1. 01-0031
V*Cl
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
11.4000 11.3965 .0035 1 0 0
5.6000 5.5988 .0012 1 1 1
5.2000 5.2060 -.0060 2 1 0
4.3000 4.2972 .0028 2 1 1
4.0000 3.9969 .0031 1 3 0
3.6800 3.6799 .0001 0 3 1
3.5000 3.4965 .0035 1 0 2
3.3000 3.3004 -.0004 3 1 1
3.1100 3.1128 -.0028 2 0 2
3.0100 3.0137 -.0037 3 2 1
2.7800 2.7811 -.0011 4 1 0
2.6300 2.6274 .0026 4 1 1
a= 11.403 b=12.804 c= 7.269 beta= 87.99
da=.003 db=.006 dc=.001 dbeta= .02
V= 1060.7
Triklin
Dexp Dcal d(D) h k l
11.4000 11.3981 .0019 0 0 1
5.6000 5.6010 -.0010 -2 0 1
5.2000 5.1978 .0022 2 2 1
4.3000 4.3001 -.0001 1 2 2
4.0000 3.9999 .0001 -2 -1 2
3.6800 3.6796 .0004 4 2 0
3.5000 3.5005 -.0005 -2 2 1
3.3000 3.2993 .0007 5 1 1
3.1100 3.1100 .0000 4 2 3
3.0100 3.0097 .0003 -2 2 2
2.7800 2.7795 .0005 4 3 3
2.6300 2.6301 -.0001 4 -2 2
A= 16.5233 DA= .0009
B= 11.475 DB= .002
C= 11.916 DC= .003
GAMMA= 70.11 DGAMMA= .01
BETA = 73.09 DBETA = .03
ALPHA= 83.34 DALPHA= .02
V= 2032.1
2. 1-0246
NaVO3*H2O
Rombik
Groupa 31,59
Dexp. Dcal. d(D) h k l
7.1000 7.0830 .0170 1 0 2
5.0000 4.9995 .0005 3 0 0
4.2500 4.2450 .0050 3 0 2
3.5400 3.5415 -.0015 2 0 4
3.2400 3.2436 -.0036 3 1 0
3.1300 3.1318 -.0018 3 0 4
3.0100 3.0078 .0022 3 1 2
2.9500 2.9488 .0012 5 0 1
2.8100 2.8103 -.0003 5 0 2
2.6800 2.6785 .0015 0 0 6
2.5300 2.5296 .0004 1 1 5
2.3600 2.3610 -.0010 3 0 6
a=14.999 b= 4.262 c=16.071
da= .005 db= .005 dc= .001
V=1027
3. 1-0312
Na3VO4*16H2O
Triklin
Dexp Dcal d(D) h k l
8.5000 8.4941 .0059 0 1 1
8.0000 7.9995 .0005 1 0 1
7.3000 7.3041 -.0041 0 -1 1
4.6300 4.6300 .0000 -1 2 0
4.2100 4.2100 -.0000 2 0 1
4.0800 4.0793 .0007 -2 1 0
3.8900 3.8899 .0001 1 2 1
3.6900 3.6902 -.0002 -2 1 1
3.0900 3.0900 -.0000 0 3 2
2.9800 2.9799 .0001 -1 -2 2
2.8500 2.8500 -.0000 3 -1 1
2.7500 2.7500 .0000 2 2 3
A= 8.5929 DA= .0005
B= 9.9284 DB= .0006
C= 14.166 DC= .004
GAMMA=101.473 DGAMMA= .008
BETA = 75.234 DBETA = .008
ALPHA= 84.2868 DALPHA= .0008
V= 1130.9
4. 1-323
{VO2}2{SO4}3*16H2O
Triklin
Dexp Dcal d(D) h k l
6.3000 6.2929 .0071 0 1 1
5.8000 5.7939 .0061 -1 0 1
5.4000 5.4019 -.0019 0 -1 1
5.1000 5.0990 .0010 0 2 0
4.5500 4.5503 -.0003 -1 -1 1
4.3500 4.3522 -.0022 -2 1 1
3.9000 3.9003 -.0003 1 2 1
3.7000 3.6995 .0005 -3 1 0
3.5100 3.5098 .0002 0 1 2
3.3000 3.3003 -.0003 1 1 2
3.1600 3.1600 .0000 -3 0 1
3.0400 3.0400 -.0000 1 3 0
A= 11.173 DA= .001
B= 10.6419 DB= .0003
C= 7.1399 DC= .0004
GAMMA=103.816 DGAMMA= .007
BETA = 89.768 DBETA = .003
ALPHA= 81.014 DALPHA= .001
V= 813.5
5. 1-417
MgVO
Triklin
Dexp Dcal d(D) h k l
7.2000 7.1940 .0060 0 0 2
5.4000 5.3972 .0028 -1 1 0
4.7900 4.7876 .0024 1 -1 2
4.1700 4.1709 -.0009 2 1 0
3.9800 3.9841 -.0041 -1 0 3
3.8000 3.8008 -.0008 1 1 3
3.5500 3.5487 .0013 -1 -2 1
3.4000 3.4015 -.0015 -2 1 1
3.2800 3.2795 .0005 2 1 3
3.0700 3.0681 .0019 -2 0 3
2.9700 2.9703 -.0003 -1 -2 3
2.8400 2.8404 -.0004 -2 -2 2
A= 9.387 DA= .004
B= 7.504 DB= .003
C= 14.686 DC= .001
GAMMA= 83.05 DGAMMA= .01
BETA = 81.179 DBETA = .003
ALPHA= 96.28 DALPHA= .02
V= 1006
6. 1-762
NH4VO3
Triklin
Dexp Dcal d(D) h k l
5.9000 5.8978 .0022 1 0 0
4.9200 4.9208 -.0008 -1 1 1
4.1400 4.1406 -.0006 -1 -1 1
3.7800 3.7774 .0026 0 -2 1
3.1700 3.1720 -.0020 -1 -1 2
2.9100 2.9129 -.0029 0 0 3
2.7200 2.7188 .0012 2 0 1
2.6200 2.6214 -.0014 0 -1 3
2.4500 2.4497 .0003 -1 -1 3
2.1200 2.1197 .0003 1 3 3
1.8600 1.8600 .0000 0 5 0
1.7900 1.7900 .0000 0 1 5
A= 5.9591 DA= .0003
B= 9.5871 DB= .0005
C= 9.014 DC= .001
GAMMA= 96.30 DGAMMA= .01
BETA = 96.589 DBETA = .008
ALPHA= 76.8276 DALPHA= .0003
V= 496.2
7. 1-795
KVO3
Triklin
Dexp Dcal d(D) h k l
5.3000 5.3026 -.0026 0 1 1
3.9000 3.8991 .0009 -1 1 1
3.7100 3.7106 -.0006 0 -1 1
3.1100 3.1102 -.0002 -1 2 1
2.8200 2.8196 .0004 -2 2 0
2.6000 2.5993 .0007 -2 1 1
2.4300 2.4310 -.0010 2 1 0
2.3000 2.2988 .0012 -1 0 2
1.9500 1.9502 -.0002 1 3 1
1.8900 1.8897 .0003 -3 2 1
1.7700 1.7700 -.0000 3 1 0
1.6900 1.6895 .0005 -2 4 0
A= 7.19709 DA= .00008
B= 6.967 DB= .001
C= 6.718 DC= .001
GAMMA=106.293 DGAMMA= .007
BETA = 69.177 DBETA = .001
ALPHA= 77.99 DALPHA= .01
V= 283.8
8. 1-0946
Ag4V2O7
Triklin
Dexp Dcal d(D) h k l
4.6000 4.5993 .0007 0 1 1
2.8800 2.8799 .0001 0 -1 1
2.7700 2.7703 -.0003 -1 -1 1
2.5600 2.5593 .0007 0 0 2
2.4900 2.4911 -.0011 -2 -1 1
2.3100 2.3099 .0001 1 2 0
2.1800 2.1819 -.0019 2 2 2
2.0300 2.0292 .0008 -3 1 2
1.9300 1.9313 -.0013 -3 2 1
1.8700 1.8692 .0008 -4 -1 1
1.7800 1.7803 -.0003 4 2 2
1.6900 1.6893 .0007 -4 2 1
A= 9.80 DA= .02
B= 5.231 DB= .003
C= 5.722 DC= .001
GAMMA= 83.96 DGAMMA= .09
BETA = 84.47 DBETA = .06
ALPHA= 63.63 DALPHA= .02
V= 261.0
9. 3-0791
InVO4
Triklin
Dexp Dcal d(D) h k l
4.7700 4.7653 .0047 0 1 1
4.6900 4.6911 -.0011 -1 1 1
4.5500 4.5477 .0023 0 -1 1
4.3500 4.3451 .0049 -1 2 1
4.2800 4.2826 -.0026 -1 -1 1
3.9600 3.9622 -.0022 -2 2 1
3.8700 3.8740 -.0040 1 2 1
3.6100 3.6066 .0034 -2 3 1
3.4700 3.4695 .0005 3 2 0
3.3700 3.3679 .0021 -4 1 0
3.3200 3.3206 -.0006 -4 2 0
3.2100 3.2119 -.0019 -3 3 1
A= 13.536 DA= .006
B= 16.35 DB= .02
C= 4.9058 DC= .0001
GAMMA=104.63 DGAMMA= .04
BETA = 95.12 DBETA = .01
ALPHA= 84.13 DALPHA= .03
V= 1043.3
10. 3-0909
Cu3VS4
Triklin
Dexp Dcal d(D) h k l
5.2000 5.1990 .0010 -1 0 1
4.1500 4.1456 .0044 0 1 0
3.7000 3.6991 .0009 1 0 1
3.1100 3.1086 .0014 -1 -1 1
2.8400 2.8372 .0028 0 -1 2
2.6900 2.6944 -.0044 -1 -1 2
2.4000 2.4005 -.0005 -2 1 0
1.8000 1.8005 -.0005 0 0 4
1.6200 1.6198 .0002 -3 -1 1
1.5000 1.4997 .0003 -2 0 5
1.3500 1.3501 -.0001 -4 1 3
1.3000 1.3000 -.0000 -3 -2 1
A= 5.6805 DA= .0006
B= 4.196 DB= .001
C= 7.6729 DC= .0005
GAMMA= 97.58 DGAMMA= .03
BETA =109.644 DBETA = .002
ALPHA= 91.895 DALPHA= .002
V= 170.2
11. 4-526
{NH4}30V12W44P4O175*106H2O
Triklin
Dexp Dcal d(D) h k l
5.4300 5.4321 -.0021 -1 1 0
4.9700 4.9663 .0037 1 1 1
4.7100 4.7058 .0042 1 -1 1
4.1600 4.1633 -.0033 0 2 0
3.8300 3.8265 .0035 -1 1 1
3.5300 3.5322 -.0022 1 1 2
3.3200 3.3198 .0002 1 -2 1
3.2200 3.2185 .0015 -1 2 1
3.1100 3.1112 -.0012 2 0 0
2.8100 2.8100 .0000 0 3 1
2.7200 2.7191 .0009 2 -2 1
2.5700 2.5694 .0006 2 2 1
2.4400 2.4401 -.0001 -1 2 2
A= 6.864 DA= .004
B= 8.598 DB= .002
C= 7.41 DC= .02
GAMMA= 94.25 DGAMMA= .05
BETA = 66.81 DBETA = .08
ALPHA= 79.07 DALPHA= .04
V= 389.4
12. 4-541
6.5{NH4}*2O*2P2O5*4V2O5*14WO3*28H2O
Triklin
Dexp Dcal d(D) h k l
5.0300 5.0330 -.0030 0 0 1
3.8900 3.8888 .0012 0 -2 1
3.4200 3.4197 .0003 -1 1 0
3.2700 3.2689 .0011 0 -3 1
3.0800 3.0818 -.0018 1 -1 1
2.8600 2.8600 .0000 1 -2 1
2.7600 2.7562 .0038 1 3 1
2.6300 2.6290 .0010 -1 1 1
2.5600 2.5568 .0032 1 -4 0
2.3200 2.3209 -.0009 0 6 1
2.0500 2.0504 -.0004 -1 5 1
1.8100 1.8101 -.0001 -1 7 0
1.6300 1.6302 -.0002 2 3 0
1.4900 1.4901 -.0001 2 -3 2
A= 3.5728 DA= .0004
B= 14.721 DB= .005
C= 5.1967 DC= .0002
GAMMA= 89.86 DGAMMA= .01
BETA = 78.124 DBETA = .002
ALPHA= 81.93 DALPHA= .03
V= 264.7
13. 5-0191
K2O*2UO*V2O5*3H2O
Triklin
Dexp Dcal d(D) h k l
11.1420 11.1525 -.0105 0 1 0
6.4250 6.4229 .0021 0 -1 2
5.0630 5.0632 -.0002 -1 0 1
3.4930 3.4915 .0015 -1 -2 3
3.2080 3.2078 .0002 1 -2 3
3.0920 3.0902 .0018 1 -3 2
2.9980 2.9984 -.0004 1 2 2
2.8220 2.8211 .0009 -2 -1 1
2.7420 2.7421 -.0001 -2 0 1
2.5520 2.5534 -.0014 2 0 2
2.4520 2.4509 .0011 2 1 2
2.3560 2.3556 .0004 1 1 4
A= 5.7208 DA= .0006
B= 12.5528 DB= .0002
C= 12.915 DC= .001
GAMMA= 81.649 DGAMMA= .002
BETA = 93.14 DBETA = .01
ALPHA=116.28 DALPHA= .01
V= 822.7
8-0166
{Fe+2,U,Ca,Zr,Th,Ln}{TiFe=3,V,Cr}3*O
Ñì. U
8-0288
Ca{UO2}2V10O28*16H2O
Ñì.U
8-0293
{U,Fe,V}{Ti,Sn}2O6
Ñì. U
8-0322
U2V6O21*15H2O
Cì. U
8-0323
U2V6O21*15H2O
Ñì. U
14. 8-0329
Ni{VO3}2
Triklin
Dexp Dcal d(D) h k l
3.4900 3.4916 -.0016 -1 1 0
3.3500 3.3518 -.0018 1 1 1
3.2600 3.2577 .0023 1 -1 1
2.9900 2.9907 -.0007 -1 2 0
2.8600 2.8566 .0034 1 -2 1
2.7700 2.7716 -.0016 -1 2 1
2.5200 2.5197 .0003 0 4 1
2.4800 2.4814 -.0014 1 -2 2
2.4400 2.4397 .0003 1 -3 1
2.0600 2.0596 .0004 0 -1 4
1.9100 1.9106 -.0006 1 -3 3
1.8500 1.8499 .0001 2 1 1
1.7400 1.7400 .0000 2 3 0
1.7000 1.7001 -.0001 2 -1 2
A= 3.810 DA= .001
B= 10.8623 DB= .00020
C= 8.30 DC= .02
GAMMA= 85.268 DGAMMA= .009
BETA = 89.50 DBETA = .09
ALPHA= 93.69 DALPHA= .02
V= 341.
15. 10-0055
VO1.8
Triklin
Dexp Dcal d(D) h k l
7.7400 7.7412 -.0012 0 1 0
5.1000 5.0994 .0006 2 1 0
3.9700 3.9715 -.0015 -3 -1 1
3.3600 3.3598 .0002 2 2 0
3.3200 3.3198 .0002 1 2 1
3.2800 3.2819 -.0019 -2 2 1
3.1700 3.1726 -.0026 -4 0 2
3.0800 3.0816 -.0016 2 -1 2
3.0400 3.0395 .0005 2 1 2
2.9000 2.8996 .0004 -3 0 3
2.8600 2.8599 .0001 -2 2 2
2.6700 2.6691 .0009 3 -2 1
A= 14.1565 DA= .0006
B= 7.7436 DB= .0006
C= 9.350 DC= .002
GAMMA= 89.704 DGAMMA= .005
BETA =106.46 DBETA = .03
ALPHA= 91.42 DALPHA= .05
V= 983
16. 10-0196
VO1.86
TRiklin
Dexp Dcal d(D) h k l
5.1500 5.1487 .0013 2 1 0
4.6500 4.6517 -.0017 0 2 0
4.0400 4.0468 -.0068 -3 1 0
3.7400 3.7393 .0007 1 0 1
3.3000 3.2974 .0026 -3 2 0
3.2500 3.2499 .0001 4 0 0
3.0900 3.0904 -.0004 -1 2 1
2.9700 2.9698 .0002 3 1 1
2.7200 2.7201 -.0001 2 3 0
2.7100 2.7106 -.0006 1 -2 1
2.6000 2.5999 .0001 5 0 0
2.5700 2.5696 .0004 -1 -2 1
A= 13.124 DA= .003
B= 9.4760 DB= .0009
C= 3.849 DC= .001
GAMMA= 93.09 DGAMMA= .01
BETA = 83.413 DBETA = .004
ALPHA= 79.94 DALPHA= .02
V= 466.4
17. 10-349
VO1.87
Triklin
Dexp. Dcal. d(D) h k l
4.4400 4.4395 .0005 2 -1 0
3.6600 3.6600 .0000 -1 -3 0
3.2800 3.2823 -.0023 0 2 1
3.1000 3.1000 .0000 -3 -2 0
2.9800 2.9798 .0002 -2 0 1
2.5700 2.5700 .0000 -4 -1 0
2.5600 2.5600 -.0000 4 0 0
2.4930 2.4916 .0014 -3 0 1
2.4390 2.4380 .0010 -3 -1 1
2.4250 2.4260 -.0010 -3 1 1
2.3550 2.3555 -.0005 -2 3 1
2.2570 2.2576 -.0006 -1 4 1
A= 10.335 DA= .001
B= 11.372 DB= .002
C= 3.734 DC= .001
GAMMA= 82.29 DGAMMA= .01
BETA = 88.19 DBETA = .08
ALPHA= 82.63 DALPHA= .08
V= 431.3
18. 11-0003
VO1.75
Triklin
Dexp Dcal d(D) h k l
6.0600 6.0588 .0012 1 1 0
5.1600 5.1601 -.0001 -2 1 1
4.1000 4.1003 -.0003 -2 -1 1
3.7000 3.6988 .0012 -3 1 1
3.3300 3.3295 .0005 -3 0 2
3.2800 3.2796 .0004 0 1 3
3.0600 3.0600 -.0000 -3 -1 1
2.9800 2.9800 .0000 3 1 0
2.8600 2.8600 .0000 -2 -2 2
2.7800 2.7803 -.0003 -1 -2 3
2.7500 2.7493 .0007 -2 3 2
2.7400 2.7396 .0004 1 -2 3
2.4870 2.4865 .0005 -4 1 3
2.4850 2.4848 .0002 4 -1 1
2.4200 2.4202 -.0002 -4 0 3
2.3800 2.3803 -.0003 3 1 2
A= 11.2252 DA= .0001
B= 9.450 DB= .001
C= 11.090 DC= .002
GAMMA=106.13 DGAMMA= .01
BETA =104.753 DBETA = .001
ALPHA= 88.064 DALPHA= .00457
V= 1092.0
19. 11-0004
VO1.84
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.0600 5.0596 .0004 2 0 1
4.8700 4.8592 .0108 0 0 2
3.8400 3.8455 -.0055 -1 2 1
3.3200 3.3191 .0009 2 2 1
3.1900 3.1907 -.0007 -1 0 3
3.0600 3.0601 -.0001 -3 1 2
2.9300 2.9317 -.0017 0 3 0
2.7900 2.7891 .0009 2 0 3
2.6200 2.6210 -.0010 -3 2 2
2.5800 2.5816 -.0016 -4 1 2
2.5300 2.5298 .0002 4 0 2
2.4580 2.4551 -.0029 -2 2 3
a=12.42 b= 8.795 c=9.7436 beta=94.12
da=.01 db=.007 dc=.0007 dbeta=.02
V= 1061.2
Triklin
Dexp Dcal d(D) h k l
5.0600 5.0599 .0001 0 1 2
4.8700 4.8696 .0004 2 1 0
3.8400 3.8394 .0006 3 1 0
3.3200 3.3206 -.0006 -3 0 2
3.1900 3.1897 .0003 2 2 2
3.0600 3.0602 -.0002 2 -2 1
2.9300 2.9299 .0001 5 0 1
2.7900 2.7899 .0001 -4 -1 1
2.6200 2.6199 .0001 -1 -1 3
2.5800 2.5804 -.0004 5 1 2
2.5300 2.5300 .0000 0 2 4
2.4580 2.4578 .0002 6 0 1
A= 14.922 DA= .003
B= 7.8567 DB= .0007
C= 10.839 DC= .003
GAMMA= 95.93 DGAMMA= .03
BETA = 85.02 DBETA = .03
ALPHA= 70.80 DALPHA= .01
V= 1183.4
20. 11-0130
AlVO4
Rombik
Grupa 16
Dexp. Dcal. d(D) h k l
4.4400 4.4411 .0011 0 3 0
3.2700 3.2743 .0043 2 1 0
2.5100 2.5096 -.0004 2 3 1
2.4300 2.4298 -.0002 2 0 2
2.3700 2.3717 .0017 2 4 0
2.3400 2.3365 .0035 1 5 1
2.1200 2.1196 -.0004 0 5 2
1.8660 1.8656 -.0004 3 4 0
1.6890 1.6889 -.0001 4 0 0
1.6290 1.6294 .0004 4 1 1
1.5530 1.5530 .0000 2 0 4
1.4230 1.4233 .0003 3 7 1
1.3980 1.3978 -.0002 4 5 1
a= 6.7557 b= 13.3234 c=6.995
da=.0009 db=.0007 dc=.001
V= 629.6
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
4.4400 4.4310 .0090 2 0 0
3.2700 3.2722 -.0022 2 1 0
2.5100 2.5108 -.0008 3 0 2
2.4300 2.4303 -.0003 1 1 3
2.3700 2.3705 -.0005 -2 0 3
2.3400 2.3404 -.0004 1 2 0
2.1200 2.1201 -.0001 0 2 2
1.8660 1.8655 .0005 4 1 2
1.6890 1.6894 -.0004 3 1 4
1.6290 1.6287 .0003 1 1 5
1.5530 1.5528 .0002 4 2 2
1.4230 1.4230 -.0000 6 0 2
1.3980 1.3972 .0008 -3 2 4
a= 8.8756 b= 4.853 c= 8.731 beta= 86.82
da=.0007 db=.001 dc=.001 dbeta=.01
V= 375.5
Triklin
Dexp Dcal d(D) h k l
4.4400 4.4409 -.0009 -1 0 1
3.2700 3.2699 .0001 -1 -2 1
2.5100 2.5099 .0001 -2 -1 1
2.4300 2.4301 -.0001 -2 -1 2
2.3700 2.3698 .0002 -2 0 1
2.3400 2.3407 -.0007 -1 -3 2
2.1200 2.1203 -.0003 2 2 0
1.8660 1.8660 -.0000 -2 1 2
1.6890 1.6887 .0003 0 -4 2
1.6290 1.6291 -.0001 1 1 4
1.5530 1.5530 .0000 1 -3 4
1.4230 1.4232 -.0002 -1 -5 3
1.3980 1.3980 .0000 1 3 3
A= 5.027 DA= .004
B= 7.125 DB= .001
C= 9.417 DC= .001
GAMMA= 71.450 DGAMMA= .001
BETA =106.77 DBETA = .04
ALPHA=115.44 DALPHA= .01
V= 284.2
21. 11-209
VO{OH}2
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
6.1000 5.4006 .0094 0 1 0
5.1000 5.0976 .0024 0 0 1
4.3200 4.3104 .0096 -2 0 1
3.5800 3.5753 .0047 -2 1 1
3.2000 3.2003 -.0003 0 2 0
2.9300 2.9328 -.0028 4 1 0
2.6400 2.6396 .0004 5 0 0
2.4500 2.4492 .0008 2 2 1
2.2300 2.2302 -.0002 5 0 1
2.0000 2.0013 -.0013 -1 2 2
1.9200 1.9197 .0003 3 3 0
1.8300 1.8297 .0003 5 2 1
a= 13.31 b= 6.4006 c= 5.1406 beta= 97.36
da=.03 db=.0005 dc=.0001 dbeta=.01
V= 434.2
Triklin
Dexp Dcal d(D) h k l
6.4100 6.4091 .0009 1 0 0
5.1000 5.0998 .0002 1 1 0
4.3200 4.3195 .0005 1 -1 1
3.5800 3.5797 .0003 -1 -2 1
3.2000 3.1986 .0014 0 -2 2
2.9300 2.9307 -.0007 0 2 1
2.6400 2.6400 .0000 -2 -2 1
2.4500 2.4500 .0000 1 -3 1
2.2300 2.2313 -.0013 1 -1 3
2.0000 2.0000 .0000 2 -3 1
1.9200 1.9198 .0002 -1 1 3
1.8300 1.8297 .0003 0 -2 4
A= 6.4422 DA= .0007
B= 8.296 DB= .006
C= 7.3673 DC= .0006
GAMMA= 84.79 DGAMMA= .03
BETA = 94.304 DBETA = .001
ALPHA=111.57 DALPHA= .01
V= 364.3
22. 11-210
V3O5{OH}4
Triklin
Dexp Dcal d(D) h k l
5.5400 5.5356 .0044 0 1 1
4.4600 4.4578 .0022 0 -1 1
3.9700 3.9686 .0014 -1 1 0
3.4600 3.4592 .0008 -1 1 1
3.2300 3.2311 -.0011 0 -2 0
3.1400 3.1400 .0000 2 1 0
2.7900 2.7894 .0006 1 -1 2
2.5000 2.4999 .0001 -1 2 1
2.2500 2.2503 -.0003 2 -1 2
2.1500 2.1499 .0001 3 2 2
2.0900 2.0901 -.0001 -1 1 3
1.9800 1.9800 .0000 -1 -1 3
A= 6.8475 DA= .0009
B= 7.05630 DB= .00008
C= 8.240 DC= .005
GAMMA= 69.71 DGAMMA= .02
BETA = 69.83 DBETA = .03
ALPHA= 71.97 DALPHA= .03
V= 342.2
23. 11-288
Zn3{VO4}2
Triklin
Dexp Dcal d(D) h k l
5.8100 5.8093 .0007 1 0 1
4.7600 4.7532 .0068 0 1 1
3.9100 3.9081 .0019 0 -1 1
3.3900 3.3886 .0014 -1 1 0
3.3100 3.3090 .0010 -1 -1 1
3.0700 3.0641 .0059 1 1 3
2.9100 2.9099 .0001 0 -1 2
2.7200 2.7206 -.0006 0 1 3
2.5900 2.5895 .0005 -1 1 2
2.5300 2.5299 .0001 0 2 1
2.4900 2.4896 .0004 2 0 3
2.1000 2.1004 -.0004 -1 2 0
1.9440 1.9443 -.0003 3 2 3
1.8820 1.8825 -.0005 1 1 5
A= 6.626 DA= .001
B= 5.41335 DB= .00003
C= 9.517 DC= .001
GAMMA= 69.587 DGAMMA= .007
BETA = 65.58 DBETA = .01
ALPHA= 70.530 DALPHA= .00529
V= 284.1
24. 11-297
{NH4}2{UO2}2V2O8
Rombik
Groupa 32,55
Dexp. Dcal. d(D) h k l
6.6100 6.6011 .0089 2 0 0
4.1900 4.1881 .0019 0 0 1
3.5340 3.5364 -.0024 2 0 1
3.3140 3.3117 .0023 2 1 1
3.2200 3.2192 .0008 3 2 0
3.1320 3.1331 -.0011 0 2 1
3.1150 3.1157 -.0007 4 1 0
a=13.202 b= 9.443 c= 4.1881
da= .003 db=.001344 dc=.0001
V= 522.1
25. 11-476
CaSrV2O7*3H2O
Triklin
Dexp Dcal d(D) h k l
8.3000 8.3110 -.0110 0 1 1
7.7100 7.6954 .0146 0 -1 1
7.2000 7.1924 .0076 1 0 0
6.5000 6.4860 .0140 -1 -1 1
6.2000 6.1951 .0049 1 1 1
4.9500 4.9451 .0049 1 1 2
4.7400 4.7422 -.0022 0 2 0
4.4000 4.3977 .0023 -1 1 2
3.5500 3.5502 -.0002 0 1 4
3.4500 3.4504 -.0004 -1 2 0
3.3500 3.3504 -.0004 1 3 0
3.2700 3.2707 -.0007 2 1 2
A= 7.702 DA= .004
B= 10.113 DB= .002
C= 14.9321 DC= .0004
GAMMA= 70.26 DGAMMA= .01
BETA = 95.88 DBETA = .01
ALPHA= 87.452 DALPHA= .007
V= 1085.0
26. 11-0673
V2O5*H2O
Triklin
Dexp Dcal d(D) h k l
5.7800 5.7777 .0023 -1 1 1
5.0200 5.0293 -.0093 0 -1 1
4.4600 4.4676 -.0076 1 -1 1
4.2900 4.2899 .0001 -2 1 1
3.8100 3.8129 -.0029 -2 2 1
3.5600 3.5608 -.0008 2 1 0
3.2300 3.2282 .0018 -1 0 2
3.0300 3.0279 .0021 2 -2 1
2.8920 2.8936 -.0016 1 0 2
2.7670 2.7660 .0010 1 1 2
2.6590 2.6590 .0000 1 3 0
2.5800 2.5800 .0000 -2 -2 1
A= 9.625 DA= .001
B= 10.0366 DB= .0003
C= 6.7167 DC= .0002
GAMMA=111.180 DGAMMA= .001
BETA =103.011 DBETA = .002
ALPHA= 78.6809 DALPHA= .0009
V= 584.8