1. 19-0033
Al70Mo25V5
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
4.4900 4.5197 -.0297 4 1 0
3.8300 3.8345 -.0045 0 3 0
3.6800 3.6780 .0020 0 1 1
3.3600 3.3628 -.0028 -2 1 1
3.2800 3.2766 .0034 6 0 0
3.1200 3.1192 .0008 2 2 1
3.0500 3.0571 -.0071 4 1 1
2.9320 2.9351 -.0031 -4 0 1
2.8760 2.8758 .0002 0 4 0
2.4430 2.4437 -.0007 4 3 1
2.2730 2.2735 -.0005 2 4 1
2.2270 2.2262 .0008 -2 4 1
a= 19.7 b=11.503 c=3.89405 beta=85.442280
da=.1 db= 3.979683E-03 dc=.00002 dbeta=.001
V= 880
Triklin
Dexp Dcal d(D) h k l
4.4900 4.4905 -.0005 -1 2 1
3.8300 3.8298 .0002 -1 2 3
3.6800 3.6806 -.0006 0 -1 3
3.3600 3.3598 .0002 -1 3 2
3.2800 3.2810 -.0010 -2 0 2
3.1200 3.1207 -.0007 1 3 0
3.0500 3.0505 -.0005 -2 1 3
2.9320 2.9325 -.0005 2 -1 1
2.8760 2.8744 .0016 -1 3 4
2.4430 2.4422 .0008 -2 3 0
2.2730 2.2725 .0005 -3 1 2
2.2270 2.2284 -.0014 0 -4 2
2.1180 2.1179 .0001 -1 -2 5
A= 6.8928 DA= .0002
B= 11.194 DB= .001
C= 14.277 DC= .009
GAMMA= 94.2685 DGAMMA= .0003
BETA =102.479 DBETA = .001
ALPHA= 71.17 DALPHA= .03
V= 1017.9
2. 19-0049
Ta40V23Al47
Triklin
Dexp. Dcal. d(D) h k l
4.6500 4.6500 .0000 1 -2 0
4.2700 4.2700 .0000 3 0 0
3.9500 3.9503 -.0003 -1 -2 0
3.0100 3.0095 .0005 0 -3 0
2.8820 2.8819 .0001 -1 0 1
2.7790 2.7788 .0002 -1 1 1
2.5470 2.5449 .0021 4 -3 0
2.3850 2.3850 .0000 -1 -2 1
2.3440 2.3425 .0015 -4 -2 0
2.3120 2.3130 -.0010 -5 -1 0
2.2570 2.2571 -.0001 0 -4 0
2.2330 2.2330 .0000 2 2 1
A= 13.278 DA= .001
B= 9.3489 DB= .0001
C= 2.9962 DC= .0001
GAMMA=105.02 DGAMMA= .03
BETA = 86.849 DBETA = .002
ALPHA= 91.789 DALPHA= .006
V= 358.6
Dexp Dcal d(D) h k l
4.6500 4.6592 -.0092 -1 0 1
4.2700 4.2776 -.0076 1 0 1
3.9500 3.9443 .0057 -1 2 1
3.0100 3.0106 -.0006 0 2 3
2.8820 2.8808 .0012 1 -2 1
2.7790 2.7803 -.0013 0 3 2
2.5470 2.5465 .0005 -2 2 2
2.3850 2.3859 -.0009 2 -1 1
2.3440 2.3432 .0008 -1 1 4
2.3120 2.3122 -.0002 1 -2 2
2.2570 2.2577 -.0007 -2 1 3
2.2330 2.2319 .0011 2 1 1
A= 5.460 DA= .001
B= 8.947 DB= .003
C= 9.928 DC= .001
GAMMA=108.26 DGAMMA= .01
BETA =102.91 DBETA = .01
ALPHA= 63.41 DALPHA= .04
V= 410.1
3. 19-0195
Cd0.95VO3
Triklin
Dexp Dcal d(D) h k l
7.1300 7.1304 -.0004 0 0 1
4.1800 4.1810 -.0010 -1 -1 1
3.5000 3.4993 .0007 1 -1 2
2.9950 2.9954 -.0004 2 0 2
2.9510 2.9517 -.0007 0 -2 2
2.9370 2.9378 -.0008 0 2 2
2.8870 2.8873 -.0003 3 -2 1
2.7280 2.7284 -.0004 1 3 1
2.5500 2.5496 .0004 -3 1 1
2.5290 2.5286 .0004 3 -1 2
2.4990 2.4999 -.0009 3 -2 2
1.9240 1.9238 .0002 -1 3 3
1.7970 1.7970 .0000 1 -6 1
A= 9.0423 DA= .0007
B= 11.14878 DB= .005
C= 7.275 DC= .003
GAMMA=110.44 DGAMMA= .07
BETA = 78.552 DBETA = .006
ALPHA= 94.25 DALPHA= .02
V= 673.6
4. 19-0196
Cd1.3V6O13
Triklin
Dexp Dcal d(D) h k l
5.1200 5.1202 -.0002 -1 2 0
4.6800 4.6831 -.0031 -1 1 1
4.5900 4.5910 -.0010 -1 -1 1
3.6300 3.6301 -.0001 -1 -3 1
3.4600 3.4578 .0022 0 -4 1
2.9900 2.9889 .0011 1 5 0
2.8500 2.8504 -.0004 -1 -1 2
2.6380 2.6377 .0003 -2 -3 1
2.5750 2.5749 .0001 0 -6 1
2.5060 2.5063 -.0003 2 -1 1
2.3070 2.3074 -.0004 1 6 1
2.2520 2.2521 -.0001 -2 3 2
A= 6.3560 DA= .0006
B= 17.359 DB= .001
C= 6.011 DC= .001
GAMMA= 92.035 DGAMMA= .002
BETA =102.48 DBETA = .02
ALPHA= 88.56 DALPHA= .01
V= 647.1
5. 19-0812
Mo4V6O25
Rombik
Groupa 30,53
Dexp. Dcal. d(D) h k l
6.0000 6.0066 -.0066 1 1 0
4.0900 4.0981 -.0081 0 1 1
3.5200 3.5175 .0025 5 0 0
3.3600 3.3588 .0012 3 1 1
2.9940 2.9979 -.0039 4 1 1
2.7060 2.7093 -.0033 1 2 1
2.6730 2.6703 .0027 0 0 2
2.6730 2.6691 .0039 5 1 1
2.4290 2.4301 -.0011 3 0 2
1.9960 1.9956 .0004 2 2 2
1.9300 1.9304 -.0004 2 3 1
1.8230 1.8222 .0008 5 3 0
1.5510 1.5511 -.0001 11 1 0
a=17.587 b= 6.391 c= 5.34068
da= .009 db= .006 dc= .00006
v= 600.3
6. 19-0813
Mo6V9O40
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
9.6800 9.6614 .0186 1 0 0
4.8300 4.8307 -.0007 2 0 0
4.1200 4.1196 .0004 -1 1 2
3.7800 3.7864 -.0064 -2 1 1
3.5600 3.5600 -.0000 -2 1 2
3.2300 3.2294 .0006 0 1 3
3.1600 3.1615 -.0015 -1 0 4
2.6960 2.6960 .0000 -3 1 3
2.6420 2.6420 .0000 2 0 3
2.5510 2.5506 .0004 3 1 1
2.3080 2.3077 .0003 -4 0 4
2.0600 2.0598 .0002 -2 2 4
a= 10.31 b=5.5940 c=12.66 beta=110.4
da= 4.084110E-02 db=.0004 dc=.05 dbeta=.3
V= 684.
7. 19-813
Mo6V9O40
Triklin
Dexp Dcal d(D) h k l
9.6800 9.6593 .0207 1 0 0
4.8300 4.8296 .0004 2 0 0
4.1200 4.1200 -.0000 -1 -1 1
3.7800 3.7800 .0000 2 1 0
3.5600 3.5610 -.0010 2 0 2
3.2300 3.2297 .0003 -1 -1 2
3.1600 3.1606 -.0006 1 -1 2
2.6960 2.6964 -.0004 -3 -1 1
2.6420 2.6419 .0001 3 1 2
2.5510 2.5508 .0002 -1 -1 3
2.3080 2.3083 -.0003 -4 0 1
2.0600 2.0600 .0000 -2 -2 2
1.9320 1.9319 .0001 5 0 0
1.8900 1.8900 .0000 4 2 0
A= 9.769 DA= .001
B= 5.26798 DB= .00001
C= 9.878 DC= .004
GAMMA= 82.325 DGAMMA= .007
BETA = 85.27 DBETA = .01
ALPHA= 83.316 DALPHA= .007
V= 499.2
8. 19-878
NbVO5
Triklin
Dexp Dcal d(D) h k l
7.8000 7.7972 .0028 0 2 0
5.8000 5.7991 .0009 0 1 1
4.9300 4.9348 -.0048 1 3 0
4.3500 4.3477 .0023 2 1 0
4.0600 4.0620 -.0020 -1 3 0
3.9000 3.8986 .0014 0 4 0
3.7100 3.7070 .0030 2 3 0
3.5100 3.5103 -.0003 -2 0 1
3.4000 3.4006 -.0006 1 4 1
3.3500 3.3505 -.0005 -2 -2 1
3.0700 3.0696 .0004 -2 2 1
2.8700 2.8707 -.0007 3 2 0
A= 8.710 DA= .003
B= 16.055 DB= .005
C= 6.023 DC= .007
GAMMA= 77.62 DGAMMA= .04
BETA = 90.19 DBETA = .09
ALPHA= 84.15 DALPHA= .07
V= 818.6
9. 19-1052
Na0.33V0.33V1.67O5
Triklin
Dexp Dcal d(D) h k l
9.4600 9.4656 -.0056 0 0 1
7.2700 7.2691 .0009 -1 1 0
5.0100 5.0117 -.0017 0 -2 1
4.7300 4.7328 -.0028 0 0 2
3.8500 3.8512 -.0012 2 0 1
3.6200 3.6208 -.0008 -2 1 1
3.4700 3.4700 .0000 0 -3 1
3.3700 3.3702 -.0002 -2 -1 1
3.1900 3.1886 .0014 2 0 2
3.1500 3.1512 -.0012 1 -1 3
3.0600 3.0596 .0004 2 -3 1
2.9200 2.9203 -.0003 -2 1 2
A= 8.5207 DA= .0002
B= 10.8241 DB= .0009
C= 9.806 DC= .003
GAMMA=104.293 DGAMMA= .003
BETA = 83.691 DBETA = .005
ALPHA=104.895 DALPHA= .005
V= 846.0
Dexp. Dcal. d(D) h k l
9.4600 9.4580 .0020 2 0 0
7.2700 7.2730 -.0030 1 -1 0
5.0100 5.0149 -.0049 3 -1 0
4.7300 4.7290 .0010 4 0 0
3.8500 3.8507 -.0007 0 -2 0
3.6200 3.6199 .0001 -2 0 1
3.3700 3.3692 .0008 -2 1 1
3.1900 3.1903 -.0003 -2 -1 1
3.1500 3.1527 -.0027 6 0 0
3.0600 3.0587 .0013 -4 0 1
2.9200 2.9214 -.0014 -4 1 1
2.9000 2.9021 -.0021 4 0 1
A= 18.975 DA= .005
B= 7.725 DB= .002
C= 3.8436 DC= .0009
GAMMA= 93.31 DGAMMA= .09
BETA = 93.26 DBETA = .02
ALPHA= 86.80 DALPHA= .02
V= 560.7
10. 19-1151
alfa-AgVO3
Triklin
Dexp Dcal d(D) h k l
7.0700 7.0730 -.0030 -1 0 1
3.4600 3.4609 -.0009 -1 1 2
2.9100 2.9104 -.0004 -1 -1 2
2.8400 2.8367 .0033 0 -1 2
2.6900 2.6905 -.0005 2 -1 1
2.5300 2.5294 .0006 -2 1 3
2.4900 2.4920 -.0020 0 0 3
2.4700 2.4691 .0009 -1 2 0
2.2400 2.2403 -.0003 -2 2 0
2.1400 2.1397 .0003 3 -1 1
2.0600 2.0596 .0004 1 1 3
1.9800 1.9802 -.0002 2 -2 1
A= 9.12 DA= .02
B= 5.131 DB= .007
C= 8.2143 DC= .0002
GAMMA= 98.3 DGAMMA= .1
BETA =113.47 DBETA = .07
ALPHA= 80.17 DALPHA= .04
V= 345.7
11. 19-1152
beta-AgVO3
Triklin
Dexp Dcal d(D) h k l
8.6200 8.6112 .0088 0 1 0
4.3800 4.3772 .0028 0 -1 2
3.8600 3.8577 .0023 -1 0 1
3.4500 3.4532 -.0032 1 -1 1
3.2400 3.2403 -.0003 -1 1 1
3.1000 3.0970 .0030 -1 0 2
3.0300 3.0319 -.0019 1 2 1
2.9600 2.9586 .0014 1 -1 2
2.7000 2.7017 -.0017 -1 1 2
2.6600 2.6602 -.0002 0 -3 2
2.5800 2.5798 .0002 -1 2 1
2.5400 2.5407 -.0007 -1 -1 3
A= 4.370 DA= .002
B= 8.91012 DB= .00004
C= 9.280 DC= .001
GAMMA= 79.51 DGAMMA= .01
BETA = 90.840 DBETA = .003
ALPHA=100.596 DALPHA= .006
V= 349.2
12. 19-1153
gamma-AgVO3
Triklin
Dexp Dcal d(D) h k l
5.1100 5.1017 .0083 -1 0 2
3.5400 3.5350 .0050 0 1 0
3.2200 3.2193 .0007 0 -1 2
3.1300 3.1297 .0003 -1 1 2
2.9200 2.9203 -.0003 0 -1 3
2.9100 2.9112 -.0012 0 1 3
2.8200 2.8181 .0019 -2 0 3
2.7600 2.7593 .0007 1 0 5
2.6900 2.6895 .0005 1 1 2
2.6500 2.6498 .0002 -2 1 1
2.5400 2.5415 -.0015 -1 -1 3
2.4300 2.4314 -.0014 -1 0 6
A= 6.697 DA= .005
B= 3.602 DB= .001
C= 15.482 DC= .004
GAMMA=101.11 DGAMMA= .03
BETA = 92.17 DBETA = .05
ALPHA= 89.78 DALPHA= .01
V= 366.2
13. 19-1154
Ag3VO4
Triklin
Dexp Dcal d(D) h k l
4.5800 4.5729 .0071 -1 1 1
4.3800 4.3894 -.0094 0 1 1
4.2700 4.2656 .0044 0 -1 1
3.5400 3.5430 -.0030 -1 2 1
2.8800 2.8836 -.0036 1 -1 1
2.7900 2.7898 .0002 -1 1 2
2.7500 2.7505 -.0005 -2 0 1
2.6100 2.6096 .0004 -2 2 1
2.5400 2.5387 .0013 1 -2 1
2.4800 2.4799 .0001 2 0 0
2.3000 2.2989 .0011 1 2 1
2.2300 2.2305 -.0005 1 3 0
A= 5.685 DA= .001
B= 8.5803 DB= .0006
C= 5.6843 DC= .0008
GAMMA=104.230 DGAMMA= .004
BETA =116.92 DBETA = .01
ALPHA= 82.0159 DALPHA= .0003
V= 239.6
14. 19-1164
AgV7O18
Triklin
Dexp Dcal d(D) h k l
7.1600 7.2000 -.0400 0 0 1
4.6900 4.6946 -.0046 0 -2 1
3.8100 3.8067 .0033 1 0 0
3.4500 3.4471 .0029 0 -3 1
3.4200 3.4167 .0033 -1 1 0
3.3400 3.3382 .0018 -1 0 1
3.3100 3.3060 .0040 1 1 1
3.1700 3.1719 -.0019 1 -1 1
3.0300 3.0304 -.0004 0 3 1
2.8900 2.8930 -.0030 -1 2 0
2.8600 2.8627 -.0027 1 3 0
2.7000 2.6987 .0013 0 4 0
A= 3.86025 DA= .00001
B= 11.08768 DB= .00001
C= 7.29437 DC= .00003
GAMMA= 80.5178 DGAMMA= .0001
BETA = 90.4097 DBETA = .0005
ALPHA= 99.1650 DALPHA= .0002
V= 303.95
15. 19-1165
Ag2V4O11
Triklin
Dexp Dcal d(D) h k l
7.4600 7.4644 -.0044 0 -1 1
3.7400 3.7402 -.0002 0 -1 3
3.6900 3.6899 .0001 1 -1 3
3.4100 3.4094 .0006 2 -1 2
3.0600 3.0592 .0008 2 -1 3
2.9900 2.9901 -.0001 -2 -1 2
2.9000 2.9004 -.0004 1 -1 4
2.7600 2.7599 .0001 -2 -2 2
2.6500 2.6503 -.0003 2 -2 1
2.4600 2.4597 .0003 1 1 4
2.3200 2.3200 -.0000 2 3 1
1.8600 1.8600 -.0000 4 1 4
A= 8.513 DA= .005
B= 8.1795 DB= .0006
C= 11.741 DC= .003
GAMMA= 80.57 DGAMMA= .02
BETA = 75.28 DBETA = .05
ALPHA=105.40 DALPHA= .06
V= 738.5
16. 19-1166
Ag4V2O7
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
4.7600 4.7596 .0004 -2 0 1
3.5000 3.5018 -.0018 2 1 0
3.1600 3.1586 .0014 -3 0 1
3.0000 2.9999 .0001 3 0 0
2.9500 2.9522 -.0022 -3 0 3
1.8100 1.8101 -.0001 -4 2 2
2.7300 2.7307 -.0007 3 0 1
2.6100 2.6091 .0009 -3 1 3
2.3700 2.3727 -.0027 -3 0 5
2.3700 2.3700 -.0000 2 2 0
2.1500 2.1498 .0002 3 0 3
2.1500 2.1497 .0003 -4 1 3
a= 9.522 b= 5.576 c=13.61 beta=109.06
da=.003 db=.001 dc=.02 dbeta=.04
V= 682.8
Triklin
Dexp Dcal d(D) h k l
4.7600 4.7591 .0009 -1 1 0
3.5000 3.4992 .0008 0 1 1
3.1600 3.1596 .0004 0 -1 1
3.0000 2.9933 .0067 1 0 1
2.9500 2.9460 .0040 -1 1 1
1.8100 1.8095 .0005 -1 5 0
2.7300 2.7308 -.0008 1 -1 1
2.6100 2.6127 -.0027 0 3 1
2.3700 2.3742 -.0042 1 -2 1
2.1500 2.1493 .0007 2 2 1
1.9600 1.9596 .0004 0 5 0
1.8000 1.8006 -.0006 -2 -3 1
A= 5.7047 DA= .0001
B= 9.95689 DB= .00001
C= 3.57049 DC= .00002
GAMMA= 85.4679 DGAMMA= .0008
BETA = 89.3854 DBETA = .0003
ALPHA= 80.79427 DALPHA= .00006
V= 199.56
17. 19-1229
Na4V2O7
Triklin
Dexp. Dcal. d(D) h k l
6.0300 6.0300 .0000 -1 -1 0
5.4900 5.4902 -.0002 0 1 1
4.9200 4.9200 .0000 -1 -2 0
4.1100 4.1106 -.0006 0 -2 1
3.8400 3.8415 -.0015 1 -2 0
3.6400 3.6408 -.0008 1 0 1
3.3200 3.3200 .0000 1 -1 1
3.2000 3.2001 -.0001 -2 0 1
3.0300 3.0300 .0000 0 -4 0
A= 6.668 DA= .002
B= 12.496 DB= .004
C= 6.377 DC= .001
GAMMA= 76.441 DGAMMA= .002
BETA =110.71 DBETA = .03
ALPHA= 91.26 DALPHA= .01
V= 482.1
18. 19-1255
Na3VO4
Triklin
Dexp Dcal d(D) h k l
4.3800 4.3819 -.0019 1 0 0
3.5500 3.5465 .0035 0 1 0
3.0500 3.0471 .0029 0 -1 2
2.7000 2.7001 -.0001 -1 0 4
2.5700 2.5711 -.0011 1 1 1
2.3600 2.3615 -.0015 -1 -1 2
2.2900 2.2870 .0030 0 1 5
2.1600 2.1595 .0005 -2 0 1
2.0200 2.0213 -.0013 0 1 6
1.9700 1.9693 .0007 -2 0 3
1.9000 1.9001 -.0001 2 -1 2
1.7600 1.7604 -.0004 -2 1 4
A= 4.4285 DA= .0005
B= 3.59879 DB= .00005
C= 13.918 DC= .002
GAMMA= 98.294 DGAMMA= .005
BETA = 89.976 DBETA = .006
ALPHA= 84.862 DALPHA= .008
V= 218.6
19. 19-1256
Na3.25VO4{OH}0.25*12H2O
Triklin
Dexp Dcal d(D) h k l
6.0400 6.0351 .0049 0 1 1
5.5000 5.4907 .0093 -1 1 0
4.3700 4.3630 .0070 0 -1 1
4.0400 4.0417 -.0017 0 0 2
3.4800 3.4793 .0007 1 0 2
3.3600 3.3574 .0026 1 1 2
3.2000 3.2013 -.0013 2 1 0
3.0600 3.0606 -.0006 2 1 1
3.0000 3.0017 -.0017 0 -1 2
2.9300 2.9299 .0001 -2 2 1
2.9000 2.8988 .0012 -2 -1 1
2.8300 2.8306 -.0006 0 1 3
A= 8.4165 DA= .0002
B= 6.88549 DB= .00002
C= 8.66893 DC= .00005
GAMMA=102.466 DGAMMA= .001
BETA = 99.909 DBETA = .002
ALPHA= 69.6807 DALPHA= .0002
V= 457.4
20. 19-1257
Na10V24O64
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
7.0400 7.0137 .0263 1 0 0
5.8100 5.8013 .0087 1 1 0
3.8700 3.8666 .0034 1 0 2
3.6200 3.6209 -.0009 1 1 2
3.5000 3.5065 -.0065 0 0 3
3.4500 3.4585 -.0085 -1 2 2
3.2100 3.2169 -.0069 -2 0 2
3.1000 3.0945 .0055 1 2 2
3.0100 3.0131 -.0031 2 1 1
2.6700 2.6651 .0049 -2 1 3
2.5700 2.5704 -.0004 1 3 2
2.4320 2.4329 -.0009 -2 2 3
a= 7.1468 b=10.3223 c= 10.719 beta=101.07
da=.0006 db=.0005 dc=.006 dbeta=.04
V= 776.0
Triklin
Dexp Dcal d(D) h k l
7.0400 7.0300 .0100 0 1 0
5.8100 5.8104 -.0004 2 0 0
3.8700 3.8736 -.0036 3 0 0
3.6200 3.6210 -.0010 0 0 1
3.5000 3.5016 -.0016 2 2 0
3.4500 3.4490 .0010 -1 0 1
3.2100 3.2113 -.0013 0 -1 1
3.1000 3.0997 .0003 3 2 0
3.0100 3.0099 .0001 2 1 1
2.6700 2.6697 .0003 2 -1 1
2.5700 2.5698 .0002 -1 -2 1
2.4320 2.4317 .0003 5 1 0
A= 12.167 DA= .001
B= 7.360 DB= .002
C= 3.62123 DC= .00003
GAMMA= 72.77 DGAMMA= .01
BETA = 89.409 DBETA = .009
ALPHA= 89.51 DALPHA= .01
V= 309.8
21. 19-1258
Na8V24O63
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
7.2100 7.2016 .0084 0 1 1
6.8100 6.7994 .0106 1 1 0
3.8600 3.8518 .0082 2 1 1
3.4700 3.4635 .0065 -2 0 2
3.2000 3.1972 .0028 0 3 1
3.0800 3.0788 .0012 -1 1 3
3.0100 3.0141 -.0041 1 3 1
2.6600 2.6579 .0021 -3 0 2
2.4000 2.4005 -.0005 0 3 3
2.3000 2.3002 -.0002 4 0 0
2.2500 2.2508 -.0008 -3 1 3
2.0000 2.0006 -.0006 -1 3 4
a= 9.203 b=10.092 c= 10.2818 beta= 91.17
da=.007 db=.003 dc=.0003 dbeta= .03
V= 954.7
Triklin
Dexp Dcal d(D) h k l
7.2100 7.2082 .0018 1 0 0
6.8100 6.8053 .0047 -1 1 0
3.8600 3.8604 -.0004 1 -1 2
3.4700 3.4732 -.0032 2 0 2
3.2000 3.1996 .0004 -2 1 1
3.0800 3.0801 -.0001 -1 0 2
3.0100 3.0092 .0008 0 2 2
2.6600 2.6598 .0002 1 -3 0
2.4000 2.4001 -.0001 -2 2 2
2.3000 2.3004 -.0004 -1 3 2
2.2500 2.2498 .0002 -1 2 3
2.0000 2.0000 .0000 -4 2 0
A= 8.5727 DA= .0007
B= 8.034 DB= .001
C= 8.936 DC= .003
GAMMA=113.73 DGAMMA= .02
BETA = 69.289 DBETA = .009
ALPHA= 88.82 DALPHA= .02
V= 517.4
22. 19-1259
NaV6O15
Triklin
Dexp Dcal d(D) h k l
10.4000 10.4132 -.0132 1 0 0
9.6300 9.6099 .0201 0 1 0
7.7100 7.7025 .0075 0 0 1
7.2000 7.1958 .0042 -1 0 1
4.7300 4.7312 -.0012 2 1 0
3.8100 3.8066 .0034 0 -1 2
3.6300 3.6322 -.0022 -2 -1 2
3.4700 3.4711 -.0011 3 0 0
3.3800 3.3809 -.0009 0 1 2
3.0600 3.0591 .0009 -3 -1 2
2.9100 2.9104 -.0004 1 -2 2
2.7200 2.7198 .0002 -1 3 1
A= 10.910 DA= .005
B= 9.836 DB= .005
C= 8.167 DC= .001
GAMMA= 82.583 DGAMMA= .004
BETA =106.83 DBETA = .01
ALPHA=101.52 DALPHA= .02
V= 819.1
Dexp Dcal d(D) h k l
9.6300 9.6258 .0042 0 1 1
7.7100 7.7149 -.0049 -1 1 0
7.2000 7.1972 .0028 0 -1 1
4.7300 4.7317 -.0017 -1 0 2
3.8100 3.8102 -.0002 1 -1 2
3.6300 3.6255 .0045 0 1 3
3.4700 3.4705 -.0005 0 0 3
3.3800 3.3815 -.0015 -1 0 3
3.0600 3.0586 .0014 -2 1 3
2.9100 2.9102 -.0002 2 -3 1
2.7200 2.7195 .0005 -2 4 3
2.5000 2.5004 -.0004 -1 4 4
A= 8.6726 DA= .0005
B= 14.1180 DB= .0008
C= 11.133 DC= .003
GAMMA=104.093 DGAMMA= .003
BETA =102.2459 DBETA = .0008
ALPHA= 70.93 DALPHA= .01
V= 1236.4
23. 19-1312
alfa-TaVO5
Triklin
Dexp Dcal d(D) h k l
5.9000 5.8974 .0026 -1 1 0
4.4800 4.4803 -.0003 0 -1 2
4.2900 4.2868 .0032 1 -1 2
4.0200 4.0180 .0020 0 0 2
3.4700 3.4716 -.0016 -1 0 2
3.4100 3.4082 .0018 -2 -1 1
2.9800 2.9801 -.0001 0 -1 3
2.9000 2.9012 -.0012 1 -2 3
2.8300 2.8297 .0003 -2 -1 2
2.7500 2.7514 -.0014 -2 0 2
2.7100 2.7098 .0002 -3 1 0
2.6000 2.6005 -.0005 3 -1 2
A= 8.594 DA= .003
B= 8.639 DB= .001
C= 9.132 DC= .001
GAMMA= 98.59 DGAMMA= .05
BETA = 80.05 DBETA = .02
ALPHA=117.60 DALPHA= .02
V= 590.0
24. 19-1313
beta-TaVO5
Triklin
Dexp Dcal d(D) h k l
7.8000 7.7843 .0157 0 1 0
5.8000 5.8081 -.0081 -1 -1 1
4.9300 4.9279 .0021 0 -1 2
4.2900 4.2888 .0012 -1 0 2
4.0000 3.9988 .0012 1 2 0
3.8800 3.8820 -.0020 -1 -2 1
3.6900 3.6898 .0002 2 0 2
3.4800 3.4814 -.0014 0 -2 2
3.4000 3.3980 .0020 -1 -2 2
3.3400 3.3398 .0002 -2 1 0
3.2500 3.2503 -.0003 -2 -1 2
3.1200 3.1203 -.0003 0 1 3
A= 8.9241 DA= .0007
B= 8.198 DB= .001
C= 11.3100 DC= .0008
GAMMA= 74.69 DGAMMA= .03
BETA = 82.2948 DBETA = .0008
ALPHA= 97.62 DALPHA= .01
V= 778.34
25. 19-1395
Cl3VNCl
Triklin
Dexp Dcal d(D) h k l
4.2700 4.2698 .0002 -1 -1 1
3.9300 3.9290 .0010 1 2 0
3.3200 3.3201 -.0001 -1 -3 1
3.0000 2.9988 .0012 1 1 1
2.7600 2.7602 -.0002 1 4 0
2.6200 2.6216 -.0016 1 -3 1
2.4800 2.4800 -.0000 1 3 1
2.4000 2.4014 -.0014 -2 1 1
2.3000 2.3001 -.0001 -1 -4 2
2.2200 2.2196 .0004 -2 2 0
2.0800 2.0797 .0003 1 -5 1
2.0700 2.0690 .0010 -2 3 0
A= 5.0350 DA= .0003
B= 13.4042 DB= .0006
C= 5.7512 DC= .0002
GAMMA= 85.3818 DGAMMA= .0008
BETA =108.68 DBETA = .02
ALPHA= 99.02 DALPHA= .01
V= 363.0
26. 19-1396
Cl3VNCl*SbCl5
Triklin
Dexp Dcal d(D) h k l
6.5000 6.5033 -.0033 1 0 0
5.8000 5.8058 -.0058 0 1 1
5.0000 4.9979 .0021 1 0 1
4.1900 4.1909 -.0009 -1 1 0
4.0400 4.0375 .0025 0 0 2
3.5600 3.5601 -.0001 0 2 0
3.3000 3.2995 .0005 0 -1 2
3.0800 3.0804 -.0004 -1 1 2
2.9200 2.9200 .0000 1 2 2
2.7400 2.7403 -.0003 -1 2 1
2.6600 2.6590 .0010 -2 1 0
2.5300 2.5300 -.0000 -1 -2 2
A= 6.852 DA= .001
B= 7.591 DB= .002
C= 8.176 DC= .002
GAMMA= 71.721 DGAMMA= .007
BETA = 88.721 DBETA = .003
ALPHA= 81.134 DALPHA= .003
V= 398.8
27. 19-1399
V6O13
Triklin
Dexp Dcal d(D) h k l
5.8600 5.8565 .0035 0 0 1
4.9900 4.9902 -.0002 -1 0 1
3.5000 3.4990 .0010 0 -2 1
3.3100 3.3119 -.0019 1 -1 1
3.1800 3.1782 .0018 -2 0 1
2.9620 2.9591 .0029 -1 -1 2
2.7300 2.7309 -.0009 -2 1 0
2.4860 2.4860 -.0000 -2 -2 2
2.4310 2.4320 -.0010 1 1 2
2.3370 2.3376 -.0006 -1 3 0
2.2390 2.2385 .0005 -2 2 0
1.9880 1.9883 -.0003 2 -2 1
A= 7.1523 DA= .0007
B= 9.223 DB= .005
C= 6.080 DC= .001
GAMMA= 68.80 DGAMMA= .02
BETA =105.56 DBETA = .09
ALPHA= 96.61 DALPHA= .07
V= 360.2
28. 19-1402
VPO5*H2O
Triklin
Dexp Dcal d(D) h k l
6.3000 6.3042 -.0042 1 0 0
5.7100 5.7149 -.0049 0 1 1
4.9000 4.8950 .0050 0 -1 1
4.4100 4.4066 .0034 0 0 2
3.4200 3.4202 -.0002 -1 -1 1
3.1300 3.1298 .0002 -2 2 1
3.0400 3.0431 -.0031 -2 1 2
2.8120 2.8119 .0001 -1 -1 2
2.5400 2.5407 -.0007 1 -2 2
2.1840 2.1837 .0003 0 3 0
2.1020 2.1019 .0001 -2 3 3
1.9840 1.9840 -.0000 1 2 3
A= 7.1793 DA= .0003
B= 7.5285 DB= .0002
C= 9.081 DC= .001
GAMMA=118.174 DGAMMA= .006
BETA =100.5231 DBETA = .0007
ALPHA= 76.990 DALPHA= .008
V= 419.94
29. 19-1403
VPO5
Rombik
Groupa 50
Dexp. Dcal. d(D) h k l
5.2000 5.2072 -.0072 0 0 3
4.6000 4.5992 .0008 1 1 0
3.9700 3.9632 .0068 1 1 2
3.9000 3.9054 -.0054 0 0 4
3.4800 3.4833 -.0033 2 0 0
3.4000 3.3998 .0002 2 0 1
3.1900 3.1813 .0087 2 0 2
3.0600 3.0616 -.0016 0 2 0
2.9700 2.9724 -.0024 2 1 1
2.8200 2.8230 -.0030 2 1 2
2.6400 2.6392 .0008 0 2 3
2.4100 2.4095 .0005 0 2 4
a= 6.967 b= 6.123 c=15.621
da= .004 db= .002 dc= .001
V= 666.4
Triklin
Dexp Dcal d(D) h k l
5.2000 5.2022 -.0022 -1 1 0
4.6000 4.5963 .0037 -1 1 1
3.9700 3.9683 .0017 -1 -1 1
3.9000 3.8999 .0001 1 1 0
3.4800 3.4757 .0043 -1 1 2
3.4000 3.4037 -.0037 -1 -1 2
3.1900 3.1895 .0005 -1 2 0
3.0600 3.0619 -.0019 1 -2 1
2.9700 2.9684 .0016 -1 0 3
2.8200 2.8187 .0013 0 -2 2
2.6400 2.6418 -.0018 -1 1 3
2.4100 2.4099 .0001 2 -1 2
A= 6.575 DA= .001
B= 6.6040 DB= .0005
C= 9.2551 DC= .0003
GAMMA=104.47 DGAMMA= .01
BETA =101.25 DBETA = .01
ALPHA= 96.894 DALPHA= .004
V= 375.6
30. 19-1404
VPO5*2H2O
Triklin
Dexp Dcal d(D) h k l
7.4900 7.4861 .0039 1 0 0
4.8200 4.8179 .0021 0 1 1
4.4600 4.4619 -.0019 -2 -1 1
4.0900 4.0907 -.0007 -1 -2 1
3.7500 3.7483 .0017 -1 1 1
3.1400 3.1374 .0026 2 0 1
2.9010 2.9036 -.0026 1 -1 2
2.4930 2.4930 .0000 -3 -3 1
2.4090 2.4090 .0000 0 2 2
2.3250 2.3250 -.0000 1 -2 2
2.2310 2.2310 .0000 -4 -2 2
2.1300 2.1300 .0000 -4 -3 2
A= 9.0384 DA= .0008
B= 8.304 DB= .001
C= 8.8418 DC= .0005
GAMMA= 58.239 DGAMMA= .004
BETA =111.20 DBETA = .07
ALPHA=110.15 DALPHA= .05
V= 516.0
31. 19-1406
V4S5
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.7900 5.7806 .0094 1 1 0
5.1800 5.1719 .0081 1 1 1
3.2600 3.2598 .0002 3 0 0
3.1800 3.1767 .0033 -2 1 1
2.9380 2.9358 .0022 -1 2 1
2.8820 2.8815 .0005 -1 1 2
2.6500 2.6536 -.0036 -3 0 1
2.5870 2.5859 .0011 2 2 2
2.5620 2.5602 .0018 -2 0 2
2.5060 2.5061 -.0001 3 2 1
2.1640 2.1648 -.0008 -1 3 1
2.1410 2.1398 .0012 -1 1 3
a= 10.540 b= 7.1665 c= 8.131 beta=68.088
da=.005 db=.0008 dc=.003 dbeta=.008
V= 569.8
Triklin
Dexp Dcal d(D) h k l
5.7900 5.7890 .0010 1 0 0
5.1800 5.1774 .0026 0 1 1
3.2600 3.2619 -.0019 2 -1 1
3.1800 3.1819 -.0019 -1 2 0
2.9380 2.9384 -.0004 -1 2 1
2.8820 2.8854 -.0034 2 0 2
2.6500 2.6493 .0007 -2 2 0
2.5870 2.5887 -.0017 0 2 2
2.5620 2.5621 -.0001 -1 -1 1
2.5060 2.5097 -.0037 -1 1 2
2.1640 2.1618 .0022 0 1 3
2.1410 2.1399 .0011 -1 3 1
A= 6.839 DA= .001
B= 6.516 DB= .001
C= 7.052 DC= .007
GAMMA=106.64 DGAMMA= .02
BETA = 66.92 DBETA = .02
ALPHA= 79.97 DALPHA= .01
V= 261.9
32. 19-1408
VS4
Triklin
Dexp Dcal d(D) h k l
5.6000 5.5982 .0018 1 1 0
5.1800 5.1676 .0124 0 3 0
3.7700 3.7709 -.0009 -1 3 0
3.1500 3.1508 -.0008 -1 4 0
3.1000 3.1005 -.0005 0 5 0
3.0300 3.0326 -.0026 0 1 1
2.9620 2.9640 -.0020 0 -1 1
2.7000 2.7010 -.0010 1 2 1
2.5470 2.5478 -.0008 1 3 1
2.4730 2.4730 .0000 0 4 1
2.3750 2.3768 -.0018 1 -3 1
2.2160 2.2147 .0013 0 7 0
A= 5.8963 DA= .0002
B= 15.56180 DB= .00004
C= 3.0698 DC= .0001
GAMMA= 86.396 DGAMMA= .004
BETA = 85.643 DBETA = .001
ALPHA= 86.294 DALPHA= .002
V= 279.8
33. 19-1410
ksi-Zn0.28V2O5
Triklin
Dexp Dcal d(D) h k l
6.8900 6.8745 .0155 0 1 0
5.4700 5.4749 -.0049 0 -1 2
3.6200 3.6248 -.0048 1 0 2
3.5700 3.5697 .0003 1 -1 1
3.4400 3.4402 -.0002 1 1 0
3.3200 3.3159 .0041 1 1 1
3.0700 3.0705 -.0005 1 1 2
2.9840 2.9853 -.0013 0 2 2
2.9280 2.9281 -.0001 0 -1 5
2.7150 2.7144 .0006 1 -2 1
2.6230 2.6234 -.0004 -1 -1 4
2.5330 2.5325 .0005 0 0 6
A= 4.1005 DA= .0008
B= 6.947 DB= .001
C= 15.3360 DC= .0003
GAMMA= 93.10 DGAMMA= .01
BETA = 88.82 DBETA = .01
ALPHA= 97.75 DALPHA= .01
V= 432.2
34. 19-1411
VOSO4
Groupa 30,53
Dexp. Dcal. d(D) h k l
4.4200 4.4337 -.0137 0 1 1
4.1200 4.1235 -.0035 1 0 0
3.4400 3.4446 -.0046 1 1 0
3.1300 3.1332 -.0032 0 2 0
2.4940 2.4947 -.0007 1 2 0
2.3180 2.3182 -.0002 1 2 1
2.2160 2.2168 -.0008 0 2 2
1.9820 1.9818 .0002 0 3 1
1.9520 1.9525 -.0005 1 2 2
1.8640 1.8634 .0006 1 3 0
1.6610 1.6609 .0001 2 2 1
1.6030 1.6020 .0010 1 3 2
a= 4.124 b= 6.266 c= 6.274
da= .001 db= .001 dc= .003
V= 162.1
35. 19-1413
VOSO4*H2O
Triklin
Dexp Dcal d(D) h k l
11.5000 11.5109 -.0109 1 0 0
8.0700 8.0614 .0086 0 1 1
7.2200 7.2164 .0036 1 0 1
6.2100 6.2139 -.0039 -1 0 1
5.5200 5.5156 .0044 -1 2 1
4.7500 4.7504 -.0004 2 -1 1
4.4600 4.4609 -.0009 2 1 0
3.6700 3.6697 .0003 -1 0 2
3.5200 3.5200 .0000 1 -1 2
3.2800 3.2796 .0004 -3 0 1
3.1900 3.1904 -.0004 -2 3 2
3.0800 3.0801 -.0001 -1 -1 2
A= 12.285 DA= .001
B= 12.099 DB= .002
C= 8.77502 DC= .00005
GAMMA=108.42 DGAMMA= .02
BETA = 88.02 DBETA = .01
ALPHA= 70.41 DALPHA= .01
V= 1151.3
36. 19-1414
VOSO4*5H2O
Triklin
Dexp Dcal d(D) h k l
5.8100 5.8114 -.0014 -1 1 1
5.2400 5.2414 -.0014 -1 -1 1
4.7500 4.7502 -.0002 -2 0 1
3.7600 3.7580 .0020 1 -2 1
3.6500 3.6501 -.0001 -2 2 1
3.4000 3.3974 .0026 -3 1 1
3.3500 3.3498 .0002 -2 1 2
3.1200 3.1205 -.0005 -2 -1 2
2.9660 2.9644 .0016 -1 2 2
2.8730 2.8729 .0001 0 -3 1
2.7440 2.7457 -.0017 0 3 1
2.6050 2.6053 -.0003 2 -3 1
A= 10.485 DA= .003
B= 9.381 DB= .002
C= 7.6676 DC= .0007
GAMMA=103.19 DGAMMA= .03
BETA =106.44 DBETA = .03
ALPHA= 89.736 DALPHA= .003
V= 702.8
37. 19-1415
VOSO4*4H2O
Triklin
Dexp Dcal d(D) h k l
4.7600 4.7579 .0021 1 0 0
4.7300 4.7369 -.0069 -1 1 1
4.3200 4.3201 -.0001 -1 -1 1
4.1700 4.1671 .0029 -1 2 0
4.0000 3.9987 .0013 1 2 0
3.7400 3.7411 -.0011 0 2 2
3.3200 3.3216 -.0016 -1 4 1
3.1600 3.1602 -.0002 0 5 1
2.9910 2.9909 .0001 -1 -2 2
2.8660 2.8643 .0017 -1 5 1
2.6980 2.6987 -.0007 -1 5 0
2.5830 2.5828 .0002 -1 0 3
A= 5.011 DA= .005
B= 16.289 DB= .008
C= 8.193 DC= .005
GAMMA= 96.45 DGAMMA= .03
BETA =108.10 DBETA = .02
ALPHA= 77.19 DALPHA= .05
V= 619.0
38. 19-1416
VOSO4*3H2O
Triklin
Dexp Dcal d(D) h k l
8.3600 8.3791 -.0191 1 0 0
6.2000 6.2035 -.0035 -1 1 1
5.7100 5.7047 .0053 1 -1 1
5.3500 5.3499 .0001 1 2 0
5.0700 5.0710 -.0010 -1 2 0
4.5000 4.5045 -.0045 1 0 2
4.3300 4.3261 .0039 0 2 2
4.1300 4.1295 .0005 -1 -2 2
4.0600 4.0600 .0000 2 1 0
3.8600 3.8596 .0004 0 0 3
3.6800 3.6820 -.0020 -1 3 1
3.4600 3.4588 .0012 -2 2 0
A=8.461 DA= .007
B=13.308 DB= .007
C= 11.676 DC= .001
GAMMA= 86.70 DGAMMA= .04
BETA = 97.329 DBETA = .002
ALPHA= 91.439 DALPHA= .003
V= 1301
39. 19-1462
Zn{VO3}2
Triklin
Dexp Dcal d(D) h k l
4.3300 4.3310 -.0010 1 0 0
3.2700 3.2695 .0005 -1 1 0
3.0800 3.0792 .0008 -1 -1 2
3.0400 3.0374 .0026 1 -1 2
2.7300 2.7302 -.0002 0 2 2
2.3100 2.3091 .0009 -1 2 0
2.2220 2.2226 -.0006 1 -2 2
2.1710 2.1711 -.0001 -1 -2 3
2.1510 2.1509 .0001 2 0 2
2.1030 2.1032 -.0002 -1 2 2
2.0400 2.0400 .0000 0 0 6
1.9250 1.9249 .0001 1 3 2
A= 4.45758 DA= .00001
B= 6.199 DB= .001
C= 12.4001 DC= .0003
GAMMA= 79.711 DGAMMA= .007
BETA = 80.785 DBETA = .009
ALPHA= 88.329 DALPHA= .004
V= 332.8
40. 19-1468
beta-Zn3{VO4}2
Triklin
Dexp Dcal d(D) h k l
8.5000 8.5142 -.0142 0 1 0
5.3000 5.2954 .0046 -1 0 1
4.2500 4.2562 -.0062 0 -1 2
4.1700 4.1749 -.0049 0 -2 1
3.4500 3.4501 -.0001 1 -2 1
3.1800 3.1791 .0009 -1 1 2
3.1200 3.1193 .0007 1 1 2
3.0700 3.0706 -.0006 -2 0 1
2.9500 2.9473 .0027 0 -1 3
2.8400 2.8381 .0019 0 3 0
2.7800 2.7819 -.0019 0 2 2
2.6700 2.6708 -.0008 0 -2 3
A= 6.4748 DA= .0002
B= 8.6977 DB= .0005
C= 8.9397 DC= .0006
GAMMA= 88.420 DGAMMA= .004
BETA = 92.414 DBETA = .005
ALPHA=101.74 DALPHA= .01
V= 492.4
41. 19-1469
alfa-Zn3{VO4}2
Triklin
Dexp Dcal d(D) h k l
5.8000 5.8056 -.0056 1 1 1
4.7200 4.7190 .0010 2 0 1
4.1300 4.1316 -.0016 1 -1 1
3.3600 3.3590 .0010 3 1 0
3.2900 3.2905 -.0005 2 2 0
3.0300 3.0311 -.0011 3 1 2
2.8800 2.8811 -.0011 -1 -2 1
2.7000 2.7007 -.0007 1 -2 1
2.5600 2.5613 -.0013 4 1 0
2.4900 2.4905 -.0005 -2 2 0
2.4600 2.4581 .0019 4 0 0
2.3700 2.3694 .0006 -2 -1 2
A= 11.00 DA= .02
B= 7.374 DB= .002
C= 7.403 DC= .006
GAMMA= 69.53 DGAMMA= .04
BETA = 69.04 DBETA = .09
ALPHA= 75.82 DALPHA= .03
V= 520.4
42. 19-1470
gamma-Zn3{VO4}2
Triklin
Dexp Dcal d(D) h k l
4.7200 4.7222 -.0022 -1 1 1
4.2100 4.2091 .0009 -2 1 1
4.1300 4.1282 .0018 2 -1 1
3.2500 3.2490 .0010 3 -1 1
3.1800 3.1796 .0004 1 0 2
3.1000 3.0992 .0008 -1 -2 1
3.0000 3.0001 -.0001 -3 -1 1
2.8700 2.8693 .0007 2 -1 2
2.6600 2.6599 .0001 2 2 0
2.6200 2.6202 -.0002 -1 -2 2
2.5600 2.5603 -.0003 2 -2 2
2.4800 2.4804 -.0004 4 0 1
A= 11.9521 DA= .0005
B= 7.393 DB= .002
C= 7.1668 DC= .0006
GAMMA=105.157 DGAMMA= .002
BETA = 97.478 DBETA = .004
ALPHA= 98.57 DALPHA= .01
V= 594.8
43. 19-1471
Zn3{{P0.8V0.2}O4}2
Triklin
Dexp Dcal d(D) h k l
7.7000 7.7070 -.0070 -1 1 0
5.0400 5.0440 -.0040 -1 1 1
4.4400 4.4377 .0023 -1 -1 1
4.0200 4.0190 .0010 -1 3 0
3.9900 3.9902 -.0002 1 2 1
3.8000 3.8001 -.0001 1 3 0
3.6600 3.6678 -.0078 -1 -2 1
3.6300 3.6281 .0019 1 -2 1
3.4300 3.4281 .0019 -2 -1 1
3.2500 3.2513 -.0013 -2 3 0
3.0900 3.0894 .0006 -2 3 1
3.0200 3.0182 .0018 -1 -3 1
A= 9.15 DA= .01
B= 13.214 DB= .003
C= 5.862 DC= .001
GAMMA= 95.05 DGAMMA= .04
BETA = 95.69 DBETA = .03
ALPHA= 79.89 DALPHA= .03
V= 692.3
44. 19-1473
Zn2V2O7
Triklin
Dexp Dcal d(D) h k l
5.3400 5.3435 -.0035 1 0 0
4.7200 4.7199 .0001 0 1 1
4.1700 4.1729 -.0029 0 -1 1
3.4700 3.4719 -.0019 -1 2 0
3.1200 3.1160 .0040 1 2 0
3.0400 3.0420 -.0020 2 0 1
2.7700 2.7693 .0007 0 3 0
2.6600 2.6590 .0010 -1 2 1
2.5800 2.5786 .0014 -1 3 0
2.4900 2.4895 .0005 2 1 2
2.4000 2.4007 -.0007 2 2 1
2.3600 2.3599 .0001 0 2 2
A= 6.097 DA= .002
B= 8.398 DB= .004
C= 5.977 DC= .002
GAMMA= 93.04 DGAMMA= .01
BETA = 61.882 DBETA = .007
ALPHA= 84.56 DALPHA= .03
V= 267.0
45. 19-1474
beta-Zn2V2O7
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
3.2100 3.2103 -.0003 3 1 0
2.6100 2.6100 -.0000 4 1 2
2.4100 2.4101 -.0001 4 1 3
2.2120 2.2123 -.0003 1 2 1
2.1800 2.1799 .0001 4 1 4
2.1320 2.1320 .0000 0 2 2
1.9410 1.9412 -.0002 -4 1 4
1.7840 1.7839 .0001 7 1 2
1.7370 1.7371 -.0001 -6 1 3
1.7070 1.7073 -.0003 8 0 2
1.6640 1.6640 -.0000 5 2 3
1.6100 1.6095 .0005 8 1 1
a=13.772 b=4.5383 c=12.5875 beta= 81.62
da=.006 db=.0001 dc=.0008 dbeta=.02
V= 778
Triklin
Dexp. Dcal. d(D) h k l
3.2100 3.2101 -.0001 3 0 0
2.6100 2.6099 .0001 -1 -2 0
2.4100 2.4076 .0024 4 0 0
2.2120 2.2122 -.0002 -3 -2 0
2.1800 2.1802 -.0002 2 0 1
2.1320 2.1321 -.0001 1 -1 1
1.9410 1.9409 .0001 -4 -2 0
1.7840 1.7840 .0000 -1 -2 1
1.7370 1.7374 -.0004 1 -2 1
1.7070 1.7073 -.0003 5 -1 0
1.6640 1.6639 .0001 -3 1 1
1.6100 1.6100 .0000 4 -1 1
A= 9.804 DA= .001
B= 5.2458 DB= .0004
C= 2.3716 DC= .0004
GAMMA= 79.90 DGAMMA= .01
BETA = 86.69 DBETA = .02
ALPHA= 92.40 DALPHA= .02
V= 119.71
46. 19-1710
C10H10Cl4N6V
Triklin
Dexp Dcal d(D) h k l
5.0000 4.9975 .0025 0 1 1
4.7000 4.7025 -.0025 0 -1 1
4.3500 4.3514 -.0014 -1 1 0
3.9700 3.9753 -.0053 -1 1 1
3.6500 3.6497 .0003 1 -1 1
3.4200 3.4220 -.0020 2 1 1
3.2100 3.2125 -.0025 0 -1 2
2.9800 2.9829 -.0029 1 2 1
2.7100 2.7089 .0011 -2 -2 1
2.5600 2.5596 .0004 -1 0 3
2.4400 2.4419 -.0019 1 -2 1
2.3300 2.3317 -.0017 -2 -2 2
A= 8.455 DA= .004
B= 6.431 DB= .002
C= 7.866 DC= .001
GAMMA= 74.00 DGAMMA= .03
BETA = 95.21 DBETA = .01
ALPHA= 88.013 DALPHA= .005
V= 408.7
47. 19-1747
C20H26N4O19V3*6H2O
Triklin
Dexp Dcal d(D) h k l
6.3200 6.3277 -.0076 1 0 0
5.1500 5.1533 -.0033 0 1 1
4.7200 4.7081 .0119 0 -1 1
4.2700 4.2752 -.0052 1 0 2
3.8600 3.8598 .0002 1 -1 1
3.6700 3.6678 .0022 1 1 1
3.4500 3.4506 -.0006 0 0 4
3.2500 3.2519 -.0019 0 -1 3
2.9200 2.9182 .0018 -2 1 2
2.7300 2.7282 .0018 -1 0 5
2.5900 2.5913 -.0013 -2 0 4
2.4500 2.4500 .0000 -1 2 3
A= 6.52200 DA= .00006
B= 5.37198 DB= .00000
C= 14.25121 DC= .00005
GAMMA= 98.7549 DGAMMA= .0006
BETA =102.1813 DBETA = .0005
ALPHA= 80.6325 DALPHA= .0001
V= 477.9
48. 19-1748
C20H26N4O19V3*8H2O
Triklin
Dexp Dcal d(D) h k l
6.1500 6.1504 -.0004 1 0 0
4.8700 4.8712 -.0012 0 1 0
4.5700 4.5721 -.0021 0 1 1
4.2300 4.2297 .0003 -1 0 1
3.8300 3.8308 -.0008 -1 1 1
2.9800 2.9800 .0000 1 1 2
2.7000 2.7000 -.0000 2 0 2
2.4900 2.4899 .0001 0 2 1
2.2000 2.2001 -.0001 -2 2 0
2.0500 2.0501 -.0001 3 0 0
1.8000 1.8000 -.0000 3 0 3
1.6100 1.6100 .0000 4 -1 1
1.5100 1.5100 .0000 -1 3 3
A= 6.4842 DA= .0002
B= 5.1201 DB= .0007
C= 7.673 DC= .003
GAMMA=102.08 DGAMMA= .02
BETA = 78.70 DBETA = .02
ALPHA= 79.60 DALPHA= .02
V= 237.67