330. 35-0024
Pb9Bi7Sb4S44
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
4.6400 4.6543 -.0143 0 0 2
4.1300 4.1316 -.0016 2 1 0
3.8400 3.8423 -.0023 0 2 1
3.6000 3.6059 -.0059 2 0 1
3.5200 3.5246 -.0046 -3 0 1
3.4100 3.4118 -.0018 -2 0 3
3.2500 3.2522 -.0022 -3 1 1
3.1500 3.1508 -.0008 2 2 0
3.0900 3.0827 .0073 -2 2 2
3.0100 3.0106 -.0006 -3 0 3
2.9600 2.9585 .0015 3 1 0
2.9100 2.9121 -.0021 0 1 3
a= 10.670 b= 8.437 c= 10.480 beta= 117.345
da=.001 db=.001 dc= .004 dbet=.001
V= 838.0
331. 35-0025
Pb3{Sb0.8Bi0.2}2S6
Triklin
Dexp Dcal d(D) h k l
6.5500 6.5476 .0024 1 0 0
5.1400 5.1443 -.0043 -1 1 1
4.4200 4.4178 .0022 -1 -1 1
4.1300 4.1305 -.0005 -1 2 0
3.6700 3.6722 -.0022 -1 -1 2
3.6100 3.6061 .0039 1 1 1
3.4700 3.4672 .0028 0 -2 2
3.3700 3.3670 .0030 -2 1 1
3.2900 3.2920 -.0020 1 -2 2
3.0900 3.0944 -.0044 -1 -2 1
2.9100 2.9095 .0005 -2 1 2
2.8200 2.8230 -.0030 1 1 2
A= 7.036 DA= .001
B= 8.745 DB= .004
C= 9.504 DC= .002
GAMMA=108.702 DGAMMA= .005
BETA = 96.40 DBETA = .02
ALPHA=101.153 DALPHA= .008
V= 533.9
332. 35-0274
Pb5SiO7
Triklin
Dexp Dcal d(D) h k l
6.6300 6.6309 -.0009 1 0 1
5.9000 5.8939 .0061 1 -1 1
5.6800 5.6698 .0102 -1 1 0
5.5000 5.4922 .0078 1 1 1
4.2890 4.2785 .0105 0 1 2
4.2100 4.2058 .0042 -1 2 0
4.0240 4.0248 -.0008 0 -2 2
3.6790 3.6752 .0038 0 3 0
3.4890 3.4910 -.0020 -1 2 1
3.4310 3.4307 .0003 1 -1 3
3.3620 3.3608 .0012 2 0 0
3.3620 3.3608 .0012 2 0 0
A= 7.0918 DA= .0006
B= 11.1736 DB= .0006
C= 10.6132 DC= .0001
GAMMA= 91.436 DGAMMA= .001
BETA = 71.474 DBETA = .005
ALPHA= 99.211 DALPHA= .003
V=787.3
333. 35-0275
Pb11Si3O17
Triklin
Dexp Dcal d(D) h k l
7.2500 7.2494 .0006 0 0 1
5.4400 5.4374 .0026 -1 0 1
4.6100 4.5969 .0131 -1 -1 1
3.6630 3.6604 .0026 -1 -2 1
3.6360 3.6339 .0021 1 -3 1
3.4940 3.4958 -.0018 0 -3 1
3.4600 3.4616 -.0016 0 -1 2
3.2360 3.2411 -.0051 1 3 0
3.2030 3.2035 -.0005 2 -3 1
3.1470 3.1449 .0021 1 1 2
3.1150 3.1179 -.0029 0 2 2
3.0340 3.0320 .0020 2 2 0
A= 8.969 DA= .001
B= 12.726 DB= .004
C= 7.2521 DC= .0002
GAMMA=108.98 DGAMMA= .08
BETA = 88.55 DBETA = .013
ALPHA= 89.9694 DALPHA= .0006
V= 782.4
334. 35-0382
Pb17.19Sb14.81S35.20Cl8.64
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
4.2100 4.2109 -.0009 -2 1 2
3.7000 3.6963 .0037 -4 0 1
3.5400 3.5385 .0015 -4 0 2
3.4000 3.4003 -.0003 0 1 3
3.1500 3.1500 .0000 -4 0 3
3.0200 3.0205 -.0005 -2 2 1
2.9500 2.9495 .0005 -5 0 1
2.8500 2.8491 .0009 -4 1 3
2.7900 2.7874 .0026 2 1 3
2.7100 2.7083 .0017 0 1 4
2.4500 2.4494 .0006 -5 0 4
2.2800 2.2810 -.0010 4 2 1
a= 14.7860 b= 6.6800 c= 12.4490 beta= 107.825
da= .0008 db=.0004 dc=.0001 dbet= .001
V= 1170.5
Triklin
Dexp Dcal d(D) h k l
4.2100 4.2085 .0015 1 2 0
3.7000 3.6979 .0021 -1 0 1
3.5400 3.5424 -.0024 -1 -2 1
3.4000 3.3989 .0011 1 4 0
3.1500 3.1478 .0022 1 1 1
3.0200 3.0217 -.0017 1 2 1
2.9500 2.9477 .0023 -1 5 0
2.8500 2.8476 .0024 1 3 1
2.7900 2.7888 .0012 -1 -5 1
2.7100 2.7116 -.0016 1 -4 1
2.4500 2.4502 -.0002 0 8 0
2.2800 2.2802 -.0002 -1 2 2
A= 4.6549 DA= .0006
B= 19.660 DB= .004
C= 5.1877 DC= .0005
GAMMA= 87.95 DGAMMA= .01
BETA = 98.397 DBETA = .006
ALPHA= 94.169 DALPHA= .007
V= 468.3
335. 35-0537
Pb8Sb6As8S29
Triklin
Dexp Dcal d(D) h k l
4.2400 4.2394 .0006 -2 0 2
4.1500 4.1518 -.0018 -1 1 1
3.8800 3.8793 .0007 1 -1 1
3.7900 3.7936 -.0036 -2 1 0
3.6200 3.6208 -.0008 -1 0 3
3.4800 3.4786 .0014 -3 0 2
3.3100 3.3107 -.0007 0 -1 2
3.2200 3.2214 -.0014 0 1 3
3.1500 3.1486 .0014 2 1 3
3.0400 3.0413 -.0013 -3 -1 1
2.9800 2.9801 -.0001 4 1 1
2.8500 2.8477 .0023 5 0 2
A= 15.0313 DA= .0009
B= 4.5610 DB= .0001
C= 12.0829 DC= .0007
GAMMA= 86.74 DGAMMA= .01
BETA = 79.433 DBETA = .005
ALPHA= 80.096 DALPHA= .009
V=801.6
336. 35-0840
Pb3MoO5Cl2
Rombik
Grupa 17
Dexp. Dcal. d(D) h k l
6.4900 6.5264 -.0364 0 1 0
5.5900 5.6202 -.0302 1 1 0
4.9600 4.9292 .0308 1 1 1
3.7900 3.7890 .0010 1 1 2
3.4200 3.4201 -.0001 0 0 3
3.2600 3.2582 .0018 2 1 2
3.1300 3.1297 .0003 1 2 0
2.9100 2.9085 .0015 2 0 3
2.7700 2.7640 .0060 4 0 0
2.7200 2.7206 -.0006 3 1 2
2.3600 2.3610 -.0010 0 2 3
2.1600 2.1616 -.0016 5 0 1
2.0900 2.0898 .0002 1 3 1
1.9500 1.9507 -.0007 4 2 2
1.7600 1.7597 .0003 3 3 2
a=11.06 b= 6.526 c=10.260
da= .01 db= .004 dc= .001
V= 740
337. 35-1505
C6H4N2O2Pb
Triklin
Dexp Dcal d(D) h k l
11.8000 11.8000 .0000 1 0 0
10.2000 10.2000 .0000 1 -1 0
9.5000 9.5000 .0000 0 0 1
9.0000 9.0000 .0000 1 -1 1
4.7200 4.7216 -.0016 -2 0 1
3.9700 3.9761 -.0061 2 1 1
3.8700 3.8706 -.0006 3 -2 2
3.5800 3.5795 .0005 -3 1 1
3.5200 3.5191 .0009 3 -3 2
3.1800 3.1866 -.0066 4 -2 2
3.0600 3.0587 .0013 -3 -1 1
3.0000 3.0000 .0000 3 -3 3
A= 13.601 DA= .004
B= 12.4400 DB= .0008
C= 10.402 DC= .001
GAMMA=118.795 DGAMMA= .009
BETA = 72.54 DBETA = .04
ALPHA=112.71 DALPHA= .01
V= 1408.7
338. 36-0094
Pb2Sb2S6
Triklin
Dexp Dcal d(D) h k l
6.7000 6.6978 .0022 1 1 0
4.2100 4.2127 -.0027 -1 1 1
3.9200 3.9161 .0039 -1 -1 1
3.8000 3.7969 .0031 0 2 0
3.7800 3.7779 .0021 1 2 0
3.5500 3.5550 -.0050 0 2 1
3.4500 3.4463 .0037 2 -1 1
3.3900 3.3891 .0009 -1 2 0
3.2400 3.2391 .0009 -2 1 1
3.1000 3.1017 -.0017 -1 2 1
3.0400 3.0390 .0010 2 1 2
2.9600 2.9638 -.0038 0 -2 1
A= 10.979 DA= .008
B= 7.952 DB= .004
C= 6.434 DC= .008
GAMMA= 77.09 DGAMMA= .05
BETA = 74.45 DBETA = .04
ALPHA= 75.66 DALPHA= .03
V= 516.7
339. 36-0198
PbMoP2O9
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
4.2000 4.2006 -.0006 1 0 1
3.3300 3.3423 -.0123 1 2 1
3.0800 3.0884 -.0084 1 3 0
3.0000 2.9995 .0005 0 1 2
2.7300 2.7331 -.0031 1 0 2
2.4800 2.4821 -.0021 1 4 0
2.0800 2.0806 -.0006 0 5 1
1.9200 1.9218 -.0018 1 1 3
1.8000 1.8012 -.0012 0 5 2
1.5600 1.5584 .0016 0 0 4
1.4800 1.4820 -.0020 3 3 2
1.4400 1.4378 .0022 3 5 0
a= 5.68 b=11.035 c= 6.234
da= .02 db= .004 dc= .003
V= 391
Monoklin
Grupa 4,11
Dexp Dcal d(D) h k l
4.2000 4.2021 -.0021 2 1 0
3.3300 3.3330 -.0030 3 0 1
3.0800 3.0828 -.0028 0 2 1
3.0000 3.0027 -.0027 1 2 1
2.7300 2.7292 .0008 2 2 1
2.4800 2.4799 .0001 4 1 0
2.0800 2.0808 -.0008 3 0 3
1.9200 1.9200 .0000 3 3 0
1.8000 1.7992 .0008 -3 1 3
1.5600 1.5606 -.0006 4 0 4
1.4800 1.4795 .0005 -6 1 2
1.4400 1.4400 .0000 4 4 0
a= 10.717 b= 6.8500 c= 7.1250 beta= 83.193
da= .001 db=.0003 dc=.0002 dbet=.004
V= 519.4
340. 36-1035
PbAs2F12
Monoklin
Grupa 4,11
Dexp Dcal d(D) h k l
5.3100 5.3050 .0050 0 2 0
4.5400 4.5488 -.0088 0 1 2
4.1900 4.2003 -.0103 1 0 0
4.0100 4.0131 -.0031 1 0 1
3.7500 3.7531 -.0031 -1 0 1
3.3400 3.3369 .0031 0 3 1
3.2300 3.2256 .0044 1 1 2
3.0800 3.0857 -.0057 -1 0 2
2.8900 2.8941 -.0041 0 3 2
2.7500 2.7515 -.0015 1 0 3
2.6700 2.6673 .0027 -1 2 2
2.5200 2.5175 .0025 0 0 4
a= 4.2190 b= 10.610 c= 10.115 beta= 84.593
da=.0001 db=.001 dc= .001 dbet=.002
V= 450.8
341. 36-1118
PbMo6S8
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
6.1200 6.1141 .0059 1 1 0
4.6500 4.6316 .0184 1 1 1
3.8240 3.8213 .0027 2 1 0
3.3650 3.3643 .0007 2 1 1
3.2670 3.2726 -.0056 1 0 2
3.0550 3.0571 -.0021 2 2 0
2.6000 2.5999 .0001 2 1 2
2.3650 2.3650 .0000 0 0 3
2.2850 2.2844 .0006 0 1 3
2.2780 2.2780 -.0000 1 0 3
2.0380 2.0380 -.0000 3 3 0
a= 8.48 b= 8.82 c= 7.095
da= .01 db= .01 dc= .003
v= 530.8
342. 36-1964
C16H18PbS3
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
8.5057 8.5070 -.0013 1 1 0
8.0431 8.0113 .0318 1 1 1
7.0251 7.0253 -.0002 2 0 1
6.5107 6.5214 -.0107 2 0 0
6.0669 6.0734 -.0065 0 0 2
5.6088 5.6114 -.0026 0 2 0
4.9828 4.9801 .0027 -2 0 1
4.8217 4.8214 .0003 -1 0 2
a= 14.21 b= 11.22 c= 13.236 beta= 66.58
da=.04 db=.04 dc=.008 dbeta=.02
V=1937