229. 27-0266
Pb3Sb2S6
Triklin
Dexp Dcal d(D) h k l
4.6200 4.6262 -.0062 -2 2 0
4.2300 4.2315 -.0015 0 1 1
4.0800 4.0811 -.0011 0 -1 1
3.8700 3.8692 .0008 -2 4 0
3.8000 3.7984 .0016 0 -2 1
3.7400 3.7428 -.0028 1 2 1
3.6900 3.6922 -.0022 -1 2 1
3.4100 3.4084 .0016 0 6 0
3.3300 3.3267 .0033 -1 -2 1
3.2700 3.2696 .0004 -1 4 1
3.2400 3.2385 .0015 2 1 1
3.0600 3.0633 -.0033 -1 -3 1
A= 9.58979 DA= .00007
B= 20.95196 DB= .00000
C= 4.27715 DC= .00000
GAMMA=101.4465 DGAMMA= .0005
BETA = 84.9279 DBETA = .0001
ALPHA= 85.9203 DALPHA= .0001
V=835.7
230. 27-0267
Pb2{As0.6Bi0.4}2S5
Triklin
Dexp Dcal d(D) h k l
3.8500 3.8492 .0008 -1 1 0
3.7400 3.7379 .0021 -1 1 1
3.6300 3.6292 .0008 -1 -1 1
3.5500 3.5481 .0019 1 1 0
3.4900 3.4894 .0006 -1 -1 2
3.2900 3.2904 -.0004 1 0 2
3.1200 3.1217 -.0017 0 1 4
3.0800 3.0823 -.0023 0 2 3
3.0200 3.0209 -.0009 -1 -2 2
3.9300 3.9282 .0018 0 1 3
2.9400 2.9410 -.0010 1 1 2
2.8940 2.8937 .0003 0 -3 4
A= 4.0093 DA= .0005
B= 10.612 DB= .002
C= 15.005 DC= .008
GAMMA= 95.073 DGAMMA= .005
BETA = 95.8301 DBETA = .0004
ALPHA=105.38 DALPHA= .04
V=608.2
231. 27-0268
Pb27{AsxBiz}14S48
Triklin
Dexp Dcal d(D) h k l
3.6300 3.6266 .0034 2 0 0
3.5500 3.5516 -.0016 0 2 0
3.4800 3.4791 .0009 0 0 2
3.3900 3.3917 -.0017 -1 1 1
3.2800 3.2821 -.0021 -2 -2 1
3.0700 3.0691 .0009 -1 0 2
2.9780 2.9752 .0028 0 2 1
2.8580 2.8569 .0011 1 -1 2
2.7400 2.7403 -.0003 -2 1 0
2.6230 2.6252 -.0022 2 1 2
2.5170 2.5183 -.0013 -1 1 2
2.4140 2.4143 -.0003 -1 2 1
A= 8.274 DA= .001
B= 8.1962 DB= .0002
C= 7.0522 DC= .0003
GAMMA= 61.420 DGAMMA= .001
BETA = 91.341 DBETA = .001
ALPHA= 98.783 DALPHA= .001
V=414.2
232. 27-0272
Pb2N2O7*H2O
Triklin
Dexp Dcal d(D) h k l
7.5600 7.5635 -.0035 2 0 0
6.6400 6.6261 .0139 0 2 0
6.4000 6.4123 -.0123 -1 -2 1
6.2900 6.2740 .0160 2 2 0
5.7400 5.7510 -.0110 -2 0 1
5.4900 5.5058 -.0158 2 0 1
4.9600 4.9660 -.0060 1 -2 1
4.9000 4.8977 .0023 2 -1 1
4.8200 4.8195 .0005 -3 -2 1
4.6700 4.6656 .0044 -2 -3 1
4.5800 4.5750 .0050 -2 1 1
4.3600 4.3579 .0021 -1 -1 2
A= 16.48603 DA= .00001
B= 14.88801 DB= .00001
C= 8.78014 DC= .00000
GAMMA= 66.70505 DGAMMA= .00001
BETA = 98.67262 DBETA = .00000
ALPHA=106.46840 DALPHA= .00001
V=1895.6
233. 27-0273
Pb4N2O9*3H2O
Triklin
Dexp Dcal d(D) h k l
7.6100 7.6136 -.0036 0 1 1
7.5200 7.5230 -.0030 1 0 0
7.2900 7.2865 .0035 0 -1 1
4.7200 4.7191 .0009 -1 1 1
4.2900 4.2900 -.0000 0 -2 1
4.1500 4.1430 .0070 0 0 3
3.8300 3.8310 -.0010 -1 1 2
3.7400 3.7401 -.0001 2 1 0
3.7200 3.7215 -.0015 0 -1 3
3.6600 3.6587 .0013 -1 2 0
3.1900 3.1894 .0006 -1 -1 3
3.1400 3.1417 -.0017 2 0 3
A= 7.867 DA= .003
B= 9.5046 DB= .0002
C= 12.779 DC= .006
GAMMA= 78.297 DGAMMA= .005
BETA = 76.82 DBETA = .02
ALPHA= 84.85 DALPHA= .01
V= 910.0
234. 27-0616
Ag3PbSb3S7
Triklin
Dexp Dcal d(D) h k l
3.2500 3.2503 -.0003 2 0 0
2.9000 2.9007 -.0007 2 2 0
2.8000 2.7986 .0014 1 0 2
2.7500 2.7497 .0003 2 0 1
2.5900 2.5885 .0015 -1 2 0
2.4500 2.4511 -.0011 2 2 1
2.2000 2.2004 -.0004 0 3 0
2.0700 2.0704 -.0004 1 -2 2
2.0100 2.0103 -.0003 -2 0 3
1.9660 1.9661 -.0001 3 2 1
1.8910 1.8913 -.0003 -3 -3 2
1.8170 1.8168 .0002 -3 -2 3
A= 7.1605 DA= .0004
B= 7.2111 DB= .0003
C= 6.9426 DC= .0004
GAMMA= 67.095 DGAMMA= .005
BETA =103.063 DBETA = .002
ALPHA=100.806 DALPHA= .002
V=319.75
235. 27-0692
Gd6Pb4Mo3O22
Triklin
Dexp Dcal d(D) h k l
3.1300 3.1258 .0042 2 0 0
3.0900 3.0855 .0045 0 1 1
2.7800 2.7784 .0016 0 -1 1
2.7000 2.7000 .0000 0 2 0
2.5700 2.5714 -.0014 1 -1 1
1.9400 1.9387 .0013 -1 -2 1
1.9000 1.8989 .0011 3 0 1
1.8600 1.8606 -.0006 -3 1 0
1.6700 1.6701 -.0001 -1 3 0
1.6400 1.6407 -.0007 -3 -1 1
1.5900 1.5900 .0000 -3 1 1
1.5800 1.5802 -.0002 1 -1 2
A= 6.38118 DA= .00001
B= 5.50147 DB= .00003
C= 3.53325 DC= .00001
GAMMA= 81.1528 DGAMMA= .0001
BETA = 81.48869 DBETA = .00008
ALPHA= 82.2467 DALPHA= .0003
V=120.5
236. 27-0710
Pb15Mo2B6O30
Mononklin
Grupa 4,11
Dexp Dcal d(D) h k l
9.2100 9.1852 .0248 1 0 1
5.8300 5.8286 .0014 2 0 0
4.5200 4.5245 -.0045 2 1 0
3.8700 3.8684 .0016 2 1 2
3.5900 3.5885 .0015 0 2 0
3.2800 3.2799 .0001 3 1 2
3.1600 3.1596 .0004 -1 2 1
3.0600 3.0617 -.0017 3 0 3
2.9210 2.9241 -.0031 0 2 2
2.4550 2.4538 .0012 0 2 3
2.3790 2.3795 -.0005 0 1 4
2.2980 2.2979 .0001 5 1 2
1.8370 1.8370 -.0000 5 0 5
1.7390 1.7357 .0033 0 3 4
a= 12.276 b= 7.177 c= 10.624 beta= 71.722
da= .002 db=.001 dc=.0003 dbet=.009
V= 888.8
237. 27-0712
Pb3SiO5
Monoklin
Grupa 5,8,12
Dexp Dcal d(D) h k l
6.9910 7.0199 -.0289 1 1 0
6.7180 6.7364 -.0184 -1 1 1
5.4000 5.4088 -.0088 1 1 1
2.5880 2.5847 .0033 0 4 0
5.1590 5.1695 -.0105 0 2 0
4.7720 4.7808 -.0088 2 0 0
3.9580 3.9618 -.0038 2 0 1
3.7160 3.7159 .0001 -1 1 3
3.5890 3.5883 .0007 -2 0 3
3.3740 3.3682 .0058 -2 2 2
3.2430 3.2422 .0008 1 3 0
3.2100 3.2129 -.0029 -1 3 1
a= 10.1230 b= 10.339 c= 11.975 beta= 109.165
da= .0007 db=.001 dc=.001 dbet=.002
V= 1183.8
Triklin
Dexp Dcal d(D) h k l
6.9910 6.9966 -.0056 1 -1 1
6.7180 6.7221 -.0041 -1 -1 1
5.4000 5.3955 .0045 2 0 1
5.1590 5.1577 .0013 1 -1 2
4.7720 4.7669 .0051 2 1 1
3.9580 3.9591 -.0011 -2 -2 1
3.7160 3.7156 .0004 3 0 1
3.5890 3.5862 .0028 3 0 0
3.3740 3.3741 -.0001 3 -1 1
3.2430 3.2430 .0000 -2 0 2
3.2100 3.2117 -.0017 -1 -1 3
3.1720 3.1702 .0018 -2 -3 1
A= 11.29291 DA= .00003
B= 10.7038 DB= .0005
C= 11.052 DC= .004
GAMMA= 82.243 DGAMMA= .008
BETA = 77.89 DBETA = .02
ALPHA=109.93 DALPHA= .03
V=1197.3
238. 27-1721
C3H6O3Pb
Monoklin
Grupa 4,11
Dexp Dcal d(D) h k l
6.9500 6.9513 -.0013 1 1 0
4.8500 4.8517 -.0017 1 1 2
3.7900 3.7901 -.0001 -3 0 1
3.5800 3.5810 -.0010 3 1 1
3.2500 3.2520 -.0020 0 0 4
3.1200 3.1202 -.0002 2 2 2
3.0300 3.0304 -.0004 0 2 3
2.7700 2.7691 .0009 2 2 3
2.6600 2.6581 .0019 -2 2 3
2.5900 2.5909 -.0009 0 3 2
2.4500 2.4500 .0000 -3 0 4
2.2500 2.2500 .0000 5 1 2
1.9800 1.9800 .0000 -1 4 2
1.8900 1.8898 .0002 1 4 3
1.8100 1.8104 -.0004 -5 3 1
a= 12.187 b= 8.474 c= 13.0430 beta= 85.793
da=.001 db=.001 dc=.0003 dbet=.005
V= 1343.4
239. 27-1722
C52H82N6PbS4
Triklin
Dexp Dcal d(D) h k l
11.9000 11.8783 .0217 1 0 0
10.6000 10.5970 .0030 0 1 1
9.0600 9.0555 .0045 0 -1 1
7.7300 7.7231 .0069 1 2 0
7.0200 7.0164 .0036 -1 2 0
6.5100 6.5098 .0002 -2 0 1
5.8300 5.8283 .0017 2 1 0
5.2500 5.2520 -.0020 2 2 0
4.6300 4.6302 -.0002 0 3 2
4.4600 4.4599 .0001 1 0 2
4.0500 4.0499 .0001 -1 2 3
3.8100 3.8100 .0000 -2 -4 1
3.5000 3.5001 -.0001 -3 3 1
3.3600 3.3601 -.0001 1 -3 2
A= 13.102 DA= .002
B= 18.9907 DB= .0008
C= 12.7169 DC= .0008
GAMMA= 88.43 DGAMMA= .01
BETA =114.36 DBETA = .01
ALPHA= 81.477 DALPHA= .003
V= 2836.9
240. 27-1723
C16H10N2S2Pb
Monoklin
Grupa 4,11
Dexp Dcal d(D) h k l
8.0400 8.0469 -.0069 1 1 0
6.0100 6.0069 .0031 -2 0 1
5.8800 5.8848 -.0048 2 0 1
4.9100 4.9126 -.0026 1 1 2
4.5000 4.5006 -.0006 3 0 0
3.8800 3.8763 .0037 3 1 1
3.7000 3.7002 -.0002 -3 0 2
3.4100 3.4095 .0005 -2 2 2
3.0400 3.0388 .0012 1 0 4
2.9300 2.9316 -.0016 3 2 2
2.7600 2.7605 -.0005 -2 1 4
2.4800 2.4795 .0005 -3 3 2
a= 13.5060 b= 10.0210 c= 12.5500 beta= 91.403
da= .009 db=.0007 dc=.0004 dbet=.003
V= 1698.0
241. 27-1724
C8H4O4Pb
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
13.8000 13.8212 -.0212 0 0 2
6.9800 6.9790 .0010 2 0 0
6.8000 6.8032 -.0032 1 1 0
4.6700 4.6700 .0000 -2 1 2
4.4800 4.4792 .0008 3 0 3
4.0000 4.0005 -.0005 3 1 2
3.7400 3.7416 -.0016 1 2 1
3.7000 3.6952 .0048 -1 2 1
3.6400 3.6373 .0027 -1 0 7
3.5200 3.5223 -.0023 0 1 7
3.4800 3.4799 .0001 -3 1 3
3.4200 3.4197 .0003 -1 2 3
a= 14.175 b= 7.7914 c= 28.07 beta= 79.96
da=.002 db=.0006 dc=.04 dbeta=.06
V= 3052.9
Triklin
Dexp Dcal d(D) h k l
13.8000 14.2691 -.4691 2 0 0
6.9800 6.9811 -.0011 -1 0 1
6.8000 6.8105 -.0105 1 -1 1
4.6700 4.6698 .0002 1 -2 1
4.4800 4.4788 .0012 2 -2 1
4.0000 3.9991 .0009 -4 1 1
3.7400 3.7441 -.0041 2 -1 2
3.7000 3.6987 .0013 -2 -1 2
3.6400 3.6376 .0024 0 0 2
3.5200 3.5303 -.0103 7 -1 1
3.4800 3.4786 .0014 1 -2 2
3.4200 3.4170 .0030 -1 2 1
A= 28.581 DA= .003
B= 10.0200 DB= .0007
C= 7.7231 DC= .0005
GAMMA= 87.94246 DGAMMA= .00004
BETA = 88.47 DBETA = .02
ALPHA=109.479 DALPHA= .007
V=2083.2
242. 27-1725
C15H29N3PbS2
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
10.0000 10.0474 -.0474 1 0 1
7.8300 7.7099 .1201 0 0 2
6.6200 6.6226 -.0026 2 0 0
5.8100 5.8311 -.0211 0 1 1
5.1200 5.1399 -.0199 0 0 3
4.8100 4.7918 .0182 1 0 3
4.5900 4.5774 .0126 1 1 2
3.8500 3.8549 -.0049 0 0 4
3.7000 3.7014 -.0014 1 0 4
3.5200 3.5199 .0001 3 1 1
3.3500 3.3491 .0009 3 0 3
2.9300 2.9310 -.0010 4 1 0
2.7400 2.7397 .0003 4 1 2
a=13.25 b= 6.30 c=15.420
da= .01 db= .01 dc= .002
v=1286
Monoklin
Grupa 4,11
Dexp Dcal d(D) h k l
10.0000 10.3481 -.3481 1 0 0
7.8300 7.8194 .0106 1 1 0
6.6200 6.6207 -.0007 -1 0 2
5.8100 5.8085 .0015 1 0 2
5.1200 5.1189 .0011 -2 0 1
4.8100 4.8038 .0062 1 2 1
4.5900 4.5924 -.0024 -2 0 2
3.8500 3.8475 .0025 0 0 4
3.7000 3.6997 .0003 2 2 1
3.5200 3.5240 -.0040 1 2 3
3.3500 3.3495 .0005 2 2 2
2.9300 2.9299 .0001 0 4 1
2.7400 2.7398 .0002 -1 3 4
a= 10.4450 b= 11.938 c= 15.534 beta= 97.804
da= .0008 db=.003 dc=.001 dbet=.005
V= 1919.0
243. 27-1726
C30H35N3PbS2
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
10.3000 10.0779 .2221 1 0 1
8.6100 8.6247 -.0147 1 1 0
6.5100 6.5167 -.0067 1 0 2
5.7900 5.7928 -.0028 1 2 0
5.3200 5.3298 -.0098 2 1 1
4.5200 4.5142 .0058 0 3 0
4.3300 4.3311 -.0011 0 0 3
3.8400 3.8395 .0005 -2 2 1
3.4000 3.4003 -.0003 1 0 4
3.2100 3.2094 .0006 1 4 1
2.9900 2.9900 .0000 -3 2 1
2.3500 2.3499 .0001 -2 2 4
2.1600 2.1603 -.0003 -1 6 1
2.0600 2.0599 .0001 2 6 2
a= 11.71 b= 13.543 c= 13.60 beta= 72.8
da=.02 db=.006 dc=.01 dbeta=.01
V= 2061