383. 46-0063
AgPb4I9
Monoklin
Grupa 4,11
Dexp Dcal d(D) h k l
6.9680 6.9771 -.0091 -1 0 1
3.8410 3.8397 .0013 2 1 0
3.1520 3.1510 .0010 1 2 0
2.8810 2.8798 .0012 2 0 2
2.3990 2.3983 .0007 1 1 3
2.3460 2.3443 .0017 4 0 0
2.2820 2.2840 -.0020 3 2 0
2.1920 2.1968 -.0048 -3 1 3
2.1720 2.1716 .0004 -1 2 3
1.9730 1.9729 .0001 0 3 2
1.8550 1.8550 .0000 -3 1 4
1.7610 1.7615 -.0005 5 0 1
a= 9.552 b= 6.6911 c= 8.6179 beta= 100.974
da=.001 db= .0006 dc=.0003 dbet=.003
V= 540.7
384. 47-0859
K2PbP2O7
Triklin
Dexp Dcal d(D) h k l
9.7300 9.6755 .0545 1 0 1
6.3800 6.3743 .0057 2 0 1
5.3950 5.3975 -.0025 1 1 2
5.1390 5.1379 .0011 0 2 1
4.8390 4.8378 .0012 2 0 2
4.7380 4.7387 -.0007 2 2 0
4.5250 4.5245 .0005 0 -2 1
4.3370 4.3341 .0029 1 -1 2
4.2770 4.2744 .0026 -2 -1 1
4.2390 4.2318 .0072 3 2 1
3.9610 3.9627 -.0017 3 0 2
3.8770 3.8816 -.0046 2 3 1
A= 14.03 DA= .01
B= 11.942 DB= .005
C= 11.061 DC= .003
GAMMA= 69.20 DGAMMA= .04
BETA = 62.81 DBETA = .04
ALPHA= 73.46 DALPHA= .05
V= 1524.1
385. 48-1541
Bi4PbS7
Triklin
exp Dcal d(D) h k l
5.9500 5.9430 .0070 -1 1 0
4.9500 4.9479 .0021 1 1 1
3.7700 3.7685 .0015 2 0 0
3.5900 3.5909 -.0009 1 -2 1
3.5000 3.5009 -.0009 1 0 2
3.4200 3.4175 .0025 0 1 2
3.3200 3.3217 -.0017 1 1 2
3.3000 3.3018 -.0018 0 -1 2
3.2400 3.2385 .0015 1 -1 2
2.9700 2.9715 -.0015 -2 2 0
2.9100 2.9093 .0007 -1 3 0
2.8600 2.8595 .0005 1 3 0
A= 7.6632 DA= .0005
B= 9.3786 DB= .0003
C= 7.3228 DC= .0002
GAMMA= 90.893 DGAMMA= .005
BETA = 79.684 DBETA = .002
ALPHA= 87.267 DALPHA= .001
V=517.2
386. 48-1981
C28H54O4Pb*0.05C36H72NO8P
Tetragon
Groupa 90,113
Dexp. Dcal. d(D) h k l
42.4400 40.5548 1.8852 0 0 1
20.3400 20.2774 .0626 0 0 2
13.5900 13.5183 .0717 0 0 3
10.1600 10.1387 .0213 0 0 4
8.0700 8.0659 .0041 1 0 1
6.7400 6.7591 -.0191 0 0 6
5.7600 5.7607 -.0007 1 1 1
5.0700 5.0694 .0006 0 0 8
a= 8.230 c= 40.554
da= .003 dc= .009
V=2747
387. 48-1982
C36H70O4Pb*0.08C44H88NO8P
Rombik
Groupa 31,59
Dexp. Dcal. d(D) h k l
50.4800 50.3966 .0834 1 0 0
25.0800 25.1983 -.1183 2 0 0
16.6600 16.7989 -.1389 3 0 0
12.6200 12.5991 .0209 4 0 0
10.0600 10.0566 .0034 1 1 0
8.4000 8.3994 .0006 6 0 0
7.1900 7.1912 -.0012 5 1 0
6.2800 6.2800 .0000 4 0 1
5.6000 5.5996 .0004 9 0 0
a=50.396 b=10.263 c= 7.244
da= .008 db= .005 dc= .005
V=3747
388. 48-2083
C14H10O4Pb*H2O
Triklin
Dexp Dcal d(D) h k l
14.7300 14.7269 .0031 0 0 1
7.6800 7.6818 -.0018 0 1 1
6.2700 6.2693 .0007 2 0 1
5.7300 5.7275 .0025 2 0 2
5.1200 5.1200 .0000 -2 1 0
4.2300 4.2372 -.0072 1 -1 3
3.8100 3.8080 .0020 1 2 1
3.3400 3.3404 -.0004 0 -2 2
3.0800 3.0804 -.0004 1 1 5
2.8400 2.8346 .0054 4 1 2
2.7700 2.7667 .0033 -1 2 4
2.5600 2.5606 -.0006 0 3 3
A= 12.6068 DA= .0002
B= 8.302 DB= .001
C= 16.001 DC= .006
GAMMA= 95.86 DGAMMA= .02
BETA = 68.91 DBETA = .03
ALPHA= 83.387 DALPHA= .007
V=1533.5
389. 48-2084
C14H10O4Pb*10CH2O2*H2O
Triklin
Dexp Dcal d(D) h k l
6.0200 6.0182 .0018 0 1 1
5.5400 5.5366 .0034 -1 1 0
4.5900 4.5821 .0079 0 -1 1
4.4800 4.4838 -.0038 -1 1 2
3.8700 3.8668 .0032 -2 1 1
3.7800 3.7876 -.0076 2 0 0
3.7100 3.7074 .0026 -2 0 1
3.3800 3.3802 -.0002 -1 2 1
3.1300 3.1271 .0029 0 0 3
2.9100 2.9100 -.0000 2 1 0
2.8000 2.7978 .0022 2 1 1
2.6700 2.6718 -.0018 1 2 1
A= 8.0796 DA= .0001
B= 6.80171 DB= .00001
C= 10.09898 DC= .00001
GAMMA=108.5715 DGAMMA= .0004
BETA =103.93970 DBETA = .00009
ALPHA= 69.9304 DALPHA= .0001
V=488.7
390. 48-2085
C14H10O6Pb*10CH2O2
Triklin
Dexp Dcal d(D) h k l
5.6400 5.6476 -.0076 -1 0 1
5.2100 5.2109 -.0009 0 1 1
5.0000 4.9984 .0016 0 -1 1
4.3700 4.3715 -.0015 1 0 1
4.2600 4.2599 .0001 1 1 0
3.6000 3.6010 -.0010 -1 0 2
3.3100 3.3062 .0038 0 1 2
3.2500 3.2572 -.0072 0 2 1
3.0200 3.0214 -.0014 1 -2 1
2.9800 2.9836 -.0036 -1 -1 2
2.8300 2.8314 -.0014 -1 2 2
2.7100 2.7108 -.0008 -2 -1 1
A= 7.154 DA= .001
B= 7.506 DB= .002
C= 7.6046 DC= .0004
GAMMA=108.08 DGAMMA= .01
BETA =106.03 DBETA = .03
ALPHA= 82.90 DALPHA= .01
V= 372.8
391. 49-0135
Pb3Cr2{SCN}12
Triklin
Dexp Dcal d(D) h k l
7.9000 7.8996 .0004 1 0 0
5.3400 5.3413 -.0013 -1 1 1
4.9800 4.9834 -.0034 -1 -1 1
4.4800 4.4770 .0030 -2 1 0
4.1100 4.1104 -.0004 0 -2 1
3.0200 3.0212 -.0012 0 1 2
2.9600 2.9578 .0022 -3 1 0
2.8400 2.8418 -.0018 1 -3 0
2.8100 2.8092 .0008 0 -1 3
2.7500 2.7493 .0007 2 -2 2
2.6200 2.6218 -.0018 3 -2 1
2.5800 2.5807 -.0007 -1 -2 3
A= 9.218 DA= .001
B= 8.9575 DB= .0002
C= 8.676 DC= .001
GAMMA=112.591 DGAMMA= .006
BETA =103.43 DBETA = .07
ALPHA=105.06 DALPHA= .01
V= 592.9
392. 49-1418
Bi1.42Pb3.23S5.35
Triklin
Dexp Dcal d(D) h k l
4.5700 4.5757 -.0057 -1 2 1
3.9000 3.9012 -.0012 -1 -2 1
3.7200 3.7206 -.0006 1 2 3
3.5100 3.5078 .0022 0 4 0
3.3800 3.3778 .0022 1 -2 3
3.3200 3.3221 -.0021 0 0 4
3.2300 3.2312 -.0012 -1 2 3
3.1400 3.1392 .0008 2 0 2
3.0800 3.0807 -.0007 1 -4 1
2.9900 2.9930 -.0030 -2 2 0
2.9200 2.9157 .0043 -2 0 1
2.8400 2.8378 .0022 -2 2 1
A= 6.48411 DA= .00000
B= 14.33354 DB= .00005
C= 13.87337 DC= .00002
GAMMA= 93.6813 DGAMMA= .0002
BETA = 77.54459 DBETA = .00008
ALPHA= 79.8954 DALPHA= .0002
V=1233
393. 49-1419
Bi1.94Pb2.58S5.48
Triklin
Dexp Dcal d(D) h k l
4.0400 4.0401 -.0001 -1 1 1
3.6400 3.6302 .0098 0 2 0
3.4800 3.4775 .0025 2 0 0
3.3800 3.3732 .0068 2 -1 1
3.3500 3.3482 .0018 2 0 2
3.3100 3.3103 -.0003 0 2 1
3.1800 3.1810 -.0010 2 1 1
3.1000 3.0998 .0002 0 0 3
3.0400 3.0458 -.0058 -1 1 2
2.9900 2.9913 -.0013 1 -2 2
2.0000 2.0006 -.0006 -3 -1 1
2.7600 2.7583 .0017 -2 1 1
A= 7.3622 DA= .0001
B= 7.29230 DB= .0001
C= 9.85432 DC= .00006
GAMMA= 93.990 DGAMMA= .002
BETA = 71.02737 DBETA = .00008
ALPHA= 94.782 DALPHA= .002
V=498.0
394. 49-1961
C20H38O4Pb
Geksagon
Groupa 186,190,194
Dexp. Dcal. d(D) h k l
30.7000 30.5450 .1550 0 0 1
15.2800 15.2725 .0075 0 0 2
10.1300 10.1351 -.0051 1 0 0
7.6400 7.6362 .0038 0 0 4
6.1000 6.0989 .0011 1 0 4
5.0900 5.0908 -.0008 0 0 6
a= 11.703 c= 30.54
da= .004 dc= .01
V=3622.9
395. 49-1963
C20H38O4Pb*0.04C28H56NO8P
Geksagon
Groupa 143
Dexp. Dcal. d(D) h k l
32.7000 32.2293 .4707 0 0 1
16.3500 16.1147 .2353 0 0 2
10.6700 10.7431 -.0731 0 0 3
8.0100 7.9898 .0202 1 0 3
6.3400 6.3434 -.0034 1 1 2
a= 13.8 c= 32.2
da= .01 dc=.1
v=5316
396. 49-1964
C28H54O4Pb
Geksagon
Groupa 143
Dexp. Dcal. d(D) h k l
41.6400 40.0612 1.5788 0 0 1
19.9700 20.0306 -.0606 0 0 2
13.3400 13.3537 -.0137 0 0 3
9.9700 10.0153 -.0453 0 0 4
8.0100 8.0100 .0000 1 0 0
6.6800 6.6769 .0031 0 0 6
5.7200 5.7230 -.0030 0 0 7
5.0100 5.0076 .0024 0 0 8
a= 9.2492 c= 40.061
da= .0002 dc=.03
V=2968
397. 49-1986
C14H10O4Pb*4C2H4O2*H2O
Triklin
Dexp Dcal d(D) h k l
11.5400 11.5401 -.0001 1 0 0
7.2900 7.2825 .0075 0 1 0
5.9600 5.9616 -.0016 -1 0 1
5.7100 5.7045 .0055 2 0 1
5.4300 5.4198 .0102 1 -1 1
5.1000 5.1006 -.0006 -1 -1 1
4.2900 4.2885 .0015 2 -1 1
3.8700 3.8756 -.0056 0 -1 2
3.7100 3.7069 .0031 1 1 2
3.3400 3.3410 -.0010 1 2 1
3.1200 3.1173 .0027 -3 -1 1
3.0600 3.0610 -.0010 -2 -2 1
A= 12.3492 DA= .0009
B= 7.4318 DB= .0002
C= 8.96194 DC= .00602
GAMMA= 81.06 DGAMMA= .01
BETA = 72.04 DBETA = .01
ALPHA= 94.07 DALPHA= .02
V= 766.7
398. 49-1987
C14H10O6Pb*2H2O
Triklin
Dexp Dcal d(D) h k l
16.9900 16.7216 .2684 0 0 1
8.3000 8.3608 -.0608 0 0 2
5.6600 5.6548 .0052 0 1 1
4.2800 4.2805 -.0005 1 1 2
3.7700 3.7687 .0013 1 -1 1
3.4200 3.4201 -.0001 1 1 4
3.1900 3.1884 .0016 -1 1 3
2.8500 2.8500 -.0000 0 2 0
2.6500 2.6505 -.0005 1 2 3
2.4500 2.4505 -.0005 -1 2 1
2.3600 2.3586 .0014 -2 1 2
2.1800 2.1799 .0001 -1 2 4
A= 6.0298 DA= .0007
B= 5.824 DB= .002
C= 17.14 DC= .03
GAMMA= 81.65 DGAMMA= .07
BETA = 80.5 DBETA = .2
ALPHA= 80.4 DALPHA= .1
V= 581.0
399. 49-2312
C12H36O6S6*Pb3Cr3{SCN}12
Triklin
Dexp Dcal d(D) h k l
8.4400 8.4465 -.0065 1 0 0
7.5800 7.5903 -.0103 1 1 0
6.2100 6.2172 -.0072 1 0 1
5.7900 5.7773 .0127 -1 0 1
5.3600 5.3644 -.0044 1 -1 1
4.7300 4.7351 -.0051 1 2 0
4.5700 4.5736 -.0036 0 2 0
4.3200 4.3163 .0037 -1 -1 2
4.2100 4.2008 .0092 0 -2 2
3.9900 3.9930 -.0030 1 -1 2
3.6700 3.6747 -.0047 -2 0 1
3.5400 3.5395 .0005 1 2 1
A= 8.995 DA= .009
B= 10.899 DB= .006
C= 9.557 DC= .005
GAMMA= 70.32 DGAMMA= .05
BETA = 95.30 DBETA = .03
ALPHA=117.14 DALPHA= .05
V= 782.9
400. 49-2313
C18H42N6O6*Pb3Cr2{SCN}12
Triklin
Dexp Dcal d(D) h k l
8.4000 8.3997 .0003 -1 1 0
7.5600 7.5572 .0028 1 1 0
6.2000 6.2106 -.0106 0 0 1
5.7500 5.7506 -.0006 0 1 1
5.3300 5.3230 .0070 1 2 0
4.7000 4.6985 .0015 0 2 1
4.5500 4.5480 .0020 0 3 0
4.3100 4.3109 -.0009 -1 3 0
4.2000 4.1998 .0002 -2 2 0
3.9600 3.9584 .0016 1 3 0
3.6500 3.6481 .0019 -2 0 1
3.5300 3.5304 -.0004 -1 3 1
A= 9.8909 DA= .0009
B= 13.737 DB= .001
C= 6.2528 DC= .0004
GAMMA= 96.15 DGAMMA= .02
BETA = 83.859 DBETA = .008
ALPHA= 88.125 DALPHA= .009
V= 839.0