 .0037 -2 0 2
4.9900 4.9845 .0055 -1 1 3
4.9200 4.9287 -.0087 0 1 3
4.6100 4.6057 .0043 1 0 3
4.2200 4.2174 .0026 1 1 3
3.8200 3.8192 .0008 -1 -1 3
3.7800 3.7801 -.0001 -3 0 2
3.7700 3.7700 .0000 -3 1 0
A= 12.2544 DA= .0004
B= 8.107 DB= .003
C= 16.66 DC= .01
GAMMA=101.09 DGAMMA= .04
BETA =100.91 DBETA = .06
ALPHA= 75.41 DALPHA= .04
V= 1554.7
29. 28-0607
Li3VF6
Monoklin
Crupa 3
Dexp Dcal d(D) h k l
4.2900 4.2946 -.0046 2 1 0
4.2100 4.2117 -.0017 0 1 2
4.1500 4.1424 .0076 -2 0 2
4.0100 4.0141 -.0041 1 1 2
3.8800 3.8796 .0004 3 0 1
3.6800 3.6776 .0024 -1 0 3
3.2300 3.2311 -.0011 -2 0 3
3.0300 3.0305 -.0005 0 2 0
2.8820 2.8830 -.0010 -3 1 2
2.4790 2.4775 .0015 2 2 2
2.4500 2.4501 -.0001 2 1 4
2.3590 2.3594 -.0004 1 2 3
a=12.1809 b=6.061 c=11.72 beta= 87.82
da=.0002 db=.006 dc=.01 dbeta=.06
V= 864.8
30. 28-608
Li3V2Mo3O15
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
4.3400 4.3331 .0069 2 1 0
4.2200 4.2254 -.0054 0 2 1
3.5800 3.5808 -.0008 2 1 1
3.3600 3.3600 .0000 -1 1 2
3.2400 3.2418 -.0018 1 3 0
3.1500 3.1490 .0010 1 1 2
3.0700 3.0708 -.0008 2 2 1
2.9170 2.9169 .0001 -3 1 1
2.7950 2.7941 .0009 2 3 0
2.7080 2.7096 -.0016 3 2 0
2.3820 2.3826 -.0006 -1 4 1
2.2740 2.2730 .0010 2 4 0
a= 9.600 b= 10.340 c= 7.376 beta= 96.16
da=.009 db=.006 dc=.009 dbeta=.05
V= 727.9
31. 28-0641
MgV20O48.5
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.7000 5.7041 -.0041 1 0 3
5.5300 5.5361 -.0061 2 0 2
3.6400 3.6466 -.0066 -2 0 4
3.5800 3.5761 .0039 0 1 0
3.4500 3.4505 -.0005 1 -1 0
3.3300 3.3317 -.0017 0 -1 2
3.2000 3.2007 -.0007 -4 0 1
3.0600 3.0596 .0004 0 0 6
2.9340 2.9351 -.0011 -1 0 6
2.6240 2.6225 .0015 0 0 7
2.5690 2.5693 -.0003 3 1 3
2.5420 2.5409 .0011 4 0 5
A= 13.197 DA= .006
B= 3.5761 DB= .0001
C= 18.40 DC= .01
BETA = 85.98 DBETA = .02
V=866.5
Triklin
Dexp Dcal d(D) h k l
5.7000 5.6961 .0039 -1 0 1
5.5300 5.5292 .0008 1 1 0
3.6400 3.6383 .0017 -1 -2 1
3.5800 3.5816 -.0016 0 2 1
3.4500 3.4482 .0018 2 1 0
3.3300 3.3299 .0001 -1 0 2
3.2000 3.1990 .0010 0 3 0
3.0600 3.0596 .0004 -1 1 2
2.9340 2.9344 -.0004 1 -2 2
2.6240 2.6245 -.0005 -1 2 2
2.5690 2.5686 .0004 -3 2 1
2.5420 2.5435 -.0015 3 -1 1
A= 8.61738 DA= .00005
B= 10.153 DB= .002
C= 6.988 DC= .002
GAMMA=104.81 DGAMMA= .01
BETA = 96.00 DBETA = .03
ALPHA=100.088 DALPHA= .009
V= 574.8
32. 28-0643
Mg2V6O17
Triklin
Dexp Dcal d(D) h k l
9.5600 9.5601 -.0001 0 0 1
6.2800 6.2794 .0006 1 1 0
4.7500 4.7526 -.0026 0 -2 1
4.6000 4.5990 .0010 2 0 0
4.3100 4.3071 .0029 1 2 0
4.1700 4.1712 -.0012 2 1 1
3.8400 3.8400 .0000 1 -3 1
3.5300 3.5273 .0027 3 -1 1
3.3300 3.3302 -.0002 2 -1 3
3.2300 3.2314 -.0014 -3 1 0
2.1400 2.1400 .0000 0 -2 4
3.0500 3.0502 -.0002 3 -3 1
A= 10.615 DA= .006
B= 12.20195 DB= .00007
C= 10.494 DC= .003
GAMMA=108.17 DGAMMA= .02
BETA = 66.19 DBETA = .0145
ALPHA= 92.65 DALPHA= .02
V= 1176.5
33. 28-677
Nd5VO10
Triklin
Dexp Dcal d(D) h k l
3.5400 3.5402 -.0002 1 -1 1
3.4900 3.4898 .0002 1 0 1
3.2500 3.2505 -.0005 -1 2 1
3.2000 3.1991 .0009 2 0 0
3.1600 3.1620 -.0020 -2 2 0
3.0100 3.0057 .0043 1 2 1
2.7500 2.7533 -.0033 0 4 1
1.9100 1.9103 -.0003 -3 2 1
1.8900 1.8901 -.0001 3 0 1
1.8660 1.8662 -.0002 1 2 2
1.8540 1.8537 .0003 -1 3 2
1.6390 1.6388 .0002 -3 6 1
A= 6.4960 DA= .0002
B= 16.145 DB= .003
C= 4.227 DC= .001
GAMMA= 99.92 DGAMMA= .02
BETA = 89.973 DBETA = .006
ALPHA= 95.46 DALPHA= .03
V=434.9
34. 28-0712
Ni7V5O17
Triklin
Dexp Dcal d(D) h k l
8.3500 8.3607 -.0107 1 0 0
5.1000 5.1014 -.0014 0 1 1
4.1600 4.1657 -.0057 0 -1 1
3.5000 3.4975 .0025 2 1 1
3.2300 3.2299 .0001 -1 2 1
3.0800 3.0790 .0010 2 -1 1
3.0200 3.0213 -.0013 -2 1 1
2.7760 2.7756 .0004 1 1 2
2.7330 2.7325 .0005 0 3 0
2.6880 2.6893 -.0013 0 3 1
2.6270 2.6276 -.0006 1 3 0
2.3770 2.3765 .0005 2 3 1
A= 8.457 DA= .002
B= 8.417 DB= .004
C= 5.686 DC= .003
GAMMA= 85.99 DGAMMA= .01
BETA = 81.64 DBETA = .01
ALPHA= 77.09 DALPHA= .02
V= 390.0
35. 28-0800
KAgV2O6
Monoklin
GRUPA 4,11
Dexp. Dcal. d(D) h k l
7.3200 7.3102 .0098 1 1 0
5.2600 5.2543 .0057 1 1 1
5.0800 5.0750 .0050 -2 0 1
4.8300 4.8393 -.0093 0 1 2
4.1900 4.1854 .0046 1 2 1
3.6500 3.6551 -.0051 2 2 0
3.2800 3.2801 -.0001 -1 3 2
3.1900 3.1890 .0010 0 3 2
3.1400 3.1402 -.0002 -2 3 1
2.8700 2.8696 .0004 -2 0 4
2.8300 2.8300 -.0000 1 1 3
2.7900 2.7908 -.0008 -2 1 4
a= 10.152 b= 11.992 c=11.645 beta= 114.712
da=.008 db=.004 dc=.005 dbet=.007
V-1287.7
Triklin
Dexp Dcal d(D) h k l
7.3200 7.3256 -.0056 1 0 0
5.2600 5.2615 -.0015 0 1 1
5.0800 5.0788 .0012 0 -1 1
4.8300 4.8282 .0018 -1 0 2
4.1900 4.1973 -.0073 -1 -1 1
3.2800 3.2820 -.0020 1 -1 2
3.1900 3.1865 .0035 1 1 2
3.1400 3.1416 -.0016 -2 1 2
2.8700 2.8705 -.0005 -1 2 1
2.8300 2.8277 .0023 0 -2 1
2.7900 2.7898 .0002 -2 -1 2
2.7150 2.7170 -.0020 2 0 2
A= 7.6024 DA= .0008
B= 5.9996 DB= .0002
C= 10.799 DC= .001
GAMMA= 97.618 DGAMMA= .005
BETA =103.962 DBETA = .004
ALPHA= 85.905 DALPHA= .006
V=473.3
36. 28-0836
Ca2V2O7
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
3.0400 3.0415 -.0015 3 0 2
2.9380 2.9360 .0020 3 1 0
2.7780 2.7767 .0013 0 0 3
2.2630 2.2631 -.0001 0 1 3
2.1300 2.1314 -.0014 5 1 1
1.9880 1.9881 -.0001 2 0 4
1.8720 1.8733 -.0013 4 1 3
1.7890 1.7883 .0007 3 2 0
1.7380 1.7368 .0012 6 0 3
1.6790 1.6792 -.0002 7 1 1
1.6520 1.6522 -.0002 4 2 1
a=13.356 b= 3.906 c= 8.330
da= .005 db= .001 dc= .003
V= 434.5
37. 28-0837
K2Cl5*H2O
Triklin
Dexp Dcal d(D) h k l
6.3300 6.3352 -.0052 0 1 1
5.6400 5.6357 .0043 -1 1 0
5.2700 5.2698 .0002 0 -1 1
4.8700 4.8744 -.0044 0 0 2
3.3900 3.3901 -.0001 -1 2 1
3.1400 3.1407 -.0007 0 -2 1
3.0400 3.0383 .0017 -2 1 1
2.9910 2.9901 .0009 2 -1 2
2.9360 2.9326 .0034 -2 0 1
2.8470 2.8488 -.0018 2 1 1
2.7760 2.7754 .0006 1 2 2
2.4370 2.4372 -.0002 0 0 4
A= 7.0197 DA= .0004
B= 7.409 DB= .002
C= 10.1400 DC= .0006
GAMMA=103.13 DGAMMA= .01
BETA = 78.394 DBETA = .005
ALPHA= 82.14 DALPHA= .04
V= 493.7
38. 28-0838
K4{V{CN}7}*H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
6.7200 6.7074 .0126 1 0 1
6.4900 6.4861 .0039 0 1 1
4.5800 4.5758 .0042 0 1 2
3.8200 3.8189 .0011 1 1 2
3.7500 3.7505 -.0005 0 2 1
2.9820 2.9831 -.0011 3 1 1
2.9430 2.9431 -.0001 -4 0 3
2.8890 2.8881 .0009 -4 1 1
2.5020 2.5024 -.0004 3 2 1
2.4690 2.4679 .0011 1 3 1
2.4360 2.4365 -.0005 -1 3 2
a= 12.600010 b= 7.962068 c= 12.33 beta= 114.86
da=.005 db=.002 dc=.03 dbeta=.01
V= 1122
Triklin
Dexp. Dcal. d(D) h k l
6.7200 6.7344 -.0144 1 -1 0
6.4900 6.4415 .0485 1 1 0
4.5800 4.5799 .0001 0 -3 0
3.8200 3.8200 .0000 -1 -3 0
3.7500 3.7500 .0000 2 0 0
2.9820 2.9819 .0001 0 0 1
2.9430 2.9433 -.0003 0 -1 1
2.8890 2.8889 .0001 1 -1 1
2.5020 2.5019 .0002 2 -1 1
2.4690 2.4688 .0002 -2 -4 0
2.4360 2.4359 .0001 2 1 1
A= 7.59 DA= .01
B= 13.780 DB= .003
C= 3.0155 DC= .0001
GAMMA= 93.45 DGAMMA= .06
BETA = 81.89 DBETA = .01
ALPHA= 93.20 DALPHA= .04
V= 311.2
39. 28-0839
K2VF15
Triklin
Dexp Dcal d(D) h k l
6.3000 6.2973 .0027 -1 1 1
5.7700 5.7630 .0070 0 1 1
5.3000 5.3094 -.0094 0 -1 1
4.9100 4.9051 .0049 1 1 0
4.2400 4.2363 .0037 1 0 1
3.7600 3.7576 .0024 -1 1 2
3.3700 3.3666 .0034 1 -2 1
3.2300 3.2301 -.0001 -1 3 0
3.1500 3.1486 .0014 -2 2 2
3.0000 3.0001 -.0001 2 1 0
2.9000 2.9014 -.0014 0 3 1
2.8820 2.8815 .0005 0 2 2
A= 8.243 DA= .004
B= 10.023 DB= .003
C= 7.602 DC= .002
GAMMA=112.56 DGAMMA= .02
BETA =114.47 DBETA = .08
ALPHA= 76.678 DALPHA= .002
V= 526.1
40. 28-0840
K2V3F11
Triklin
Dexp Dcal d(D) h k l
7.6800 7.6842 -.0042 1 0 0
5.4300 5.4308 -.0008 0 1 1
5.1200 5.1180 .0020 0 -1 1
3.7200 3.7197 .0003 0 2 1
3.6000 3.5998 .0002 -2 1 0
3.3900 3.3891 .0009 -2 0 1
3.3300 3.3304 -.0004 0 0 2
3.2700 3.2703 -.0003 2 0 1
3.0600 3.0603 -.0003 -2 -1 1
3.0000 3.0006 -.0006 -1 1 2
1.8590 1.8590 .0000 3 -3 1
1.5860 1.5860 .0000 0 2 4
A= 7.710 DA= .001
B= 8.6437 DB= .0003
C= 6.68019 DC= .00008
GAMMA= 94.0280 DGAMMA= .0009
BETA = 92.62 DBETA = .01
ALPHA= 86.327 DALPHA= .001
V= 442.8
41. 28-0841
alfa-k3VF6
Triklin
Dexp Dcal d(D) h k l
4.9600 4.9603 -.0003 -1 0 1
4.3600 4.3647 -.0047 1 1 1
4.1900 4.1958 -.0058 -1 -1 1
3.3500 3.3509 -.0009 2 1 1
3.3100 3.3142 -.0042 1 1 2
3.0800 3.0798 .0002 -2 -1 1
3.0200 3.0178 .0022 -2 0 1
2.4840 2.4825 .0015 0 2 0
2.4420 2.4419 .0001 3 1 1
2.3950 2.3951 -.0001 0 1 3
2.3490 2.3489 .0001 2 1 3
2.3240 2.3258 -.0018 3 0 1
A= 7.459 DA= .001
B= 5.3044 DB= .0007
C= 8.7265 DC= .0005
GAMMA= 69.93 DGAMMA= .01
BETA = 80.79 DBETA = .01
ALPHA= 91.24 DALPHA= .01
V=318.8
42. 28-0842
KVMo7O24
Triklin
Dexp Dcal d(D) h k l
3.4500 3.4520 -.0020 1 0 1
3.0600 3.0600 .0000 1 1 1
2.6250 2.6257 -.0007 -1 -1 1
2.5250 2.5264 -.0014 0 -1 1
2.0870 2.0859 .0011 3 1 1
1.9840 1.9848 -.0008 1 1 2
1.9380 1.9387 -.0007 4 1 0
1.8520 1.8512 .0008 -3 0 2
1.8150 1.8158 -.0008 -4 -1 1
1.6320 1.6313 .0007 -2 -2 1
1.5860 1.5863 -.0003 0 -2 1
1.4950 1.4951 -.0001 -4 1 2
1.3870 1.3869 .0001 5 0 1
A= 8.2013 DA= .0002
B= 3.984 DB= .001
C= 4.4498 DC= .0008
GAMMA= 79.3231 DGAMMA= .0009
BETA = 99.189 DBETA = .004
ALPHA= 77.49 DALPHA= .01
V=136.4
43. 28-0843
K3V3Mo2O15
Triklin
Dexp Dcal d(D) h k l
3.2500 3.2467 .0033 0 -1 1
3.2300 3.2296 .0004 0 1 1
3.1400 3.1389 .0011 -1 2 0
3.0600 3.0594 .0006 0 -3 1
3.0100 3.0094 .0006 -1 3 0
2.9140 2.9149 -.0009 0 -4 1
2.6990 2.7031 -.0041 0 5 1
2.6550 2.6557 -.0007 -1 0 1
2.5750 2.5742 .0008 -1 2 1
2.3660 2.3664 -.0004 -1 7 0
2.2280 2.2267 .0013 0 8 1
2.0740 2.0740 .0000 1 0 1
A= 3.375 DA= .002
B= 24.84 DB= .03
C= 3.368 DC= .001
GAMMA= 87.78 DGAMMA= .09
BETA =104.08 DBETA = .01
ALPHA= 91.69 DALPHA= .01
V=272.9
44. 28-0844
K7V7Mo3O30
Triklin
Dexp. Dcal. d(D) h k l
3.2600 3.2610 -.0010 1 -2 0
3.1800 3.1815 -.0015 -1 -2 0
3.0300 3.0294 .0006 1 0 1
2.9150 2.9146 .0004 2 -1 0
2.8570 2.8575 -.0005 -2 -1 0
2.6220 2.6224 -.0004 -1 0 1
2.3930 2.3939 -.0009 1 -2 1
1.9600 1.9597 .0003 1 -3 1
1.8790 1.8789 .0001 0 -4 0
1.8010 1.8009 .0001 -3 -2 0
1.2390 1.2390 .0000 -2 -2 2
A= 6.356 DA= .001
B= 7.520 DB= .002
C= 3.1895 DC= .0002
GAMMA= 91.81 DGAMMA= .02
BETA = 79.68 DBETA = .02
ALPHA= 91.29 DALPHA= .02
V= 149.9
45. 28-0845
K2V3O8
Triklin
Dexp Dcal d(D) h k l
7.0700 7.0443 .0257 1 0 0
5.3000 5.3006 -.0006 1 1 0
4.0200 4.0239 -.0039 0 2 0
3.4100 3.4110 -.0010 1 2 1
3.1700 3.1697 .0003 1 2 2
2.8000 2.7954 .0046 -2 0 3
2.6200 2.6201 -.0001 2 2 1
2.4800 2.4780 .0020 -2 0 4
2.3500 2.3501 -.0001 0 2 5
2.2400 2.2396 .0004 3 1 1
2.0000 1.9996 .0004 -3 2 1
1.9200 1.9201 -.0001 1 4 1
a=7.049 b= 8.048 c= 14.486 beta= 87.84
da=.003 db=.003 dc=.005 dbeta=.01
V= 821.2
46. 28-0846
K3VO4
Triklin
Dexp Dcal d(D) h k l
5.1600 5.1604 -.0004 -1 1 0
4.2900 4.2903 -.0003 -1 1 1
3.5400 3.5378 .0022 -1 3 0
3.1200 3.1188 .0012 0 -2 2
2.9400 2.9435 -.0035 -1 -2 2
2.8800 2.8797 .0003 -1 1 2
2.7900 2.7890 .0010 -1 -4 1
2.7100 2.7097 .0003 1 4 0
2.6200 2.6200 .0000 -1 2 2
2.5800 2.5802 -.0002 -2 2 0
2.4400 2.4412 -.0012 2 2 0
2.3800 2.3812 -.0012 1 1 2
A= 5.5726 DA= .0001
B= 13.3685 DB= .0002
C= 6.6423 DC= .0002
GAMMA= 91.993 DGAMMA= .005
BETA =102.1840 DBETA = .0003
ALPHA=101.019 DALPHA= .002
V=473.5
47. 28-847
Ca3V2O8
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
3.4200 3.4201 -.0001 1 1 1
3.2100 3.2097 .0003 2 0 1
2.8640 2.8637 .0003 2 0 3
2.6200 2.6205 -.0005 0 1 5
2.5330 2.5315 .0015 2 1 1
1.9630 1.9624 .0006 1 2 0
1.9090 1.9100 -.0010 3 1 1
1.8290 1.8293 -.0003 1 1 8
1.7380 1.7383 -.0003 2 2 0
1.6520 1.6520 .0000 -2 2 3
1.5840 1.5839 .0001 -3 0 7
a= 6.493 b= 4.118 c=17.000 beta= 87.74
da=.004 db=.001 dc=.01 dbeta=.08
V= 454.1
48. 28-0848
K3V2F3O5
Triklin
Dexp Dcal d(D) h k l
6.2200 6.2228 -.0028 2 1 0
5.7200 5.7224 -.0024 2 2 0
5.3700 5.3660 .0040 1 0 1
5.1400 5.1397 .0003 0 3 0
4.7900 4.7856 .0044 2 3 0
4.4900 4.4887 .0013 -2 -2 1
4.1800 4.1815 -.0015 2 1 1
3.9100 3.9103 -.0003 2 -1 1
3.7000 3.7001 -.0001 1 -3 1
3.6100 3.6109 -.0009 -2 -4 1
3.4900 3.4895 .0005 2 -2 1
3.1400 3.1401 -.0001 1 4 1
A= 12.486 DA= .002
B= 16.808 DB= .002
C= 6.188 DC= .001
GAMMA= 68.793 DGAMMA= .004
BETA = 94.421 DBETA = .004
ALPHA=101.144 DALPHA= .006
V=1188.6
49. 28-0849
K0.56V0.56W0.44O3
Triklin
Dexp Dcal d(D) h k l
12.0000 11.9727 .0273 0 1 0
9.4400 9.4383 .0017 1 -1 0
6.4400 6.4377 .0023 2 1 0
5.5800 5.5790 .0010 1 -2 0
4.7100 4.7083 .0017 2 2 0
3.9900 3.9909 -.0009 0 3 0
3.8600 3.8594 .0006 1 3 0
3.8200 3.8234 -.0034 4 0 0
3.6400 3.6397 .0003 4 1 0
3.5300 3.5346 -.0046 2 3 0
3.1400 3.1389 .0011 3 3 0
3.0600 3.0588 .0012 5 0 0
2.9650 2.9652 -.0002 5 -1 0
2.9370 2.9361 .0009 1 4 0
2.8720 2.8720 .0000 1 1 1
A= 15.2965 DA= .0002
B= 12.042 DB= .001
C= 2.9638 DC= .00003
GAMMA= 90.26 DGAMMA= .03
BETA = 91.08 DBETA = .01
ALPHA= 83.8769 DALPHA= .0003
V=542.5
50. 28-0944
RbAgV2O6
Triklin
Dexp Dcal d(D) h k l
7.3100 7.3177 -.0077 0 1 1
5.2000 5.1980 .0020 0 -1 1
4.8600 4.8620 -.0020 -1 -1 1
3.8400 3.8397 .0003 0 2 0
3.6900 3.6892 .0008 -2 1 1
3.3200 3.3166 .0034 -1 2 2
3.2100 3.2100 .0000 0 -2 1
3.1300 3.1313 -.0013 -1 0 3
3.0600 3.0603 -.0003 2 0 2
2.9400 2.9392 .0008 3 0 0
2.9000 2.9007 -.0007 3 1 0
2.8340 2.8350 -.0010 -2 2 1
A= 8.954 DA= .007
B= 8.220 DB= .006
C= 10.212 DC= .003
GAMMA= 82.96 DGAMMA= .06
BETA = 94.43 DBETA = .03
ALPHA= 71.076 DALPHA= .03
V= 700.1
50. 28-0976
Rb2VCl5*H2O
Triklin
Dexp Dcal d(D) h k l
6.9200 6.9096 .0104 -1 0 1
6.3500 6.3646 -.0146 0 1 1
5.8000 5.7893 .0107 0 -1 1
5.6800 5.6784 .0016 -1 -1 1
5.2700 5.2566 .0134 -1 1 0
4.9800 4.9787 .0013 1 0 1
3.9000 3.8977 .0023 -2 -1 1
3.5100 3.5048 .0052 -1 2 1
3.4400 3.4414 -.0014 -2 1 1
3.1000 3.1017 -.0017 -2 1 2
3.0400 3.0423 -.0023 -1 2 2
2.9980 3.0000 -.0020 1 -2 1
A= 8.265 DA= .001
B= 8.807 DB= .001
C= 8.9749 DC= .0003
GAMMA= 79.7786 DGAMMA= .0009
BETA =107.87 DBETA = .03
ALPHA= 88.06 DALPHA= .03
V-609.2
51. 28-0977
RbVCl4*6H2O
Triklin
Dexp Dcal d(D) h k l
8.6000 8.5979 .0021 1 0 0
4.7700 4.7737 -.0037 -1 2 1
5.9900 5.9949 -.0049 -1 0 1
4.6300 4.6291 .0009 0 -2 1
4.2900 4.2903 -.0003 -2 1 0
4.1500 4.1516 -.0016 -1 3 0
4.0600 4.0581 .0019 -2 1 1
3.9000 3.9023 -.0023 2 1 0
3.7400 3.7385 .0015 0 3 1
3.6800 3.6788 .0012 -2 -1 1
3.2400 3.2402 -.0002 -1 -1 2
3.1100 3.1096 .0004 2 -2 1
A= 8.9177 DA= .0004
B= 13.2374 DB= .0007
C= 7.0243 DC= .0002
GAMMA= 99.8572 DGAMMA= .0003
BETA =102.444 DBETA = .003
ALPHA= 85.645 DALPHA= .004
V=796.9
52. 28-0978
Rb2V4O9
Triklin
Dexp Dcal d(D) h k l
7.4000 7.3982 .0018 1 0 0
5.2900 5.2930 -.0030 0 1 1
3.8600 3.8602 -.0002 0 -1 1
3.6800 3.6747 .0053 0 0 2
3.1000 3.0973 .0027 -2 0 1
2.8310 2.8295 .0015 1 2 0
2.6380 2.6372 .0008 3 1 1
2.6140 2.6141 -.0001 -2 1 1
2.5290 2.5283 .0007 1 -1 2
2.4490 2.4498 -.0008 0 0 3
2.3930 2.3923 .0007 -1 2 0
2.3690 2.3681 .0009 1 2 3
A= 7.958 DA= .001
B= 6.163 DB= .004
C= 8.065 DC= .005
GAMMA= 70.70 DGAMMA= .02
BETA = 74.00 DBETA = .03
ALPHA= 67.68 DALPHA= .03
V= 340.2
53. 28-0979
Rb2V10O21
Triklin
Dexp Dcal d(D) h k l
9.0800 9.0772 .0028 -1 0 1
4.3400 4.3374 .0026 -1 -1 1
3.0600 3.0605 -.0005 -1 -1 3
3.0100 3.0098 .0002 -3 1 0
2.9760 2.9776 -.0016 0 -1 3
2.8290 2.8262 .0028 1 0 3
2.7400 2.7401 -.0001 0 2 0
2.6730 2.6723 .0007 1 -2 1
2.5610 2.5618 -.0008 0 0 4
2.2550 2.2553 -.0003 -4 1 4
2.1620 2.1620 -.0000 3 -2 1
2.1300 2.1292 .0008 -3 1 5
A= 10.530 DA= .001
B= 5.6638 DB= .0007
C= 11.3930 DC= .0002
GAMMA=104.262 DGAMMA= .003
BETA =115.73 DBETA = .03
ALPHA= 86.79 DALPHA= .01
V= 592.3
54. 28-0980
Rb6V2O8
Triklin
Dexp Dcal d(D) h k l
6.9400 6.9505 -.0105 0 1 1
6.5800 6.5769 .0031 1 1 0
5.2100 5.2134 -.0034 0 -1 1
4.2600 4.2611 -.0011 -1 -1 1
3.4600 3.4595 .0005 0 -2 1
3.3100 3.3083 .0017 2 2 2
3.1900 3.1886 .0014 -1 0 2
3.1000 3.1038 -.0038 -1 1 2
2.7800 2.7786 .0014 -2 1 1
2.4880 2.4877 .0003 -2 2 0
2.4270 2.4277 -.0007 3 0 0
2.1470 2.1468 .0002 2 2 4
A= 8.053 DA= .001
B= 9.862 DB= .002
C= 8.797 DC= .007
GAMMA= 68.46 DGAMMA= .02
BETA = 70.26 DBETA = .02
ALPHA= 68.27 DALPHA= .02
V= 586.9
55. 28-1041
alfa-Cs3VF6
Rombik
Groupa 33,49,62
Dexp. Dcal. d(D) h k l
5.1800 5.1734 .0066 0 2 0
3.2600 3.2617 -.0017 0 2 2
3.1700 3.1667 .0033 1 1 2
2.7050 2.7040 .0010 0 1 3
2.5900 2.5867 .0033 0 4 0
2.5900 2.5893 .0007 2 0 1
2.3360 2.3363 -.0003 1 4 0
2.2310 2.2307 .0003 2 1 2
1.8300 1.8300 .0000 2 4 1
1.6310 1.6308 .0002 0 4 4
1.5830 1.5833 -.0003 2 2 4
a= 5.44348 b=10.347 c= 8.404
da= .00003 db= .001 dc= .001
v= 473.3
56. 28-1099
Cs2MoV10O28.75
Rombik
Groupa 16
Dexp. Dcal. d(D) h k l
7.7400 7.7603 -.0203 0 1 0
6.9000 6.9261 -.0261 1 1 0
4.3700 4.3654 .0046 3 0 1
3.8400 3.8389 .0011 4 0 0
3.5200 3.5196 .0004 0 2 1
3.4300 3.4307 -.0007 1 2 1
3.1800 3.1820 -.0020 4 1 1
3.0900 3.0921 -.0021 3 2 0
2.5970 2.5943 .0027 4 2 1
2.4720 2.4712 .0008 0 3 1
2.1930 2.1936 -.0006 7 0 0
2.1140 2.1146 -.0006 2 3 2
1.5480 1.5479 .0001 9 1 2
a=15.355450 b= 7.760336 c= 8.361097
da= .005983 db= .001946 dc= .019111
v= 996
57. 28-1103
Cs4Mo2V10O33
Rombik
Groupa 16
Dexp. Dcal. d(D) h k l
4.3400 4.3334 .0066 0 0 3
4.0700 4.0640 .0060 1 2 0
3.9500 3.9460 .0040 0 1 3
3.7800 3.7818 -.0018 1 0 3
3.7000 3.7118 -.0118 2 0 1
3.3200 3.3271 -.0071 2 0 2
3.2500 3.2500 -.0000 0 0 4
3.1400 3.1418 -.0018 2 1 2
3.0900 3.0913 -.0013 0 3 1
3.0100 3.0076 .0024 2 2 0
2.9410 2.9438 -.0028 1 3 0
2.6830 2.6816 .0014 1 3 2
a= 7.75 b= 9.55 c=13.000
da= .01 db= .01 dc= .001
v= 961
Triklin
Dexp Dcal d(D) h k l
4.3400 4.3384 .0016 0 0 1
4.0700 4.0696 .0004 0 -2 1
3.9500 3.9501 -.0001 -1 -1 1
3.7800 3.7775 .0025 1 -2 1
3.7000 3.7038 -.0038 -1 1 1
3.3200 3.3220 -.0020 2 -1 1
3.2500 3.2484 .0016 -2 -1 1
3.1400 3.1394 .0006 1 3 1
3.0900 3.0909 -.0009 -1 -4 1
3.0100 3.0098 .0002 -1 3 1
2.9410 2.9407 .0003 2 -3 1
2.6830 2.6831 -.0001 2 -4 1
A= 10.092 DA= .003
B= 16.877 DB= .001
C= 4.3769 DC= .0004
GAMMA= 86.15 DGAMMA= .01
BETA = 88.147 DBETA = .001
ALPHA= 97.242 DALPHA= .004
V=737.2
58. 28-1168
Na2V2Mo3O15
Triklin
Dexp Dcal d(D) h k l
4.4300 4.4318 -.0018 0 0 1
3.4000 3.4001 -.0001 0 -2 1
3.3300 3.3296 .0004 1 -1 1
3.2600 3.2583 .0017 1 1 1
2.3780 2.3765 .0015 2 0 1
2.3610 2.3611 -.0001 2 -1 1
2.3170 2.3164 .0006 0 -4 1
2.2490 2.2486 .0004 2 -2 1
1.9490 1.9494 -.0004 -2 -3 1
1.7690 1.7688 .0002 -2 2 2
1.6890 1.6891 -.0001 0 -6 1
1.6090 1.6093 -.0003 -3 4 1
1.5540 1.5538 .0002 -2 -3 2
1.4730 1.4729 .0001 -2 7 0
1.4200 1.4201 -.0001 3 4 1
A= 5.8398 DA= .0003
B= 11.2504 DB= .0007
C= 4.4413 DC= .0001
GAMMA= 97.025 DGAMMA= .007
BETA = 92.840 DBETA = .008
ALPHA= 87.241 DALPHA= .001
V= 289.0
59. 28-1169
NaVO2
Triklin
Dexp Dcal d(D) h k l
5.6200 5.6168 .0032 1 0 1
5.3700 5.3696 .0004 -1 1 0
2.8180 2.8174 .0006 1 -2 1
2.6910 2.6899 .0011 0 -1 2
2.5740 2.5728 .0012 2 1 2
2.4750 2.4748 .0002 -2 2 1
2.4050 2.4049 .0001 1 1 3
2.3830 2.3825 .0005 1 0 3
2.1860 2.1856 .0004 0 2 3
2.1590 2.1585 .0005 2 2 1
2.1180 2.1186 -.0006 2 2 2
2.0990 2.0995 -.0005 1 -1 3
A= 6.849 DA= .002
B= 6.9624 DB= .0006
C= 7.347 DC= .007
GAMMA=102.15 DGAMMA= .05
BETA = 75.04 DBETA = .06
ALPHA= 76.784 DALPHA= .009
V= 315.6
60. 28-1170
NaV3O8
Triklin
Dexp Dcal d(D) h k l
9.5100 9.5027 .0073 1 0 0
6.9700 6.9802 -.0102 -1 1 0
5.7900 5.7922 -.0022 1 0 1
5.3200 5.3165 .0035 1 -1 1
4.5600 4.5586 .0014 -2 1 1
4.4700 4.4597 .0103 0 0 2
3.8800 3.8856 -.0056 -1 1 2
3.6400 3.6424 -.0024 1 -1 2
3.4700 3.4713 -.0013 2 1 0
3.3800 3.3790 .0010 -3 1 1
3.2100 3.2089 .0011 0 2 1
3.0100 3.0099 .0001 1 1 2
A= 10.372 DA= .007
B= 7.6643 DB= .0003
C= 9.2478 DC= .0005
GAMMA=108.37 DGAMMA= .03
BETA =103.58 DBETA = .06
ALPHA= 92.37 DALPHA= .01125
V=674
61. 28-1172
Na2V6O15
Triklin
Dexp Dcal d(D) h k l
7.3100 7.3135 -.0035 1 0 0
5.8700 5.8785 -.0085 0 1 1
5.5000 5.4950 .0050 0 -1 1
5.0900 5.0931 -.0031 -1 0 1
4.7700 4.7697 .0003 -1 1 0
3.8400 3.8400 .0000 2 0 1
3.6300 3.6382 -.0082 2 1 1
3.4800 3.4777 .0023 2 0 2
3.3700 3.3649 .0051 2 1 2
3.1800 3.1814 -.0014 1 1 3
3.0700 3.0675 .0025 1 2 2
2.9200 2.9202 -.0002 2 -1 2
A= 7.805 DA= .008
B= 7.1650 DB= .0003
C= 10.150 DC= .002
GAMMA= 80.60 DGAMMA= .03
BETA = 70.98 DBETA = .03
ALPHA= 83.17 DALPHA= .02
V= 528.1
62. 28-1173
Na2O*xV2O4*zV2O5
Monoklin
GRUPA 4,11
Dexp. Dcal. d(D) h k l
7.0200 7.0290 -.0090 0 1 1
4.7100 4.7188 -.0088 0 2 1
3.3700 3.3706 -.0006 2 1 0
3.0900 3.0899 .0001 -2 0 1
2.9200 2.9243 -.0043 1 1 3
2.7200 2.7226 -.0026 2 2 2
1.8900 1.8873 .0027 2 4 3
1.8000 1.8000 .0000 0 1 5
1.5300 1.5300 .0000 -4 1 2
a= 7.2394 b= 11.028 c= 9.3277 beta= 77.95
da=.0003 db=.002 dc=.0001 dbet=.005
V-725.7
63. 28-1174
Na3VO4
Triklin
Dexp Dcal d(D) h k l
8.0000 7.9842 .0158 0 1 1
6.3900 6.3904 -.0004 0 -1 1
5.7900 5.7883 .0017 1 0 1
5.0200 5.0275 -.0075 -1 1 0
4.5200 4.5232 -.0032 0 -1 2
4.3200 4.3155 .0045 0 2 0
3.9700 3.9710 -.0010 -1 0 3
3.5400 3.5375 .0025 -2 0 2
3.2800 3.2787 .0013 1 0 3
3.1100 3.1105 -.0005 -2 0 3
3.0400 3.0397 .0003 2 1 2
2.8400 2.8407 -.0007 2 2 2
A= 7.7700 DA= .0003
B= 9.08 DB= .01
C= 12.79 DC= .01
GAMMA= 77.82 DGAMMA= .04
BETA =100.11 DBETA = .04
ALPHA= 79.24 DALPHA= .09
V=845.4
64. 28-1175
Na3VO4
Triklin
Dexp Dcal d(D) h k l
6.1500 6.1482 .0018 -1 0 1
5.5700 5.5645 .0055 -1 1 0
4.7000 4.7014 -.0014 1 -1 2
3.8500 3.8517 -.0017 -1 -1 1
3.5900 3.5915 -.0015 0 -1 3
3.3600 3.3607 -.0007 -1 -1 2
3.1500 3.1510 -.0010 1 -1 4
2.8850 2.8852 -.0002 2 1 2
2.6450 2.6461 -.0011 -2 2 1
2.3620 2.3621 -.0001 3 -2 1
2.2590 2.2586 .0004 -2 -1 3
2.0670 2.0666 .0004 -3 2 2
A= 8.409 DA= .003
B= 6.231 DB= .001
C= 14.185 DC= .006
GAMMA=106.852 DGAMMA= .001
BETA = 75.26 DBETA = .03
ALPHA= 93.116 DALPHA= .003
V= 687.8
65. 28-1176
Na3VO4
Triklin
Dexp Dcal d(D) h k l
4.3300 4.3286 .0014 2 2 0
4.1900 4.1967 -.0067 -2 3 0
3.9900 3.9874 .0026 0 3 0
3.6400 3.6380 .0020 1 3 0
3.5500 3.5497 .0003 0 0 1
3.4500 3.4499 .0001 -1 0 1
3.1700 3.1720 -.0020 -2 4 0
3.0690 3.0693 -.0003 0 -2 1
2.9450 2.9458 -.0008 6 0 0
2.7880 2.7867 .0013 -5 4 0
2.7060 2.7059 .0001 3 -3 1
2.5640 2.5640 -.0000 5 0 1
A= 18.773 DA= .004
B= 12.6934 DB= .0004
C= 3.5549 DC= .0003
GAMMA=109.538 DGAMMA= .004
BETA = 86.98 DBETA = .03
ALPHA= 91.686 DALPHA= .009
V=797.9
66. 28-1177
Na4V2O7
Triklin
Dexp Dcal d(D) h k l
9.8800 9.8817 -.0017 1 0 0
6.0900 6.0968 -.0068 0 1 1
4.8000 4.8021 -.0021 0 -1 1
4.0100 4.0121 -.0021 -2 1 0
3.5500 3.5507 -.0007 0 -2 1
3.4900 3.4883 .0017 2 3 1
3.3300 3.3313 -.0013 3 1 1
2.8600 2.8592 .0008 1 3 2
2.8000 2.7975 .0025 2 3 2
2.7000 2.7002 -.0002 -1 2 2
2.6500 2.6506 -.0006 3 -1 1
2.2200 2.2190 .0010 2 -3 1
A= 10.623 DA= .001
B= 11.527 DB= .003
C= 6.5974 DC= .0007
GAMMA= 69.43 DGAMMA= .01
BETA = 77.74 DBETA = .02
ALPHA= 71.46 DALPHA= .01
V= 712.5
67. 28-1178
Na4V2O7
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
8.1000 8.1124 -.0124 0 1 0
4.9100 4.9104 -.0004 1 1 0
3.6100 3.6109 -.0009 1 1 2
3.2000 3.1977 .0023 -1 0 3
2.8100 2.8112 -.0012 -2 1 1
2.6500 2.6500 -.0000 2 0 2
2.4100 2.4104 -.0004 -2 2 1
1.8000 1.7999 .0001 3 2 1
1.6600 1.6601 -.0001 -2 2 5
1.5100 1.5100 .0000 -3 3 3
a= 6.173 b=8.11 c=10.990 beta= 91.99
da=.001 db=.01 dc=.006 dbeta=.06
V= 550.0
68. 28-1179
alfa-Na4V2O7
Triklin
Dexp Dcal d(D) h k l
6.5600 6.5606 -.0006 -1 0 1
4.8000 4.8001 -.0001 -1 2 0
4.6000 4.5981 .0019 -1 -2 1
4.3500 4.3490 .0010 -2 -1 1
4.0000 4.0008 -.0008 -2 1 1
3.7900 3.7899 .0001 0 3 0
3.6300 3.6302 -.0002 0 1 2
3.5500 3.5492 .0008 0 -3 1
3.3000 3.2995 .0005 0 3 1
3.0100 3.0100 .0000 3 2 0
2.8620 2.8620 -.0000 2 1 2
2.7390 2.7395 -.0005 -1 -4 1
A= 10.2271 DA= .0002
B= 11.46467 DB= .00005
C= 7.98795 DC= .00006
GAMMA= 84.920 DGAMMA= .001
BETA = 96.2193 DBETA = .00011
ALPHA= 95.8649 DALPHA= .00036
V=923.9
69. 28-1180
beta-Na4V2O7
Triklin
Dexp Dcal d(D) h k l
5.6100 5.5963 .0137 0 1 1
5.3700 5.3692 .0008 0 -1 1
4.9300 4.9345 -.0045 -1 0 1
4.6500 4.6627 -.0127 1 -1 1
4.5300 4.5297 .0003 0 -1 2
4.2300 4.2425 -.0125 -1 0 2
4.0800 4.0827 -.0027 -1 1 2
3.8400 3.8470 -.0070 0 0 4
3.3900 3.3898 .0002 1 1 1
3.2400 3.2392 .0008 1 0 4
3.1300 3.1285 .0015 0 -1 4
2.9790 2.9783 .0007 1 -2 1
A= 5.69776 DA= .00009
B= 6.24688 DB= .00050
C= 15.44322 DC= .00042
GAMMA=109.88090 DGAMMA= .00407
BETA = 86.73113 DBETA = .00138
ALPHA= 87.77197 DALPHA= .00237
V=514.7
70. 28-1181
5Na2O*xV2O4*zV2O5
Groupa 34,58
Dexp. Dcal. d(D) h k l
6.6900 6.7060 -.0160 2 1 0
3.8500 3.8453 .0047 0 1 1
3.4700 3.4650 .0050 1 3 0
3.2000 3.1997 .0003 3 1 1
3.0200 3.0151 .0049 3 3 0
2.6500 2.6518 -.0018 5 0 1
2.2600 2.2613 -.0013 4 4 0
1.9900 1.9915 -.0015 3 5 0
1.8100 1.8091 .0009 5 5 0
1.7200 1.7200 .0000 9 1 1
a=17.307 b=10.610 c= 4.126
da= .006 db= .001 dc= .001
V= 757.6
71. 28-1182
NaVO2F2
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
6.6900 6.6854 .0046 1 1 0
5.9300 5.9308 -.0008 -1 1 1
5.4900 5.4893 .0007 1 1 1
3.3400 3.3397 .0003 -1 2 2
3.1300 3.1307 -.0007 3 0 1
3.0800 3.0800 .0000 1 1 3
2.9800 2.9770 .0030 -2 1 3
2.6000 2.6019 -.0019 0 1 4
2.5600 2.5597 .0003 -4 0 1
2.2800 2.2798 .0002 2 0 4
2.2300 2.2301 -.0001 -4 0 3
2.0500 2.0497 .0003 0 4 2
a= 10.293 b=.0008 c= 10.985 beta= 97.585
da=.002 db=.0008 dc=.002 dbeta=.007
V= 991.9
Triklin
Dexp Dcal d(D) h k l
6.6900 6.6902 -.0002 1 0 0
5.9300 5.9267 .0033 0 1 1
5.4900 5.4896 .0004 0 -1 1
3.3400 3.3401 -.0001 1 0 2
3.1300 3.1294 .0006 2 1 0
3.0800 3.0834 -.0034 0 4 0
2.9800 2.9791 .0009 1 2 2
2.6000 2.6007 -.0007 -1 1 2
2.5600 2.5601 -.0001 -2 2 1
2.2800 2.2796 .0004 1 -5 1
2.2300 2.2301 -.0001 3 0 0
2.0500 2.0500 -.0000 2 4 2
A= 7.0973 DA= .0005
B= 12.455 DB= .001
C= 6.7863 DC= .0004
GAMMA= 95.938 DGAMMA= .002
BETA = 71.877 DBETA = .002
ALPHA= 86.791 DALPHA= .003
V= 564.6
72. 28-1183
Na3VO2F4
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.1500 5.1433 .0067 -1 0 3
4.5500 4.5492 .0008 -1 1 1
4.4200 4.4201 -.0001 1 1 1
3.1600 3.1602 -.0002 2 1 1
3.1000 3.1019 -.0019 0 1 5
2.6200 2.6205 -.0005 -3 0 2
2.5600 2.5609 -.0009 2 1 4
2.3100 2.3101 -.0001 -2 2 1
2.2700 2.2703 -.0003 -3 0 5
2.2000 2.2012 -.0012 3 0 4
2.1500 2.1489 .0011 2 1 6
1.8100 1.8100 -.0000 0 3 3
1.7400 1.7398 .0002 3 2 4
1.6400 1.6413 -.0013 -3 1 9
1.5800 1.5801 -.0001 4 2 2
a= 7.9903 b=5.6799 c=18.62 beta= 96.035
da= .0002 db=.0008 dc=.01 dbeta=.008
V= 840.2
Triklin
Dexp Dcal d(D) h k l
5.1500 5.1496 .0004 -1 1 0
4.5500 4.5491 .0009 0 1 1
4.4200 4.4182 .0018 0 -1 1
3.1600 3.1599 .0001 2 0 0
3.1000 3.0995 .0005 0 2 1
2.6200 2.6202 -.0002 1 -1 2
2.5600 2.5595 .0005 1 1 2
2.3100 2.3099 .0001 2 0 2
2.2700 2.2704 -.0004 -1 -1 2
2.2000 2.1994 .0006 0 -3 1
2.1500 2.1497 .0003 2 1 2
1.8100 1.8102 -.0002 0 4 0
1.7400 1.7402 -.0002 3 1 2
1.6400 1.6400 .0000 1 4 1
1.5800 1.5799 .0001 4 0 0
A= 6.470 DA= .002
B= 7.31998 DB= .00006
C= 5.7819 DC= .0009
GAMMA= 98.26 DGAMMA= .02
BETA = 80.94 DBETA = .01
ALPHA= 89.62 DALPHA= .02
V= 267.5
74. 28-1267
SrV2O6
Triklin
Dexp Dcal d(D) h k l
4.3500 4.3478 .0022 -1 0 2
4.0800 4.0761 .0039 0 1 1
3.6700 3.6719 -.0019 0 -1 1
3.6200 3.6218 -.0018 -1 1 0
3.3100 3.3067 .0033 -1 1 2
3.2400 3.2355 .0045 1 1 1
3.1300 3.1272 .0028 -1 0 3
2.8400 2.8450 -.0050 2 0 1
2.6800 2.6831 -.0031 0 1 3
2.5500 2.5507 -.0007 1 0 3
2.3900 2.3919 -.0019 -1 0 4
2.3400 2.3405 -.0005 -2 -1 2
A= 6.747 DA= .001
B= 4.296 DB= .001
C= 9.734 DC= .001
GAMMA= 94.67 DGAMMA= .01
BETA =105.51 DBETA = .01
ALPHA= 81.149 DALPHA= .002
V=268.6
75. 28-1268
Sr2V2O7
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
3.9100 3.9146 -.0046 0 1 2
3.5100 3.5099 .0001 3 1 0
3.3300 3.3349 -.0049 1 0 3
3.1900 3.1930 -.0030 4 0 1
3.1400 3.1430 -.0030 0 2 1
3.1000 3.1002 -.0002 4 0 0
2.9800 2.9806 -.0006 1 1 3
2.9300 2.9287 .0013 2 2 0
2.8100 2.8095 .0005 4 1 0
2.7100 2.7109 -.0009 4 1 2
2.5900 2.5897 .0003 3 2 0
2.5500 2.5486 .0014 -4 1 1
a= 12.806 b=6.645 c= 10.01 beta= 75.54
da= .005 db= .001 dc=.02 dbeta=.09
V= 824.5
Triklin
Dexp. Dcal. d(D) h k l
3.9100 3.9104 -.0004 -3 -1 0
3.5100 3.5157 -.0057 1 0 1
3.3300 3.3300 .0000 4 0 0
3.1900 3.1874 .0026 -1 -2 0
3.1400 3.1397 .0003 -4 -1 0
3.1000 3.1008 -.0008 0 1 1
2.9800 2.9815 -.0015 2 1 1
2.9300 2.9277 .0023 -1 1 1
2.8100 2.8114 -.0014 -2 -1 1
2.7100 2.7136 -.0036 2 -2 0
2.5900 2.5927 -.0027 -5 -1 0
2.5500 2.5508 -.0008 3 -1 1
A= 13.510 DA= .001
B= 6.404 DB= .005
C= 3.574 DC= .004
GAMMA= 81.71 DGAMMA= .04
BETA = 85.06 DBETA = .04
ALPHA= 89.4 DALPHA= .1
V= 304.8
76. 28-1269
Sr3V2O8
Rombik
Groupa 26,28,51
Dexp. Dcal. d(D) h k l
3.0800 3.0808 -.0008 2 1 0
2.7980 2.7957 .0023 2 0 1
2.3570 2.3580 -.0010 0 0 2
2.2280 2.2282 -.0002 0 3 0
2.1860 2.1870 -.0010 3 1 0
2.1450 2.1444 .0006 2 2 1
2.0780 2.0776 .0004 3 0 1
1.8560 1.8566 -.0006 1 2 2
1.6710 1.6712 -.0002 0 4 0
1.6200 1.6195 .0005 0 3 2
a= 6.9430 b= 6.6847 c= 4.7159
da= .0005 db= .0006 dc= .0001
v= 218.87
77. 28-1270
Sr4V2O9
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
4.7900 4.7902 -.0002 -3 0 2
4.3300 4.3281 .0019 -3 0 3
3.9500 3.9526 -.0026 1 0 4
3.7100 3.7112 -.0012 2 1 0
3.4900 3.4890 .0010 0 1 3
3.4000 3.3987 .0013 2 0 4
3.2800 3.2777 .0023 1 1 3
2.9900 2.9876 .0024 -5 0 2
2.8900 2.8897 .0003 5 0 0
2.8100 2.8120 -.0020 -4 1 2
2.5290 2.5297 -.0007 0 0 7
2.4680 2.4672 .0008 -6 0 3
a= 14.971 b= 4.326 c=18.349 beta=105.182
da=.004 db= .001 dc=.005 dbeta=.008
V=1147
78. 28-1271
Sr6V6O19
Triklin
Dexp. Dcal. d(D) h k l
3.5100 3.5108 -.0008 4 0 0
3.2700 3.2741 -.0041 0 0 1
3.0900 3.0886 .0014 -4 -1 0
3.0350 3.0347 .0003 -1 -3 0
2.9100 2.9102 -.0002 -2 0 1
2.8790 2.8804 -.0014 5 -1 0
2.8060 2.8086 -.0026 5 0 0
2.7340 2.7341 -.0001 -2 -3 0
2.6320 2.6317 .0003 -3 1 1
2.3650 2.3649 .0001 -4 1 1
2.2270 2.2272 -.0002 -5 -2 0
2.1880 2.1883 -.0003 -4 -1 1
A= 14.443 DA= .001
B= 10.079 DB= .001
C= 3.279 DC= .001
GAMMA=103.19 DGAMMA= .03
BETA = 87.33 DBETA = .02
ALPHA= 89.1 DALPHA= .1
V= 464.0
79. 28-1348
alfa-Tl3VF6
Triklin
Dexp Dcal d(D) h k l
5.1800 5.1772 .0028 0 1 1
4.4800 4.4817 -.0017 0 -1 1
3.4900 3.4873 .0027 -1 0 1
3.2600 3.2625 -.0025 1 1 1
3.1800 3.1781 .0019 -1 2 0
2.0760 2.0760 .0000 2 2 0
2.7150 2.7122 .0028 0 1 2
2.6040 2.6041 -.0001 0 4 1
2.4920 2.4930 -.0010 0 -1 2
2.3490 2.3501 -.0011 -1 1 2
2.2600 2.2595 .0005 -1 -1 2
2.2390 2.2393 -.0003 -1 2 2
A= 4.3222 DA= .0001
B= 11.0282 DB= .0001
C= 5.44823 DC= .00001
GAMMA= 84.012 DGAMMA= .004
BETA = 93.624 DBETA = .002
ALPHA= 80.097 DALPHA= .002
V=253.5
80. 28-1349
Tl0.30V2O5
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
12.9000 12.9204 -.0204 0 0 1
12.3000 12.2249 .0751 1 0 1
6.1200 6.1125 .0075 2 0 2
5.6900 5.6767 .0133 0 1 0
4.9300 4.9305 -.0005 2 1 0
4.3000 4.3068 -.0068 0 0 3
4.0700 4.0750 -.0050 3 0 3
3.8100 3.8108 -.0008 5 0 2
3.6500 3.6523 -.0023 -2 0 3
3.5600 3.5583 .0017 -4 0 2
3.5200 3.5178 .0022 4 1 2
3.4900 3.4923 -.0023 1 1 3
3.3100 3.3104 -.0004 3 1 3
a= 20.468 b= 5.677 c=13.2913 beta= 76.42
da=.002 db=.001 dc=.0005 dbeta=.04
V= 1501
81. 28-1350
TiVO4
Triklin
Dexp Dcal d(D) h k l
4.9500 4.9565 -.0065 0 1 1
4.8200 4.8209 -.0009 0 -1 1
4.3300 4.3356 -.0056 -1 1 1
3.9400 3.9311 .0089 0 -1 2
3.6500 3.6555 -.0055 -1 -1 1
3.5000 3.4980 .0020 2 0 0
3.4000 3.3959 .0041 1 1 2
3.1900 3.1905 -.0005 -1 -1 2
3.0300 3.0284 .0016 -1 1 3
2.9100 2.9107 -.0007 1 1 3
2.8500 2.8513 -.0013 1 0 4
2.7800 2.7804 -.0004 -2 1 2
A= 7.1289 DA= .0001
B= 5.434 DB= .004
C= 12.127 DC= .004
GAMMA=100.28 DGAMMA= .05
BETA = 86.16 DBETA = .03
ALPHA= 88.582 DALPHA= .007
V=460.4
82. 28-1352
Tl3VO4
Rombik
Grupa 16
Dexp. Dcal. d(D) h k l
5.1300 5.1483 .0183 4 0 0
4.7700 4.7827 .0127 4 0 1
4.2900 4.3076 .0176 0 0 3
4.1200 4.1186 -.0014 5 0 0
3.1500 3.1496 -.0004 0 1 0
2.9770 2.9769 -.0001 5 0 3
2.9280 2.9231 -.0049 3 0 4
2.6320 2.6304 -.0016 4 1 1
2.5260 2.5245 -.0015 8 0 1
2.5060 2.5068 .0008 2 0 5
2.3920 2.3914 -.0006 8 0 2
2.1480 2.1499 .0019 7 1 0
a= 20.593 b= 3.1496 c= 12.92
da=.003 db= .0009 dc=.04
V= 838
Triklin
Dexp Dcal d(D) h k l
5.1300 5.1313 -.0013 1 1 0
4.7700 4.7666 .0034 -1 1 1
4.2900 4.2954 -.0054 -1 -1 1
4.1200 4.1246 -.0046 1 1 1
3.1500 3.1515 -.0015 1 2 1
2.9770 2.9772 -.0002 -1 2 2
2.9280 2.9285 -.0005 1 1 2
2.6320 2.6337 -.0017 2 1 1
2.5260 2.5268 -.0008 -2 1 3
2.5060 2.5047 .0013 2 0 1
2.3920 2.3904 .0016 2 2 1
2.1480 2.1477 .0003 -2 -2 2
A= 6.8538 DA= .0006
B= 7.178 DB= .001
C= 8.597 DC= .001
GAMMA= 85.78 DGAMMA= .05
BETA =111.75 DBETA = .08
ALPHA= 70.431 DALPHA= .001
V= 360.6
Rombik
Grupa 16
Dexp. Dcal. d(D) h k l
5.1300 5.1483 .0183 4 0 0
4.7700 4.7827 .0127 4 0 1
4.2900 4.3076 .0176 0 0 3
4.1200 4.1186 -.0014 5 0 0
3.1500 3.1496 -.0004 0 1 0
2.9770 2.9769 -.0001 5 0 3
2.9280 2.9231 -.0049 3 0 4
2.6320 2.6304 -.0016 4 1 1
2.5260 2.5245 -.0015 8 0 1
2.5060 2.5068 .0008 2 0 5
2.3920 2.3914 -.0006 8 0 2
2.1480 2.1499 .0019 7 1 0
a= 20.593 b= 3.1496 c= 12.92
da=.003 db= .0009 dc=.04
V= 838
83. 28-1358
Tl3YbF6
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
3.8000 3.7998 .0002 -2 1 1
3.3600 3.3616 -.0016 -1 0 2
3.1400 3.1416 -.0016 1 1 2
2.9610 2.9622 -.0012 -1 1 2
2.7840 2.7844 -.0004 -1 2 1
2.6880 2.6893 -.0013 5 1 0
2.5600 2.5613 -.0013 3 2 1
2.5100 2.5092 .0008 5 0 2
2.3730 2.3719 .0011 1 2 2
2.3490 2.3514 -.0024 4 2 1
2.1030 2.1022 .0008 -6 1 1
1.9400 1.9405 -.0005 5 1 3
a= 15.10 b=6.265 c=7.282 beta= 80.27
da=.01 db=.001 dc=.001 dbeta=.01
V= 679.2
Triklin
Dexp Dcal d(D) h k l
3.8000 3.8008 -.0008 2 0 1
3.3600 3.3599 .0001 2 -1 1
3.1400 3.1402 -.0002 0 -2 1
2.9610 2.9616 -.0006 3 1 0
2.7840 2.7846 -.0006 2 2 0
2.6880 2.6914 -.0034 -3 -1 1
2.5600 2.5571 .0029 2 0 2
2.5100 2.5098 .0002 2 -2 1
2.3730 2.3741 -.0011 -2 0 2
2.3490 2.3466 .0024 4 0 0
2.1030 2.1014 .0016 1 3 0
1.9400 1.9401 -.0001 -1 -1 3
A= 9.482 DA= .009
B= 6.566 DB= .003
C= 6.0150 DC= .0007
GAMMA= 83.40 DGAMMA= .07
BETA = 87.20 DBETA = .02
ALPHA=105.41 DALPHA= .02
V= 357.4
84. 28-1429
VBr3*6H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
6.0000 6.0084 -.0084 3 0 0
5.8500 5.8493 .0007 -1 0 3
4.7800 4.7809 -.0009 0 1 0
4.7200 4.7264 -.0064 0 0 4
4.5100 4.5113 -.0013 -1 0 4
4.4600 4.4733 -.0133 3 0 3
4.2300 4.2338 -.0038 -3 0 3
4.1600 4.1576 .0024 4 0 2
3.7400 3.7411 -.0011 3 1 0
3.4300 3.4319 -.0019 5 0 2
3.3300 3.3277 .0023 1 1 4
3.1900 3.1904 -.0004 2 1 4
3.0600 3.0604 -.0004 -4 1 2
a=18.05 b= 4.781 c= 18.93 beta=86.8
da=.01 db=.001 dc=.05 dbeta=.1
V= 1632
85. 28-1431
VH{SO4}2*4H2O
Rombik
Groupa 48
Dexp. Dcal. d(D) h k l
9.1400 9.0801 .0599 2 0 0
5.1700 5.1449 .0251 1 1 0
4.8500 4.8301 .0199 0 0 2
4.7200 4.6900 .0300 0 1 1
4.2700 4.2643 .0057 2 0 2
4.1700 4.1670 .0030 2 1 1
4.0200 4.0149 .0051 3 1 0
3.5300 3.5214 .0086 1 1 2
3.3100 3.3081 .0019 4 0 2
3.2600 3.2620 -.0020 4 1 1
3.0900 3.0875 .0025 3 1 2
2.7610 2.7609 .0001 0 1 3
a=18.16 b= 5.365 c= 9.66
da= .021966 db= .009815 dc= .010169
v= 941
Triklin
Dexp Dcal d(D) h k l
9.1400 9.1367 .0033 1 -1 0
5.1700 5.1759 -.0059 -1 0 1
4.8500 4.8526 -.0026 -1 -2 1
4.7200 4.7206 -.0006 0 -4 1
4.2700 4.2690 .0010 -2 3 0
4.1700 4.1731 -.0031 0 -5 1
4.0200 4.0202 -.0002 -1 6 0
3.5300 3.5288 .0012 2 -4 1
3.3100 3.3103 -.0003 -1 6 1
3.2600 3.2565 .0035 0 0 2
3.0900 3.0923 -.0023 0 -3 2
2.7610 2.7612 -.0002 -1 -4 2
A= 9.730 DA= .001
B= 26.335 DB= .007
C= 6.549 DC= .005
GAMMA= 91.21 DGAMMA= .01
BETA = 84.38 DBETA = .02
ALPHA= 92.341 DALPHA= .002
V= 1668.5
86. 28-1432
C6H6N3O6V*7H2O
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
6.1200 6.1416 -.0216 2 1 0
5.8200 5.7668 .0532 1 2 0
5.4000 5.4260 -.0260 0 0 1
4.9800 4.9865 -.0065 0 1 1
4.2900 4.2944 -.0044 2 0 1
4.0700 4.0664 .0036 2 1 1
3.5600 3.5527 .0073 2 2 1
3.2400 3.2395 .0005 1 3 1
3.0700 3.0708 -.0008 4 2 0
2.8700 2.8717 -.0017 4 1 1
2.6100 2.6066 .0034 1 1 2
2.4800 2.4817 -.0017 2 1 2
2.2600 2.2627 -.0027 1 5 1
2.1200 2.1197 .0003 6 1 1
2.0200 2.0190 .0010 2 6 0
a=14.0510 b=12.648 c= 5.4260
da= .000358 db= .009230 dc= .000387
v= 964.3
Triklin
Dexp Dcal d(D) h k l
6.1200 6.1219 -.0019 1 0 0
5.8200 5.8226 -.0026 0 -1 1
5.4000 5.3934 .0066 -1 0 1
4.9800 4.9639 .0161 -1 1 1
4.2900 4.2894 .0006 1 -1 1
4.0700 4.0814 -.0114 0 0 2
3.5600 3.5641 -.0041 -1 1 2
3.2400 3.2395 .0005 -1 -1 2
3.0700 3.0677 .0023 1 -1 2
2.8700 2.8699 .0001 0 2 2
2.6100 2.6093 .0007 -1 1 3
2.4800 2.4800 -.0000 -1 -1 3
2.2600 2.2596 .0004 -2 1 3
2.1200 2.1200 .0000 1 -2 3
2.0200 2.0201 -.0001 -1 1 4
A= 6.399 DA= .004
B= 8.41 DB= .01
C= 8.31 DC= .01
GAMMA=103.32 DGAMMA= .0438
BETA =100.6 DBETA = .2
ALPHA= 88.36 DALPHA= .06
V= 427.7
87. 28-1435
VOH5O4
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.1500 5.1512 -.0012 1 1 0
4.7600 4.7556 .0044 1 1 1
3.5900 3.5911 -.0011 0 2 0
3.2600 3.2607 -.0007 1 1 2
3.1700 3.1730 -.0030 2 0 2
3.1200 3.1254 -.0054 1 2 1
2.5630 2.5632 -.0002 1 2 2
2.3800 2.3778 .0022 2 2 2
2.2750 2.2776 -.0026 1 3 0
2.2410 2.2400 .0010 1 3 1
2.0290 2.0291 -.0001 3 1 3
2.0050 2.0035 .0015 1 3 2
a= 7.991 b= 7.182 c= 7.346 beta= 67.667
da=.003 db=.005 dc=.009 dbeta=.003
V= 390.0
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.1500 5.1512 -.0012 1 1 0
4.7600 4.7556 .0044 1 1 1
3.5900 3.5911 -.0011 0 2 0
3.2600 3.2607 -.0007 1 1 2
3.1700 3.1730 -.0030 2 0 2
3.1200 3.1254 -.0054 1 2 1
2.5630 2.5632 -.0002 1 2 2
2.3800 2.3778 .0022 2 2 2
2.2750 2.2776 -.0026 1 3 0
2.2410 2.2400 .0010 1 3 1
2.0290 2.0291 -.0001 3 1 3
2.0050 2.0035 .0015 1 3 2
a= 7.991 b= 7.182 c= 7.346 beta= 67.667
da=.003 db=.005 dc=.009 dbeta=.003
V= 390.0
88. 28-1436
V2S6O23*H2O
Triklin
Dexp Dcal d(D) h k l
12.6000 12.5921 .0079 0 0 1
6.2900 6.2874 .0026 0 1 1
5.8900 5.8851 .0049 2 0 1
5.2100 5.2145 -.0045 -2 1 0
5.0000 4.9977 .0023 2 -1 1
4.7900 4.7943 -.0043 -2 0 2
4.5000 4.5074 -.0074 2 0 2
4.4000 4.3971 .0029 -3 0 1
4.1600 4.1578 .0022 0 -1 3
4.1200 4.1222 -.0022 -1 -2 1
4.0000 3.9990 .0010 1 -2 1
3.7400 3.7382 .0018 2 1 2
A= 13.799 DA= .002
B= 8.548 DB= .001
C= 12.985 DC= .00372
GAMMA= 87.25 DGAMMA= .01
BETA = 94.103 DBETA = .005
ALPHA=103.69 DALPHA= .01
V=1486.3
89. 28-1437
V2S4O17*2H2O
Triklin
Dexp Dcal d(D) h k l
7.6000 7.5994 .0006 1 1 0
5.5600 5.5604 -.0004 -1 1 1
5.3000 5.2995 .0005 -1 -1 1
4.8000 4.7980 .0020 0 -1 1
3.7100 3.7101 -.0001 -2 1 1
3.3000 3.2999 .0001 -2 1 2
3.2150 3.2160 -.0010 2 0 1
3.1620 3.1635 -.0015 1 3 1
3.0850 3.0858 -.0008 0 3 1
2.8560 2.8559 .0001 2 3 1
2.6550 2.6552 -.0002 1 -2 1
2.2250 2.2249 .0001 -4 0 2
A= 9.463 DA= .001
B= 9.614 DB= .004
C= 8.3318 DC= .0001
GAMMA= 74.35 DGAMMA= .03
BETA =105.18 DBETA = .02
ALPHA= 73.756 DALPHA= .003
V= 652.5
90. 28-1438
V2S4O17*3H2O
Rombik
Grupa 16
Dexp. Dcal. d(D) h k l
9.1500 9.1734 .0234 2 0 0
6.3900 6.4082 .0182 2 1 0
5.1300 5.1201 -.0099 2 1 1
4.4900 4.4778 -.0122 0 2 0
4.3400 4.3438 .0038 3 1 1
4.1400 4.1471 .0071 1 0 2
4.0800 4.0824 .0024 4 1 0
4.0300 4.0240 -.0060 2 2 0
3.9600 3.9632 .0032 0 2 1
3.8700 3.8738 .0038 1 2 1
3.7600 3.7632 .0032 1 1 2
3.6800 3.6812 .0012 4 1 1
a= 18.35 b= 8.956 c= 8.515
da=.02 db=.002 dc=.004
V= 1399
Triklin
Dexp Dcal d(D) h k l
9.1500 9.1743 -.0243 0 0 1
6.3900 6.3865 .0035 1 0 1
5.1300 5.1309 -.0009 0 -2 1
4.4900 4.4890 .0010 2 0 0
4.3400 4.3396 .0005 0 -3 0
4.1400 4.1370 .0030 2 1 1
4.0800 4.0820 -.0020 -2 -1 1
4.0300 4.0296 .0004 1 3 1
3.9600 3.9596 .0004 -1 -1 2
3.8700 3.8722 -.0022 2 2 1
3.7600 3.7583 .0017 1 2 2
3.6800 3.6790 .0010 -2 1 1
A= 9.2466 DA= .0001
B= 13.45 DB= .01
C= 9.2003 DC= .0006
GAMMA= 76.17 DGAMMA= .03
BETA = 89.51 DBETA = .02
ALPHA= 85.72 DALPHA= .01
V=1107.8
91. 28-1439
{VO}2H2{SO4}3
Tetrag.
Groupa 90,113
Dexp. Dcal. d(D) h k l
7.8000 7.7912 .0088 0 0 1
5.8800 5.8851 -.0051 1 0 1
4.4900 4.4902 -.0002 2 0 0
4.0200 4.0161 .0039 2 1 0
3.9000 3.8956 .0044 0 0 2
3.5900 3.5738 .0162 1 0 2
3.1700 3.1750 -.0050 2 2 0
2.9390 2.9403 -.0013 2 2 1
2.7980 2.7962 .0018 2 1 2
2.4920 2.4907 .0013 3 2 0
2.4610 2.4611 -.0001 2 2 2
2.2450 2.2451 -.0001 4 0 0
a= 8.9807 c= 7.791
da= .001 dc= .008
V= 628.3
Triklin
Dexp Dcal d(D) h k l
7.8000 7.7951 .0049 1 0 0
5.8800 5.8768 .0032 0 -1 0
4.4900 4.4920 -.0020 0 -1 1
4.0200 4.0224 -.0024 1 -1 0
3.9000 3.8975 .0025 2 0 0
3.5900 3.5895 .0005 -2 0 1
3.1700 3.1703 -.0003 1 2 0
2.9390 2.9384 .0006 0 -2 0
2.7980 2.7980 .0000 0 -1 2
2.4920 2.4925 -.0005 0 2 1
2.4610 2.4614 -.0004 -1 2 0
2.2450 2.2460 -.0010 0 -2 2
A= 8.737 DA= .001
B= 6.526 DB= .001
C= 6.1854 DC= .0001
GAMMA= 65.470 DGAMMA= .007
BETA =105.72 DBETA = .03
ALPHA=103.69 DALPHA= .06
V= 305.7
92. 28-1965
C15H30N3OS6V
Triklin
Dexp Dcal d(D) h k l
8.4500 8.4526 -.0026 0 1 1
7.3300 7.3269 .0031 -1 1 0
6.8100 6.7853 .0247 1 0 1
6.0400 6.0553 -.0153 0 0 2
5.6900 5.6757 .0143 1 -1 1
5.3800 5.3678 .0122 -1 1 2
4.9800 4.9808 -.0008 0 2 1
4.7900 4.7930 -.0030 -1 2 1
4.6000 4.6042 -.0042 -2 0 1
4.3500 4.3517 -.0017 1 1 2
4.0300 4.0290 .0010 2 1 0
3.8700 3.8720 -.0020 2 -1 1
A= 9.516 DA= .003
B= 10.464 DB= .007
C= 12.503 DC= .008
GAMMA= 98.935 DGAMMA= .004
BETA =101.65 DBETA = .01
ALPHA= 79.964 DALPHA= .05
V=1194
93. 28-1966
C3H18N9O19VW
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
11.1000 11.1028 -.0028 1 0 0
10.4000 10.3576 .0424 0 1 0
7.6000 7.5813 .0187 1 0 1
6.1200 6.1176 .0024 1 1 1
5.5500 5.5514 -.0014 2 0 0
5.1900 5.1826 .0074 -2 0 1
3.7900 3.7906 -.0006 2 0 2
3.7000 3.7009 -.0009 3 0 0
3.4800 3.4777 .0023 1 0 3
3.4500 3.4525 -.0025 0 3 0
3.1900 3.1897 .0003 -1 3 1
3.1200 3.1185 .0015 -2 1 3
a=11.153 b= 10.36 c=11.384 beta= 95.41
da= .004 db=.01 dc=.005 dbeta=.01
V= 1309.2
Triklin
Dexp Dcal d(D) h k l
11.1000 11.0994 .0006 1 0 0
10.4000 10.3854 .0146 1 1 0
7.6000 7.6003 -.0003 0 0 1
6.1200 6.1207 -.0007 0 -1 1
5.5500 5.5497 .0003 2 0 0
5.1900 5.1927 -.0027 2 2 0
3.7900 3.7899 .0001 0 2 2
3.7000 3.6998 .0002 3 0 0
3.4800 3.4781 .0019 3 3 1
3.4500 3.4499 .0001 0 3 2
3.1900 3.1903 -.0003 -1 4 0
3.1200 3.1195 .0005 -2 3 1
A= 11.715 DA= .004
B= 15.8369 DB= .0003
C= 7.9451 DC= .0003
GAMMA= 71.65 DGAMMA= .01
BETA = 81.77 DBETA = .01
ALPHA= 73.39 DALPHA= .005
V= 1338.3
94. 28-1967
C3H19-xN9O19VxW4+x
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
11.1000 11.0265 .0735 1 0 0
10.3000 10.2935 .0065 0 1 0
7.5000 7.5244 -.0244 1 1 0
6.0800 6.0799 .0001 0 1 1
5.9500 5.9517 -.0017 1 0 1
5.5300 5.5143 .0157 -1 1 1
5.1600 5.1524 .0076 1 1 1
3.7600 3.7622 -.0022 2 2 0
3.6800 3.6785 .0015 -1 0 2
3.4600 3.4610 -.0010 -2 2 1
3.4400 3.4408 -.0008 -3 0 1
3.1800 3.1812 -.0012 3 0 1
a=11.08 b=10.29 c=7.572 beta=95.7
da=.01 db=.01 dc=.007 dbeta=.1
V= 859
Triklin
Dexp Dcal d(D) h k l
11.1000 10.9652 .1348 0 0 1
10.3000 10.3055 -.0055 0 1 0
7.5000 7.5069 -.0069 -1 0 1
6.0800 6.0796 .0004 0 -1 2
5.9500 5.9518 -.0018 1 0 1
5.5300 5.5270 .0030 -1 -1 2
5.1600 5.1671 -.0071 -1 0 2
3.7600 3.7594 .0006 -2 1 1
3.6800 3.6811 -.0011 -1 0 3
3.4600 3.4601 -.0001 -1 -3 1
3.4400 3.4399 .0001 1 2 1
3.1800 3.1809 -.0009 -2 -2 3
A= 8.508 DA= .001
B= 11.4984 DB= .0003
C= 12.569 DC= .001
GAMMA= 87.296 DGAMMA= .002
BETA =103.52 DBETA = .03
ALPHA=116.103 DALPHA= .008
V= 1071.6
95. 28-1968
C12H36N3O19VW5
Triklin
Dexp Dcal d(D) h k l
8.4000 8.3991 .0009 1 0 0
7.3000 7.3052 -.0052 -1 1 0
7.2000 7.1987 .0013 0 0 1
5.1700 5.1721 -.0021 -2 1 1
4.2500 4.2508 -.0008 1 1 1
4.2000 4.1996 .0004 2 0 0
3.3700 3.3701 -.0001 1 2 0
3.3400 3.3396 .0004 -3 2 1
2.9880 2.9880 -.0000 1 1 2
2.8340 2.8342 -.0002 0 3 0
2.2070 2.2070 -.0000 -3 -1 2
2.4510 2.4509 .0001 1 3 0
2.0610 2.0613 -.0003 -5 3 2
A= 10.391 DA= .002
B= 10.695 DB= .001
C= 9.050 DC= .001
GAMMA=121.13 DGAMMA= .03
BETA =121.07 DBETA = .01
ALPHA= 57.41 DALPHA= .01
V= 684.87