1. 31-0073
{NH4}2{UO2}2{+OH}2{NO3}4*H2O
Triklin
Dexp Dcal d(D) h k l
8.5000 8.5047 -.0047 0 1 1
8.1200 8.1274 -.0074 0 -1 1
7.6500 7.6578 -.0078 -1 1 1
6.2500 6.2533 -.0033 1 0 1
6.1300 6.1337 -.0037 0 2 0
4.8100 4.8142 -.0042 -2 1 1
4.5400 4.5374 .0026 -2 1 0
4.4900 4.4874 .0026 1 -2 1
4.3300 4.3276 .0024 -2 1 2
4.1300 4.1303 -.0003 -2 2 1
3.9300 3.9314 -.0014 -2 2 0
3.8300 3.8289 .0011 -2 2 2
A= 10.005 DA= .001
B= 12.389 DB= .001
C= 12.025 DC= .004
GAMMA= 97.59 DGAMMA= .02
BETA =109.90 DBETA = .02
ALPHA= 84.9962 DALPHA= .0006
V= 1388
2. 31-0074
{NH4}2{UO2}4O2{OH}2Cl4*2H2O
Triklin
Dexp Dcal d(D) h k l
10.1000 10.0992 .0008 1 1 1
9.4700 9.4728 -.0028 1 1 0
6.5500 6.5502 -.0002 1 -1 1
6.0200 6.0158 .0042 -1 1 1
5.5700 5.5706 -.0006 0 -2 1
5.3400 5.3410 -.0010 2 2 1
4.7400 4.7364 .0036 2 2 0
4.3500 4.3487 .0013 0 3 2
4.2700 4.2689 .0011 -1 -1 2
3.8400 3.8398 .0002 -1 3 1
3.7380 3.7368 .0012 3 2 2
3.4400 3.4402 -.0002 -1 3 2
A= 11.361 DA= .008
B= 16.109 DB= .002
C= 13.74 DC= .01
GAMMA= 67.58 DGAMMA= .03
BETA = 65.74 DBETA = .05
ALPHA= 67.85 DALPHA= .02
V= 2045
3. 31-0175
Ba2UO2{PO4}2
Triklin
Dexp Dcal d(D) h k l
6.8500 6.8407 .0093 0 1 1
6.2000 6.1982 .0018 -1 1 1
5.5300 5.5307 -.0007 0 -1 1
5.1800 5.1841 -.0041 2 0 0
4.3100 4.3129 -.0029 0 2 0
4.1800 4.1798 .0002 2 1 0
4.0500 4.0499 .0001 -1 0 2
3.6800 3.6812 -.0012 -2 -1 1
3.5000 3.4983 .0017 -2 1 2
3.4200 3.4203 -.0003 0 2 2
3.3500 3.3515 -.0015 -1 -1 2
3.3100 3.3120 -.0020 -3 1 1
A= 10.529 DA= .001
B= 8.942 DB= .003
C= 8.811 DC= .003
GAMMA= 99.43 DGAMMA= .02
BETA = 95.39 DBETA = .03
ALPHA= 77.23 DALPHA= .01
V= 796.7
4. 31-0388
Cs10U{PW11O39}2*20H2O
Triklin
Dexp Dcal d(D) h k l
5.7500 5.7548 -.0048 -1 1 1
5.4000 5.4001 -.0001 1 1 0
4.7900 4.7860 .0040 -1 -1 1
4.0700 4.0701 -.0001 1 2 0
3.6900 3.6930 -.0030 -1 1 2
3.5800 3.5779 .0021 -1 0 2
3.4500 3.4494 .0006 -2 0 1
3.4100 3.4089 .0011 -2 1 1
3.3400 3.3378 .0022 0 1 2
3.2500 3.2514 -.0014 0 0 2
3.1700 3.1711 -.0011 -2 -1 1
3.1000 3.1000 .0000 1 -3 0
A= 6.955 DA= .004
B= 11.102 DB= .002
C= 7.450 DC= .003
GAMMA= 96.52 DGAMMA= .01
BETA =116.09 DBETA = .03
ALPHA= 74.92 DALPHA= .003
V= 498.9
5. 31-0389
Cs2{UO2}2{OH}2{NO3}4*H2O
Triklin
Dexp Dcal d(D) h k l
8.6700 8.6620 .0080 1 0 0
8.3000 8.2966 .0034 0 1 0
6.9700 6.9655 .0045 0 -1 2
6.8300 6.8324 -.0024 1 -1 1
5.8500 5.8587 -.0087 0 1 2
5.2000 5.1991 .0009 1 1 1
4.7600 4.7568 .0032 0 1 3
4.2000 4.2060 -.0060 -2 1 0
3.9600 3.9618 -.0018 -2 1 1
3.7800 3.7788 .0012 1 -1 5
3.6300 3.6258 .0042 -2 1 2
3.5700 3.5697 .0003 1 1 4
A= 8.942 DA= .003
B= 8.649 DB= .001
C= 20.183 DC= .007
GAMMA=103.08 DGAMMA= .03
BETA = 81.634 DBETA = .009
ALPHA=101.569 DALPHA= .001
V= 1481.4
6. 31-0390
{UO2}4O2Cl8
Triklin
Dexp Dcal d(D) h k l
10.5000 10.5040 .0040 1 0 0
8.5900 8.5683 .0217 0 1 0
7.8300 7.8235 .0065 0 1 1
6.1700 6.1878 -.0178 -1 1 0
5.8300 5.8260 .0040 -1 1 1
5.7300 5.7384 -.0084 0 -1 1
5.0800 5.0684 .0116 0 0 2
4.7400 4.7420 -.0020 2 1 1
4.2800 4.2842 -.0042 0 2 0
3.8700 3.8708 -.0008 -1 2 1
3.7100 3.7095 .0005 2 0 2
3.5300 3.5319 -.0019 0 1 3
A= 10.671 DA= .002
B= 9.134 DB= .005
C= 10.682 DC= .006
GAMMA= 80.04 DGAMMA= .02
BETA = 85.10 DBETA = .02
ALPHA= 71.720 DALPHA= .005
V= 973.1
7. 31-0769
Li2U2O5Cl4
Triklin
Dexp Dcal d(D) h k l
8.5700 8.5812 -.0112 0 1 1
8.0600 8.0486 .0114 1 1 0
7.5600 7.5401 .0199 0 -1 1
7.2400 7.2366 .0034 1 1 1
6.4700 6.4657 .0043 -1 1 0
5.6300 5.6265 .0035 1 -1 1
4.8800 4.8764 .0036 1 2 1
4.7800 4.7845 -.0045 -1 1 2
4.6700 4.6625 .0075 -2 0 1
4.2100 4.2119 -.0019 0 1 3
4.0100 4.0092 .0008 -2 1 1
3.8000 3.8019 -.0019 -2 -1 2
A= 10.279 DA= .008
B= 10.481 DB= .008
C= 13.203 DC= .006
GAMMA= 77.35 DGAMMA= .06
BETA = 87.59 DBETA = .06
ALPHA= 82.03 DALPHA= .03
V= 1374.2
8. 31-0770
L2UO2Cl4
Triklin
Dexp Dcal d(D) h k l
6.3800 6.3831 -.0031 1 -1 1
5.9700 5.9690 .0010 1 1 0
5.6200 5.6209 -.0009 1 -1 2
5.5100 5.5143 -.0043 -1 -1 1
5.4200 5.4095 .0105 1 1 1
4.8200 4.8165 .0035 -1 1 1
4.7400 4.7477 -.0077 2 1 1
4.3100 4.3130 -.0030 3 -1 2
4.1700 4.1664 .0036 0 -1 3
4.1300 4.1284 .0016 -2 0 2
3.9100 3.9080 .0020 4 0 2
3.8600 3.8631 -.0031 -1 0 3
A= 15.821 DA= .001
B= 6.74238 DB= .00005
C= 15.3369 DC= .0003
GAMMA= 95.509 DGAMMA= .001
BETA = 64.732 DBETA = .004
ALPHA=103.821 DALPHA= .002
V= 1436.5
9. 31-0841
MnUO3O10
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.1100 5.1054 .0046 2 1 0
4.7000 4.7006 -.0006 0 2 1
4.1300 4.1295 .0005 2 1 1
3.4700 3.4698 .0002 2 0 2
3.3500 3.3495 .0005 1 0 3
3.3000 3.3021 -.0021 3 0 1
3.2700 3.2692 .0008 1 3 0
2.8000 2.8003 -.0003 1 2 3
2.5600 2.5598 .0002 -3 3 3
2.4200 2.4196 .0004 3 2 2
2.3500 2.3503 -.0003 0 4 2
2.0600 2.0600 -.0000 -5 1 6
a= 13.414 b=10.208 c= 13.725 beta= 118.470
da=.001 db=.003 dc=.001 dbeta=.004
V= 1652
Triklin
Dexp Dcal d(D) h k l
5.1100 5.1171 -.0071 0 1 1
4.7000 4.7020 -.0020 0 -1 1
4.1300 4.1273 .0027 -1 0 2
3.4700 3.4715 -.0015 -1 1 2
3.3500 3.3506 -.0006 1 1 0
3.3000 3.2963 .0037 0 -1 3
3.2700 3.2700 .0000 -1 -1 1
2.8000 2.8007 -.0007 -1 1 4
2.5600 2.5586 .0014 0 2 2
2.4200 2.4204 -.0004 1 1 4
2.3500 2.3510 -.0010 0 -2 2
2.0600 2.0600 -.0000 -2 -1 1
A= 4.674 DA= .003
B= 5.28060 DB= .00009
C= 14.45 DC= .01
GAMMA= 94.836 DGAMMA= .09
BETA = 98.20 DBETA = .08
ALPHA= 81.932 DALPHA= .001
V= 349.0
10. 31-0918
Ni{UO2{SO4}2}*4H2O
Triklin
Dexp Dcal d(D) h k l
8.3300 8.3268 .0032 1 0 0
7.0200 7.0172 .0028 1 1 0
6.7600 6.7561 .0039 1 -1 1
6.7000 6.6995 .0005 -1 -1 1
6.4200 6.4221 -.0021 0 -2 1
5.8800 5.8803 -.0003 1 0 2
5.2700 5.2702 -.0002 0 0 3
5.0600 5.0605 -.0005 1 -2 1
4.6200 4.6202 -.0002 1 -1 3
4.1500 4.1499 .0001 0 3 0
4.0600 4.0598 .0002 -1 -2 3
3.9000 3.9004 -.0004 -2 -1 1
A= 8.33815 DA= .00005
B= 12.9455 DB= .0003
C= 16.453 DC= .0012
GAMMA= 89.064 DGAMMA= .005
BETA = 87.534 DBETA = .007
ALPHA=105.831 DALPHA= .009
V= 1706.5
11. 31-1121
K2U{WO4}4
Triklin
Dexp Dcal d(D) h k l
13.6000 13.5596 .0404 1 0 0
7.0400 7.0521 -.0121 1 1 0
6.7700 6.7614 .0086 -1 0 1
5.1400 5.1410 -.0010 2 1 0
4.9200 4.9217 -.0017 0 -1 1
4.1400 4.1455 -.0055 -3 1 1
3.8800 3.8795 .0005 3 1 0
3.3800 3.3807 -.0007 -2 0 2
3.2700 3.2703 -.0003 -3 2 0
3.2400 3.2400 -.0000 1 -2 1
3.1800 3.1795 .0005 1 0 2
3.0800 3.0796 .0004 -3 0 2
2.9700 2.9699 .0001 2 -2 1
2.9430 2.9430 .0000 -4 -1 1
2.8460 2.8455 .0005 -2 3 1
2.8100 2.8101 -.0001 2 1 2
A= 14.014 DA= .009
B= 8.961 DB= .003
C= 7.2569 DC= .0009
GAMMA= 97.72 DGAMMA= .03
BETA =103.9 DBETA = .1
ALPHA= 76.55 DALPHA= .08
V= 857.6
12. 31-1122
K2{UO2}2{OH}2{NO3}4*H2O
Triklin
Dexp Dcal d(D) h k l
10.7000 10.6801 .0199 1 0 0
9.5700 9.5782 -.0082 1 1 0
8.1200 8.1295 -.0095 0 0 1
7.5000 7.5114 -.0114 1 2 0
7.3500 7.3479 .0021 0 -1 1
6.8600 6.8597 .0003 -1 0 1
6.4000 6.3979 .0021 -1 -1 1
6.1300 6.1311 -.0011 0 -2 1
5.8700 5.8756 -.0056 -1 2 1
5.5000 5.4962 .0038 0 3 1
5.0400 5.0396 .0004 0 -3 1
4.7200 4.7190 .0010 -2 0 1
A= 10.7523 DA= .0005
B= 20.7310 DB= .0003
C= 8.2138 DC= .0001
GAMMA= 89.236 DGAMMA= .002
BETA = 96.514 DBETA = .005
ALPHA= 85.09456 DALPHA= .00002
V= 1812.0
13. 31-1123
K2{UO2}4O2{OH}2Br4*2H2O
Triklin
Dexp Dcal d(D) h k l
10.3000 10.2890 .0110 0 0 1
9.7600 9.7785 -.0185 1 1 0
6.4300 6.4313 -.0013 0 -2 1
5.9200 5.9301 -.0101 -1 -2 1
5.5700 5.5636 .0064 2 0 1
5.1900 5.1934 -.0034 2 1 1
4.9000 4.9028 -.0028 0 -2 2
4.6600 4.6624 -.0024 0 2 1
4.4400 4.4379 .0021 0 -3 1
4.2600 4.2598 .0002 0 1 2
4.0400 4.0412 -.0012 2 -2 1
3.8430 3.8420 .0010 3 1 1
A= 11.994 DA= .003
B= 13.592 DB= .009
C= 11.1065 DC= .0009
GAMMA= 78.87 DGAMMA= .01
BETA = 81.57 DBETA = .01
ALPHA=108.18 DALPHA= .02
V= 1645
14. 31-1125
K2{UO2}4O2{OH}2Cl4*2H2O
Triklin
Dexp Dcal d(D) h k l
10.2000 10.2083 -.0083 1 1 0
9.4500 9.4510 -.0010 0 0 1
6.3700 6.3736 -.0036 0 -2 1
5.8700 5.8681 .0019 1 -1 1
5.5400 5.5445 -.0045 1 3 0
5.0700 5.0767 -.0067 0 3 1
4.7500 4.7502 -.0002 -1 -1 2
4.6000 4.5993 .0007 0 1 2
4.3600 4.3579 .0021 2 0 1
4.2200 4.2209 -.0009 0 2 2
3.9690 3.9684 .0006 0 -4 1
3.8170 3.8171 -.0001 -1 -3 2
A= 12.019 DA= .007
B= 17.87 DB= .01
C= 9.8756 DC= .0005
GAMMA= 82.84 DGAMMA= .05
BETA =106.791 DBETA = .003
ALPHA= 90.496 DALPHA= .007
V= 2014
15. 31-1126
K2U2O5O{NO3}2
Triklin
Dexp Dcal d(D) h k l
9.0800 9.0752 .0048 1 0 0
7.0600 7.0551 .0049 1 1 1
6.1900 6.1855 .0045 1 -1 1
4.5000 4.4992 .0008 2 1 0
4.2100 4.2102 -.0002 1 3 1
3.8300 3.8299 .0001 -2 0 1
3.6000 3.6004 -.0004 -2 1 1
3.5300 3.5277 .0023 1 3 2
3.4700 3.4718 -.0018 -2 0 5
3.2300 3.2309 -.0009 0 1 3
3.0900 3.0886 .0014 -2 -3 1
3.0700 3.0703 -.0003 -1 -4 1
A= 9.3887 DA= .0001
B= 13.9264 DB= .0004
C= 10.0993 DC= .0002
GAMMA= 81.159 DGAMMA= .001
BETA = 77.4543 DBETA = .0002
ALPHA= 85.1282 DALPHA= .0004
V= 1271.8
16. 31-1127
K2U2O5{NO3}4
Triklin
Dexp Dcal d(D) h k l
6.0700 6.0678 .0022 1 1 0
5.3300 5.3304 -.0004 0 2 1
4.7800 4.7800 -.0000 0 4 0
4.5800 4.5799 .0001 1 3 0
4.0400 4.0434 -.0034 -1 -1 1
3.9300 3.9313 -.0013 -1 2 1
3.7500 3.7548 -.0048 -1 -2 1
3.0600 3.0590 .0010 -1 -4 1
2.9600 2.9602 -.0002 -2 2 0
2.8600 2.8602 -.0002 2 1 1
2.7200 2.7193 .0007 -2 0 1
2.6000 2.6001 -.0001 -2 -2 1
A= 6.3283 DA= .0001
B= 19.2978 DB= .0005
C= 5.958 DC= .001
GAMMA= 87.203 DGAMMA= .004
BETA = 86.44 DBETA = .01
ALPHA= 82.59 DALPHA= .01
V= 719.4
17. 31-1411
UF2{SO3F}3
Triklin
Dexp Dcal d(D) h k l
8.6600 8.6629 -.0029 1 0 0
7.5300 7.5367 -.0067 1 1 1
5.7300 5.7256 .0044 -1 -1 1
5.4100 5.4095 .0005 -1 1 0
5.1500 5.1457 .0043 0 0 2
4.7700 4.7641 .0059 2 1 1
4.3300 4.3314 -.0014 2 0 0
4.1700 4.1707 -.0007 1 2 2
3.9100 3.9139 -.0039 -1 -1 2
3.7500 3.7475 .0025 0 2 2
3.5200 3.5181 .0019 -2 -2 1
3.3600 3.3596 .0004 2 -1 1
3.2600 3.2596 .0004 -1 -2 2
A= 9.755 DA= .008
B= 10.648 DB= .009
C= 10.703 DC= .009
GAMMA= 64.24 DGAMMA= .06
BETA = 75.96 DBETA = .05
ALPHA= 77.23 DALPHA= .05
V= 963
18. 31-1412
UF3{SO3F}2
Triklin
Dexp Dcal d(D) h k l
6.3200 6.3109 .0091 1 2 0
6.1000 6.0952 .0048 -2 1 0
5.2100 5.2103 -.0003 0 3 0
5.0300 5.0309 -.0009 -1 3 0
4.6200 4.6232 -.0032 1 3 0
4.2000 4.1955 .0045 3 0 0
3.9100 3.9078 .0022 0 4 0
3.7450 3.7452 -.0002 0 -2 1
3.5120 3.5129 -.0009 -2 4 0
3.1730 3.1727 .0003 -3 0 1
3.1180 3.1183 -.0003 -3 1 1
3.0150 3.0159 -.0009 4 1 0
A= 12.8165 DA= .0004
B= 15.7929 DB= .0004
C= 4.1123 DC= .0006
GAMMA= 96.089 DGAMMA= .003
BETA = 98.47 DBETA = .01
ALPHA= 94.55 DALPHA= .02
V= 814.9
19. 31-1414
U3NbO9.8
Triklin
Dexp Dcal d(D) h k l
6.4100 6.4152 -.0052 1 0 0
4.8100 4.8101 -.0001 -1 1 0
4.0000 4.0002 -.0002 -1 0 1
3.2120 3.2106 .0014 0 1 2
3.1900 3.1936 -.0036 2 -1 1
2.9280 2.9271 .0009 1 2 0
2.5100 2.5109 -.0009 -1 -2 1
2.3130 2.3123 .0007 3 0 2
2.0450 2.0450 .0000 1 -2 3
1.9950 1.9953 -.0003 2 2 3
1.8680 1.8679 .0001 2 3 1
1.8500 1.8499 .0001 2 -3 2
A= 7.080 DA= .001
B= 6.8009 DB= .0003
C= 7.846 DC= .002
GAMMA= 92.65 DGAMMA= .02
BETA = 65.21 DBETA = .01
ALPHA= 88.79 DALPHA= .02
V= 342.3
20. 31-1432
4UO3*HCl*8H2O
Triklin
Dexp Dcal d(D) h k l
14.9000 14.9211 -.0211 -1 1 0
13.2000 13.1417 .0583 1 1 0
11.6000 11.6083 -.0083 0 1 1
7.5000 7.4984 .0016 -1 2 1
7.4600 7.4605 -.0005 -2 2 0
7.3700 7.3683 .0017 -1 3 0
7.3400 7.3400 .0000 0 0 2
7.3100 7.3108 -.0008 0 -1 2
6.7100 6.7086 .0014 0 1 2
6.5700 6.5708 -.0008 2 2 0
6.5100 6.5105 -.0005 -2 -1 1
6.4000 6.4016 -.0016 0 3 1
A= 18.366 DA= .005
B= 23.529 DB= .005
C= 15.378 DC= .001
GAMMA= 99.944 DGAMMA= .009
BETA = 74.844 DBETA = .003
ALPHA=100.700 DALPHA= .03
V= 6250
21. 31-1433
{UO2}2P2O7
Triklin
Dexp Dcal d(D) h k l
12.6000 12.6046 -.0046 1 0 0
10.5000 10.5130 -.0130 0 1 0
6.2300 6.2322 -.0022 0 -1 2
5.7100 5.7125 -.0025 0 0 2
5.1800 5.1806 -.0006 2 -1 1
4.7900 4.7889 .0011 -1 0 2
4.5290 4.5286 .0004 1 1 2
4.2910 4.2910 .0000 3 0 1
3.8180 3.8177 .0003 1 -2 3
3.3260 3.3260 .0000 -1 -3 3
3.2430 3.2430 .0000 2 1 3
2.9980 2.9980 .0000 2 -1 4
A= 13.325 DA= .004
B= 11.881 DB= .001
C= 12.693 DC= .002
GAMMA= 77.0208 DGAMMA= .0003
BETA = 82.38 DBETA = .03
ALPHA=112.01 DALPHA= .02
V= 1762.4
22. 31-1434
{U,Fe,V}{Ti,Sn}2O6
Groupa 31,59
Dexp. Dcal. d(D) h k l
3.1200 3.1222 -.0022 1 1 1
2.8700 2.8667 .0033 3 0 0
2.6700 2.6724 -.0024 3 1 0
2.5200 2.5191 .0009 1 2 1
2.2800 2.2797 .0003 3 0 1
2.1500 2.1500 .0000 4 0 0
a= 8.600 b= 7.386 c= 3.760
da= .001 db= .007 dc= .001
v= 238.8
23. 31-1532
C13H18N6O9U
Triklin
Dexp Dcal d(D) h k l
9.5200 9.5169 .0031 1 0 0
7.7100 7.6991 .0109 0 1 0
6.6300 6.6220 .0080 0 1 1
6.0000 6.0013 -.0013 -1 0 1
5.4200 5.4154 .0046 -1 1 0
4.4100 4.4087 .0013 2 1 1
4.2200 4.2193 .0007 2 0 1
4.0000 4.0012 -.0012 -2 0 1
3.8200 3.8207 -.0007 1 0 2
3.6900 3.6908 -.0008 -2 1 0
3.5500 3.5485 .0015 -1 1 2
3.3100 3.3110 -.0010 0 2 2
A= 9.8619 DA= .0005
B= 8.3164 DB= .0004
C= 8.56267 DC= .00001
GAMMA= 75.202 DGAMMA= .007
BETA = 82.233 DBETA = .006
ALPHA= 71.903 DALPHA= .009
V= 644.1
24. 31-1533
C12H18F2N6O6U
Triklin
Dexp Dcal d(D) h k l
9.5200 9.4945 .0255 0 1 0
7.6300 7.6284 .0016 -1 0 1
6.6200 6.6062 .0138 0 -1 2
5.9000 5.8997 .0003 1 -1 1
5.4300 5.4248 .0052 -1 1 1
4.4000 4.4080 -.0080 -1 -1 3
4.1900 4.1917 -.0017 -2 0 1
3.9500 3.9500 -.0000 0 -2 3
3.8100 3.8093 .0007 -2 1 0
3.7000 3.7021 -.0021 -1 2 1
3.5000 3.4996 .0004 -1 -1 4
3.3000 3.3031 -.0031 0 -2 4
A= 8.56961 DA= .00003
B= 9.9897 DB= .0001
C= 14.6063 DC= .0008
GAMMA= 85.192 DGAMMA= .001
BETA = 97.744 DBETA = .001
ALPHA=107.945 DALPHA= .002
V= 1177.6
25. 31-1534
H18N6O10U
Triklin
Dexp Dcal d(D) h k l
9.6000 9.5646 .0354 1 0 0
7.6000 7.6101 -.0101 -1 1 0
6.7000 6.7116 -.0116 -1 0 1
5.9000 5.9005 -.0005 1 1 0
5.4000 5.4015 -.0015 1 -1 1
4.4000 4.4036 -.0036 -2 1 1
4.2000 4.2043 -.0043 0 2 1
4.1000 4.1024 -.0024 -1 0 2
3.8200 3.8176 .0024 0 -1 2
3.6800 3.6766 .0034 -2 2 1
3.5500 3.5493 .0007 1 1 2
3.3300 3.3313 -.0013 2 -2 1
A= 9.925 DA= .01
B= 9.464 DB= .003
C= 8.860 DC= .004
GAMMA=104.95 DGAMMA= .07
BETA = 95.65 DBETA = .01
ALPHA= 83.41 DALPHA= .04
V= 797.2
26. 31-1634
C15H15ClU
Groupa 26,28,51
Dexp. Dcal. d(D) h k l
6.8600 6.8625 -.0025 1 1 0
6.1700 6.1444 .0256 1 1 1
5.7200 5.7182 .0018 2 0 1
4.8700 4.8651 .0049 1 1 2
4.3100 4.3187 -.0087 1 0 3
4.1100 4.0959 .0141 0 2 0
4.0100 4.0082 .0018 3 0 1
3.8200 3.8203 -.0003 1 1 3
3.7200 3.7110 .0090 2 0 3
3.5200 3.5219 -.0019 0 2 2
3.3260 3.3261 -.0001 1 0 4
3.2780 3.2808 -.0028 3 1 2
2.3530 2.3540 -.0010 2 3 2
a=12.566570 b= 8.191838 c=13.796560
da= .010568 db= .016725 dc= .005202
V=1420
Triklin
Dexp Dcal d(D) h k l
6.8600 6.8649 -.0049 0 1 1
6.1700 6.1642 .0058 0 -1 1
5.7200 5.7195 .0005 -1 1 1
4.8700 4.8760 -.0060 1 1 1
4.3100 4.3127 -.0027 0 2 0
4.1100 4.1099 .0001 -1 1 2
4.0100 4.0032 .0068 -1 2 1
3.8200 3.8182 .0018 1 -1 2
3.7200 3.7218 -.0018 1 -2 1
3.5200 3.5190 .0010 1 2 0
3.3260 3.3266 -.0006 -2 2 0
3.2780 3.2775 .0005 2 1 1
2.3530 2.3530 -.0000 -3 -1 1
A= 8.32342 DA= .00074
B= 8.87234 DB= .00245
C= 9.89962 DC= .00056
GAMMA=102.07590 DGAMMA= .09601
BETA = 90.86345 DBETA = .02282
ALPHA= 83.75428 DALPHA= .01306
V= 710.6
27. 31-1635
C10H10C12U
Triklin
Dexp Dcal d(D) h k l
9.2600 9.2532 .0068 2 1 0
7.6000 7.5992 .0008 1 2 0
6.8600 6.8630 -.0030 2 2 0
6.3900 6.3883 .0017 -1 0 1
6.1500 6.1477 .0023 0 -1 1
5.7200 5.7192 .0008 -2 0 1
5.3400 5.3398 .0002 1 1 1
4.8700 4.8750 -.0050 4 1 0
4.6100 4.6086 .0014 4 0 0
4.4200 4.4203 -.0003 -2 -3 1
4.3000 4.3005 -.0005 -1 2 1
4.0500 4.0489 .0011 4 3 0
A= 19.976 DA= .008
B= 15.516 DB= .006
C= 6.620 DC= .002
GAMMA= 69.29 DGAMMA= .01
BETA =102.54 DBETA = .03
ALPHA=100.95 DALPHA= .02
V= 1859
28. 31-1636
C9H15Cl3O2U
Triklin
Dexp Dcal d(D) h k l
9.2600 9.2397 .0203 1 0 0
7.5600 7.5540 .0060 0 1 0
6.7300 6.7290 .0010 1 0 1
6.3700 6.3661 .0039 0 -1 1
5.8700 5.8723 -.0023 0 1 1
5.5900 5.5901 -.0001 1 1 0
5.3700 5.3695 .0005 1 -1 1
4.6200 4.6199 .0001 2 0 0
4.4500 4.4522 -.0022 0 -1 2
2.4390 2.4389 .0001 -1 -1 4
2.3590 2.3590 .0000 -3 0 3
A= 9.292 DA= .001
B= 7.614 DB= .003
C= 10.409 DC= .007
GAMMA= 95.32 DGAMMA= .07
BETA = 92.47 DBETA = .01
ALPHA= 94.61 DALPHA= .03
V= 729.9
29. 31-1977
C12H10N4O6U*2H2O
Triklin
Dexp Dcal d(D) h k l
10.0000 10.0058 -.0058 1 1 0
6.6000 6.6055 -.0055 -1 1 1
6.0000 6.0064 -.0064 -1 -1 1
5.7000 5.7023 -.0023 1 1 1
5.1800 5.1854 -.0054 1 2 1
5.0000 5.0029 -.0029 2 2 0
4.8000 4.8026 -.0026 -2 -1 1
4.4000 4.4015 -.0015 1 3 1
4.2000 4.1966 .0034 2 3 0
3.7500 3.7478 .0022 -1 1 2
3.6500 3.6493 .0007 2 3 1
3.4400 3.4403 -.0003 -2 1 2
A= 11.86 DA= .01
B= 16.32 DB= .03
C= 7.5568 DC= .0004
GAMMA= 84.46 DGAMMA= .02
BETA =101.68 DBETA = .02
ALPHA= 78.39 DALPHA= .03
V= 1388
Triklin
Dexp. Dcal. d(D) h k l
10.0000 10.0000 .0000 1 -1 0
6.6000 6.6000 .0000 2 0 0
6.0000 5.9790 .0210 0 -3 0
5.7000 5.7000 .0000 -2 -2 0
5.1800 5.1868 -.0068 1 -3 0
5.0000 5.0000 .0000 2 -2 0
4.8000 4.7998 .0002 0 -1 1
4.4000 4.4000 .0000 3 0 0
4.2000 4.1994 .0006 -1 -2 1
3.7500 3.7529 -.0029 3 -2 0
3.6500 3.6498 .0002 -2 -2 1
3.4400 3.4400 -.0000 3 0 1
A= 13.3840 DA= .0006
B= 18.222 DB= .001
C= 4.8708 DC= .0002
GAMMA= 82.859 DGAMMA= .001
BETA = 84.61 DBETA = .03
ALPHA= 96.46 DALPHA= .04
V= 1164.1
30. 31-1978
C24H22N8O13U2*2H2O
Triklin
Dexp Dcal d(D) h k l
10.0000 10.0153 -.0153 1 0 0
9.5000 9.4824 .0176 1 1 0
9.0000 8.9989 .0011 0 0 1
5.8000 5.8134 -.0134 1 -1 1
5.4500 5.4442 .0058 2 1 0
5.2200 5.2149 .0051 2 1 1
5.0000 5.0076 -.0076 2 0 0
4.8500 4.8586 -.0086 -1 -2 1
4.6000 4.5877 .0123 1 0 2
4.4200 4.4199 .0001 0 2 1
4.3500 4.3533 -.0033 0 -1 2
4.3000 4.3139 -.0139 1 1 2
A= 11.23985 DA= .00000
B= 11.86222 DB= .00004
C= 9.33996 DC= .00004
GAMMA= 67.618 DGAMMA= .006
BETA = 76.1715 DBETA = .0006
ALPHA= 91.176 DALPHA= .003
V= 1109.4