157. 28-0035
Al0.2Ti2.3{SO3}1.3
Rombik
Groupa 16,25,47
Dexp. Dcal. d(D) h k l
4.8000 4.7991 .0009 0 0 3
3.9200 3.9100 .0100 3 0 2
3.4800 3.4855 -.0055 1 0 4
3.3500 3.3420 .0080 3 0 3
3.2400 3.2343 .0057 2 1 0
2.8700 2.8723 -.0023 3 1 0
2.5600 2.5625 -.0025 0 1 4
2.2700 2.2694 .0006 2 0 6
2.2200 2.2185 .0015 5 1 0
1.9950 1.9958 -.0008 7 0 0
1.9230 1.9232 -.0002 7 0 2
1.6070 1.6071 -.0001 4 2 1
a=13.97 b= 3.6491 c=14.40
da= .01 db= .0001 dc= .01
V= 734.0
Dexp Dcal d(D) h k l
4.8000 4.7992 .0008 1 1 0
3.9200 3.9206 -.0006 -1 0 1
3.4800 3.4814 -.0014 -1 -2 1
3.3500 3.3488 .0012 -1 1 0
3.2400 3.2397 .0003 1 2 0
2.8700 2.8696 .0004 1 0 2
2.5600 2.5601 -.0001 -2 -1 1
2.2700 2.2706 -.0006 1 -2 2
2.2200 2.2198 .0002 -2 -1 2
1.9950 1.9947 .0003 0 -3 3
1.9230 1.9230 .0000 1 3 1
1.6070 1.6071 -.0001 -2 -2 4
A= 5.2971 DA= .0006
B= 7.429 DB= .001
C= 7.5248 DC= .0003
GAMMA= 68.256 DGAMMA= .001
BETA = 96.696 DBETA = .009
ALPHA=114.124 DALPHA= .004
V= 250.82
158. 28-0103
Sb3Ti2O10
Triklin
Dexp Dcal d(D) h k l
3.5200 3.5201 -.0001 1 2 0
3.2600 3.2602 -.0002 1 0 2
3.0100 3.0100 -.0000 1 -1 2
2.7500 2.7500 -.0000 0 -2 2
2.5600 2.5603 -.0003 1 3 0
2.3900 2.3900 -.0000 2 1 2
2.2900 2.2913 -.0013 -2 -2 2
2.1800 2.1798 .0002 -2 3 3
2.1100 2.1086 .0014 -1 -3 2
1.9800 1.9797 .0003 -2 0 4
1.9400 1.9392 .0008 3 2 1
1.9100 1.9112 -.0012 -3 4 1
A= 8.169 DA= .003
B= 9.0021 DB= .0001
C= 8.4150 DC= .0003
GAMMA=103.02 DGAMMA= .01
BETA =105.611 DBETA = .007
ALPHA= 78.577 DALPHA= .001
V= 574.4
159. 28-0161
BaTiOF4
Triklin
Dexp Dcal d(D) h k l
4.8000 4.7886 .0114 1 0 1
4.3000 4.3013 -.0013 -1 2 0
3.6800 3.6745 .0055 1 -2 1
3.6300 3.6282 .0018 -1 1 1
3.4300 3.4310 -.0010 -1 3 0
3.1600 3.1613 -.0013 -1 -1 1
2.9120 2.9120 .0000 0 4 1
2.7540 2.7543 -.0003 0 3 2
2.5830 2.5843 -.0013 -1 4 1
2.3940 2.3943 -.0003 2 0 2
2.3940 2.3943 -.0003 2 0 2
2.2890 2.2899 -.0009 -1 5 0
A= 5.5499 DA= .0002
B= 12.0813 DB= .0007
C= 6.6322 DC= .0002
GAMMA= 96.621 DGAMMA= .006
BETA = 74.13 DBETA = .01
ALPHA= 79.22 DALPHA= .01
V=413.7
160. 28-0103
Sb3Ti2O10
Triklin
Dexp Dcal d(D) h k l
6.5300 6.5282 .0018 1 1 0
5.7000 5.7038 -.0038 -1 0 1
4.2100 4.2156 -.0056 -1 -2 1
3.6800 3.6821 -.0021 -1 0 2
3.6300 3.6281 .0019 1 -1 1
3.5200 3.5175 .0025 1 2 1
3.2100 3.2117 -.0017 -1 -2 2
3.1200 3.1213 -.0013 -1 1 2
2.9360 2.9326 .0034 1 1 2
2.9090 2.9091 -.0001 2 1 1
2.8520 2.8519 .0001 -2 0 2
2.4390 2.4397 -.0007 2 -1 1
A= 7.392 DA= .001
B= 9.364 DB= .005
C= 7.848 DC= .002
GAMMA= 66.93 DGAMMA= .01
BETA =106.30 DBETA = .03
ALPHA= 98.26 DALPHA= .04
V=479.0
161. 28-0161
BaTiOF4
Triklin
Dexp Dcal d(D) h k l
4.8000 4.7874 .0126 1 0 1
4.3000 4.3013 -.0013 -1 2 0
3.6800 3.6743 .0057 1 -2 1
3.6300 3.6282 .0018 -1 1 1
3.4300 3.4310 -.0010 -1 3 0
3.1600 3.1615 -.0015 -1 -1 1
2.9120 2.9117 .0003 0 4 1
2.7540 2.7538 .0002 0 3 2
2.5830 2.5842 -.0012 -1 4 1
2.4200 2.4215 -.0015 0 4 2
2.3940 2.3937 .0003 2 0 2
2.2890 2.2899 -.0009 -1 5 0
A= 5.549 DA= .001
B= 12.0811 DB= .0004
C= 6.631 DC= .001
GAMMA= 96.63 DGAMMA= .01
BETA = 74.142 DBETA = .01
ALPHA= 79.231 DALPHA= .005
V=413.7
162. 28-0162
alfa-Ba3Ti2O2F10
Triklin
Dexp Dcal D(d) h k l
6.5300 6.5241 .0059 -1 0 1
5.7000 5.7035 -.0035 1 1 0
4.2100 4.2083 .0017 -1 -1 2
3.6800 3.6830 -.0030 1 2 0
3.6300 3.6340 -.0040 1 -1 1
3.5200 3.5162 .0038 -1 1 2
3.2100 3.2097 .0003 -1 -2 2
3.1200 3.1216 -.0016 1 2 1
2.9360 2.9368 -.0008 -1 2 1
2.9090 2.9130 -.0040 -2 1 1
2.8520 2.8518 .0002 2 2 0
2.4390 2.4370 .0020 0 -3 1
A= 7.3911 DA= .0002
B= 7.85316 DB= .00003
C= 9.3466 DC= .0001
GAMMA= 73.8398 DGAMMA= .0008
BETA =112.976 DBETA = .001
ALPHA= 98.2139 DALPHA= .0006
V=479.3
163. 28-0347
Cs4Ti4O{SO4}9
Triklin
Dexp Dcal d(D) h k l
4.5200 4.5200 -.0000 1 1 0
4.3300 4.3304 -.0004 0 -1 2
4.1100 4.1095 .0005 -1 -1 2
3.7500 3.7477 .0023 2 1 0
3.5000 3.4997 .0003 1 -1 3
3.3600 3.3558 .0042 0 1 3
3.1900 3.1874 .0026 0 -1 4
3.0300 3.0301 -.0001 1 -1 4
2.9600 2.9612 -.0012 -3 1 0
2.8800 2.8777 .0023 2 1 3
2.8700 2.8712 -.0012 0 1 4
2.8200 2.8216 -.0016 -4 0 1
A= 11.41 DA= .01
B= 4.904 DB= .001
C= 15.470 DC= .008
GAMMA= 88.37 DGAMMA= .06
BETA = 92.57 DBETA = .01
ALPHA= 96.22 DALPHA= .01
V= 859.1
164. 28-0348
Cs4Ti4O{SO4}9
Triklin
Dexp Dcal d(D) h k l
4.5000 4.5076 -.0076 -1 2 1
3.8300 3.8295 .0005 -1 -2 1
3.6800 3.6810 -.0010 0 -2 2
3.4900 3.4904 -.0004 1 2 3
3.4300 3.4318 -.0018 3 -1 1
3.2700 3.2707 -.0007 -2 0 2
3.1300 3.1302 -.0002 1 -2 3
2.9500 2.9497 .0003 0 0 4
2.7200 2.7225 -.0025 -3 -1 1
2.6600 2.6600 .0000 0 4 0
2.5800 2.5805 -.0005 -3 3 0
2.4800 2.4799 .0001 4 0 0
A= 10.629 DA= .002
B= 10.796 DB= .006
C= 12.697 DC= .007
GAMMA= 94.22 DGAMMA= .06
BETA = 70.10 DBETA = .05
ALPHA= 83.21 DALPHA= .06
V= 1350.2
165. 28-0374
Cr0.2TiO2.3{SO3}1.4
Triklin
Dexp Dcal d(D) h k l
4.8000 4.8008 -.0008 -1 0 1
3.9000 3.9006 -.0006 1 2 0
3.4500 3.4539 -.0039 0 -2 1
3.3200 3.3215 -.0015 1 2 1
3.2300 3.2307 -.0007 -1 0 2
2.8700 2.8700 -.0000 0 2 2
2.5600 2.5602 -.0002 -2 -2 1
2.2700 2.2698 .0002 0 1 3
2.2400 2.2397 .0003 -2 1 2
1.9990 1.9991 -.0001 -1 -2 3
1.9930 1.9931 -.0001 -2 2 2
1.6050 1.6050 .0000 2 2 3
A= 5.7100 DA= .0001
B= 8.9977 DB= .0004
C= 7.011 DC= .001
GAMMA= 76.6553 DGAMMA= .0006
BETA =101.687 DBETA = .008
ALPHA= 85.37 DALPHA= .01
V= 340.1
166. 28-0647
Bi14Mo3Ti6O42
Triklin
Dexp Dcal d(D) h k l
3.3000 3.3004 -.0004 2 0 0
3.2700 3.2694 .0006 -1 0 2
2.9600 2.9585 .0015 1 -2 1
2.7100 2.7099 .0001 2 1 1
2.6900 2.6864 .0036 -1 -2 1
2.3600 2.3597 .0003 -1 1 3
2.2800 2.2795 .0005 -2 2 2
2.0200 2.0204 -.0004 -3 2 0
1.9200 1.9193 .0007 0 -3 2
1.9000 1.8998 .0002 1 -2 3
1.8200 1.8201 -.0001 2 3 1
1.7700 1.7699 .0001 3 2 0
A= 6.677 DA= .001
B= 7.433 DB= .001
C= 7.5801 DC= .0001
GAMMA= 98.681 DGAMMA= .009
BETA = 91.52 DBETA = .01
ALPHA= 81.898 DALPHA= .002
V=368.2
167. 28-0724
TiP2Cl8O3
Triklin
Dexp Dcal d(D) h k l
9.7900 9.7985 -.0085 0 1 1
7.6000 7.6023 -.0023 -1 0 1
6.7800 6.7821 -.0021 0 -1 1
5.9600 5.9586 .0014 -1 1 0
5.5200 5.5210 -.0010 1 1 1
4.5200 4.5182 .0018 -1 -2 1
4.2500 4.2519 -.0019 0 3 1
4.0800 4.0799 .0001 -2 0 1
3.9100 3.9080 .0020 0 3 2
3.7800 3.7810 -.0010 1 3 1
3.5000 3.4997 .0003 2 2 0
3.2200 3.2200 -.0000 -2 0 3
3.0700 3.0702 -.0002 -2 2 3
2.9580 2.9580 -.0000 -1 1 4
2.8560 2.8559 .0001 -1 4 1
A= 8.1723 DA= .0002
B= 12.779 DB= .004
C= 11.8838 DC= .0003
GAMMA= 86.85 DGAMMA= .02
BETA =108.89 DBETA = .02
ALPHA= 71.490 DALPHA= .006
V= 1096.1
168. 28-0825
K2TiF6
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
9.1300 9.1768 -.0468 1 0 0
4.5800 4.5884 -.0084 2 0 0
3.3500 3.3554 -.0054 2 1 0
2.8300 2.8313 -.0013 -3 0 1
2.3000 2.3012 -.0012 0 2 1
2.1700 2.1696 .0004 3 0 2
2.0800 2.0804 -.0004 -3 1 2
1.6850 1.6848 .0002 -5 1 1
1.5470 1.5464 .0006 0 1 4
1.4520 1.4522 -.0002 -1 3 2
1.3580 1.3582 -.0002 0 2 4
1.3090 1.3087 .0003 0 3 3
1.1930 1.1931 -.0001 7 0 2
1.1570 1.1569 .0001 7 2 0
1.1280 1.1280 -.0000 -3 4 1 2
a= 9.191 b= 4.9193 c= 6.526 beta= 93.24
da= .002 db=.0003 dc=.005 dbeta=.05
V= 294.6
169. 28-0828
K4Ti4O6F8*3H2O
Triklin
Dexp Dcal d(D) h k l
6.1000 6.1029 -.0029 1 0 0
3.6200 3.6178 .0022 1 1 0
3.2500 3.2504 -.0004 -1 -1 2
3.1000 3.1018 -.0018 1 -1 3
2.9700 2.9727 -.0027 2 -1 1
2.7200 2.7193 .0007 2 -1 2
2.6300 2.6301 -.0001 -1 0 4
2.4000 2.3993 .0007 2 1 0
2.1000 2.0998 .0002 1 1 4
1.9900 1.9897 .0003 -1 1 5
1.9300 1.9305 -.0005 2 1 3
1.8200 1.8200 .0000 -2 3 0
1.6390 1.6391 -.0001 1 3 0
1.5390 1.5391 -.0001 -4 1 2
1.4520 1.4519 .0001 3 -3 4
A= 6.3631 DA= .0007
B= 5.812 DB= .001
C= 11.460 DC= .002
GAMMA=106.10 DGAMMA= .02
BETA = 91.077 DBETA = .004
ALPHA= 97.879 DALPHA= .005
V= 402.6
170. 28-0829
K6Ti4O3F16*4H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
6.1000 6.1027 -.0027 1 1 0
3.1000 3.0993 .0007 1 1 2
2.8800 2.8828 -.0028 -2 0 2
2.6300 2.6310 -.0010 -1 2 2
2.3300 2.3296 .0004 -3 2 1
2.0500 2.0497 .0003 -3 2 2
1.9900 1.9899 .0001 -2 3 2
1.9300 1.9300 .0000 -4 2 1
1.8210 1.8209 .0001 0 0 4
1.7710 1.7713 -.0003 5 1 0
1.6530 1.6527 .0003 3 4 1
1.5390 1.5390 -.0000 3 0 4
1.4520 1.4518 .0002 -5 1 3
a= 9.072 b= 8.251 c= 7.2871 beta= 91.75
da=.003 db=.005 dc= .0006 dbeta=.06
V= 545.2
171. 28-0963
Rb2TiO{SO4}2
Triklin
Dexp Dcal d(D) h k l
4.6700 4.6639 .0061 0 -1 1
4.2300 4.2307 -.0007 -2 0 1
4.0600 4.0603 -.0003 0 0 2
3.7100 3.7148 -.0048 2 0 1
3.5500 3.5523 -.0023 2 1 0
3.3500 3.3524 -.0024 2 1 1
3.3300 3.3313 -.0013 2 -1 1
3.1700 3.1648 .0052 -2 -1 1
3.1600 3.1648 -.0048 -2 -1 1
3.0000 3.0024 -.0024 0 -2 1
2.8300 2.8297 .0003 -2 3 2
2.8000 2.7987 .0013 0 3 1
A= 9.674 DA= .005
B= 8.954 DB= .002
C= 9.361 DC= .006
GAMMA=109.107 DGAMMA= .003
BETA =106.450 DBETA = .006
ALPHA= 61.37 DALPHA= .04
V=664.8
172. 28-0964
Rb2TiO{SO4}2
Triklin
Dexp Dcal d(D) h k l
4.0600 4.0597 .0003 1 2 2
3.7500 3.7558 -.0058 1 1 3
3.7100 3.7103 -.0003 0 -3 1
3.5900 3.5920 -.0020 1 3 1
3.3500 3.3516 -.0016 -2 -1 1
3.2700 3.2703 -.0003 1 2 3
3.1600 3.1586 .0014 -2 -2 1
3.0200 3.0205 -.0005 2 3 1
2.8700 2.8714 -.0014 -1 1 3
2.8200 2.8226 -.0026 0 -4 1
2.7500 2.7494 .0006 -2 -2 2
2.7100 2.7094 .0006 2 0 4
A= 7.9046 DA= .0002
B= 11.644 DB= .007
C= 12.248 DC= .001
GAMMA= 78.309 DGAMMA= .006
BETA = 74.112 DBETA = .006
ALPHA= 92.308 DALPHA= .004
V=1056.6
173. 28-0965
Rb2TiO{SO4}2
Triklin
Dexp Dcal d(D) h k l
4.6700 4.6717 -.0017 0 1 1
4.2700 4.2780 -.0080 2 0 0
4.0600 4.0672 -.0072 0 2 0
3.8800 3.8909 -.0109 2 2 0
3.7500 3.7455 .0045 2 0 1
3.5900 3.5891 .0009 1 2 1
3.3600 3.3612 -.0012 2 2 1
3.2700 3.2687 .0013 -2 0 1
3.1900 3.1841 .0059 -1 2 0
3.0400 3.0428 -.0028 2 -1 1
3.0200 3.0174 .0026 3 2 0
2.8600 2.8587 .0013 1 1 2
A= 9.5351 DA= .0005
B= 8.9945 DB= .0005
C= 6.0606 DC= .0003
GAMMA= 65.051 DGAMMA= .003
BETA = 82.821 DBETA = .002
ALPHA= 90.641 DALPHA= .005
V=466.3
174. 28-0966
Rb4Ti2O{SO4}5
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
3.8200 3.8159 .0041 1 0 2
3.6900 3.6951 -.0051 -1 1 1
3.6300 3.6297 .0003 -3 0 2
3.5500 3.5487 .0013 2 0 2
3.3300 3.3287 .0013 -4 0 2
3.2400 3.2418 -.0018 3 0 2
3.1700 3.1668 .0032 3 1 1
3.0200 3.0205 -.0005 -5 0 2
2.7300 2.7320 -.0020 -6 0 2
2.6100 2.6096 .0004 -4 1 2
2.2200 2.2192 .0008 -6 0 3
2.1900 2.1912 -.0012 7 0 2
1.7100 1.7099 .0001 6 2 1
a= 20.135 b= 4.203 c= 8.036 beta= 97.3278
da= .007 db= .003 dc=.001 dbeta=.0005
V= 674.6
175. 28-0968
Rb2Ti{SO4}3
Geksagon
Groupa 186,190,194
Dexp. Dcal. d(D) h k l
8.6700 8.7621 -.0921 0 0 1
4.3700 4.3811 -.0111 0 0 2
3.7100 3.7179 -.0079 3 0 0
3.0400 3.0377 .0023 2 1 2
3.0200 3.0222 -.0022 2 2 1
2.9300 2.9207 .0093 0 0 3
2.1500 2.1495 .0005 1 0 4
1.4600 1.4604 -.0004 0 0 6
1.4100 1.4099 .0001 4 4 3
a= 12.88 c= 8.762
da= .01 dc= .008
V=1258.6
176. 28-0993
Cs2TiO{SO4}2
Triklin
Dexp Dcal d(D) h k l
13.6000 13.9697 -.3697 0 1 0
9.6500 9.6589 -.0089 0 0 1
6.8100 6.8131 -.0031 0 -2 1
4.7500 4.7473 .0027 2 0 0
4.5500 4.5474 .0026 1 -2 2
4.3300 4.3307 -.0007 2 -2 1
3.8300 3.8271 .0029 2 -3 1
3.7800 3.7810 -.0010 2 1 1
3.6500 3.6514 -.0014 2 -1 2
3.4300 3.4302 -.0002 2 -3 2
3.3500 3.3500 .0000 -2 0 2
3.2700 3.2708 -.0008 2 -4 1
A= 9.718 DA= .00270
B= 15.12214 DB= .00003
C= 10.2607 DC= .0005
GAMMA=102.25 DGAMMA= .01
BETA = 84.783 DBETA = .002
ALPHA=109.6924 DALPHA= .0005
V=1387.1
177. 28-1153
Na4Ti0.3O2.6
Triklin
Dexp Dcal d(D) h k l
9.4500 9.4413 .0087 -1 0 1
9.1100 9.1080 .0020 0 1 0
6.6300 6.6333 -.0033 1 0 1
6.2700 6.2705 -.0005 -1 -1 1
6.1700 6.1674 .0026 2 0 0
4.7200 4.7207 -.0007 -2 0 2
4.6300 4.6297 .0003 0 1 2
2.7100 2.7103 -.0003 -2 -3 1
2.6600 2.6600 .0000 1 -1 3
2.5100 2.5112 -.0012 -3 1 4
2.4960 2.4944 .0016 -5 -1 2
2.2500 2.2498 .0002 4 3 0
A= 13.16 DA= .01
B= 9.224 DB= .001
C= 10.562 DC= .009
GAMMA= 88.711 DGAMMA= .006
BETA =109.97 DBETA = .04
ALPHA= 82.006 DALPHA= .008
V= 1190.0
178. 28-1154
Na6Ti2O7
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.2300 5.2305 -.0005 2 1 0
4.4800 4.4828 -.0028 -2 0 1
4.1700 4.1663 .0037 0 0 2
3.2300 3.2346 -.0046 3 2 0
2.9050 2.9067 -.0017 -2 3 1
2.7360 2.7350 .0010 3 3 0
2.7080 2.7081 -.0001 0 4 1
2.6010 2.6016 -.0006 4 2 1
2.5090 2.5090 -.0000 2 4 1
2.2490 2.2486 .0004 1 5 0
2.2020 2.2018 .0002 5 0 2
2.1060 2.1065 -.0005 3 4 2
a= 11.9072 b= 11.4543 c= 8.438 beta= 80.93
da= .0002 db=.0006 dc=.0002 dbeta=.03
V= 1136.5
179. 28-1257
alfa-SrTiOF4
Triklin
Dexp Dcal d(D) h k l
7.3300 7.3218 .0082 -1 0 1
5.5500 5.5490 .0010 -1 1 1
4.8100 4.8105 -.0005 1 -1 1
4.4200 4.4197 .0003 0 -1 2
3.6700 3.6709 -.0009 -1 2 0
3.6300 3.6302 -.0002 0 2 0
3.4300 3.4263 .0037 1 -2 1
3.2500 3.2524 -.0024 0 0 3
3.2000 3.1977 .0023 -2 -1 1
3.0600 3.0628 -.0028 -2 0 3
2.6640 2.6628 .0012 0 -2 3
2.5950 2.5937 .0013 2 1 1
A= 8.13478 DA= .00001
B= 7.564 DB= .002
C= 10.5346 DC= .0007
GAMMA=102.9295 DGAMMA= .0005
BETA =109.88 DBETA = .03
ALPHA= 94.767 DALPHA= .007
V= 585.1
180. 28-1339
alfa-Ti2Ti3O7
Triklin
Dexp Dcal d(D) h k l
8.5000 8.5010 -.0010 1 0 0
4.2300 4.2328 -.0028 1 1 1
3.9900 3.9926 -.0026 -1 -1 1
3.6400 3.6407 -.0007 -2 1 0
3.5200 3.5192 .0008 -2 0 1
3.2100 3.2140 -.0040 2 0 1
3.1100 3.1099 .0001 2 2 0
2.7500 2.7487 .0013 0 3 0
2.5600 2.5596 .0004 1 1 2
2.5000 2.4999 .0001 -3 -1 1
2.4800 2.4797 .0003 0 2 2
A= 8.566 DA= .002
B= 8.393 DB= .001
C= 5.566 DC= .003
GAMMA= 85.41 DGAMMA= .01
BETA = 94.53 DBETA = .02
ALPHA= 80.73 DALPHA= .01
V= 391.9
181. 28-1353
GaTi{PO3}3Cl16
Triklin
Dexp Dcal d(D) h k l
7.7900 7.7902 -.0002 0 -1 1
6.6000 6.6089 -.0089 2 0 0
5.8800 5.8790 .0010 0 2 0
5.7400 5.7379 .0021 -1 1 1
5.5300 5.5266 .0034 -1 -2 1
4.7900 4.7935 -.0035 2 2 0
4.6100 4.6135 -.0035 -2 1 1
4.5100 4.5068 .0032 2 1 1
4.3400 4.3459 -.0059 0 -1 2
3.9100 3.9087 .0013 1 0 2
3.7000 3.7000 .0000 3 0 1
3.6400 3.6386 .0014 2 3 0
A= 13.6479 DA= .0002
B= 12.3057 DB= .0001
C= 8.95352 DC= .00003
GAMMA= 78.383 DGAMMA= .001
BETA =101.0911 DBETA = .0004
ALPHA=104.50180 DALPHA= .00009
V=1409.7
182. 28-1399
TiOSO4
Triklin
Dexp Dcal d(D) h k l
5.4000 5.3788 .0212 1 0 1
4.6000 4.5953 .0047 2 0 0
4.1300 4.1378 -.0078 0 2 0
3.7800 3.7819 -.0019 0 -1 2
3.5900 3.5916 -.0016 0 0 2
3.4900 3.4894 .0006 -2 -1 2
3.2300 3.2267 .0033 1 0 2
3.0500 3.0498 .0002 -2 1 1
2.9900 2.9948 -.0048 -2 0 2
2.6900 2.6894 .0006 2 0 2
2.6300 2.6300 -.0000 -4 -2 1
2.5700 2.5710 -.0010 3 2 1
A= 10.5403 DA= .0007
B= 9.993 DB= .002
C= 7.9448 DC= .0003
GAMMA= 61.324 DGAMMA= .007
BETA =106.7111 DBETA = .0005
ALPHA=114.543 DALPHA= .003
V=663.8
183. 28-1925
C4H12BCl7N2Ti2
Triklin
Dexp Dcal d(D) h k l
9.4100 9.4043 .0057 1 0 0
7.4000 7.4006 -.0006 0 1 0
6.0000 6.0001 -.0001 1 0 1
5.5400 5.5358 .0042 0 -1 1
4.5400 4.5431 -.0031 1 1 1
4.2700 4.2679 .0021 -2 1 1
3.6000 3.5985 .0015 2 -1 1
3.3100 3.3054 .0046 2 1 1
2.8900 2.8899 .0001 0 1 3
2.7300 2.7298 .0002 2 1 2
2.6500 2.6494 .0006 -1 -2 2
2.5100 2.5097 .0003 -3 2 2
A= 9.743 DA= .001
B= 7.552 DB= .001
C= 9.337 DC= .004
GAMMA=100.58 DGAMMA= .01
BETA =101.88 DBETA = .04
ALPHA= 83.51 DALPHA= .02
V= 658.9
184. 28-1926
C2Cl3N*TiCl4
Rombik
Groupa 39,67
Dexp. Dcal. d(D) h k l
4.3300 4.3293 .0007 0 0 2
2.6700 2.6676 .0024 1 1 1
2.0900 2.0912 -.0012 3 1 1
2.0100 2.0111 -.0011 1 1 3
1.9700 1.9707 -.0007 2 0 4
1.7270 1.7267 .0003 3 1 3
1.4270 1.4268 .0002 1 0 6
1.3610 1.3609 .0001 7 0 0
1.2730 1.2729 .0001 3 2 2
1.2000 1.2001 -.0001 4 2 2
a= 9.526 b= 2.9339 c= 8.6586
da= .006 db= .0003 dc= .0006
V= 242.0
185. 28-1927
C54H42Cl3N6O6Ti
Triklin
Dexp Dcal d(D) h k l
9.7200 9.7348 -.0148 0 1 1
8.5100 8.5074 .0026 0 -1 1
6.6100 6.6086 .0014 1 1 1
5.7000 5.6990 .0010 1 0 2
5.5200 5.5336 -.0136 0 2 0
5.2600 5.2572 .0028 0 0 3
5.0800 5.0801 -.0001 1 -1 1
4.8100 4.8034 .0066 -1 1 1
4.5100 4.5064 .0036 0 -1 3
4.1800 4.1798 .0002 1 2 3
3.9400 3.9429 -.0029 0 0 4
3.6900 3.6891 .0009 0 3 0
3.6000 3.5998 .0002 1 3 0
3.4000 3.4015 -.0015 2 0 1
3.2700 3.2694 .0006 2 1 3
A= 7.0649 DA= .0005
B= 11.611 DB= .007
C= 16.450 DC= .01
GAMMA= 74.36 DGAMMA= .02
BETA = 75.62 DBETA = .01
ALPHA= 78.47 DALPHA= .03
V= 1245.8