1. 20-0189
CdV2O6
Triklin
Dexp Dcal d(D) h k l
6.4600 6.4387 .0213 0 0 1
4.4600 4.4773 -.0173 0 -2 1
4.3400 4.3436 -.0036 1 0 0
3.3000 3.3037 -.0037 1 2 0
3.2300 3.2289 .0011 -1 -1 2
3.1700 3.1673 .0027 1 0 1
3.1000 3.1015 -.0015 1 -1 1
2.7800 2.7773 .0027 1 -2 1
2.7300 2.7296 .0004 -1 1 2
2.4900 2.4901 -.0001 0 -4 1
2.3400 2.3391 .0009 -1 3 1
2.3000 2.3003 -.0003 -2 -1 1
A= 4.62274 DA= .00004
B= 10.124 DB= .001
C= 7.100 DC= .002
GAMMA= 81.979 DGAMMA= .004
BETA =109.87 DBETA = .02
ALPHA=107.14 DALPHA= .02
V= 298.4
2. 20-0190
Cd2V2O7
Triklin
Dexp Dcal d(D) h k l
5.4500 5.4444 .0056 0 1 1
4.8400 4.8400 -.0000 -1 0 1
4.4600 4.4587 .0013 0 -1 1
3.4400 3.4382 .0018 1 0 1
3.3400 3.3440 -.0040 0 -2 1
3.2900 3.2874 .0026 0 3 0
3.1700 3.1714 -.0014 0 3 1
2.7500 2.7495 .0005 -2 -1 1
2.7300 2.7301 -.0001 2 1 0
2.5900 2.5896 .0004 0 -3 1
2.5500 2.5499 .0001 0 -1 2
2.4900 2.4901 -.0001 2 2 0
A= 5.93121 DA= .00416
B= 10.13553 DB= .00564
C= 6.10127 DC= .00070
GAMMA= 91.50013 DGAMMA= .09772
BETA =109.06740 DBETA = .02579
ALPHA= 76.99567 DALPHA= .03069
V= 337.1
3. 20-0191
Cd4V2O9
Triklin
Dexp Dcal d(D) h k l
4.9600 4.9514 .0086 -2 1 0
4.4800 4.4810 -.0010 -1 2 0
3.7400 3.7485 -.0085 -2 2 0
3.4400 3.4456 -.0056 2 2 0
3.1000 3.0973 .0027 -1 3 0
3.0000 3.0000 .0000 2 0 1
2.8700 2.8700 .0000 -1 -1 1
2.8400 2.8401 -.0001 -2 3 0
2.7600 2.7591 .0009 4 0 0
2.7100 2.7100 .0000 -2 0 1
2.6400 2.6392 .0008 2 3 0
2.5100 2.5100 .0000 3 1 1
A= 11.145 DA= .00112
B= 9.486 DB= .005
C= 3.3437 DC= .0006
GAMMA= 94.58 DGAMMA= .05
BETA = 83.641 DBETA = .003
ALPHA= 87.59 DALPHA= .02
V= 349.6
4. 20-0192
Cd4V2O9
Triklin
Dexp Dcal d(D) h k l
8.0200 8.0365 -.0165 0 1 1
7.5700 7.5571 .0129 0 -1 1
6.9400 6.9563 -.0163 1 1 0
6.7400 6.7401 -.0001 -1 0 1
6.1900 6.1911 -.0011 1 0 1
5.9600 5.9702 -.0102 1 -1 1
5.6400 5.6389 .0011 -1 -1 1
5.4700 5.4636 .0064 1 1 1
5.0400 5.0381 .0019 1 -2 1
4.8100 4.8098 .0002 -1 3 0
4.5200 4.5190 .0010 2 0 0
4.4600 4.4605 -.0005 -1 -2 1
A= 9.3777 DA= .0003
B= 15.135 DB= .003
C= 9.2750 DC= .0002
GAMMA=104.712 DGAMMA= .008
BETA = 96.037 DBETA = .004
ALPHA= 84.717 DALPHA= .001
V= 1263.3
5. 20-0300
Cs2VCl5*H2O
Triklin
Dexp Dcal d(D) h k l
5.9500 5.9493 .0007 -1 2 0
5.1700 5.1699 .0001 -2 1 0
4.5700 4.5712 -.0012 0 3 0
4.2900 4.2975 -.0075 -1 3 0
4.1700 4.1693 .0007 2 2 0
3.9600 3.9597 .0003 1 2 1
3.7300 3.7324 -.0024 -2 2 1
3.6100 3.6081 .0019 -1 3 1
3.4600 3.4593 .0007 0 -3 1
3.2500 3.2514 -.0014 2 2 1
2.9250 2.9241 .0009 -3 3 0
2.8170 2.8165 .0005 1 4 1
A= 11.0480 DA= .0002
B= 13.760 DB= .001
C= 5.7107 DC= .0007
GAMMA= 93.453 DGAMMA= .005
BETA = 97.854 DBETA = .005
ALPHA= 86.34148 DALPHA= .00004
V=857.2
6. 20-0301
Cs2VCl5*4H2O
Triklin
Dexp Dcal d(D) h k l
6.7000 6.6929 .0071 0 1 1
6.1900 6.1853 .0047 0 -1 1
5.2200 5.2195 .0005 -1 1 1
4.2600 4.2548 .0052 0 2 0
4.2300 4.2352 -.0052 -1 0 2
4.1600 4.1589 .0011 -1 1 2
3.5100 3.5071 .0029 -1 -1 2
3.3800 3.3807 -.0007 -1 2 2
3.2900 3.2893 .0007 1 -2 1
3.0900 3.0926 -.0026 0 -2 2
2.9710 2.9705 .0005 0 -1 3
2.9290 2.9296 -.0006 1 2 1
A= 6.024 DA= .003
B= 8.747 DB= .002
C= 10.154 DC= .001
GAMMA=102.60 DGAMMA= .01
BETA =104.60 DBETA = .01
ALPHA= 82.537 DALPHA= .002
V=503.7
7. 20-318
Cr{V2O7}3*xH2O
Rombik
Groupa 27
Dexp. Dcal. d(D) h k l
7.0800 7.0677 .0123 0 1 0
6.4200 6.3771 .0429 1 1 0
3.8600 3.8580 .0020 0 0 2
3.6900 3.6979 -.0079 4 0 0
3.5800 3.5817 -.0017 3 1 1
3.3000 3.3009 -.0009 1 1 2
3.1900 3.1886 .0014 2 2 0
3.0800 3.0789 .0011 2 1 2
3.0200 3.0159 .0041 4 1 1
2.9600 2.9583 .0017 5 0 0
2.8700 2.8723 -.0023 3 2 0
2.7900 2.7914 -.0014 3 1 2
2.1300 2.1301 -.0001 4 2 2
a=14.792 b= 7.068 c= 7.7159
da= .008 db= .005 dc= .0004
V= 807
8. 20-0320
{Cr{H2O}6{VO3}3*2H2O
Triklin
Dexp Dcal d(D) h k l
9.4600 9.4848 -.0248 1 0 0
8.3200 8.3128 .0072 0 1 1
7.2300 7.1935 .0365 0 -1 1
7.0800 7.0650 .0150 0 0 2
6.8600 6.8614 -.0014 -1 1 1
5.9700 5.9603 .0097 1 0 2
4.7100 4.7100 -.0000 0 0 3
4.6300 4.6388 -.0088 2 0 1
4.1400 4.1346 .0054 2 0 2
4.1000 4.1011 -.0011 -1 1 3
4.0600 4.0591 .0009 -1 0 3
4.0100 4.0113 -.0013 1 1 3
A= 9.827 DA= .005
B= 9.573 DB= .004
C= 14.337 DC= .006
GAMMA=104.06 DGAMMA= .01
BETA = 86.37 DBETA = .03
ALPHA= 82.141 DALPHA= .007
V= 1289.5
9. 20-0350
{Cu{NH3}4}{VO3}2*2H2O
Triklin
Dexp Dcal d(D) h k l
7.0500 7.0811 -.0311 0 1 0
5.8200 5.8223 -.0023 0 -1 2
5.2700 5.2710 -.0010 1 0 0
4.7500 4.7573 -.0073 0 -1 3
4.5100 4.5086 .0014 1 0 2
4.3400 4.3443 -.0043 1 1 0
4.1500 4.1483 .0017 1 1 1
4.0700 4.0703 -.0003 1 -1 1
4.0000 3.9984 .0016 -1 -1 2
3.9100 3.9080 .0020 0 -1 4
3.5500 3.5484 .0016 0 -2 1
3.4800 3.4802 -.0002 0 0 5
A= 5.2791 DA= .0001
B= 7.137 DB= .006
C= 17.5124 DC= .0003
GAMMA= 86.83 DGAMMA= .02
BETA = 90.35 DBETA = .06
ALPHA= 96.48 DALPHA= .05
V= 654.6
10. 20-0374
Cu2V2O7
Triklin
Dexp Dcal d(D) h k l
7.6900 7.6962 -.0062 1 0 0
5.3200 5.3207 -.0007 -1 1 0
4.9000 4.9036 -.0036 -1 1 1
3.5200 3.5193 .0007 -1 1 2
3.2400 3.2408 -.0008 0 2 0
3.1800 3.1792 .0008 -1 2 1
2.8700 2.8694 .0006 1 -1 2
2.8500 2.8507 -.0007 -2 1 2
2.6200 2.6197 .0003 0 1 3
2.4700 2.4698 .0002 -3 0 1
2.4300 2.4302 -.0002 1 0 3
2.2000 2.2000 .0000 -2 0 3
A= 7.7888 DA= .0009
B= 6.71728 DB= .00001
C= 8.0172 DC= .0002
GAMMA= 98.48 DGAMMA= .02
BETA = 94.392 DBETA = .007
ALPHA= 76.829 DALPHA= .002
V=403
11. 20-0375
CuV2O6*2H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.3400 5.3542 -.0142 2 0 0
4.2100 4.2064 .0036 2 0 1
4.1000 4.0856 .0144 -1 0 2
3.6800 3.6748 .0052 1 0 2
3.5900 3.5834 .0066 2 1 1
3.2600 3.2588 .0012 1 2 0
2.1600 2.1585 .0015 -1 2 3
3.1100 3.1060 .0040 3 0 1
3.0800 3.0832 -.0032 -1 2 1
3.0500 3.0531 -.0031 2 0 2
2.6300 2.6284 .0016 -2 0 3
2.4900 2.4898 .0002 -4 1 1
a=10.84 b=6.84 c=8.39 beta=99.02
da=.01 db=.01 dc= .01 dbeta=.03
V= 614.7
12. 20-0950
K2VCl5*H2O
Triklin
Dexp Dcal d(D) h k l
5.6600 5.6662 -.0062 0 1 1
5.5300 5.5299 .0001 0 -1 1
5.2200 5.2170 .0030 -1 1 1
4.8600 4.8568 .0032 1 -1 1
3.0300 3.0304 -.0004 -1 0 3
2.9780 2.9762 .0018 -1 2 2
2.9340 2.9339 .0001 0 -1 3
2.8350 2.8365 -.0015 -2 0 2
2.7730 2.7739 -.0009 1 -1 3
2.6670 2.6661 .0009 2 0 2
2.5740 2.5748 -.0008 1 2 1
2.5220 2.5218 .0002 2 1 1
A= 7.058 DA= .001
B= 7.2366 DB= .0004
C= 9.918 DC= .002
GAMMA=110.17 DGAMMA= .03
BETA = 94.64 DBETA = .03
ALPHA= 87.01 DALPHA= .01
V= 473.8
13. 20-0953
K0.38Ag0.62VO3
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
7.2400 7.2443 -.0043 1 0 0
5.2000 5.1996 .0004 1 1 0
5.0000 5.0015 -.0015 1 1 1
4.8000 4.7981 .0019 -1 0 1
3.2700 3.2656 .0044 1 2 1
2.8500 2.8494 .0006 0 0 3
2.8100 2.8119 -.0019 0 2 2
2.7200 2.7196 .0004 2 0 3
2.6700 2.6703 -.0003 2 2 1
2.6000 2.5998 .0002 2 2 0
2.5000 2.5007 -.0007 2 2 2
2.3900 2.3899 .0001 0 3 1
a= 7.6776 b= 7.4675 c=9.06 beta=70.65
da=.0005 db=.0001 dc=.012 dbeta=.04
V= 490.1
Triklin
Dexp Dcal d(D) h k l
7.2400 7.2397 .0003 0 1 1
5.2000 5.2005 -.0005 -1 -1 1
5.0000 4.9998 .0002 0 -1 1
4.8000 4.8023 -.0023 1 1 1
3.2700 3.2706 -.0006 0 -1 2
2.8500 2.8516 -.0016 -2 2 3
2.8100 2.8092 .0008 -3 1 1
2.7200 2.7195 .0005 1 3 1
2.6700 2.6702 -.0002 1 -1 2
2.6000 2.6002 -.0002 -2 -2 2
2.5000 2.4999 .0001 0 -2 2
2.3900 2.3898 .0002 -3 2 1
A=9.212 DA= .007
B= 8.6758 DB= .0001
C= 9.981 DC= .004
GAMMA= 91.31 DGAMMA= .04
BETA =116.54 DBETA = .05
ALPHA= 70.9159 DALPHA= .0008
V= 667.2
14. 20-0954
K2VOCl4
Triklin
Dexp Dcal d(D) h k l
7.9400 7.9330 .0070 -1 1 0
7.3800 7.3788 .0012 0 0 1
4.1700 4.1700 -.0000 3 0 0
4.0200 4.0175 .0025 0 2 0
3.4600 3.4600 .0000 -3 2 0
3.1400 3.1400 -.0000 0 -2 1
2.6780 2.6784 -.0004 0 3 0
2.5020 2.5020 .0000 5 0 0
2.2050 2.2050 -.0000 -5 0 1
2.1330 2.1330 .0000 -4 0 2
1.9890 1.9890 .0000 -5 1 2
1.9550 1.9550 -.0000 -6 3 0
A= 13.32861 DA= .00004
B= 8.71638 DB= .00001
C= 7.89298 DC= .00002
GAMMA=103.9561 DGAMMA= .0009
BETA = 79.815 DBETA = .001
ALPHA= 75.1685 DALPHA= .0009
V=832.1
15. 20-1013
RbVCl4*6H2O
Triklin
Dexp Dcal d(D) h k l
5.9100 5.9102 -.0002 0 1 0
5.1000 5.0980 .0020 -1 1 0
4.6600 4.6608 -.0008 0 -1 2
4.6000 4.5955 .0045 -1 1 1
4.3200 4.3144 .0056 -1 -1 2
4.1800 4.1816 -.0016 1 -1 2
4.0900 4.0879 .0021 0 1 2
3.8600 3.8585 .0015 -2 1 0
3.2300 3.2314 -.0014 -2 1 2
3.1000 3.1002 -.0002 -1 0 4
2.9860 2.9860 -.0000 3 1 0
2.8670 2.8677 -.0007 -1 -2 1
A= 10.31333 DA= .00001
B= 5.96254 DB= .00000
C= 12.9522 DC= .0001
GAMMA= 88.9295 DGAMMA= .0001
BETA = 92.603 DBETA = .001
ALPHA= 97.5655 DALPHA= .0003
V=788.4
16. 20-1014
Rb2VCl5*H2O
Triklin
Dexp Dcal d(D) h k l
5.7000 5.7018 -.0018 -1 1 1
5.1300 5.1283 .0017 1 -1 1
4.9300 4.9298 .0002 0 -1 1
4.4000 4.4019 -.0019 -2 2 0
3.8800 3.8805 -.0005 -1 -1 1
3.4600 3.4605 -.0005 0 -2 1
3.4100 3.4108 -.0008 0 0 2
3.3000 3.2979 .0021 1 1 2
3.0700 3.0697 .0003 1 -1 2
3.0200 3.0204 -.0004 -3 1 1
2.8520 2.8509 .0011 -2 2 2
2.7970 2.7977 -.0007 2 2 0
A= 10.5085 DA= .0004
B= 10.640 DB= .001
C= 7.0832 DC= .0008
GAMMA=113.795 DGAMMA= .007
BETA = 87.47211 DBETA = .00005
ALPHA= 76.991 DALPHA= .005
V=697.8
17. 20-1015
Rb2VOCl4
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
6.3800 6.3772 .0028 1 1 0
5.1700 5.1702 -.0002 1 1 1
3.6800 3.6812 -.0012 -2 0 2
3.2700 3.2699 .0001 0 0 3
2.7700 2.7713 -.0013 -2 2 2
2.5800 2.5799 .0001 1 3 1
2.3560 2.3561 -.0001 -3 1 3
2.1110 2.1110 .0000 -3 3 1
2.0200 2.0195 .0005 -2 2 4
1.9600 1.9597 .0003 -5 0 1
1.8120 1.8121 -.0001 4 1 3
1.7980 1.7982 -.0002 -4 1 4
a=9.833 b= 8.420 c= 9.877 beta= 96.67
da=.005 db=.003 dc=.002 dbeta=.03
V= 812.2
Triklin
Dexp Dcal d(D) h k l
6.3800 6.3853 -.0053 1 0 0
5.1700 5.1693 .0007 -1 0 1
3.6800 3.6788 .0012 -1 -2 1
3.2700 3.2710 -.0010 0 0 2
2.7700 2.7685 .0015 0 2 1
2.5800 2.5812 -.0012 -1 -3 1
2.3560 2.3554 .0006 -1 -2 3
2.1110 2.1111 -.0001 -3 -1 2
2.0200 2.0204 -.0004 -1 2 2
1.9600 1.9594 .0006 1 3 1
1.8120 1.8117 .0003 2 -3 1
1.7980 1.7984 -.0004 0 4 0
A= 6.7117 DA= .0001
B= 7.879 DB= .001
C= 7.2840 DC= .0005
GAMMA= 77.158 DGAMMA= .003
BETA =106.46 DBETA = .02
ALPHA=113.02 DALPHA= .01
V= 337.29
18. 20-1168
NaVO3
Triklin
Dexp Dcal d(D) h k l
6.8000 6.7967 .0033 -1 1 0
3.5600 3.5600 .0000 0 3 0
3.4600 3.4605 -.0005 0 0 1
3.4200 3.4205 -.0005 3 3 0
3.2400 3.2385 .0015 4 2 0
3.1800 3.1796 .0004 1 1 1
3.1300 3.1297 .0003 -2 -1 1
3.0800 3.0798 .0002 0 -2 1
3.0300 3.0306 -.0006 4 0 0
2.9800 2.9802 -.0002 2 1 1
2.9500 2.9504 -.0004 4 3 0
2.7500 2.7502 -.0002 -3 -2 1
A= 13.194 DA= .004
B= 11.710 DB= .005
C= 3.48875 DC= .00002
GAMMA= 66.77 DGAMMA= .01
BETA = 92.133 DBETA = .001
ALPHA= 97.256 DALPHA= .002
V=491.4
19. 20-1169
Na3VO4
Rombik
Groupa 27
Dexp. Dcal. d(D) h k l
4.4300 4.4361 -.0061 2 1 1
4.3000 4.3019 -.0019 2 2 0
4.1300 4.1203 .0097 5 0 0
3.9000 3.8979 .0021 3 2 0
3.7800 3.7781 .0019 5 1 0
3.5600 3.5558 .0042 4 1 1
3.4900 3.4856 .0044 4 2 0
2.7300 2.7271 .0029 1 1 2
2.6900 2.6912 -.0012 4 3 0
2.5100 2.5106 -.0006 4 0 2
2.4400 2.4403 -.0003 1 2 2
2.2800 2.2811 -.0011 8 1 1
2.1250 2.1256 -.0006 0 3 2
1.8940 1.8938 .0002 0 5 0
a=20.60 b= 9.469 c= 5.7507
da= .03 db= .003 dc= .0007
V=1122
Monoklin
Grupa 4,11
Dexp Dcal d(D) h k l
4.4300 4.4357 -.0057 1 0 2
4.3000 4.2988 .0012 3 0 0
4.1300 4.1278 .0022 2 1 0
3.9000 3.8997 .0003 -2 0 3
3.7800 3.7873 -.0073 -2 1 2
3.5600 3.5595 .0005 -3 0 3
3.4900 3.4907 -.0007 -4 0 1
2.7300 2.7297 .0003 0 0 4
2.6900 2.6865 .0035 0 2 0
2.5100 2.5111 -.0011 1 2 1
2.4400 2.4400 -.0000 2 1 3
2.2800 2.2796 .0004 -3 2 2
2.1250 2.1248 .0002 5 1 1
1.8940 1.8936 .0004 -4 2 4
a= 14.05 b=5.373 c=11.89 beta=113.35
da=.01 db=.02 dc=.01 dbeta=.09
V= 824
Triklin
Dexp Dcal d(D) h k l
4.4300 4.4289 .0011 1 1 1
4.3000 4.3005 -.0005 0 -1 1
4.1300 4.1318 -.0018 -1 -1 1
3.9000 3.8996 .0004 2 0 0
3.7800 3.7883 -.0083 -1 1 1
3.5600 3.5586 .0014 -2 0 1
3.4900 3.4879 .0021 1 0 2
2.7300 2.7307 -.0007 2 0 2
2.6900 2.6884 .0016 0 2 1
2.5100 2.5100 -.0000 0 -2 1
2.4400 2.4394 .0006 -2 1 2
2.2800 2.2791 .0009 -1 -1 3
2.1250 2.1245 .0005 1 -1 3
1.8940 1.8942 -.0002 -2 2 2
A= 8.011 DA= .003
B= 5.669 DB= .003
C= 8.008 DC= .001
GAMMA= 77.01 DGAMMA= .02
BETA = 90.88 DBETA = .01
ALPHA= 83.99 DALPHA= .01
V= 352.1
20. 20-1171
"ýòà" - Na1.33V2O5
Triklin
Dexp Dcal d(D) h k l
9.6000 9.5917 .0083 1 0 0
8.0500 8.0461 .0039 1 1 1
4.9800 4.9825 -.0025 1 -1 1
4.8300 4.8252 .0048 2 0 1
4.6900 4.6956 -.0056 2 1 0
4.5700 4.5678 .0022 1 1 2
4.4600 4.4540 .0060 -1 -1 1
4.1600 4.1607 -.0007 0 1 2
4.0700 4.0722 -.0022 1 0 2
3.7700 3.7700 .0000 0 3 1
3.4800 3.4802 -.0002 -1 -2 1
3.2500 3.2502 -.0002 -1 0 2
A= 10.741 DA= .003
B= 12.058 DB= .001
C= 9.1677 DC= .0009
GAMMA= 70.45 DGAMMA= .01
BETA = 65.19 DBETA =.01
ALPHA= 63.12 DALPHA= .01
V=946.2
21. 20-1172
Na3VO4*2.5H2O
Triklin
Dexp Dcal d(D) h k l
5.2100 5.2155 -.0055 0 1 1
4.3300 4.3348 -.0048 1 0 1
4.2300 4.2340 -.0040 0 -1 1
3.4900 3.4895 .0005 1 -1 1
3.3900 3.3873 .0027 1 2 1
3.3700 3.3714 -.0014 -1 1 1
3.0000 2.9993 .0007 0 -2 1
2.7900 2.7902 -.0002 -1 2 1
2.6300 2.6279 .0021 2 0 1
2.5800 2.5814 -.0014 -1 -2 1
2.4100 2.4102 -.0002 1 -1 2
2.2250 2.2251 -.0001 1 3 2
2.1780 2.1763 .0017 -2 -1 1
1.7810 1.7816 -.0006 3 1 0
A= 5.521 DA= .001
B= 8.36 DB= .01
C= 5.962 DC= .004
GAMMA= 82.17 DGAMMA= .03
BETA = 77.58 DBETA = .02
ALPHA= 76.08 DALPHA= .03
V=259.8
22. 20-1173
Na6V10O28*4H2O
Triklin
Dexp Dcal d(D) h k l
9.0600 9.0441 .0159 1 0 0
8.0000 7.9810 .0190 0 1 1
7.4300 7.4261 .0039 1 0 1
6.2100 6.2124 -.0024 1 1 0
4.7900 4.7842 .0058 0 1 2
3.9500 3.9509 -.0009 -1 1 2
3.8600 3.8594 .0006 0 -2 1
3.7400 3.7387 .0013 -2 0 1
3.6200 3.6204 -.0004 2 1 2
3.1100 3.1103 -.0003 0 0 3
3.0300 3.0304 -.0004 -2 1 2
2.9700 2.9702 -.0002 1 3 2
A= 9.3268 DA= .0003
B= 10.140 DB= .001
C= 9.973 DC= .001
GAMMA= 93.88 DGAMMA= .03
BETA = 78.02 DBETA = .02
ALPHA= 74.29 DALPHA= .01
V-880.8
23. 20-1174
Na3VO4*3.5H2O
Triklin
Dexp Dcal d(D) h k l
5.8900 5.8746 .0154 0 1 1
5.5000 5.5051 -.0051 0 -1 1
4.6200 4.6160 .0040 1 0 0
4.5300 4.5361 -.0061 -1 1 0
4.3700 4.3754 -.0054 0 -2 1
4.0400 4.0367 .0033 1 0 1
3.5300 3.5309 -.0009 1 -2 1
3.4800 3.4786 .0014 -1 1 1
3.3600 3.3621 -.0021 1 2 1
3.3000 3.2990 .0010 0 4 0
3.0600 3.0591 .0009 1 -3 1
2.9300 2.9309 -.0009 -1 3 1
A= 4.704 DA= .004
B= 13.327 DB= .003
C= 6.387 DC= .006
GAMMA= 96.48 DGAMMA= .05
BETA = 81.48 DBETA = .04
ALPHA= 86.26 DALPHA= .07
V=391
24. 20-1175
Na4V2O7*18H2O
Triklin
Dexp Dcal d(D) h k l
7.1400 7.1552 -.0152 -1 2 0
6.8200 6.8278 -.0078 0 1 1
6.5400 6.5445 -.0045 0 -1 1
6.1000 6.1070 -.0070 -1 1 1
5.7800 5.7725 .0075 0 -2 1
5.5700 5.5747 -.0047 -1 2 1
5.1900 5.1876 .0024 1 0 1
4.9600 4.9621 -.0021 1 -1 1
4.5700 4.5702 -.0002 1 -2 1
4.4900 4.4879 .0021 1 3 1
4.2100 4.2113 -.0013 2 3 0
4.1000 4.0973 .0027 -2 2 1
A= 9.876 DA= .002
B= 23.01 DB= .02
C= 7.145 DC= .002
GAMMA= 87.00 DGAMMA= .01
BETA =101.356 DBETA = .006
ALPHA= 86.336 DALPHA= .002
V=880.8
25. 20-1176
Na6V10O28*18H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
10.8000 10.8821 -.0821 0 1 0
10.0000 10.0102 -.0102 1 0 1
8.8400 8.8619 -.0219 1 1 0
8.0400 8.0543 -.0143 -1 0 1
7.3700 7.3673 .0027 1 1 1
5.9000 5.9159 -.0159 2 1 1
3.6300 3.6274 .0026 0 3 0
3.4500 3.4479 .0021 0 1 3
3.3600 3.3607 -.0007 -3 0 2
2.8600 2.8593 .0007 -3 2 2
2.4400 2.4395 .0005 -5 0 2
2.2600 2.2596 .0004 5 1 4
a= 15.68 b= 10.882 c= 11.20 beta=76.9
da=.01 db=.002 dc=.03 dbeta=.3
V= 1860
26.20-1177
Na6V10O28*26H2O
Monoklin
GRUPA 3
Dexp. Dcal. d(D) h k l
9.0600 9.0312 .0288 0 0 1
6.5000 6.4835 .0165 0 1 1
5.2100 5.2189 -.0089 1 1 1
4.1100 4.1076 .0024 2 1 0
3.2400 3.2418 -.0018 0 2 2
3.1500 3.1506 -.0006 2 0 2
3.0400 3.0416 -.0016 2 2 1
2.9400 2.9400 .0000 1 3 0
2.7300 2.7300 .0000 3 1 1
2.0100 2.0084 .0016 4 0 2
a=9.161 b=9.313 c= 9.04 beta= 92.34
da=.009 db=.0023 dc= .01 dbet= .09
V=769
27. 20-1178
Na2V6O15{NO3}2
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.5000 5.5018 -.0018 0 1 2
4.2000 4.1996 .0004 2 1 0
3.9800 3.9805 -.0005 -1 1 3
3.3400 3.3400 -.0000 -2 1 3
2.9900 2.9891 .0009 3 1 0
2.8200 2.8202 -.0002 -3 0 3
2.7400 2.7398 .0002 0 3 2
2.5800 2.5796 .0004 1 0 5
2.5100 2.5102 -.0002 -2 2 4
2.2900 2.2902 -.0002 4 0 1
2.1600 2.1600 -.0000 -1 4 1
2.1000 2.0998 .0002 4 2 0
a=9.619 b=8.94 c= 14.12 beta=98.41
da=.001 db=.003 dc=.002 dbeta=.02
V= 1200
Triklin
Dexp Dcal d(D) h k l
5.5000 5.4990 .0010 1 1 1
4.2000 4.1988 .0012 2 1 1
3.9800 3.9822 -.0022 1 -1 1
3.3400 3.3395 .0005 2 1 2
2.9900 2.9921 -.0021 2 2 0
2.8200 2.8258 -.0058 0 -2 1
2.7400 2.7395 .0005 3 1 2
2.5800 2.5763 .0037 1 -2 1
2.5100 2.5099 .0001 0 1 3
2.2900 2.2902 -.0002 1 2 3
2.1600 2.1603 -.0003 2 3 0
2.1000 2.0994 .0006 4 2 2
A= 9.40 DA= .01
B= 6.804 DB= .004
C= 8.032 DC= .008
GAMMA= 72.65 DGAMMA= .06
BETA = 75.5 DBETA = .1
ALPHA= 78.08 DALPHA= .07
V= 470.1
28. 20-1283
ThV2O7
Triklin
Dexp Dcal d(D) h k l
6.6000 6.6014 -.0014 1 1 0
5.6600 5.6622 -.0022 0 -1 1
5.0800 5.0790 .0010 -1 -1 1
4.8400 4.8386 .0014 -3 1 1
4.1400 4.1386 .0014 -2 -1 1
3.7800 3.7832 -.0032 0 -2 1
3.5800 3.5813 -.0013 1 1 2
3.4200 3.4195 .0005 -3 0 2
3.3500 3.3487 .0013 1 -1 2
3.1100 3.1086 .0014 2 2 1
3.0300 3.0291 .0009 -2 -2 1
2.9400 2.9409 -.0009 -5 2 1
A= 14.8121 DA= .0002
B= 10.95866 DB= .00004
C= 9.142 DC= .001
GAMMA=116.45 DGAMMA= .01
BETA =110.75 DBETA = .01
ALPHA= 69.5137 DALPHA= .0005
V= 1209
29. 20-1284
Th{VO3}4
rombik.
Grupa 19
Dexp. Dcal. d(D) h k l
7.3200 7.3209 -.0009 2 0 0
5.5700 5.5790 -.0090 0 0 3
3.7700 3.7671 .0029 1 1 3
3.6700 3.6734 -.0034 3 0 3
3.5500 3.5527 -.0027 3 1 1
3.1800 3.1766 .0034 3 0 4
2.0200 2.0198 .0002 5 0 6
2.7600 2.7605 -.0005 3 0 5
2.6570 2.6577 -.0007 2 1 5
2.6060 2.6067 -.0007 2 0 6
2.3600 2.3598 .0002 1 0 7
2.3220 2.3219 .0001 2 2 3
a=14.64 b= 5.449 c=16.737
da= .01 db= .001 dc= .003
V=1335
Triklin
Dexp Dcal d(D) h k l
7.3200 7.3194 .0006 1 0 0
5.5700 5.5715 -.0015 0 1 0
3.7700 3.7710 -.0010 0 -1 2
3.6700 3.6721 -.0021 1 0 2
3.5500 3.5481 .0019 -2 0 2
3.1800 3.1801 -.0001 2 1 1
2.0200 2.0194 .0006 -1 2 3
2.7600 2.7596 .0004 1 2 1
2.6570 2.6568 .0002 -2 1 0
2.6060 2.6076 -.0016 2 0 2
2.3600 2.3611 -.0011 -3 -2 2
2.3220 2.3212 .0008 0 -1 4
A= 8.3227 DA= .0006
B= 6.013 DB= .003
C= 10.8248 DC= .0003
GAMMA= 67.919 DGAMMA= .001
BETA =109.86 DBETA = .01
ALPHA= 97.68 DALPHA= .01
V= 472.1
30. 20-1364
VUO5.5
Triklin
Dexp Dcal d(D) h k l
5.6100 5.6015 .0085 -2 0 1
4.9000 4.9060 -.0060 -1 1 1
4.5700 4.5716 -.0016 -1 -1 1
4.1700 4.1691 .0009 0 1 2
3.9400 3.9369 .0031 -2 1 1
3.5800 3.5832 -.0032 3 1 0
3.4100 3.4101 -.0001 -1 -1 2
3.3000 3.2981 .0019 3 1 1
3.1600 3.1607 -.0007 0 0 3
3.0800 3.0798 .0002 -2 0 3
2.9300 2.9295 .0005 -3 -1 2
2.8000 2.8008 -.0008 -4 0 2
A= 12.271 DA= .002
B= 5.971 DB= .001
C= 9.919 DC= .002
GAMMA= 81.78 DGAMMA= .02
BETA =100.43 DBETA = .02
ALPHA= 78.29 DALPHA= .01
V-688.2
31. 20-1365
V2UO8
Rombik
Groupa 26,28,51
Dexp. Dcal. d(D) h k l
7.7400 7.7924 -.0524 1 0 2
5.9700 5.9853 -.0153 2 0 2
5.0000 5.0050 -.0050 0 1 0
4.6200 4.6176 .0024 1 1 1
3.9400 3.9465 -.0065 4 0 1
3.8400 3.8395 .0005 2 1 2
3.6700 3.6697 .0003 3 1 0
3.3400 3.3424 -.0024 4 0 3
3.1200 3.1200 .0000 3 1 3
2.9700 2.9693 .0007 3 0 5
2.6700 2.6714 -.0014 4 0 5
2.6200 2.6172 .0028 5 0 4
a=16.189760 b= 5.004951 c=17.779770
da= .006344 db= .000863 dc= .019296
V=1440
Triklin
Dexp Dcal d(D) h k l
7.7400 7.7389 .0011 1 0 0
5.9700 5.9625 .0075 -1 1 1
5.0000 4.9940 .0060 1 -1 1
4.6200 4.6210 -.0010 0 0 2
3.9400 3.9395 .0005 -1 2 1
3.8400 3.8388 .0012 2 0 1
3.6700 3.6720 -.0020 -1 0 2
3.3400 3.3404 -.0004 -2 2 0
3.1200 3.1197 .0003 -2 1 2
2.9700 2.9710 -.0010 2 -2 1
2.6700 2.6703 -.0003 2 0 3
2.6200 2.6196 .0004 1 -1 3
A= 8.485 DA= .003
B= 7.9741 DB= .0002
C= 9.922 DC= .001
GAMMA=111.73 DGAMMA= .08
BETA = 87.10 DBETA = .04
ALPHA= 71.582 DALPHA= .003
V= 580.9
32. 20-1371
{NH4}2VOCl4
Triklin
Dexp Dcal d(D) h k l
7.5100 7.5096 .0004 -1 1 0
3.7800 3.7800 -.0000 0 1 1
3.5400 3.5366 .0034 0 -1 1
3.1900 3.1899 .0001 0 2 1
2.7230 2.7226 .0004 -3 2 0
2.5410 2.5412 -.0002 2 -3 1
2.3270 2.3272 -.0002 -2 3 1
2.1710 2.1709 .0001 -1 4 1
2.0280 2.0291 -.0011 1 -5 0
1.9060 1.9052 .0008 -3 5 0
1.8900 1.8900 -.0000 0 2 2
1.8190 1.8189 .0001 -1 0 2
A= 8.482 DA= .001
B= 10.242 DB= .001
C= 4.0629 DC= .0009
GAMMA=111.38 DGAMMA= .04
BETA = 78.00 DBETA = .01
ALPHA= 89.46 DALPHA= .01
V= 320.1
33. 20-1374
VCl3*6H2O
Triklin
Dexp Dcal d(D) h k l
6.3900 6.3893 .0007 1 0 0
5.9100 5.9062 .0038 0 1 1
5.6800 5.6814 -.0014 -1 0 1
4.6900 4.6885 .0015 1 1 0
4.4000 4.4006 -.0006 -1 -1 1
4.1000 4.0995 .0005 -1 1 1
3.2400 3.2393 .0007 -1 0 4
3.1400 3.1400 .0000 0 -2 1
2.9880 2.9885 -.0005 0 -2 2
2.8360 2.8366 -.0006 -2 -1 1
2.7130 2.7133 -.0003 2 0 4
2.6430 2.6434 -.0004 1 2 3
A= 6.47268 DA= .00003
B= 6.394 DB= .001
C= 16.526 DC= .005
GAMMA= 85.91 DGAMMA= .02
BETA = 81.81 DBETA = .01
ALPHA= 90.42 DALPHA= .02
V= 675.1
34. 20-1376
V2Cu2O7
Rombik
Grupa 16
Dexp. Dcal. d(D) h k l
5.3800 5.3687 -.0113 2 0 2
4.2200 4.2235 .0035 0 1 0
4.1300 4.1224 -.0076 0 1 1
3.7000 3.6990 -.0010 1 1 2
3.5800 3.5791 -.0009 3 0 3
3.1600 3.1590 -.0010 0 0 6
3.0900 3.0909 .0009 2 1 3
3.0800 3.0806 .0006 4 0 2
2.8200 2.8211 .0011 0 1 5
2.6500 2.6511 .0011 1 0 7
2.5100 2.5127 -.0027 5 0 2
2.3700 2.3692 -.0008 0 0 8
a= 13.029 b= 4.224 c= 18.954
da=.0005 db=.005 dc=.007
V= 1043
Triklin
Dexp Dcal d(D) h k l
5.3800 5.3692 .0108 -1 1 1
4.2200 4.2200 .0000 1 1 0
4.1300 4.1338 -.0038 -1 -1 1
3.7000 3.7018 -.0018 1 0 1
3.5800 3.5795 .0005 -1 0 2
3.1600 3.1617 -.0017 0 1 2
3.0900 3.0920 -.0020 -1 -1 2
3.0800 3.0812 -.0012 -2 0 1
2.8200 2.8211 -.0011 0 3 0
2.6500 2.6496 .0004 -2 -1 1
2.5100 2.5101 -.0001 1 0 2
2.3700 2.3692 .0008 2 -1 1
A= 6.46723 DA= .00006
B= 8.878 DB= .006
C= 7.411 DC= .002
GAMMA=107.555 DGAMMA= .003
BETA =114.10 DBETA = .01
ALPHA= 81.97 DALPHA= .01
V= 370.3
35. 20-1381
VReO6
Triklin
Dexp Dcal d(D) h k l
7.8600 7.8621 -.0021 -1 1 0
6.5500 6.5533 -.0033 1 2 0
5.2100 5.2028 .0072 -2 1 0
5.0000 5.0116 -.0116 -1 2 0
4.7600 4.7674 -.0074 3 1 0
4.5500 4.5531 -.0031 0 0 1
4.4800 4.4768 .0032 3 0 0
4.3300 4.3330 -.0030 -1 0 1
4.2300 4.2298 .0002 2 3 0
3.9800 3.9786 .0014 -2 -1 1
3.7800 3.7804 -.0004 -2 -2 1
3.6700 3.6730 -.0030 2 1 1
A= 14.333 DA= .004
B= 13.34 DB= .01
C= 4.5985 DC= .0004
GAMMA= 69.58 DGAMMA= .03
BETA = 93.64 DBETA = .01
ALPHA= 98.015 DALPHA= .007
V-816.5
36. 20-1382
VReO5.5*3.5H2O
Rombik
Grupa 16
Dexp. Dcal. d(D) h k l
8.3400 8.2935 -.0465 1 0 0
6.3600 6.3332 -.0268 1 1 0
5.8200 5.8446 .0246 1 1 1
5.6000 5.5980 -.0020 1 0 2
5.0600 5.0581 -.0019 0 0 3
4.4800 4.4956 .0156 0 1 3
4.3300 4.3183 -.0117 1 0 3
4.1500 4.1468 -.0032 2 0 0
4.0000 4.0001 .0001 2 0 1
3.6300 3.6387 .0087 2 0 2
3.5200 3.5210 .0010 0 2 3
3.4500 3.4498 -.0002 1 0 4
3.2700 3.2697 -.0003 0 3 0
a= 8.293513 b=9.8090 c= 15.174
da=.008 db=.0009 dc=.007
V= 1234
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
8.3400 8.2855 .0545 0 1 0
6.3600 6.3427 .0173 0 1 1
5.8200 5.8409 -.0209 1 1 1
5.6000 5.6000 -.0000 2 1 0
5.0600 5.0656 -.0056 3 0 0
4.4800 4.4885 -.0085 3 0 1
4.3300 4.3218 .0082 3 1 0
4.1500 4.1427 .0073 0 2 0
4.0000 3.9969 .0031 1 2 0
3.6300 3.6373 -.0073 2 2 0
3.5200 3.5162 .0038 3 0 2
3.4500 3.4534 -.0034 4 1 0
a= 15.197370 b= 8.29 c= 9.86 beta= 90.5
da=.05 db=.02 dc=.006 dbeta=.2
V= 1241
Triklin
Dexp Dcal d(D) h k l
8.3400 8.3517 -.0117 1 0 0
6.3600 6.3723 -.0123 0 1 1
5.8200 5.8256 -.0056 0 -1 1
5.6000 5.6069 -.0069 1 -1 1
5.0600 5.0611 -.0011 1 0 2
4.4800 4.4840 -.0040 1 1 1
4.3300 4.3412 -.0112 1 -1 2
4.1500 4.1405 .0095 0 0 3
4.0000 3.9966 .0034 2 0 1
3.6300 3.6253 .0047 -1 2 1
3.5200 3.5174 .0026 2 0 2
3.4500 3.4523 -.0023 0 2 1
A= 8.85210 DA= .00001
B= 7.42821 DB= .00003
C= 12.4904 DC= .0002
GAMMA=109.2837 DGAMMA= .0006
BETA = 90.193 DBETA = .001
ALPHA= 84.26784 DALPHA= .00001
V=771.1
37. 20-1383
VReO5.5*H2O
Triklin
Dexp Dcal d(D) h k l
7.3000 7.2964 .0036 1 0 0
6.2700 6.2833 -.0133 1 1 0
6.0200 6.0148 .0052 -1 -1 1
4.5500 4.5478 .0022 -2 -1 1
4.0400 4.0415 -.0015 -2 0 1
3.8600 3.8657 -.0057 -1 0 2
3.6600 3.6581 .0019 -2 -1 2
3.3600 3.3581 .0019 -2 0 2
3.1700 3.1691 .0009 0 2 0
3.0800 3.0792 .0008 0 -1 2
3.0200 3.0183 .0017 0 1 2
2.8900 2.8906 -.0006 2 1 1
A= 9.278 DA= .004
B= 7.244 DB= .007
C= 8.009 DC= .001
GAMMA= 61.07 DGAMMA= .01
BETA =119.73 DBETA = .01
ALPHA=104.95 DALPHA= .02
V= 409.0
38. 20-1385
Ag2V4O11
Monoklin
GRUPA 4,11
Dexp. Dcal. d(D) h k l
7.5000 7.5072 -.0072 0 0 1
3.7500 3.7536 -.0036 0 0 2
3.7100 3.7079 .0021 0 2 1
3.4300 3.4356 -.0056 0 1 2
3.0800 3.0817 -.0017 3 0 2
3.0000 2.9991 .0009 4 2 0
2.9200 2.9232 -.0032 -5 1 1
2.7700 2.7694 .0006 1 2 2
2.6600 2.6588 .0012 -6 0 1
2.4650 2.4651 -.0001 1 0 3
2.3250 2.3264 -.0014 -2 1 3
2.8050 2.8048 .0002 -4 2 1
a= 16.88 b= 8.53 c= 7.510 beta= 91.6
da=.09 db= .01 dc=.005 dbet=.2
V-1081
Triklin
Dexp Dcal d(D) h k l
7.5000 7.5023 -.0023 0 1 0
3.7500 3.7511 -.0011 0 2 0
3.7100 3.7099 .0001 0 -1 2
3.4300 3.4308 -.0008 0 0 2
3.0800 3.0781 .0019 1 -2 2
3.0000 2.9979 .0021 -1 1 1
2.9200 2.9208 -.0008 -1 2 0
2.7700 2.7693 .0007 2 1 1
2.6600 2.6611 -.0011 2 -1 2
2.4650 2.4652 -.0002 -1 -3 1
2.3250 2.3253 -.0003 -2 0 1
2.8050 2.8038 .0012 2 0 0
A= 5.9898 DA= .0009
B= 8.1375 DB= .0009
C= 7.8574 DC= .0002
GAMMA= 89.0045 DGAMMA= .0007
BETA = 71.278 DBETA = .009
ALPHA=111.160 DALPHA= .007
V=334.5