181. 22-0381
Pb5Sb2O8
Monoklin
Grupa 4,11
Dexp Dcal d(D) h k l
7.1200 7.1174 .0026 0 1 1
3.6100 3.6106 -.0006 -3 0 1
3.2200 3.2198 .0002 2 2 1
3.1100 3.1117 -.0017 -3 1 2
2.9300 2.9294 .0006 2 0 3
2.7700 2.7700 .0000 0 1 4
2.7000 2.7007 -.0007 1 0 4
2.6400 2.6394 .0006 -2 1 4
2.2300 2.2343 -.0043 4 1 2
2.0200 2.0201 -.0001 2 0 5
1.9860 1.9853 .0007 -5 1 3
1.9190 1.9194 -.0004 -3 2 5
a= 10.9450 b= 8.9920 c= 11.8100 beta= 99.544
da=.0006 db= .0008 dc=.0004 dbet=.002
V= 1146.2
182. 22-0383
Pb4As2O9
Triklin
Dexp Dcal d(D) h k l
7.1000 7.0941 .0059 0 1 0
5.3000 5.2981 .0019 1 1 0
5.0700 5.0681 .0019 0 -1 2
4.4300 4.4266 .0034 1 0 2
4.1500 4.1538 -.0038 -1 -1 2
3.3600 3.3579 .0021 0 -2 2
3.1400 3.1381 .0019 2 0 0
3.0000 3.0009 -.0009 2 1 1
2.9500 2.9491 .0009 0 -2 3
2.8400 2.8407 -.0007 2 0 2
2.6300 2.6324 -.0024 1 -1 4
2.4300 2.4296 .0004 -1 -3 1
A= 6.4265 DA= .0004
B= 7.409 DB= .002
C= 12.020 DC= .002
GAMMA= 78.071 DGAMMA= .004
BETA = 89.03 DBETA = .02
ALPHA=101.40 DALPHA= .04
V= 547.9
183. 22-0390
Pb6O5{NO3}2
Triklin
Dexp Dcal d(D) h k l
9.1600 9.1440 .0160 -1 0 1
8.0500 8.0875 -.0375 0 1 0
6.7000 6.7118 -.0118 1 0 1
4.8700 4.8702 -.0002 1 1 1
4.5700 4.5720 -.0020 -2 0 2
3.7500 3.7475 .0025 -1 2 1
3.6000 3.5972 .0028 -3 0 1
3.4100 3.4102 -.0002 -3 1 1
3.2500 3.2490 .0010 2 -1 2
3.0800 3.0835 -.0035 -2 2 2
2.9230 2.9212 .0018 1 1 3
2.7620 2.7602 .0018 2 -2 2
A= 10.8415 DA= .0003
B= 8.155 DB= .001
C= 12.0209 DC= .0004
GAMMA= 95.512 DGAMMA= .005
BETA =107.1337 DBETA = .0009
ALPHA= 93.080 DALPHA= .004
V=1007.7
184. 22-0553
CsPbBr3
Triklin
Dexp Dcal d(D) h k l
5.6200 5.6171 .0029 0 1 1
4.2900 4.2895 .0005 0 -1 1
3.3700 3.3698 .0002 -1 2 0
2.8760 2.8735 .0025 1 0 2
2.8320 2.8325 -.0005 -2 2 2
2.3590 2.3587 .0003 -1 3 2
2.2490 2.2490 .0000 -3 2 1
2.0470 2.0475 -.0005 3 0 0
1.9400 1.9401 -.0001 1 -1 3
1.8290 1.8288 .0002 -2 4 2
1.6760 1.6757 .0003 -3 -1 2
1.6120 1.6120 .0000 -4 3 3
A= 6.954 DA= .001
B= 7.3833 DB= .0002
C= 8.0173 DC= .0005
GAMMA=115.301 DGAMMA= .007
BETA =109.710 DBETA = .008
ALPHA= 68.299 DALPHA= .004
V=337.8
185. 22-0653
PbClI
Triklin
Dexp Dcal d(D) h k l
4.1400 4.1406 -.0006 -1 1 1
3.5500 3.5558 -.0058 1 -1 1
3.0900 3.0907 -.0007 -2 1 0
3.0300 3.0328 -.0028 0 0 2
2.9400 2.9418 -.0018 2 0 1
2.6500 2.6523 -.0023 2 -1 1
2.5200 2.5204 -.0004 0 2 2
2.4200 2.4181 .0019 1 -1 2
2.4100 2.4075 .0025 -2 2 1
2.3200 2.3193 .0007 1 2 2
2.2400 2.2401 -.0001 3 0 0
2.0900 2.0891 .0009 -3 1 1
A= 6.739 DA= .003
B= 6.815 DB= .002
C= 6.206 DC= .001
GAMMA= 94.26 DGAMMA= .09
BETA = 90.79 DBETA = .02
ALPHA= 77.788 DALPHA= .006
V=278.1
186. 22-0659
Pb3{NO3}{OH}5
Triklin
Dexp Dcal d(D) h k l
9.9300 9.9320 -.0020 0 1 0
8.6100 8.6245 -.0145 0 1 1
7.4700 7.4574 .0126 0 -1 1
5.2400 5.2325 .0075 1 0 1
4.4600 4.4586 .0014 1 0 2
4.3000 4.3012 -.0012 1 -1 1
4.2500 4.2483 .0017 -1 1 1
3.3600 3.3582 .0018 -1 2 1
3.3000 3.2995 .0005 1 -2 1
3.2800 3.2806 -.0006 -1 0 3
9.9300 9.9320 -.0020 0 1 0
2.9980 2.9972 .0008 1 0 4
A= 5.532 DA= .001
B= 10.173 DB= .002
C= 13.665 DC= .007
GAMMA= 80.973 DGAMMA= .008
BETA = 82.49 DBETA = .01
ALPHA= 80.32 DALPHA= .01
V= 744.3
187. 22-0660
Pb2Mg2Si2O7{OH}2
Triklin
Dexp Dcal d(D) h k l
13.8000 14.0763 -.2763 0 0 1
8.0000 8.0024 -.0024 1 0 0
7.1000 7.1024 -.0024 -1 0 1
4.6000 4.5919 .0081 -1 -2 1
4.2000 4.1931 .0069 0 2 1
3.9000 3.8985 .0015 1 2 1
3.8000 3.8018 -.0018 2 0 1
3.2700 3.2674 .0026 -2 -1 3
3.0400 3.0385 .0015 0 1 4
2.9500 2.9437 .0063 0 3 1
2.8400 2.8418 -.0018 -1 -1 5
2.7500 2.7545 -.0045 -1 -2 5
A= 8.1222 DA= .0002
B= 10.13464 DB= .00007
C= 14.73406 DC= .00001
GAMMA= 80.526 DGAMMA= .002
BETA = 95.323 DBETA = .005
ALPHA=106.984 DALPHA= .001
V=1144.6
188. 22-0661
Pb2{NO3}{OH}3
Monoklin
Grupa 4,11
Dexp Dcal d(D) h k l
7.7100 7.4999 .2101 0 1 1
7.5300 7.4999 .0301 0 1 1
4.7400 4.7334 .0066 1 2 1
4.3200 4.3102 .0098 2 1 0
4.1700 4.1686 .0014 2 0 2
3.8400 3.8381 .0019 1 2 2
3.7500 3.7500 .0000 0 2 2
3.7300 3.7285 .0015 2 2 1
3.6600 3.6566 .0034 -1 1 2
3.2000 3.2030 -.0030 -1 2 2
3.1400 3.1404 -.0004 2 1 3
3.0400 3.0408 -.0008 3 1 2
a= 9.888 b= 11.500 c= 10.521 beta= 70.102
da=.001 db=.001 dc= .001 dbet=.008
V= 1125.0
Triklin
Dexp Dcal d(D) h k l
7.7100 7.6813 .0287 1 0 0
7.5300 7.4961 .0339 0 0 1
4.7400 4.7401 -.0001 0 -2 1
4.3200 4.3135 .0065 1 2 0
4.1700 4.1731 -.0031 -1 -2 1
3.8400 3.8407 -.0007 2 0 0
3.7500 3.7480 .0020 0 0 2
3.7300 3.7231 .0069 -2 0 1
3.6600 3.6592 .0008 -1 0 2
3.2000 3.1993 .0007 -1 -3 1
3.1400 3.1408 -.0008 1 -1 2
3.0400 3.0393 .0007 -2 2 1
A= 7.832 DA= .004
B= 10.958 DB= .001
C= 7.719 DC= .002
GAMMA= 91.597 DGAMMA= .004
BETA =100.82 DBETA = .03
ALPHA= 98.18 DALPHA= .02
V= 643.1
189. 22-0666
Pb3N2O8
Triklin
Dexp Dcal d(D) h k l
9.2400 9.2377 .0023 1 0 0
7.4900 7.5011 -.0111 0 1 0
7.0200 7.0075 .0125 1 0 1
5.8600 5.8739 -.0139 0 1 1
4.8400 4.8309 .0091 0 -1 1
3.9900 4.0001 -.0101 1 2 1
3.7100 3.7120 -.0020 0 0 2
3.5000 3.5037 -.0037 2 0 2
3.2400 3.2424 -.0024 3 0 1
3.1500 3.1528 -.0028 3 1 0
3.1300 3.1261 .0039 3 1 2
3.0800 3.0792 .0008 3 0 0
A= 10.428 DA= .009
B= 8.160 DB= .007
C= 8.24 DC= .01
GAMMA= 69.54 DGAMMA= .04
BETA = 66.60 DBETA = .09
ALPHA= 72.26 DALPHA= .05
V= 591.9
190. 22-0667
Pb5O3{NO3}4*xH2O
Triklin
Dexp Dcal d(D) h k l
7.3100 7.3099 .0001 0 1 1
6.8000 6.7923 .0077 0 -1 1
5.4800 5.4683 .0117 -1 -1 1
4.3100 4.3035 .0065 -1 1 0
4.1500 4.1492 .0008 0 2 1
4.0000 3.9997 .0003 1 2 1
3.9300 3.9272 .0028 1 -1 1
3.8300 3.8242 .0058 0 1 3
3.4000 3.3961 .0039 0 -2 2
3.2000 3.2001 -.0001 2 1 0
3.0800 3.0825 -.0025 0 0 4
2.9760 2.9756 .0004 0 1 4
A= 6.423 DA= .005
B= 9.101 DB= .008
C= 12.410 DC= .002
GAMMA= 70.83 DGAMMA= .04
BETA = 94.74 DBETA = .06
ALPHA= 87.34 DALPHA= .02
V= 680.7
191. 22-0671
Pb3Si2O7
Triklin
Dexp Dcal d(D) h k l
8.6200 8.6117 .0083 1 0 0
4.9700 4.9645 .0055 -1 1 0
4.3900 4.3850 .0050 1 -1 2
4.3000 4.3058 -.0058 2 0 0
3.7500 3.7482 .0018 -2 0 1
3.5600 3.5594 .0006 0 2 0
3.2900 3.2919 -.0019 2 1 2
3.2500 3.2489 .0011 -1 -1 3
3.2200 3.2194 .0006 1 -2 1
3.1700 3.1733 -.0033 -1 1 2
3.0700 3.0720 -.0020 -2 0 2
2.8960 2.8971 -.0011 2 -1 3
A= 8.926 DA= .005
B= 7.559 DB= .007
C= 11.2609 DC= .0004
GAMMA= 79.62 DGAMMA= .05
BETA = 82.015 DBETA = .006
ALPHA=104.83 DALPHA= .05
V= 708.6
192. 22-0829
KPbBr3
Monoklin
Grupa 4,11
Dexp Dcal d(D) h k l
4.1100 4.1050 .0050 2 1 0
3.8200 3.8070 .0130 -1 0 2
3.0400 3.0440 -.0040 2 0 2
3.0100 3.0118 -.0018 0 2 2
2.8800 2.8808 -.0008 -1 2 2
2.8000 2.8006 -.0006 1 3 0
2.7300 2.7302 -.0002 3 1 1
2.6500 2.6457 .0043 1 3 1
2.4800 2.4819 -.0019 2 3 0
2.4100 2.4106 -.0006 -3 1 2
2.3400 2.3395 .0005 2 0 3
2.3200 2.3195 .0005 4 0 0
a= 9.281 b= 8.8130 c= 8.255 beta= 91.483
da=.001 db=.0006 dc= .0008 dbet=.005
V= 675.0
Triklin
Dexp Dcal d(D) h k l
4.1100 4.1086 .0014 0 1 1
3.8200 3.8316 -.0116 0 -1 1
3.0400 3.0409 -.0009 -2 0 2
3.0100 3.0141 -.0041 -2 1 0
2.8800 2.8818 -.0018 0 -1 3
2.8000 2.8023 -.0023 0 1 4
2.7300 2.7286 .0014 -2 0 3
2.6500 2.6481 .0019 2 -1 2
2.4800 2.4781 .0019 0 -1 4
2.4100 2.4130 -.0030 0 1 5
2.3400 2.3365 .0035 2 1 0
2.3200 2.3240 -.0040 2 1 1
A= 6.9681 DA= .0001
B= 4.3242 DB= .0002
C= 13.702 DC= .001
GAMMA=105.05 DGAMMA= .01
BETA = 93.23 DBETA = .01
ALPHA= 82.25 DALPHA= .01
V=395
193. 22-0831
KPbI3
Triklin
Dexp Dcal d(D) h k l
4.1100 4.1076 .0024 -2 2 0
3.5700 3.5692 .0008 1 0 1
3.3800 3.3801 -.0001 1 -2 1
3.2900 3.2895 .0005 -1 0 1
3.0300 3.0302 -.0002 -1 2 1
2.8500 2.8502 -.0002 -1 -4 1
2.7800 2.7804 -.0004 3 4 0
2.5700 2.5710 -.0010 -2 2 1
2.5200 2.5213 -.0013 3 -1 1
2.4300 2.4308 -.0008 1 -6 1
2.4000 2.4012 -.0012 -1 5 1
2.3600 2.3606 -.0006 4 2 0
A= 9.60708 DA= .00000
B= 19.54126 DB= .00000
C= 3.69980 DC= .00000
GAMMA= 84.73351 DGAMMA= .00000
BETA = 83.3804 DBETA = .0001
ALPHA= 93.16752 DALPHA= .00001
V=685.4
194. 22-0922
Pb2Ti3Br7
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
3.8400 3.8433 -.0033 1 0 2
3.5700 3.5723 -.0023 1 1 0
3.0600 3.0595 .0005 2 0 2
2.8200 2.8189 .0011 2 1 0
2.7700 2.7710 -.0010 1 1 2
2.6700 2.6701 -.0001 -2 0 2
2.6100 2.6086 .0014 -1 1 2
1.6300 1.6299 .0001 0 0 5
1.4200 1.4198 .0002 -3 1 4
a= 8.022 b= 3.999 c= 8.2250 beta= 82.213
da= .001 db=.001 dc=.0001 dbet=.009
V= 261.4
195. 22-0923
Pb2TiBr5
Triklin
Dexp Dcal d(D) h k l
4.1400 4.1400 -.0000 1 0 1
3.8400 3.8398 .0002 1 -1 1
3.8100 3.8116 -.0016 -1 2 0
3.0100 3.0092 .0008 1 1 2
2.9800 2.9814 -.0014 -1 3 0
2.8000 2.8000 .0000 0 0 3
2.7200 2.7202 -.0002 1 2 2
2.6500 2.6507 -.0007 1 3 0
2.4500 2.4500 .0000 -1 4 1
2.2400 2.2401 -.0001 1 -1 3
2.1900 2.1898 .0002 -2 3 1
2.0700 2.0700 -.0000 2 0 2
A= 5.0858 DA= .0005
B= 10.4654 DB= .0006
C= 8.6371 DC= .0004
GAMMA= 98.523 DGAMMA= .007
BETA = 96.872 DBETA = .001
ALPHA= 77.582 DALPHA= .006
V=441.9
196. 22-0924
Pb2TiCl5
Triklin
Dexp Dcal d(D) h k l
4.0500 4.0517 -.0017 2 0 0
3.5500 3.5514 -.0014 -2 1 1
3.1900 3.1905 -.0005 2 -1 1
3.0000 3.0002 -.0002 2 0 2
2.9500 2.9517 -.0017 1 -2 1
2.7500 2.7492 .0008 2 2 0
2.7200 2.7200 -.0000 1 2 3
2.6000 2.6001 -.0001 1 3 1
2.3800 2.3796 .0004 1 -2 2
2.1600 2.1602 -.0002 3 2 2
2.1400 2.1405 -.0005 2 -2 2
2.1000 2.1016 -.0016 1 0 4
A= 8.11001 DA= .00006
B= 8.3467 DB= .0002
C= 9.31311 DC= .00004
GAMMA= 91.508 DGAMMA= .004
BETA = 88.949 DBETA = .002
ALPHA= 68.042 DALPHA= .002
V=584.1
197. 22-0925
PbTl3Cl5
Monoklin
Grupa 14
Dexp Dcal d(D) h k l
3.8400 3.8457 -.0057 -1 1 2
3.8100 3.8088 .0012 2 1 0
2.9200 2.9183 .0017 1 2 0
2.8500 2.8485 .0015 -3 1 2
2.5200 2.5192 .0008 -3 1 3
2.3400 2.3394 .0006 -4 1 2
2.1200 2.1194 .0006 2 2 2
2.0600 2.0604 -.0004 4 1 1
1.9800 1.9803 -.0003 -1 3 1
1.9500 1.9504 -.0004 -4 2 2
1.8700 1.8704 -.0004 0 2 4
1.8300 1.8294 .0006 -5 0 4
a= 10.3170 b= 6.1180 c= 10.0210 beta=109.345
da=.0007 db= .0007 dc=.0002 dbet=.001
V= 596.8
198. 22-1132
Pb7{NO3}4{OH}10
Triklin
Dexp Dcal d(D) h k l
7.5100 7.5150 -.0050 -1 1 1
7.3000 7.2770 .0230 1 -1 1
6.7200 6.7247 -.0047 1 3 1
6.5900 6.5935 -.0035 -1 -2 1
5.7400 5.7416 -.0016 0 4 0
5.5600 5.5598 .0002 -1 -3 1
5.3200 5.3124 .0076 -2 2 0
5.2400 5.2474 -.0074 -2 1 1
5.1500 5.1470 .0030 0 0 2
5.0000 4.9988 .0012 1 -3 1
4.8800 4.8813 -.0013 -1 4 0
4.6400 4.6385 .0015 1 5 1
A= 14.100 DA= .004
B= 24.112 DB= .002
C= 10.501 DC= .007
GAMMA= 75.095 DGAMMA= .007
BETA = 84.02 DBETA = .01
ALPHA= 79.12 DALPHA= .03
V=3384.5
199. 22-1149
Sb0.8{Pb,Mg}0.2
Triklin
Dexp Dcal d(D) h k l
3.9000 3.9005 -.0005 1 1 0
3.6600 3.6602 -.0002 -1 1 1
3.4400 3.4400 .0000 -1 -1 1
2.6430 2.6433 -.0003 -1 1 2
2.3870 2.3871 -.0001 -2 1 1
2.2660 2.2656 .0004 0 -2 3
2.0400 2.0408 -.0008 2 -2 3
1.9190 1.9191 -.0001 -2 -1 2
1.8920 1.8930 -.0010 2 2 1
1.7260 1.7258 .0002 2 -2 4
1.6940 1.6939 .0001 1 1 4
1.6380 1.6380 .0000 0 -3 4
A= 5.622 DA= .002
B= 7.696 DB= .001
C= 7.7864 DC= .0003
GAMMA=105.62 DGAMMA= .03
BETA = 77.8924 DBETA = .0007
ALPHA=103.58 DALPHA= .02
V= 311.5
200. 22-1469
PbTlI3
Triklin
Dexp Dcal d(D) h k l
4.5000 4.5031 -.0031 -1 2 0
3.4400 3.4404 -.0004 0 1 2
3.3800 3.3769 .0031 0 -1 2
3.2300 3.2303 -.0003 -1 0 2
2.9400 2.9442 -.0042 -2 3 0
2.6300 2.6283 .0017 -3 3 0
2.5100 2.5082 .0018 0 0 3
2.4400 2.4403 -.0003 2 -3 2
2.3200 2.3194 .0006 3 -3 2
2.2900 2.2899 .0001 -1 3 2
2.0800 2.0803 -.0003 3 0 3
1.9400 1.9395 .0005 -2 -2 2
A= 9.73560 DA= .00008
B= 9.029 DB= .001
C= 7.6718 DC= .0002
GAMMA=116.936 DGAMMA= .002
BETA = 78.845 DBETA = .002
ALPHA= 93.814 DALPHA= .008
V=589.7
201. 22-1470
PbTl3I5
Triklin
Dexp Dcal d(D) h k l
3.2500 3.2481 .0019 0 -1 2
3.1500 3.1544 -.0044 2 1 0
3.0400 3.0369 .0031 0 1 2
3.0100 3.0057 .0043 -2 -1 1
2.9200 2.9224 -.0024 0 2 0
2.8000 2.7980 .0020 -2 0 2
2.6200 2.6202 -.0002 2 0 2
2.3200 2.3214 -.0014 1 0 3
2.2700 2.2689 .0011 -1 -2 2
2.1700 2.1688 .0012 3 1 1
2.1600 2.1634 -.0034 -2 0 3
2.0200 2.0207 -.0007 -2 -2 2
A= 7.922 DA= .002
B= 5.8772 DB= .0005
C= 7.470 DC= .005
GAMMA= 94.28 DGAMMA= .01
BETA = 93.46 DBETA = .02
ALPHA= 93.98 DALPHA= .02
V=345.8