1. 24-0173
Cd2V2O7
Triklin
Dexp Dcal d(D) h k l
5.4700 5.4757 -.0057 0 1 1
4.8400 4.8396 .0004 0 -1 1
4.5100 4.5062 .0038 -1 1 1
4.0100 4.0098 .0002 1 -1 1
3.4500 3.4508 -.0008 1 1 1
3.3430 3.3421 .0009 -1 1 2
3.2970 3.2969 .0001 -1 0 2
3.1750 3.1748 .0002 1 0 2
2.7520 2.7531 -.0011 -1 2 2
2.7390 2.7379 .0011 0 2 2
2.5930 2.5933 -.0003 0 1 3
2.5470 2.5471 -.0001 1 2 0
A= 5.7381 DA= .0007
B= 7.0359 DB= .0005
C= 8.09862 DC= .00065
GAMMA=107.004 DGAMMA= .001
BETA = 94.5402 DBETA = .0001
ALPHA= 81.832 DALPHA= .006
V-309.3
2. 24-0174
beta-Cd4V2O9
Triklin
Dexp Dcal d(D) h k l
5.1800 5.1825 -.0025 -1 2 0
4.5500 4.5504 -.0004 0 -1 2
4.1500 4.1514 -.0014 -1 -1 2
3.8200 3.8197 .0003 0 -2 2
3.4700 3.4687 .0013 1 -3 1
3.4000 3.4000 .0000 -2 1 2
3.1800 3.1807 -.0007 1 3 0
3.1440 3.1452 -.0012 0 -1 3
3.0350 3.0348 .0002 -2 3 1
3.0000 2.9990 .0010 -2 -2 1
2.9400 2.9397 .0003 1 2 2
2.8970 2.8971 -.0001 1 3 1
A= 8.204 DA= .006
B= 11.734 DB= .002
C= 9.841 DC= .001
GAMMA=101.67 DGAMMA= .07
BETA =101.621 DBETA = .009
ALPHA= 91.592 DALPHA= .003
V= 906.5
3. 24-0665
LiV10O24
Triklin
Dexp Dcal d(D) h k l
5.5400 5.5413 -.0013 -1 0 1
3.6000 3.5973 .0027 0 1 0
3.4400 3.4408 -.0008 0 -1 2
3.2000 3.2025 -.0025 0 -1 3
3.0000 3.0000 .0000 1 -1 1
2.9420 2.9421 -.0001 1 0 5
2.6390 2.6396 -.0006 -2 0 3
2.5470 2.5466 .0004 0 0 7
2.3940 2.3947 -.0007 0 -1 6
2.1830 2.1836 -.0006 -2 -1 3
1.8130 1.8131 -.0001 -2 0 8
1.7080 1.7081 -.0001 -1 2 0
A= 5.72370 DA= .00008
B= 3.6117 DB= .0007
C= 17.931 DC= .003
GAMMA= 88.81 DGAMMA= .02
BETA = 93.71 DBETA = .01
ALPHA= 95.04 DALPHA= .03
V= 368.4
4. 24-0667
Li3VO4
Triklin
Dexp Dcal d(D) h k l
5.5000 5.4994 .0006 0 1 0
4.1700 4.1569 .0131 0 -1 2
3.9600 3.9623 -.0023 -2 0 1
3.9200 3.9126 .0074 2 0 1
3.7100 3.7045 .0055 -2 -1 1
3.6900 3.6951 -.0051 2 1 0
3.2000 3.2022 -.0022 2 1 1
3.1800 3.1821 -.0021 -2 0 2
3.1000 3.1020 -.0020 0 1 2
2.8800 2.8789 .0011 -2 1 1
2.7450 2.7448 .0002 3 1 0
2.7450 2.7448 .0002 3 1 0
A= 8.8396 DA= .0001
B= 5.8204 DB= .00020
C= 9.57256 DC= .00007
GAMMA= 80.7962 DGAMMA= .0008
BETA = 93.5931 DBETA = .0009
ALPHA=107.180 DALPHA= .001
V=464.4
5. 24-0668
Li3VO4
Triklin
Dexp Dcal d(D) h k l
5.5000 5.5023 -.0023 1 0 0
4.3300 4.3293 .0007 -1 2 1
4.1700 4.1675 .0025 1 0 1
4.1400 4.1474 -.0074 -1 1 2
3.9700 3.9672 .0028 0 2 2
3.7200 3.7271 -.0071 -1 2 0
3.2100 3.2094 .0006 1 2 1
3.2000 3.2026 -.0026 1 2 0
3.1800 3.1799 .0001 -1 3 2
3.1100 3.1126 -.0026 0 3 2
2.8800 2.8771 .0029 -1 -1 2
2.7500 2.7493 .0007 -2 1 0
A= 5.8467 DA= .0003
B= 10.20 DB= .01
C= 9.419 DC= .005
GAMMA=106.09 DGAMMA= .08
BETA =107.74 DBETA = .03
ALPHA= 60.76 DALPHA= .04
V= 461.3
6. 24-0669
Li3VO4
Triklin
Dexp Dcal d(D) h k l
5.5000 5.4988 .0012 -1 2 0
4.1800 4.1792 .0008 0 1 1
3.9700 3.9702 -.0002 0 -1 1
3.7200 3.7196 .0004 -1 4 0
3.2100 3.2105 -.0005 0 -3 1
3.1900 3.1897 .0003 1 -2 1
2.7500 2.7494 .0006 -2 4 0
2.5200 2.5207 -.0007 2 2 1
2.2500 2.2502 -.0002 3 1 0
2.1500 2.1493 .0007 1 -6 1
1.9700 1.9701 -.0001 3 1 1
1.9500 1.9502 -.0002 -1 8 1
A= 6.875 DA= .001
B= 17.226 DB= .003
C= 4.2201 DC= .0001
GAMMA= 93.37 DGAMMA= .01
BETA = 92.10 DBETA = .01
ALPHA= 83.536 DALPHA= .004
V= 495.5
7. 24-0758
beta-HgV2O7
Rombik
Groupa 16,25,47
Dexp. Dcal. d(D) h k l
8.4300 8.4232 .0068 0 0 3
4.2100 4.2116 -.0016 0 0 6
4.0800 4.0810 -.0010 3 0 0
3.1900 3.1889 .0011 0 1 0
3.1100 3.1095 .0005 2 0 7
2.9800 2.9823 -.0023 0 1 3
2.8300 2.8282 .0018 2 1 0
2.5800 2.5813 -.0013 2 1 4
2.4900 2.4892 .0008 1 1 6
2.3900 2.3900 .0000 0 1 7
a=12.243 b= 3.18892 c=25.269
da= .001 db= .00002 dc= .001
V= 986.6
8. 24-0759
alfa-Hg4V2O9
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
8.4000 8.3976 .0024 0 1 0
5.4500 5.4459 .0041 -1 1 1
3.9300 3.9326 -.0026 1 2 0
3.7800 3.7824 -.0024 0 2 1
3.6200 3.6212 -.0012 -1 2 1
3.5800 3.5810 -.0010 1 1 2
3.3600 3.3619 -.0019 2 2 0
3.3200 3.3192 .0008 2 0 2
3.2900 3.2910 -.0010 -2 1 2
3.1900 3.1863 .0037 -2 2 1
2.9040 2.9039 .0001 0 0 3
2.7980 2.7992 -.0012 0 3 0
a= 11.26 b= 8.398 c= 8.738 beta= 94.4
da=.02 db=.005 dc= .006 dbeta=.1
V= 824
Triklin
Dexp Dcal d(D) h k l
8.4000 8.3927 .0073 0 1 0
5.4500 5.4445 .0055 0 1 1
3.9300 3.9273 .0027 0 -1 2
3.7800 3.7819 -.0019 -2 1 0
3.6200 3.6187 .0013 2 -1 1
3.5800 3.5863 -.0063 2 0 1
3.3600 3.3605 -.0005 -1 2 1
3.3200 3.3162 .0038 -1 -1 2
3.2900 3.2933 -.0033 -1 -2 1
3.1900 3.1899 .0001 -1 1 2
2.9040 2.9026 .0014 2 0 2
2.7980 2.7976 .0004 0 3 0
A= 7.90 DA= .01
B= 8.6583 DB= .0005
C= 8.317 DC= .002
GAMMA=101.03 DGAMMA= .06
BETA = 84.68 DBETA = .04
ALPHA= 99.88 DALPHA= .03
V= 549.3
9. 24-0761
beta-Hg6V2O11
Triklin
Dexp Dcal d(D) h k l
6.5600 6.5515 .0085 0 1 1
5.3000 5.3007 -.0007 0 -1 1
5.1200 5.1323 -.0123 1 0 0
3.5100 3.5103 -.0003 -1 -1 2
3.4100 3.4060 .0040 0 2 1
3.3300 3.3351 -.0051 1 0 3
3.2700 3.2729 -.0029 1 -1 1
3.1600 3.1605 -.0005 -1 1 2
3.0500 3.0546 -.0046 -1 -2 1
3.0200 3.0207 -.0007 1 1 4
2.9700 2.9743 -.0043 0 2 3
2.7500 2.7495 .0005 1 2 4
A= 5.6054 DA= .0007
B= 7.4257 DB= .0002
C= 13.089 DC= .001
GAMMA= 66.558 DGAMMA= .008
BETA = 80.01 DBETA = .02
ALPHA= 72.71 DALPHA= .03
V=475.8
10. 24-0762
alfa-Hg6V2O11
Rombik
Groupa 54
Dexp. Dcal. d(D) h k l
5.8200 5.8148 .0052 0 0 4
5.7000 5.6821 .0179 0 1 0
3.9300 3.9243 .0057 2 0 2
3.5200 3.5152 .0048 1 0 6
3.3200 3.3267 -.0067 2 1 1
3.2300 3.2290 .0010 2 1 2
2.9050 2.9074 -.0024 0 0 8
2.8450 2.8411 .0039 0 2 0
2.6700 2.6714 -.0014 1 2 1
2.5430 2.5407 .0023 1 2 3
2.3780 2.3764 .0016 3 1 3
2.3630 2.3630 -.0000 2 1 7
2.3340 2.3358 -.0018 2 2 1
2.3000 2.3013 -.0013 2 2 2
a= 8.338 b= 5.6821 c=23.259
da= .004 db= .0009 dc= .001
V=1101.9
11. 24-0906
K2V8O21
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
9.5000 9.4792 .0208 0 1 1
4.7300 4.7396 -.0096 0 2 2
4.5900 4.5796 .0104 0 0 4
3.5300 3.5294 .0006 0 2 4
3.4000 3.4055 -.0055 1 1 0
3.1600 3.1597 .0003 0 3 3
3.0600 3.0557 .0043 0 2 5
2.9700 2.9663 .0037 1 2 1
2.6500 2.6509 -.0009 0 4 2
2.5600 2.5601 -.0001 1 0 5
2.3700 2.3698 .0002 0 4 4
1.9100 1.9105 -.0005 0 2 9
a= 3.579 b=11.078 c=18.32
da= .004 db= .006 dc= .03
V= 726
12. 24-0907
K2V18O45
Triklin
Dexp Dcal d(D) h k l
9.5500 9.5443 .0057 1 0 0
7.3700 7.3752 -.0052 0 1 0
5.1000 5.1008 -.0008 0 1 1
4.7800 4.7722 .0078 2 0 0
3.9000 3.9035 -.0035 1 2 0
3.6900 3.6876 .0024 0 2 0
3.5200 3.5228 -.0028 1 2 1
3.3900 3.3892 .0008 1 -1 1
3.3500 3.3477 .0023 -2 1 1
3.1800 3.1814 -.0014 3 0 0
3.1100 3.1098 .0002 -1 2 0
2.9400 2.9402 -.0002 3 2 0
A= 10.164 DA= .001
B= 7.967 DB= .001
C= 5.8499 DC= .0009
GAMMA= 72.123 DGAMMA= .003
BETA = 95.33 DBETA = .01
ALPHA= 78.98 DALPHA= .01
V= 436.6
24-0962, 24-0978 ñì. ñîåäèíåíèÿ U
13. 24-0984
Rb2V8O21
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
7.7300 7.7265 .0035 1 1 0
5.7500 5.7533 -.0033 -1 1 1
4.3600 4.3654 -.0054 0 3 0
3.9700 3.9717 -.0017 1 3 0
3.5400 3.5421 -.0021 -1 2 2
3.2100 3.2100 .0000 2 3 1
3.0300 3.0309 -.0009 -1 3 2
2.8870 2.8853 .0017 -3 0 1
2.6200 2.6192 .0008 0 5 0
2.4790 2.4791 -.0001 3 3 2
2.3870 2.3865 .0005 -2 2 3
2.2910 2.2908 .0002 4 2 1
a= 9.784 b=13.096 c=10.618 beta= 77.98
da=.005 db=.009 dc=.003 dbeta=.04
V= 1331
Triklin
Dexp Dcal d(D) h k l
7.7300 7.7315 -.0015 -1 0 1
5.7500 5.7539 -.0039 0 1 0
4.3600 4.3556 .0044 0 -1 2
3.9700 3.9747 -.0047 2 1 0
3.5400 3.5368 .0032 -1 -1 3
3.2100 3.2106 -.0006 -1 1 2
3.0300 3.0258 .0042 -1 -2 2
2.8870 2.8868 .0002 1 0 3
2.6200 2.6195 .0005 0 1 3
2.4790 2.4792 -.0002 -2 0 4
2.3870 2.3867 .0003 -4 -1 1
2.2910 2.2907 .0003 -4 -1 3
A= 9.6841 DA= .0002
B= 6.253 DB= .001
C= 11.0004 DC= .0007
GAMMA= 71.848 DGAMMA= .005
BETA =109.79 DBETA = .02
ALPHA=109.19 DALPHA= .02
V= 576.8
24-1040 ñì. ñîåäèíåíèÿ U
14. 24-1393
V2S4O17*H2O
Rombik
Groupa 31,59
Dexp. Dcal. d(D) h k l
7.3500 7.3372 .0128 2 1 0
5.4200 5.4208 -.0008 0 1 1
5.0400 5.0495 -.0095 3 0 1
4.6800 4.6777 .0023 5 0 0
4.3700 4.3700 .0000 2 2 0
3.9000 3.8981 .0019 6 0 0
3.6700 3.6686 .0014 4 2 0
3.1500 3.1491 .0009 7 1 0
3.0500 3.0496 .0004 3 0 2
3.0200 3.0200 .0000 2 1 2
3.0010 3.0034 -.0024 6 2 0
2.8180 2.8176 .0004 1 3 1
a=23.389 b= 9.42252 c= 6.627
da= .006 db= .00006 dc= .006
v=1461
Triklin
Dexp Dcal d(D) h k l
7.3500 7.3463 .0037 0 1 1
5.4200 5.4155 .0045 0 -1 1
5.0400 5.0558 -.0158 1 0 1
4.6800 4.6824 -.0024 1 1 1
4.3700 4.3700 .0000 -1 1 1
3.9000 3.9019 -.0019 -1 0 2
3.6700 3.6731 -.0031 0 2 2
3.1500 3.1539 -.0039 -1 2 1
3.0500 3.0536 -.0036 -1 2 0
3.0200 3.0211 -.0011 -1 0 3
3.0010 2.9970 .0040 -1 2 2
2.8180 2.8178 .0002 1 2 3
A= 5.746 DA= .003
B= 7.97 DB= .01
C= 11.258 DC= .003
GAMMA= 85.66 DGAMMA= .06
BETA = 88.48 DBETA = .06
ALPHA= 71.65 DALPHA= .05
V= 488.1
15. 24-1479
ZnV20O48.5
Triklin
Dexp Dcal d(D) h k l
5.7100 5.7103 -.0003 -1 0 1
5.5400 5.5363 .0037 0 -1 1
3.6400 3.6375 .0025 1 -2 1
3.5800 3.5802 -.0002 1 1 2
3.4500 3.4551 -.0051 -2 -1 1
3.3300 3.3295 .0005 -1 1 2
3.1900 3.1892 .0008 2 2 0
3.0600 3.0585 .0015 0 2 2
2.9300 2.9279 .0021 -3 0 1
2.6250 2.6263 -.0013 2 -2 2
2.5660 2.5665 -.0005 0 0 3
2.5370 2.5372 -.0002 1 1 3
2.3780 2.3784 -.0004 -1 3 2
A= 10.298 DA= .001
B= 8.907 DB= .007
C= 7.828 DC= .002
GAMMA= 94.4 DGAMMA= .1
BETA = 81.32 DBETA = .02
ALPHA= 85.0 DALPHA= .1
V= 704.2
16. 24-1480
Zn0.29V2O5
Triklin
Dexp Dcal d(D) h k l
6.8900 6.8819 .0081 1 0 0
5.4700 5.4802 -.0102 -1 1 1
3.6200 3.6187 .0013 -1 -1 1
3.5700 3.5690 .0010 -2 1 0
3.4400 3.4409 -.0009 2 0 0
3.3200 3.3249 -.0049 0 -1 2
3.0700 3.0695 .0005 1 1 3
2.9840 2.9844 -.0004 -2 0 1
2.9280 2.9274 .0006 2 1 0
2.7150 2.7156 -.0006 -1 -1 2
2.6230 2.6221 .0009 -2 3 0
2.5330 2.5333 -.0003 -2 3 2
A= 7.220 DA= .002
B= 10.023 DB= .003
C= 9.7616 DC= .0005
GAMMA=102.54 DGAMMA= .07
BETA = 84.23 DBETA = .09
ALPHA= 65.30 DALPHA= .01
V= 611.7
17. 24-1483
Zn2V2O7
Triklin
Dexp Dcal d(D) h k l
5.2800 5.2810 -.0010 1 0 0
4.1400 4.1430 -.0030 -1 1 1
3.4400 3.4417 -.0017 -1 -1 1
3.1100 3.1112 -.0012 0 2 0
2.7610 2.7637 -.0027 -1 2 0
2.6570 2.6569 .0001 0 2 2
2.5710 2.5692 .0018 -1 2 2
2.3840 2.3830 .0010 -1 0 3
2.3460 2.3458 .0002 -2 1 2
2.2110 2.2094 .0016 2 1 1
2.1350 2.1339 .0011 0 -1 3
2.0670 2.0671 -.0001 -2 -1 2
A= 5.3920 DA= .0002
B= 6.3935 DB= .0002
C= 7.6422 DC= .0002
GAMMA= 96.14 DGAMMA= .01
BETA =101.00 DBETA = .01
ALPHA= 77.290 DALPHA= .005
V=251.8
18. 24-1859
C36H30P3S6V
Triklin
Dexp Dcal d(D) h k l
16.2000 16.2149 -.0149 1 0 0
12.7000 12.6938 .0062 -1 0 1
11.8000 11.7955 .0045 -1 -2 1
9.8100 9.8135 -.0035 -1 1 1
8.5900 8.5853 .0047 -2 -2 1
8.0100 8.0107 -.0007 -1 -1 2
7.5300 7.5301 -.0001 0 -1 2
7.1400 7.1478 -.0078 -2 1 0
6.6600 6.6643 -.0043 0 1 2
5.6300 5.6270 .0030 3 1 0
5.3400 5.3391 .0009 1 2 2
5.1200 5.1208 -.0008 -2 -3 3
A= 18.111 DA= .001
B= 28.032 DB= .004
C= 16.141 DC= .004
GAMMA= 68.23 DGAMMA= .03
BETA =110.79 DBETA = .08
ALPHA=109.21 DALPHA= .05
V= 6929
19. 24-1975
C6H18O12P3V
Rombik
Groupa 16
Dexp. Dcal. d(D) h k l
13.0000 13.0114 -.0114 1 0 0
11.2000 11.2009 -.0009 0 1 0
10.0000 9.9914 .0086 1 0 1
5.2700 5.2710 -.0010 0 2 1
4.8200 4.8280 -.0080 1 0 3
4.4400 4.4336 .0064 1 1 3
3.2600 3.2602 -.0002 1 3 2
a=13.011 b=11.201 c=15.60
da= .007 db= .006 dc= .03
v=2273
20. 25-1438
{Cr,Fe,V,Ti}O
Monoklin
GRUPA 4,11
Dexp. Dcal. d(D) h k l
3.8000 3.8104 -.0104 -1 1 1
3.4700 3.4777 -.0077 -1 1 2
2.8100 2.8055 .0045 1 0 5
2.6100 2.6148 -.0048 0 2 3
2.4200 2.4235 -.0035 2 1 1
2.3700 2.3747 -.0047 -2 1 1
2.1400 2.1409 -.0009 -1 1 6
1.8900 1.8913 -.0013 1 2 6
1.8000 1.8021 -.0021 -2 0 6
1.6600 1.6596 .0004 3 0 4
1.6300 1.6297 .0003 -1 0 9
1.6000 1.6001 -.0001 3 1 4
1.4800 1.4799 .0001 0 4 2
1.4400 1.4401 -.0001 -3 2 3
a= 5.317 b= 6.03 c= 15.8290 beta= 85.7
da=.002 db=.01 dc=.0008 dbet=.1
V=504
Triklin
Dexp Dcal d(D) h k l
3.8000 3.7944 .0056 1 1 0
3.4700 3.4696 .0004 -1 0 1
2.8100 2.8117 -.0017 -1 -2 1
2.6100 2.6065 .0035 1 3 0
2.4200 2.4195 .0005 0 4 0
2.3700 2.3696 .0004 -1 3 1
2.1400 2.1413 -.0013 1 4 0
1.8900 1.8901 -.0001 -1 3 2
1.8000 1.8003 -.0003 -2 2 0
1.6600 1.6600 -.0000 1 5 1
1.6300 1.6299 .0001 -2 -2 2
1.6000 1.6001 -.0001 2 4 0
1.4800 1.4800 .0000 0 -6 1
1.4400 1.4400 .0000 2 -3 1
A= 4.12721 DA= .00001
B= 9.7344 DB= .0002
C= 4.7723 DC= .0005
GAMMA= 86.959 DGAMMA= .001
BETA =103.858 DBETA = .003
ALPHA= 85.5257 DALPHA= .0005
V=185.1
21. 27-0826
Na3VO4
Rombik
Groupa 31,59
Dexp. Dcal. d(D) h k l
4.5200 4.5304 -.0104 3 0 0
3.9300 3.9149 .0151 3 1 0
2.7630 2.7604 .0026 2 0 1
2.3500 2.3499 .0001 1 2 1
2.2490 2.2504 -.0014 3 3 0
1.9530 1.9525 .0005 4 2 1
1.7870 1.7870 -.0000 3 4 0
1.7370 1.7372 -.0002 7 2 0
1.5900 1.5898 .0002 2 4 1
1.5010 1.5012 -.0002 1 0 2
a=13.591 b= 7.779 c= 3.021
da= .006 db= .001 dc= .001
V= 319.4
22. 27-0257
Fe4+3{VO4}4*5H2O
Rombik
Groupa 33,49,62
Dexp. Dcal. d(D) h k l
8.7900 8.7870 .0030 2 0 0
6.4500 6.4411 .0089 2 1 0
3.6900 3.6925 -.0025 2 0 1
3.6900 3.6824 .0076 3 2 0
3.2900 3.2951 -.0051 5 1 0
3.2200 3.2206 -.0006 4 2 0
3.1500 3.1515 -.0015 3 1 1
2.9900 2.9855 .0045 4 0 1
2.9300 2.9290 .0010 6 0 0
2.9100 2.9117 -.0017 2 2 1
2.7800 2.7788 .0012 3 3 0
a=17.574 b= 9.469 c= 4.069
da= .002 db= .008 dc= .003
V= 677
23. 27-0826
Na3VO4
Rombik
Groupa 31,59
Dexp. Dcal. d(D) h k l
4.5200 4.5304 -.0104 3 0 0
3.9300 3.9149 .0151 3 1 0
2.7630 2.7604 .0026 2 0 1
2.3500 2.3499 .0001 1 2 1
2.2490 2.2504 -.0014 3 3 0
1.9530 1.9525 .0005 4 2 1
1.7870 1.7870 -.0000 3 4 0
1.7370 1.7372 -.0002 7 2 0
1.5900 1.5898 .0002 2 4 1
1.5010 1.5012 -.0002 1 0 2
a=13.591 b= 7.779 c= 3.021
da= .006 db= .001 dc= .001
V= 319.4
24. 27-1033
K6V10O25{SO4}3
Triklin
Dexp Dcal d(D) h k l
9.8200 9.8140 .0060 1 0 0
3.5200 3.5193 .0007 -1 0 1
3.3800 3.3799 .0001 -1 -2 1
3.3200 3.3201 -.0001 3 1 0
3.2600 3.2618 -.0018 3 2 0
3.2100 3.2097 .0003 1 0 1
3.1400 3.1422 -.0022 1 -1 1
3.0500 3.0486 .0014 0 3 1
2.9390 2.9420 -.0030 -1 3 1
2.8430 2.8428 .0002 0 -4 1
2.4770 2.4780 -.0010 4 2 0
2.2200 2.2198 .0002 4 5 0
A= 10.073 DA= .001
B= 18.554 DB= .001
C= 3.6099 DC= .0006
GAMMA= 79.8644 DGAMMA= .0002
BETA = 98.579 DBETA = .004
ALPHA= 92.77 DALPHA= .02
V= 656.5
25. 27-1604
C4H20N4O19V2W4*6H2O
Triklin
Dexp Dcal d(D) h k l
9.0300 9.0319 -.0019 1 0 0
7.6700 7.6686 .0014 0 1 1
7.4600 7.4551 .0049 0 -1 1
5.7700 5.7649 .0051 1 -1 1
3.9500 3.9477 .0023 1 2 1
3.8900 3.8879 .0021 0 3 0
3.8500 3.8533 -.0033 -2 -1 1
3.7200 3.7201 -.0001 -2 0 2
3.5300 3.5301 -.0001 2 -2 1
3.5000 3.4991 .0009 -2 2 2
3.4400 3.4391 .0009 -1 -2 2
2.9900 2.9900 .0000 -1 4 0
A= 9.504 DA= .002
B= 12.043 DB= .001
C= 10.152 DC= .003
GAMMA=104.34 DGAMMA= .02
BETA =101.978 DBETA = .005
ALPHA= 85.507 DALPHA= .006
V= 1100.8
26. 27-1606
C4H20N4O19VW5*2H2O
Triklin
Dexp Dcal d(D) h k l
9.0600 9.0695 -.0095 1 0 0
7.7800 7.7848 -.0048 0 1 0
7.5400 7.5287 .0113 0 -1 1
5.7700 5.7509 .0191 1 -1 1
3.9700 3.9734 -.0034 2 1 0
3.8600 3.8592 .0008 2 -1 1
3.7600 3.7643 -.0043 0 -2 2
3.5400 3.5366 .0034 -1 2 0
3.4600 3.4586 .0014 1 -2 2
2.9900 2.9938 -.0038 0 2 1
2.9400 2.9409 -.0009 0 -1 3
2.8860 2.8863 -.0003 0 -3 1
A= 9.074 DA= .003
B= 8.752 DB= .001
C= 8.8991 DC= .0009
GAMMA= 88.46 DGAMMA= .02
BETA = 89.874 DBETA = .001
ALPHA=117.15 DALPHA= .06
V= 628.6
27. 27-1651
C4H24N12O19VW5*6H2O
Triklin
Dexp Dcal d(D) h k l
7.7500 7.7444 .0056 0 1 1
7.4800 7.4833 -.0033 1 1 0
6.8800 6.8808 -.0008 0 -1 1
6.7600 6.7598 .0002 -1 1 0
5.3000 5.3000 .0000 1 1 2
5.1400 5.1314 .0086 -1 -1 1
3.9000 3.8997 .0003 -1 0 2
3.5200 3.5201 -.0001 3 0 1
3.3400 3.3419 -.0019 0 1 3
3.2900 3.2884 .0016 1 2 3
3.1600 3.1607 -.0007 2 3 1
2.9600 2.9600 .0000 -2 0 2
A= 10.756 DA= .002
B= 10.625 DB= .002
C= 11.3051 DC= .0004
GAMMA= 80.53 DGAMMA= .02
BETA = 64.98 DBETA = .02
ALPHA= 79.94 DALPHA= .03
V=1145
28. 27-1652
C4H24N12O19VW5*H2O
Triklin
Dexp Dcal d(D) h k l
8.5100 8.5075 .0025 0 1 1
7.3100 7.3114 -.0014 -1 1 0
7.1700 7.1682 .0018 0 -1 1
5.5100 5.5103 -.0003 1 2 1
5.2500 5.2495 .0005 0 3 0
3.6300 3.6302 -.0002 2 2 1
3.5200 3.5198 .0002 2 -1 2
3.3900 3.3905 -.0005 1 -4 1
3.2900 3.2905 -.0005 0 4 2
3.1500 3.1497 .0003 0 5 0
2.9400 2.9399 .0001 -2 4 0
2.8210 2.8211 -.0001 2 -1 3
2.2180 2.2179 .0001 1 4 4
A= 8.3480 DA= .0005
B= 16.084 DB= .001
C= 9.69366 DC= .00001
GAMMA= 92.72 DGAMMA= .01
BETA = 69.611 DBETA = .006
ALPHA= 80.285 DALPHA= .007
V= 1194.5
29. 27-1769
C2H12N2Na2O19VW5*6H2O
Triklin
Dexp. Dcal. d(D) h k l
10.2000 10.1985 .0015 1 0 0
7.2100 7.2091 .0009 0 -1 0
6.6700 6.6761 -.0061 1 -1 0
5.3300 5.3243 .0057 -1 -1 0
3.6800 3.6825 -.0025 1 -2 0
3.3900 3.3998 -.0098 3 -1 0
3.3400 3.3380 .0020 2 -2 0
3.1700 3.1715 -.0015 -1 -2 0
2.8260 2.8286 -.0026 3 -2 0
2.7600 2.7596 .0004 1 -1 1
2.6590 2.6621 -.0031 -2 -2 0
2.6320 2.6332 -.0012 -1 -1 1
A= 10.503 DA= .005
B= 7.524 DB= .006
C= 2.8709 DC= .0004
GAMMA=103.85 DGAMMA= .09
BETA = 87.69 DBETA = .01
ALPHA= 99.623 DALPHA= .007
V= 217.2
30. 27-1771
C4H16N2Na2O19V2W4*6H2O
Triklin
Dexp Dcal d(D) h k l
9.8500 9.8659 -.0159 1 0 0
7.5400 7.5275 .0125 0 1 0
7.3300 7.3363 -.0063 0 1 1
6.7600 6.7599 .0001 1 1 0
6.5300 6.5418 -.0118 1 1 1
6.4300 6.4493 -.0193 1 0 1
4.0400 4.0438 -.0038 -1 1 2
3.8100 3.8127 -.0027 1 2 0
3.6900 3.6855 .0045 1 2 2
3.3800 3.3799 .0001 2 2 0
3.2800 3.2802 -.0002 -1 2 0
3.2500 3.2516 -.0016 3 1 1
A= 10.152 DA= .005
B= 8.458 DB= .008
C= 9.527 DC= .006
GAMMA= 76.44 DGAMMA= .04
BETA = 85.73 DBETA = .03
ALPHA= 65.96 DALPHA= .04
V=726.0
31. 27-1858
C24H20OP2S4V
Triklin
Dexp Dcal d(D) h k l
10.0000 10.0326 -.0326 1 0 0
8.7200 8.7211 -.0011 0 1 0
8.3500 8.3365 .0135 1 0 1
7.9000 7.9399 -.0399 0 1 1
7.2800 7.2977 -.0177 1 1 1
6.6200 6.6104 .0096 0 -1 1
5.9500 5.9410 .0090 -1 1 0
5.6900 5.6771 .0129 0 1 2
5.1000 5.1045 -.0045 -1 0 2
4.8600 4.8570 .0030 2 1 0
4.3600 4.3605 -.0005 0 2 0
4.0600 4.0606 -.0006 1 0 3
3.7900 3.7893 .0007 -2 1 1
A= 10.45 DA= .01
B= 9.20 DB= .01
C= 13.098 DC= .007
GAMMA= 75.05 DGAMMA= .08
BETA = 80.53 DBETA = .08
ALPHA= 76.9 DALPHA= .1
V= 1178