75. 7-0011
Pb{PO2}2*H2O
Triklin
Dexp Dcal d(D) h k l
4.4300 4.4313 -.0013 1 1 1
4.2000 4.1998 .0002 -1 1 0
3.5900 3.5908 -.0008 1 -1 1
3.2600 3.2597 .0003 -1 -1 1
2.7000 2.6997 .0003 -1 3 0
2.6200 2.6196 .0004 0 3 2
2.4800 2.4786 .0014 2 2 1
2.2200 2.2191 .0009 -1 4 0
2.1100 2.1085 .0015 1 5 0
2.0900 2.0918 -.0018 -2 -1 1
2.0400 2.0393 .0007 2 -2 1
1.8790 1.8793 -.0003 1 6 1
A= 5.113 DA= .003
B= 11.411 DB= .004
C= 6.355 DC= .001
GAMMA= 77.25 DGAMMA= .02
BETA = 75.09 DBETA = .04
ALPHA= 73.96 DALPHA= .02
V= 339.9
76. 7-0224
Pb3{SbO4}2
Triklin
Dexp Dcal d(D) h k l
5.8000 5.8035 -.0035 1 0 1
4.5500 4.5512 -.0012 1 1 1
4.3500 4.3500 .0000 -1 -1 1
3.8800 3.8808 -.0008 1 0 2
3.4800 3.4790 .0010 0 -1 2
3.2000 3.2035 -.0035 -2 -1 1
3.0000 2.9990 .0010 0 0 3
2.8200 2.8223 -.0023 1 2 1
2.6500 2.6487 .0013 1 1 3
2.0800 2.0803 -.0003 3 2 1
1.8700 1.8696 .0004 4 1 1
1.8200 1.8201 -.0001 0 3 2
A= 7.6656 DA= .0002
B= 5.9593 DB= .0001
C= 9.01096 DC= .00003
GAMMA= 78.7922 DGAMMA= .0008
BETA = 88.7358 DBETA = .0002
ALPHA= 86.9050 DALPHA= .0006
V=403.1
77. 7-0374
5PbS*4Sb2S3
Triklin
Dexp Dcal d(D) h k l
5.9400 5.9465 -.0065 0 -1 1
4.3900 4.3891 .0009 0 -1 3
4.1700 4.1707 -.0007 -1 0 3
3.9300 3.9305 -.0005 -1 1 0
3.7800 3.7787 .0013 1 -1 1
3.6700 3.6697 .0003 -1 0 4
3.4500 3.4564 -.0064 1 0 4
3.2900 3.2914 -.0014 0 0 6
3.2300 3.2270 .0030 1 -1 3
3.0100 3.0103 -.0003 0 2 3
2.9500 2.9471 .0029 -1 1 5
2.8200 2.8192 .0008 0 -1 6
A= 5.146 DA= .002
B= 6.470 DB= .001
C= 19.877 DC= .006
GAMMA= 87.853 DGAMMA= .004
BETA = 93.21 DBETA = .01
ALPHA= 84.46 DALPHA= .01
V=657.4
78. 9-0244
Pb3Sn4Sb2S14
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
5.8300 5.8218 .0082 0 0 2
3.9000 3.8812 .0188 0 0 3
3.4400 3.4321 .0079 3 0 2
3.1100 3.1109 -.0009 0 1 1
2.8800 2.8799 .0001 2 1 0
2.5100 2.5101 -.0001 3 1 1
2.4000 2.4014 -.0014 3 0 4
2.3300 2.3287 .0013 0 0 5
2.1900 2.1873 .0027 2 0 5
2.0400 2.0421 -.0021 3 0 5
1.9410 1.9406 .0004 0 0 6
1.8110 1.8108 .0002 2 1 5
1.4470 1.4461 .0009 1 0 8
1.2930 1.2937 -.0007 0 0 9
a=12.75 b= 3.228 c=11.644
da= .01 db= .001 dc= .006
V= 479.1
79. 9-0615
C16H30O4Pb
Triklin
Dexp Dcal d(D) h k l
26.0000 25.5926 .4074 1 0 0
12.8000 12.7963 .0037 2 0 0
8.5600 8.5592 .0008 -2 1 1
7.0800 7.0833 -.0033 -2 -1 1
6.4200 6.4159 .0041 -2 1 2
5.6400 5.6425 -.0025 -2 2 0
5.4800 5.4812 -.0012 0 2 1
5.1300 5.1310 -.0010 3 -1 2
4.8500 4.8506 -.0006 0 1 3
4.6900 4.6892 .0008 2 2 1
4.5200 4.5155 .0045 1 -2 2
4.3900 4.3903 -.0003 4 -2 1
A= 26.215 DA= .005
B= 11.709 DB= .001
C= 15.784 DC= .001
GAMMA=101.163 DGAMMA= .007
BETA = 96.406 DBETA = .006
ALPHA= 85.7888 DALPHA= .0003
V=4717
80. 10-0003
PbBeF4
Rombik
Groupa 26,28,51
Dexp. Dcal. d(D) h k l
4.2400 4.2517 -.0117 0 0 2
3.7800 3.7836 -.0036 1 1 1
3.6200 3.6166 .0034 1 0 2
3.4300 3.4391 -.0091 2 0 0
3.3330 3.3296 .0034 0 1 2
3.1870 3.1882 -.0012 2 0 1
3.0040 2.9969 .0071 1 1 2
2.7390 2.7393 -.0003 2 1 1
2.6760 2.6770 -.0010 0 2 0
2.6190 2.6207 -.0017 1 0 3
2.3970 2.3938 .0032 1 2 1
2.2660 2.2654 .0006 0 2 2
a= 6.878 b= 5.354 c= 8.503
da= .001 db= .005 dc= .001
V= 313.1
Triklin
Dexp Dcal d(D) h k l
4.2400 4.2385 .0015 0 0 1
3.7800 3.7827 -.0027 1 2 0
3.6200 3.6220 -.0020 0 -2 1
3.4300 3.4297 .0003 1 1 1
3.3330 3.3375 -.0045 1 -1 1
3.1870 3.1837 .0033 1 2 1
3.0040 3.0084 -.0044 -1 3 0
2.7390 2.7366 .0024 0 5 0
2.6760 2.6764 -.0004 -1 -1 1
2.6190 2.6175 .0015 -1 1 1
2.3970 2.3993 -.0023 1 5 0
2.2660 2.2642 .0018 -1 3 1
A= 4.459 DA= .004
B= 13.73 DB= .01
C= 4.380 DC= .004
GAMMA= 85.33 DGAMMA= .08
BETA = 75.39 DBETA = .04
ALPHA= 89.471 DALPHA= .09
V= 258.6
81. 10-0005
Pb3BeF8
Monoklin
Grupa 14
Dexp Dcal d(D) h k l
4.8100 4.8138 -.0038 0 2 1
4.2200 4.2250 -.0050 2 1 0
4.0300 4.0321 -.0021 0 0 2
3.8300 3.8221 .0079 0 1 2
3.6500 3.6571 -.0071 1 3 0
3.4400 3.4404 -.0004 -1 3 1
3.3000 3.2961 .0039 1 1 2
3.2300 3.2307 -.0007 1 3 1
3.0100 3.0094 .0006 3 0 0
2.9200 2.9190 .0010 3 1 0
2.6200 2.6231 -.0031 0 1 3
2.3000 2.3003 -.0003 0 5 1
a= 9.2260 b= 12.0000 c= 8.241 beta= 101.884
da= .0008 db=.0005 dc=.002 dbet=.003
V= 892.8
Triklin
Dexp Dcal d(D) h k l
4.8100 4.8223 -.0123 -1 0 2
4.2200 4.2129 .0071 0 2 1
4.0300 4.0290 .0010 0 -2 1
3.8300 3.8295 .0005 -1 -2 1
3.6500 3.6567 -.0067 -2 0 1
3.4400 3.4442 -.0042 -1 0 3
3.3000 3.3000 .0000 -1 2 2
3.2300 3.2272 .0028 1 -1 2
3.0100 3.0101 -.0001 2 0 1
2.9200 2.9224 -.0024 1 2 2
2.6200 2.6200 .0000 -1 0 4
2.3000 2.2987 .0013 -1 2 4
A= 7.336 DA= .001
B= 9.0769 DB= .0005
C= 10.501 DC= .001
GAMMA= 86.215 DGAMMA= .006
BETA =107.809 DBETA = .008
ALPHA= 87.9331 DALPHA= .0001
V=663.6
82. 10-0011
Pb*Al*Si*O
Rombik
Groupa 30,53
Dexp. Dcal. d(D) h k l
14.0000 14.9984 -.9984 1 0 0
7.5000 7.4992 .0008 2 0 0
6.2000 6.2406 -.0406 1 0 2
4.2500 4.2414 .0086 1 2 0
3.8000 3.8091 -.0091 2 2 0
3.6000 3.6080 -.0080 1 2 2
3.3100 3.3122 -.0022 3 2 0
3.2100 3.2198 -.0098 3 2 1
3.1000 3.1105 -.0105 1 2 3
3.0000 2.9997 .0003 5 0 0
2.8900 2.8926 -.0026 1 3 0
2.7600 2.7557 .0043 4 1 3
a=15.00 b= 8.84 c=13.72
da= .01 db= .01 dc= .01
V=1820
Monoklin
Grupa 14
Dexp Dcal d(D) h k l
14.0000 14.3894 -.3894 2 0 0
7.5000 7.5132 -.0132 -1 1 1
6.2000 6.2031 -.0031 3 1 1
4.2500 4.2430 .0070 -1 2 1
3.8000 3.8001 -.0001 1 1 4
3.6000 3.5973 .0027 8 0 0
3.3100 3.3083 .0017 5 2 2
3.2100 3.2104 -.0004 -8 0 2
3.1000 3.1015 -.0015 6 2 2
3.0000 3.0013 -.0013 -7 1 3
2.8900 2.8912 -.0012 6 2 3
2.7600 2.7614 -.0014 2 3 2
a= 28.880 b= 8.9050 c= 16.8400 beta= 85.193
da= .001 db= .0002 dc=.0001 dbet=.001
V= 4315.6
83. 10-0212
alfa-PbO2
Monoklin
Grupa 4,11
Dexp Dcal d(D) h k l
3.8200 3.8179 .0021 2 1 0
3.1200 3.1202 -.0002 -1 1 2
2.9700 2.9696 .0004 4 0 0
2.7400 2.7402 -.0002 3 1 1
2.6100 2.6090 .0010 4 0 1
2.2100 2.2102 -.0002 1 1 3
2.0100 2.0106 -.0006 3 0 3
1.8400 1.8399 .0001 6 1 0
1.8100 1.8099 .0001 0 2 3
1.6400 1.6402 -.0002 6 0 2
1.5500 1.5501 -.0001 6 2 0
1.5300 1.5299 .0001 5 1 3
a= 12.1360 b= 4.9843 c=8.07002 beta= 101.824
da=.0008 db=.0002 dc= .00006 dbet=.001
V= 477.7
84. 10-0448
Pb5Sb2Sn3S14
Monoklin
Grupa 4,11
Dexp Dcal d(D) h k l
4.3500 4.3533 -.0033 0 1 1
3.4900 3.4863 .0037 1 1 1
3.1800 3.1799 .0001 -2 0 2
2.9100 2.9095 .0005 2 1 0
2.4600 2.4615 -.0015 -3 0 1
2.3600 2.3609 -.0009 -3 0 2
2.2500 2.2503 -.0003 1 2 1
2.0700 2.0702 -.0002 2 2 0
1.9200 1.9196 .0004 -2 1 4
1.8410 1.8412 -.0002 -4 0 1
1.7370 1.7367 .0003 1 2 3
1.5750 1.5751 -.0001 0 3 2
1.4550 1.4547 .0003 4 2 0
1.3210 1.3211 -.0001 2 1 5
a= 7.3846 b= 5.1030 c= 8.6990 beta=106.429
da= .0004 db=.0008 dc=.0002 dbet=.002
V= 314.4
85. 11-0047
Pb{SbO3}2
Triklin
Dexp Dcal d(D) h k l
5.2900 5.2880 .0020 0 0 1
4.5500 4.5518 -.0018 -1 0 1
4.0200 4.0185 .0015 0 -2 1
3.8300 3.8320 -.0020 -1 2 1
3.4700 3.4707 -.0007 1 -2 1
3.2000 3.1983 .0017 -2 2 0
3.0200 3.0219 -.0019 -2 0 1
2.9600 2.9592 .0008 -2 2 1
2.6800 2.6777 .0023 -2 3 1
2.6400 2.6440 -.0040 0 0 2
2.3800 2.3771 .0029 1 4 0
2.3100 2.3136 -.0036 1 -1 2
A= 6.791 DA= .003
B= 11.906 DB= .003
C= 5.398 DC= .003
GAMMA=105.684 DGAMMA= .003
BETA =100.983 DBETA = .09
ALPHA= 90.672 DALPHA= .002
V= 411.7
86. 11-0063
Ag4PbBi4S9
Triklin
Dexp Dcal d(D) h k l
6.1100 6.1092 .0008 1 0 0
3.3900 3.3896 .0004 0 1 1
3.2700 3.2764 -.0064 1 -1 1
3.1300 3.1271 .0029 1 1 1
2.9300 2.9312 -.0012 0 2 1
2.8200 2.8213 -.0013 -1 0 1
2.6000 2.6011 -.0011 2 0 1
2.0800 2.0805 -.0005 -2 2 1
2.0300 2.0301 -.0001 1 -4 1
1.9610 1.9628 -.0018 -1 5 0
1.7810 1.7808 .0002 1 -1 2
1.7220 1.7203 .0017 1 5 0
A= 6.4103 DA= .0003
B= 9.8514 DB= .0001
C= 3.62925 DC= .00001
GAMMA=102.894 DGAMMA= .002
BETA = 78.2807 DBETA = .0007
ALPHA= 89.552 DALPHA= .001
V=218.4
87. 11-0270
Pb{OH}2
Monoklin
Grupa 4,11
Dexp Dcal d(D) h k l
9.1000 9.1215 -.0215 1 1 0
6.6000 6.5893 .0107 2 0 0
4.8000 4.8002 -.0002 -2 1 1
3.6000 3.5990 .0010 0 1 2
3.4000 3.3984 .0016 1 1 2
3.2300 3.2277 .0023 0 2 2
3.0500 3.0501 -.0001 2 1 2
2.7600 2.7592 .0008 3 3 1
2.7000 2.6986 .0014 -2 4 1
2.6300 2.6300 -.0000 2 4 1
2.5600 2.5598 .0002 -5 0 1
2.3600 2.3599 .0001 2 5 0
2.0000 2.0005 -.0005 2 3 3
1.9300 1.9302 -.0002 -3 5 2
a= 13.2320 b= 12.6380 c= 7.5394 beta= 95.144
da= .0009 db=.0001 dc=.0008 dbet=.001
V= 1255.7
88. 11-0533
Pb5SeO8
Triklin
Dexp Dcal d(D) h k l
8.3000 8.3092 -.0092 -1 1 0
7.5000 7.4723 .0277 1 1 0
6.3000 6.3044 -.0044 1 0 1
5.9000 5.8956 .0044 0 2 0
5.5000 5.4979 .0021 1 -1 1
4.4000 4.3930 .0070 2 1 1
3.2700 3.2726 -.0026 3 1 0
3.1800 3.1823 -.0023 0 0 2
3.1100 3.1082 .0018 3 -2 1
3.0000 3.0011 -.0011 2 3 0
2.9100 2.9078 .0022 -2 -2 1
2.7100 2.7112 -.0012 3 1 2
A= 11.0372 DA= .0006
B= 11.883 DB= .001
C= 6.65591 DC= .00004
GAMMA= 94.83 DGAMMA= .01
BETA = 73.80 DBETA = .01
ALPHA= 86.323 DALPHA= .003
V=832.0
89. 11-0539
Pb2CO4
Triklin
Dexp Dcal d(D) h k l
4.0200 4.0185 .0015 0 2 2
3.9410 3.9419 -.0009 0 -2 2
3.4560 3.4550 .0010 -1 1 0
3.3050 3.3039 .0011 0 0 3
3.1490 3.1483 .0007 -1 2 0
3.1090 3.1094 -.0004 1 -1 1
2.8760 2.8766 -.0006 1 -2 1
2.8010 2.8011 -.0001 1 3 0
2.6090 2.6086 .0004 -1 1 3
2.5190 2.5193 -.0003 1 2 2
2.4510 2.4515 -.0005 1 4 0
2.2970 2.2982 -.0012 1 -4 1
A= 3.63202 DA= .00001
B= 13.35818 DB= .00001
C= 10.04778 DC= .00001
GAMMA= 89.78686 DGAMMA= .00002
BETA = 99.3771 DBETA = .0001
ALPHA= 88.9057 DALPHA= .0001
V=480.9
90. 11-0563
Pb3CO5
Triklin
Dexp Dcal d(D) h k l
2.9500 2.9506 -.0006 2 0 0
2.8700 2.8696 .0004 -2 2 0
2.8000 2.7996 .0004 1 -3 2
2.7200 2.7208 -.0008 -1 -2 2
2.4620 2.4634 -.0014 -1 -3 2
2.3770 2.3764 .0006 2 -2 2
2.3080 2.3074 .0006 2 3 0
2.2430 2.2429 .0001 0 6 0
2.1590 2.1610 -.0020 -2 5 0
2.0220 2.0206 .0014 1 -4 3
1.9670 1.9671 -.0001 3 0 0
1.8240 1.8240 .0000 2 4 2
A= 5.9935 DA= .0001
B= 13.6420 DB= .0006
C= 7.4296 DC= .0001
GAMMA= 99.097 DGAMMA= .002
BETA = 85.193 DBETA = .002
ALPHA= 93.274 DALPHA= .004
V=597.0
91. 12-0005
PbH2P2O7
Triklin
Dexp Dcal d(D) h k l
6.9500 6.9587 -.0087 0 1 1
5.4000 5.4032 -.0032 1 1 0
4.8700 4.8595 .0105 -1 -1 1
4.0000 3.9970 .0030 1 -2 1
3.6700 3.6753 -.0053 1 2 0
3.5000 3.5036 -.0036 2 -1 1
3.3200 3.3226 -.0026 -2 -1 1
3.2000 3.1998 .0002 -2 3 1
3.1600 3.1633 -.0033 0 3 1
2.9100 2.9116 -.0016 -3 2 1
2.7700 2.7696 .0004 -3 1 2
2.4200 2.4194 .0006 0 4 1
A= 8.9249 DA= .0001
B= 10.580 DB= .001
C= 9.425 DC= .002
GAMMA=111.633 DGAMMA= .002
BETA =105.963 DBETA = .004
ALPHA= 79.505 DALPHA= .001
V=791.9
92. 12-0006
Pb2{PO3}4
Triklin
Dexp Dcal d(D) h k l
7.2000 7.1893 .0107 1 0 0
5.8300 5.8280 .0020 0 1 0
4.3400 4.3446 -.0046 0 -1 1
3.8900 3.8891 .0009 1 1 0
3.2500 3.2509 -.0009 -2 0 1
3.1400 3.1464 -.0064 2 -1 1
2.9500 2.9524 -.0024 1 0 2
2.6500 2.6508 -.0008 0 -2 1
2.5600 2.5571 .0029 -1 -1 2
2.4400 2.4377 .0023 2 1 1
2.3900 2.3913 -.0013 2 -1 2
2.1600 2.1612 -.0012 -1 0 3
A= 7.738 DA= .001
B= 6.261 DB= .001
C= 6.684 DC= .006
GAMMA=111.42 DGAMMA= .03
BETA = 94.348 DBETA = .005
ALPHA= 87.37 DALPHA= .05
V= 300.5
93. 12-0018
Pb3P4O13
Triklin
Dexp Dcal d(D) h k l
7.5000 7.4924 .0076 1 0 0
6.2500 6.2270 .0230 0 1 0
5.7500 5.7503 -.0003 0 0 2
4.9600 4.9821 -.0221 1 1 2
4.6000 4.6108 -.0108 0 1 2
3.8000 3.8024 -.0024 2 1 2
3.6800 3.6796 .0004 2 1 0
3.5000 3.5037 -.0037 1 -1 2
3.3000 3.3007 -.0007 -2 0 1
3.2000 3.1979 .0021 1 2 0
3.0300 3.0282 .0018 1 1 4
2.9700 2.9665 .0035 2 2 1
A= 8.2751 DA= .0003
B= 6.691 DB= .005
C= 12.39 DC= .01
GAMMA= 70.56 DGAMMA= .06
BETA = 70.13 DBETA = .07
ALPHA= 75.17 DALPHA= .07
V=600.5
94. 13-0239
Pb2Al4{CO3}4{OH}8*3H2O
Triklin
Dexp Dcal d(D) h k l
7.9500 7.9754 -.0254 0 1 1
6.0700 6.0762 -.0062 0 -1 1
4.6400 4.6327 .0073 1 0 1
4.5800 4.5796 .0004 0 2 1
4.5400 4.5382 .0018 -1 0 1
4.3900 4.3972 -.0072 -1 1 1
4.0400 4.0449 -.0049 1 -1 1
3.6000 3.6021 -.0021 1 1 2
3.2300 3.2308 -.0008 0 2 3
3.0900 3.0900 .0000 0 3 1
3.0400 3.0381 .0019 0 -2 2
2.9760 2.9758 .0002 0 3 0
A= 5.100 DA= .001
B= 9.300 DB= .002
C= 11.035 DC= .002
GAMMA= 94.59 DGAMMA= .04
BETA = 89.78 DBETA = .03
ALPHA= 74.44 DALPHA= .01
V= 502.4
95. 13-0245
Pb5P4O15
Monoklin
Grupa 4,11
Dexp Dcal d(D) h k l
5.8700 5.8769 -.0069 -1 1 1
4.6000 4.6060 -.0060 0 0 4
4.4600 4.4541 .0059 -2 0 1
4.3500 4.3455 .0045 2 0 2
4.2900 4.2919 -.0019 1 0 4
4.1700 4.1731 -.0031 0 2 1
4.0000 3.9946 .0054 -1 0 4
3.8700 3.8756 -.0056 2 1 2
3.7900 3.7848 .0052 -1 2 1
3.5200 3.5139 .0061 0 2 3
3.4000 3.3851 .0149 0 1 5
3.3300 3.3291 .0009 -1 0 5
a= 9.429 b= 8.569 c= 18.500 beta= 84.79
da= .001 db=.007 dc=.001 dbet=.01
V= 1488
Triklin
exp Dcal d(D) h k l
5.8700 5.8747 -.0047 2 0 0
4.6000 4.6069 -.0069 1 1 0
4.4600 4.4636 -.0036 -2 0 1
4.3500 4.3521 -.0021 0 -1 1
4.2900 4.2902 -.0002 -1 1 0
4.1700 4.1621 .0079 1 -1 1
4.0000 4.0047 -.0047 -1 -1 1
3.8700 3.8579 .0121 3 0 2
3.7900 3.7880 .0020 -1 1 1
3.5200 3.5165 .0035 0 -1 2
3.4000 3.4021 -.0021 -2 -1 1
3.3300 3.3303 -.0003 -2 0 2
A= 12.664 DA= .002
B= 4.8241 DB= .0006
C= 11.073 DC= .007
GAMMA= 83.79 DGAMMA= .05
BETA = 68.85 DBETA = .02
ALPHA= 87.85 DALPHA= .06
V=627.1
96. 13-0274
5PbO*P2O5*SiO2
Triklin
Dexp Dcal d(D) h k l
4.9000 4.8832 .0168 0 1 1
4.2500 4.2414 .0086 0 -1 1
4.0800 4.0791 .0009 -2 0 1
3.6600 3.6638 -.0038 2 0 1
3.3600 3.3568 .0032 -2 1 1
3.2100 3.2063 .0037 2 1 1
2.9300 2.9262 .0038 2 -1 1
2.8500 2.8468 .0032 -2 1 2
2.2400 2.2415 -.0015 0 -1 3
2.1800 2.1807 -.0007 -2 2 2
2.1200 2.1207 -.0007 0 -2 2
2.0400 2.0395 .0005 -4 0 2
A= 8.921 DA= .001
B= 5.60694 DB= .00001
C= 7.998 DC= .002
GAMMA= 88.99 DGAMMA= .01
BETA = 96.96 DBETA = .01
ALPHA= 81.65 DALPHA= .02
V=392.6
97. 13-0275
gamma-Pb4SiO6
Triklin
Dexp Dcal d(D) h k l
7.3100 7.3173 -.0073 1 0 0
5.9100 5.9110 -.0010 0 1 1
5.4700 5.4705 -.0005 0 -1 1
4.6200 4.6199 .0001 0 0 2
3.2200 3.2224 -.0024 -2 0 1
3.1200 3.1243 -.0043 -2 1 0
3.0200 3.0211 -.0011 -2 -1 1
2.9500 2.9509 -.0009 1 2 2
2.9200 2.9214 -.0014 1 1 3
2.7200 2.7212 -.0012 2 2 0
2.6600 2.6600 -.0000 -2 0 2
2.5400 2.5379 .0021 -1 1 3
A= 7.482 DA= .003
B= 7.279 DB= .001
C= 9.419 DC= .002
GAMMA= 82.73 DGAMMA= .01
BETA = 79.779 DBETA = .01
ALPHA= 84.251 DALPHA= .007
V= 499.1
98. 13-0276
PbP2O6
Triklin
Dexp Dcal d(D) h k l
8.6700 8.6497 .0203 1 0 0
7.6300 7.6357 -.0057 0 1 0
7.2500 7.2365 .0135 0 -1 1
6.6100 6.6074 .0026 -1 1 0
5.9100 5.8896 .0204 -1 0 1
5.0700 5.0733 -.0033 1 -1 2
4.8000 4.8233 -.0233 0 0 2
4.7200 4.7250 -.0050 -1 -1 1
4.5800 4.5691 .0109 2 -1 1
4.3500 4.3454 .0046 1 1 1
3.9000 3.8989 .0011 -1 0 2
3.8200 3.8179 .0021 0 2 0
A= 9.38 DA= .02
B= 8.5822 DB= .0001
C= 10.703 DC= .007
GAMMA=109.873 DGAMMA= .005
BETA = 72.31 DBETA = .03
ALPHA=113.194 DALPHA= .008
V= 730.4
99. 13-0277
Pb8P2O13
Monoklin
Grupa 4,11
Dexp Dcal d(D) h k l
7.1400 7.1630 -.0230 0 1 1
6.8100 6.8094 .0006 1 1 0
4.8200 4.8308 -.0108 0 2 1
4.7200 4.7178 .0022 1 2 0
4.3700 4.3621 .0079 1 1 2
3.6300 3.6294 .0006 1 2 2
3.4800 3.4785 .0015 -2 0 1
3.1300 3.1399 -.0099 2 2 2
3.0500 3.0491 .0009 -1 2 2
2.9500 2.9507 -.0007 1 3 2
2.8900 2.8895 .0005 3 1 1
2.8400 2.8396 .0004 3 0 0
a= 8.965 b= 11.332 c= 9.728 beta=71.842
da= .001 db=.001 dc= .001 dbet= .008
V= 939.1
100. 13-0278
Pb3{PO4}2
Rombik
Groupa 29,57
Dexp. Dcal. d(D) h k l
6.7100 6.7439 -.0339 2 0 0
4.7200 4.6980 .0220 1 1 1
4.6000 4.5830 .0170 2 1 0
3.4900 3.4841 .0059 0 1 2
3.1200 3.1236 -.0036 0 2 0
3.0500 3.0431 .0069 1 2 0
2.8400 2.8343 .0057 2 2 0
2.7500 2.7540 -.0040 3 1 2
2.4700 2.4637 .0063 1 2 2
2.2500 2.2480 .0020 6 0 0
2.0800 2.0824 -.0024 0 3 0
2.0500 2.0511 -.0011 6 1 1
a=13.488 b= 6.247 c= 8.3951
da= .008 db= .001 dc= .0007
V= 707.4
Triklin
Dexp Dcal d(D) h k l
6.7100 6.7172 -.0072 1 0 0
4.7200 4.7209 -.0009 0 1 1
4.6000 4.5941 .0059 0 -1 1
3.4900 3.4860 .0040 1 0 2
3.1200 3.1212 -.0012 0 1 2
3.0500 3.0475 .0025 0 -1 2
2.8400 2.8391 .0009 2 1 1
2.7500 2.7554 -.0054 1 -2 1
2.4700 2.4712 -.0012 -2 -1 1
2.2500 2.2528 -.0028 1 -1 3
2.0800 2.0803 -.0003 2 -1 3
2.0500 2.0497 .0003 0 3 0
A= 6.9183 DA= .0004
B= 6.177 DB= .001
C= 7.312 DC= .001
GAMMA= 95.20 DGAMMA= .01
BETA = 77.237 DBETA = .005
ALPHA= 89.62 DALPHA= .03
V= 303.4
101. 13-0279
Pb2SiO4
Triklin
Dexp Dcal d(D) h k l
6.0300 6.0281 .0019 1 0 0
4.2900 4.2911 -.0011 -1 1 0
3.7100 3.7111 -.0011 -1 -1 2
3.5600 3.5567 .0033 0 0 2
3.2200 3.2201 -.0001 -1 -2 2
3.1300 3.1295 .0005 -2 0 1
3.0000 2.9994 .0006 -1 2 0
2.9500 2.9473 .0027 -1 1 2
2.8900 2.8846 .0054 0 -2 2
2.8000 2.8006 -.0006 1 3 0
2.5800 2.5792 .0008 -1 -3 2
2.5500 2.5496 .0004 2 1 1
A= 6.7373 DA= .0003
B= 8.788 DB= .006
C= 7.6840 DC= .0008
GAMMA= 69.58 DGAMMA= .01
BETA =110.84 DBETA = .02
ALPHA=104.17 DALPHA= .05
V= 394.7
102. 13-0280
Pb5B2SiO10
Triklin
Dexp Dcal d(D) h k l
6.6100 6.6111 -.0011 1 0 0
6.0300 6.0272 .0028 -1 1 1
4.8500 4.8413 .0087 -1 -1 1
4.3500 4.3472 .0028 -1 2 1
4.2100 4.2125 -.0025 -1 0 2
4.0000 4.0030 -.0030 1 2 0
3.8700 3.8675 .0025 0 2 2
3.7100 3.7105 -.0005 1 2 1
3.5600 3.5578 .0022 0 -2 1
3.4300 3.4291 .0009 0 3 1
3.2900 3.2917 -.0017 -2 1 2
3.2200 3.2201 -.0001 -2 0 2
A= 7.169 DA= .003
B= 10.327 DB= .004
C= 9.3698 DC= .0008
GAMMA= 94.83 DGAMMA= .08
BETA =112.43 DBETA = .09
ALPHA= 67.85 DALPHA= .01
V= 592.4
103. 13-0281
Pb3P4)O13
Triklin
Dexp Dcal d(D) h k l
7.5600 7.5863 -.0263 0 1 1
6.6100 6.6154 -.0054 0 -1 1
5.8700 5.8615 .0085 1 1 1
5.0700 5.0858 -.0158 -1 1 0
4.8200 4.8188 .0012 1 -1 1
4.7200 4.7093 .0107 0 2 1
4.5800 4.5872 -.0072 1 0 2
3.8500 3.8521 -.0021 1 -1 2
3.7900 3.7932 -.0032 0 2 2
3.6900 3.6922 -.0022 -1 2 0
3.5200 3.5199 .0001 -1 0 2
3.4100 3.4072 .0028 -1 2 1
A= 6.7705 DA= .0008
B= 10.184 DB= .001
C= 10.569 DC= .001
GAMMA= 79.66 DGAMMA= .01
BETA = 73.116 DBETA = .009
ALPHA= 79.62 DALPHA= .01
V=679.5