48. 4-0534
Pb2OF2
Geksagon
Grupa 143
Dexp. Dcal. d(D) h k l
3.3300 3.3294 .0006 1 0 1
2.8800 2.8800 .0000 0 0 2
2.0400 2.0400 .0000 2 0 0
a= 4.71118 c= 5.76000
da= - dc= -
V= 110.7
49. 4-0580
PbThO3
Tetragon
Groupa 106,135
Dexp. Dcal. d(D) h k l
3.1700 3.1635 .0065 2 0 0
2.8300 2.8295 .0005 2 1 0
2.0000 2.0007 -.0007 3 1 0
1.6900 1.6900 .0000 0 0 2
a= 6.3269 c= 3.3800
da= .000074 dc= .0001
V= 135.3
50. 4-0710
PbSeO3
Triklin
Dexp Dcal d(D) h k l
4.1300 4.1297 .0003 1 1 1
3.3900 3.3894 .0006 2 1 0
3.3100 3.3098 .0002 -1 -1 1
3.1400 3.1389 .0011 1 1 2
2.7400 2.7390 .0010 -2 -1 1
2.2400 2.2387 .0013 -3 -1 1
2.0700 2.0691 .0009 1 -2 1
2.0200 2.0204 -.0004 0 2 2
1.8900 1.8904 -.0004 5 0 2
1.7800 1.7799 .0001 0 0 4
1.7300 1.7300 -.0000 5 1 3
1.6800 1.6800 -.0000 -4 0 2
A= 9.713 DA= .005
B= 4.6470 DB= .0002
C= 7.616 DC= .002
GAMMA= 82.22 DGAMMA= .03
BETA = 69.99 DBETA = .01
ALPHA= 81.99 DALPHA= .02
V= 318.4
51. 4-0710
PbSeO3
Monoklin
Grupa 4,11
Dexp Dcal d(D) h k l
4.1300 4.1282 .0018 2 1 0
3.3900 3.3937 -.0037 -3 0 1
3.3100 3.3069 .0031 1 1 2
3.1400 3.1387 .0013 -2 1 2
2.7400 2.7379 .0021 -2 2 1
2.2400 2.2407 -.0007 -4 1 2
2.0700 2.0704 -.0004 -4 0 3
2.0200 2.0199 .0001 4 1 2
1.8900 1.8902 -.0002 -2 3 2
1.7800 1.7795 .0005 -5 2 1
1.7300 1.7298 .0002 -1 0 5
1.6800 1.6806 -.0006 3 3 2
1.5800 1.5800 -.0000 -3 1 5
1.5500 1.5501 -.0001 6 0 2
1.5100 1.5100 .0000 3 4 0
1.4500 1.4499 .0001 -3 4 2
a= 10.5740 b=6.6970 c= 8.6542 beta= 97.414
da= .0009 db=.0004 dc= .0002 dbet=.003
V= 607.7
52. 4-0735
Na15Pb4
Tetragon
Groupa 85,118,129
Dexp. Dcal. d(D) h k l
4.7100 4.7068 .0032 1 1 0
2.8400 2.8386 .0014 0 0 1
2.6100 2.6111 -.0011 1 0 1
a= 6.656 c= 2.8386
da= .009 dc= .0003
V= 125.8
53. 5-0017
C12H22O4Pb
Triklin
Dexp Dcal d(D) h k l
20.7000 20.3207 .3793 1 0 0
10.2000 10.2095 -.0095 0 1 0
6.8500 6.8483 .0017 2 0 2
6.0500 6.0275 .0225 1 -1 2
5.8400 5.8449 -.0049 2 1 2
5.0800 5.0802 -.0002 4 0 0
4.9200 4.9211 -.0011 0 2 1
4.7800 4.7825 -.0025 0 -2 1
4.5200 4.5211 -.0011 -2 2 0
4.4100 4.4117 -.0017 2 -1 3
4.2600 4.2601 -.0001 3 1 3
4.2300 4.2326 -.0026 -3 -1 2
A= 20.7220 DA= .00024
B= 10.2267 DB= .0001
C= 15.8794 DC= .0008
GAMMA= 88.1565 DGAMMA= .0008
BETA = 78.783 DBETA = .001
ALPHA= 86.9374 DALPHA= .0002
V=3295.5
54. 5-0332
C20H38PbO4
Triklin
Dexp Dcal d(D) h k l
30.9000 29.3941 1.5059 1 0 0
15.0000 14.6970 .3030 2 0 0
7.6100 7.6562 -.0462 -4 1 0
6.0300 6.0265 .0035 4 1 1
4.8030 4.7912 .0118 -1 -3 1
4.0340 4.0344 -.0004 4 -3 3
3.8800 3.8834 -.0034 7 -2 3
3.7980 3.7987 -.0007 -2 1 3
3.7210 3.7222 -.0012 6 2 0
3.6120 3.6154 -.0034 -5 -1 2
3.4800 3.4796 .0004 3 0 4
3.3970 3.3995 -.0025 2 -2 4
A= 33.15 DA= .01
B= 17.599 DB= .002
C= 14.2251 DC= .0005
GAMMA=111.03 DGAMMA= .03
BETA = 68.954 DBETA = .002
ALPHA=101.83 DALPHA= .02
V=3709.8
55. 5-0630
K2Pb4Si8O21
triklin
Dexp Dcal d(D) h k l
8.1000 8.1002 -.0002 1 0 0
6.5500 6.5504 -.0004 0 1 1
5.8000 5.8110 -.0110 0 -1 1
3.7000 3.7037 -.0037 -1 0 2
3.5000 3.5011 -.0011 2 0 1
3.2800 3.2800 .0000 -2 1 0
2.7600 2.7591 .0009 -3 -2 1
2.7100 2.7102 -.0002 3 1 1
2.6200 2.6194 .0006 1 4 0
2.5750 2.5740 .0010 -2 2 1
2.3650 2.3650 .0000 0 -3 2
2.3100 2.3101 -.0001 3 1 2
A= 8.8978 DA= .0001
B= 10.612 DB= .001
C= 8.056 DC= .002
GAMMA= 65.972 DGAMMA= .002
BETA = 91.924 DBETA = .006
ALPHA= 84.437 DALPHA= .005
V= 689.2
56. 6-0177
Pb2OBr2*H2O
Triklin
Dexp Dcal d(D) h k l
5.9600 5.9594 .0006 0 1 1
5.0300 5.0294 .0006 0 -1 1
4.1600 4.1615 -.0015 -1 2 0
3.7600 3.7606 -.0006 0 3 1
3.7100 3.7051 .0049 -1 0 1
3.4800 3.4837 -.0037 -1 2 1
3.3800 3.3846 -.0046 1 -2 1
3.0500 3.0479 .0021 1 3 1
2.9800 2.9797 .0003 0 2 2
2.9200 2.9207 -.0007 -1 -2 1
2.7500 2.7461 .0039 -1 4 0
2.7200 2.7221 -.0021 0 3 2
A= 5.277 DA= .003
B= 12.487 DB= .008
C= 6.262 DC= .005
GAMMA= 93.92 DGAMMA= .09
BETA = 82.85 DBETA = .03
ALPHA= 78.48 DALPHA= .05
V= 399.3
57. 6-0178
PbP2O7*2PbBr2
Rombik
Groupa 34,58
Dexp. Dcal. d(D) h k l
4.1400 4.1402 -.0002 1 1 0
3.7400 3.7336 .0064 1 1 1
3.2000 3.2016 -.0016 2 1 0
2.9900 2.9890 .0010 1 1 2
2.5700 2.5721 -.0021 2 1 2
2.4800 2.4774 .0026 3 1 0
2.3800 2.3814 -.0014 3 1 1
2.1600 2.1598 .0002 0 0 4
2.0700 2.0701 -.0001 2 2 0
a= 8.745 b= 4.700 c= 8.639
da= .009 db= .003 dc= .009
V= 355.1
58. 6-0269
Pb2P2O7
Triklin
Dexp Dcal d(D) h k l
6.4000 6.3621 .0379 0 2 0
6.1000 6.0977 .0023 1 0 0
5.7000 5.6956 .0044 -1 1 1
5.2000 5.1960 .0040 -1 -1 1
4.9000 4.9019 -.0019 0 0 3
4.7000 4.6979 .0021 -1 -1 2
4.4500 4.4474 .0026 0 2 2
4.0800 4.0813 -.0013 -1 2 2
3.7100 3.7061 .0039 0 -1 4
3.4600 3.4590 .0010 1 -2 3
3.3400 3.3398 .0002 -1 3 2
3.1800 3.1811 -.0011 0 4 0
A= 6.275 DA= .002
B= 13.102 DB= .001
C= 15.078 DC= .001
GAMMA= 99.66 DGAMMA= .01
BETA = 98.07 DBETA = .01
ALPHA= 98.31 DALPHA= .01
V=1192
59. 6-0272
Pb2OBr2
Triklin
Dexp Dcal d(D) h k l
8.6100 8.5650 .0450 -1 0 1
6.2000 6.2133 -.0133 1 -1 1
6.0000 6.0038 -.0038 1 0 1
4.5800 4.5703 .0097 2 0 0
4.1600 4.1566 .0034 0 2 0
3.8800 3.8831 -.0031 -2 1 2
3.6700 3.6714 -.0014 -1 -2 1
3.3200 3.3195 .0005 -3 1 1
2.9100 2.9097 .0003 3 -1 1
2.8900 2.8892 .0008 1 -3 2
2.8400 2.8396 .0004 0 -1 4
2.8000 2.7998 .0002 3 -2 1
A= 10.0562 DA= .0003
B= 9.103 DB= .001
C= 11.774 DC= .001
GAMMA=104.416 DGAMMA= .007
BETA =105.2570 DBETA = .0006
ALPHA=104.245 DALPHA= .007
V=948.6
60. 6-0369
PbSiO9Br2
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.8300 5.8250 .0050 0 1 1
3.8700 3.8691 .0009 -2 1 1
3.5000 3.4978 .0022 0 2 1
3.0000 3.0009 -.0009 2 2 0
2.9000 2.8981 .0019 -2 2 1
2.7700 2.7717 -.0017 -1 1 3
2.3200 2.3212 -.0012 4 0 1
2.2500 2.2500 -.0000 -4 0 2
2.1700 2.1692 .0008 -1 1 4
2.0000 2.0006 -.0006 3 3 0
1.9600 1.9593 .0007 -5 0 1
1.8600 1.8600 .0000 1 4 0
a= 9.874 b=7.5775 c= 9.146 beta= 95.18
da=.006 db=.001 dc=.004 dbeta=.04
V= 681.4
Triklin
Dexp Dcal d(D) h k l
5.8300 5.8288 .0012 1 0 0
3.8700 3.8715 -.0015 -1 1 1
3.5000 3.4949 .0051 0 -1 1
3.0000 2.9995 .0005 0 2 0
2.9000 2.9021 -.0021 -1 0 2
2.7700 2.7693 .0007 2 1 1
2.3200 2.3213 -.0013 -2 0 2
2.2500 2.2486 .0014 0 1 3
2.1700 2.1709 -.0009 -2 -2 1
2.0000 1.9997 .0003 0 3 0
1.9600 1.9596 .0004 -3 0 1
1.8600 1.8600 -.0000 -2 1 3
A= 6.181 DA= .001
B= 7.104 DB= .004
C= 6.838 DC= .003
GAMMA= 73.76 DGAMMA= .02
BETA = 92.10 DBETA = .04
ALPHA= 63.50 DALPHA= .03
V= 253.4
61. 6-0379
Pb4O3Br2
Triklin
Dexp Dcal d(D) h k l
6.6300 6.6248 .0052 -1 0 1
3.8400 3.8396 .0004 0 1 1
3.7700 3.7733 -.0033 0 -1 1
3.3300 3.3322 -.0022 -1 1 0
3.2600 3.2631 -.0031 1 -1 1
2.9800 2.9756 .0044 0 -1 3
2.8300 2.8311 -.0011 -1 -1 3
2.7800 2.7804 -.0004 1 0 5
2.2200 2.2199 .0001 -2 1 3
2.1900 2.1898 .0002 -2 -1 4
2.1600 2.1611 -.0011 2 0 6
2.1400 2.1397 .0003 3 2 0
A= 8.276 DA= .001
B= 4.01878 DB= .00009
C= 14.245 DC= .006
GAMMA= 79.803 DGAMMA= .001
BETA = 81.74 DBETA = .01
ALPHA= 86.676 DALPHA= .003
V= 461.2
62. 6-0381
Pb8O7Br2*5H2O
Triklin
Dexp Dcal d(D) h k l
6.0000 6.0116 -.0116 -1 -1 1
4.4800 4.4823 -.0023 0 0 4
4.3900 4.3943 -.0043 1 1 3
4.2700 4.2824 -.0124 -1 1 3
3.9400 3.9387 .0013 0 -2 2
3.3600 3.3610 -.0010 2 1 1
3.2500 3.2550 -.0050 -1 1 5
3.1100 3.1078 .0022 -2 0 3
2.9800 2.9785 .0015 0 3 4
2.8800 2.8802 -.0002 -2 0 4
2.6200 2.6198 .0002 2 2 4
2.5100 2.5103 -.0003 0 4 2
A= 6.973 DA= .001
B= 10.397 DB= .002
C= 18.47 DC= .02
GAMMA= 75.21 DGAMMA= .07
BETA = 94.89 DBETA = .07
ALPHA= 78.70 DALPHA= .05
V=1256.0
63. 6-0382
Pb3O2SO4
Triklin
Dexp Dcal d(D) h k l
7.9000 7.9023 -.0023 -1 0 1
5.9000 5.9024 -.0024 1 1 0
4.8000 4.7896 .0104 -1 -1 2
4.4700 4.4686 .0014 -1 1 1
4.1300 4.1355 -.0055 2 1 0
3.7900 3.7934 -.0034 0 1 2
3.6700 3.6717 -.0017 1 -1 2
3.5000 3.4991 .0009 -2 1 0
3.2500 3.2529 -.0029 -1 -2 2
3.1400 3.1408 -.0008 -3 0 1
2.9900 2.9887 .0013 3 1 0
2.9600 2.9610 -.0010 -1 2 0
A= 9.7073 DA= .0001
B= 6.971 DB= .001
C= 11.247 DC= .005
GAMMA= 76.504 DGAMMA= .002
BETA =106.01 DBETA = .04
ALPHA=104.44 DALPHA= .05
V= 697.4
64. 6-0386
Pb8O7Br2
Triklin
Dexp Dcal d(D) h k l
8.8700 8.8785 -.0085 1 0 0
6.2100 6.2020 .0080 0 0 1
4.0600 4.0606 -.0006 0 -2 1
3.9500 3.9541 -.0041 -1 2 0
3.8400 3.8437 -.0037 -2 1 0
3.3300 3.3272 .0028 2 -1 1
3.2100 3.2102 -.0002 -2 1 1
3.0500 3.0497 .0003 -2 2 0
2.9900 2.9875 .0025 -1 -1 2
2.9400 2.9407 -.0007 -1 -3 1
2.9000 2.9003 -.0003 1 0 2
2.8000 2.8003 -.0003 0 -2 2
A= 8.948 DA= .002
B= 9.542 DB= .002
C= 6.292 DC= .001
GAMMA= 83.076 DGAMMA= .001
BETA = 92.86 DBETA = .02
ALPHA= 99.553 DALPHA= .005
V= 525.6
65. 6-0387
Pb4O3Br2*H2O
Monoklin
Grupa 4,11
Dexp Dcal d(D) h k l
6.5000 6.5109 -.0109 -1 0 1
3.9300 3.9245 .0055 1 1 0
3.2500 3.2554 -.0054 -2 0 2
3.0600 3.0570 .0030 0 1 2
2.9800 2.9828 -.0028 -3 0 1
2.9500 2.9512 -.0012 2 1 1
2.8800 2.8779 .0021 1 1 2
2.0000 1.9997 .0003 -2 0 4
2.1700 2.1699 .0001 -2 1 3
2.0600 2.0592 .0008 4 1 0
1.9600 1.9623 -.0023 2 2 0
1.8500 1.8495 .0005 -5 0 1
a= 9.3790 b= 4.3220 c= 8.6590 beta=92.714
da= .0009 db=.0007 dc=.0001 dbet=,005
V= 350.6
Triklin
Dexp Dcal d(D) h k l
6.5000 6.4923 .0077 1 0 0
3.9300 3.9302 -.0002 0 -1 1
3.2500 3.2484 .0016 0 -1 3
3.0600 3.0607 -.0007 1 1 0
2.9800 2.9812 -.0012 1 1 1
2.9500 2.9516 -.0016 -1 0 4
2.8800 2.8770 .0030 0 1 3
2.0000 1.9999 .0001 3 0 4
2.0000 1.9999 .0001 3 0 4
2.1700 2.1698 .0002 0 -1 6
2.0600 2.0590 .0010 1 -2 1
1.9600 1.9610 -.0010 -1 2 1
A= 6.821 DA= .001
B= 4.124 DB= .001
C= 14.772 DC= .001
GAMMA=105.405 DGAMMA= .009
BETA = 78.708 DBETA = .001
ALPHA= 99.702 DALPHA= .006
V= 389.8
66. 6-0388
Pb3O2SO4
Triklin
Dexp Dcal d(D) h k l
3.7500 3.7508 -.0008 2 1 0
2.9600 2.9602 -.0002 -3 -1 1
2.8700 2.8734 -.0034 -2 1 0
2.6900 2.6976 -.0076 -2 0 2
2.3700 2.3697 .0003 3 0 1
2.3500 2.3482 .0018 -2 -2 2
2.2900 2.2873 .0027 0 1 2
2.1100 2.1116 -.0016 1 2 1
2.0600 2.0623 -.0023 2 -1 2
1.9600 1.9618 -.0018 0 0 3
1.8200 1.8217 -.0017 3 2 1
1.7900 1.7909 -.0009 -4 1 0
A= 9.2323 DA= .0006
B= 5.424 DB= .001
C= 6.366 DC= .001
GAMMA= 70.49 DGAMMA= .01
BETA =107.15 DBETA = .03
ALPHA=109.06 DALPHA= .07
V=278.04
67. 6-0390
Pb4O3Br2*xH2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
6.6000 6.6088 -.0088 1 1 0
3.8800 3.8787 .0013 0 1 2
3.2600 3.2577 .0023 -3 0 1
2.9800 2.9818 -.0018 2 2 1
2.9300 2.9290 .0010 3 0 1
2.8600 2.8604 -.0004 2 1 2
2.1800 2.1797 .0003 -1 0 4
2.1500 2.1501 -.0001 0 4 1
2.0400 2.0401 -.0001 1 0 4
1.7480 1.7482 -.0002 1 5 0
1.7320 1.7322 -.0002 -5 1 3
1.6990 1.6990 .0000 5 0 2
1.6720 1.6717 .0003 2 5 0
1.4960 1.4960 .0000 -5 2 4
a= 10.021 b= 8.881 c= 8.734 beta= 99.13
da= .001 db=.003 dc=.001 dbeta=.02
V= 767.4
68. 6-0404
Pb4O3Cl2*xH2O
Rombik
Groupa 16,25,47
Dexp. Dcal. d(D) h k l
6.0000 5.9990 .0010 0 2 0
5.4000 5.4397 -.0397 0 2 1
3.8700 3.8744 -.0044 1 0 0
3.1800 3.1557 .0243 1 2 1
2.9300 2.9216 .0084 0 4 1
2.8400 2.8408 -.0008 0 2 4
2.1500 2.1502 -.0002 0 0 6
2.1100 2.1069 .0031 1 3 4
2.0200 2.0241 -.0041 0 2 6
1.7740 1.7725 .0015 2 2 2
1.7110 1.7131 -.0021 1 6 2
1.6820 1.6830 -.0010 2 3 2
1.6560 1.6565 -.0005 0 7 2
a= 3.874 b=12.00 c=12.901
da= .005 db= .01 dc= .004
v= 599.7
Triklin
Dexp Dcal d(D) h k l
6.0000 6.0046 -.0046 0 1 1
5.4000 5.4049 -.0049 0 -1 1
3.8700 3.8694 .0006 -1 0 1
3.1800 3.1798 .0002 1 1 2
2.9300 2.9295 .0005 0 1 3
2.8400 2.8396 .0004 1 2 0
2.1500 2.1502 -.0002 2 1 0
2.1100 2.1099 .0001 -1 3 0
2.0200 2.0201 -.0001 -1 -3 1
1.7740 1.7740 -.0000 -1 3 3
1.7110 1.7110 -.0000 0 2 5
1.6820 1.6820 .0000 2 1 4
1.6560 1.6560 .0000 2 3 0
A= 4.506 DA= .001
B= 7.286 DB= .001
C= 9.2690 DC= .0006
GAMMA= 88.373 DGAMMA= .005
BETA = 83.92 DBETA = .02
ALPHA= 83.68 DALPHA= .01
V= 300.7
69. 6-0409
Pb4O3Br2*H2O
Triklin
Dexp Dcal d(D) h k l
7.0000 7.0042 -.0042 0 0 1
6.3300 6.3141 .0159 1 0 0
4.2000 4.2057 -.0057 0 -2 1
3.9500 3.9528 -.0028 1 -1 1
3.8000 3.7972 .0028 -1 2 0
3.3500 3.3479 .0021 -1 -1 2
3.1800 3.1816 -.0016 0 1 2
3.1100 3.1070 .0030 1 2 1
3.0600 3.0620 -.0020 0 -3 1
3.0000 3.0000 .0000 0 -2 2
2.9400 2.9425 -.0025 -2 1 1
2.9000 2.9001 -.0001 1 3 0
A= 6.495 DA= .001
B= 9.7489 DB= .0002
C= 7.248 DC= .001
GAMMA= 87.09473 DGAMMA= .00008
BETA =103.50 DBETA = .01
ALPHA= 96.8999 DALPHA= .0006
V=443.0
70. 6-0411
Pb4O3Br2
Triklin
Dexp Dcal d(D) h k l
6.5400 6.5432 -.0032 -1 1 1
4.5000 4.5031 -.0031 1 -1 1
3.7300 3.7291 .0009 2 0 1
3.6100 3.6098 .0002 -2 2 1
3.3600 3.3617 -.0017 -2 2 0
3.3100 3.3091 .0009 0 -2 1
3.0600 3.0577 .0023 -1 -1 2
3.0200 3.0213 -.0013 -1 3 2
2.9200 2.9169 .0031 0 2 3
2.9100 2.9033 .0067 2 0 2
2.9000 2.8968 .0032 -3 1 0
2.8600 2.8582 .0018 -1 3 0
A= 8.911 DA= .001
B= 9.510 DB= .001
C= 9.2331 DC= .0007
GAMMA=103.61 DGAMMA= .02
BETA = 99.36 DBETA = .03
ALPHA= 65.64 DALPHA= .01
V=690.8
71. 6-0435
Pb7O6Gl2
Triklin
Dexp Dcal d(D) h k l
9.7000 9.6854 .0146 1 0 0
6.1000 6.0999 .0001 -1 1 0
4.8000 4.7964 .0036 0 -1 1
3.4500 3.4525 -.0025 0 2 0
3.2300 3.2294 .0006 1 -2 1
3.0700 3.0671 .0029 -1 -2 1
2.8700 2.8693 .0007 -3 0 1
2.6400 2.6399 .0001 -2 -2 1
2.4200 2.4200 -.0000 3 -2 1
2.3200 2.3222 -.0022 -1 -2 2
2.1500 2.1497 .0003 -4 2 0
2.0400 2.0405 -.0005 4 -2 1
A= 9.831 DA= .002
B= 7.2615 DB= .0002
C= 5.32525 DC= .00094
GAMMA= 97.791 DGAMMA= .001
BETA = 93.74 DBETA = .03
ALPHA=105.61 DALPHA= .01
V= 360.7
72. 6-0437
Pb8O7Br2
Triklin
Dexp Dcal d(D) h k l
10.6300 10.6372 -.0072 1 0 0
10.3500 n.in.
10.1500 10.1237 .0263 0 0 1
6.0800 6.0791 .0009 0 1 0
5.9700 5.9699 .0001 0 -1 1
3.9100 3.9101 -.0001 -2 -1 1
3.0600 3.0601 -.0001 1 -2 1
2.9900 2.9902 -.0002 -1 -2 1
2.8700 2.8662 .0038 3 0 2
2.3700 2.3701 -.0001 2 2 1
2.0700 2.0702 -.0002 5 0 1
1.9900 1.9900 .0000 0 -3 3
A= 10.651 DA= .001
B= 6.3186 DB= .0005
C= 10.514 DC= .003
GAMMA= 92.48797 DGAMMA= .00004
BETA = 90.90 DBETA = .01
ALPHA=105.58 DALPHA= .03
V= 680.7
73. 6-0451
Pb2OBr2
Triklin
Dexp Dcal d(D) h k l
7.8000 7.8000 -.0000 -1 1 0
7.0800 7.0740 .0060 0 0 1
5.2700 5.2698 .0002 0 -2 1
4.3400 4.3396 .0004 -1 3 1
4.0000 3.9977 .0023 1 3 0
3.9000 3.9000 -.0000 -2 2 0
3.8000 3.8003 -.0003 -2 1 1
3.5100 3.5120 -.0020 0 4 1
3.2700 3.2701 -.0001 1 4 0
3.2200 3.2198 .0002 0 -2 2
3.1000 3.0998 .0002 -2 4 1
3.0400 3.0402 -.0002 -1 -2 2
2.9400 2.9392 .0008 0 5 1
2.8000 2.8001 -.0001 2 2 1
2.7500 2.7502 -.0002 1 5 0
A= 8.184 DA= .001
B= 16.5487 DB= .0009
C= 7.1875 DC= .0004
GAMMA=104.060 DGAMMA= .004
BETA =100.17 DBETA = .01
ALPHA= 86.77 DALPHA= .01
V= 929.4
74. 6-0488
Pb3{PO4}2
Monoklin
Grupa 4,11
Dexp Dcal d(D) h k l
4.7000 4.7043 -.0043 1 1 0
4.6000 4.6004 -.0004 1 0 1
3.4900 3.4941 -.0041 -1 1 2
3.1100 3.1102 -.0002 2 0 0
3.0300 3.0384 -.0084 -1 2 1
2.8300 2.8327 -.0027 1 2 1
2.7400 2.7427 -.0027 2 0 1
2.2300 2.2296 .0004 -2 2 2
2.1900 2.1908 -.0008 2 1 2
2.1000 2.0983 .0017 0 3 2
2.0800 2.0786 .0014 0 1 4
2.0400 2.0381 .0019 -3 1 1
a= 6.3770 b= 7.190 c= 8.904 beta= 102.714
da=.0007 db=.002 dc= .001 dbet=.006
V= 398.2
Triklin
Dexp Dcal d(D) h k l
4.7000 4.7012 -.0012 2 0 1
4.6000 4.5993 .0007 2 1 0
3.6000 3.5993 .0007 2 -1 1
3.4900 3.4896 .0004 0 2 0
3.1100 3.1102 -.0002 2 0 2
3.0300 3.0302 -.0002 2 2 0
2.8300 2.8304 -.0004 0 -2 1
2.7400 2.7401 -.0001 3 1 2
2.2300 2.2301 -.0001 2 0 3
2.1900 2.1900 -.0000 -2 0 3
2.1000 2.0989 .0011 -4 2 2
2.0800 2.0795 .0005 2 -2 2
A= 12.24538 DA= .00002
B= 7.27964 DB= .00000
C= 7.41761 DC= .00001
GAMMA= 89.60813 DGAMMA= .00006
BETA = 88.41457 DBETA = .00009
ALPHA= 73.48556 DALPHA= .00006
V=633.7