127. 18-0677
La2O3*4PbO
Triklin
Dexp Dcal d(D) h k l
3.2300 3.2301 -.0001 1 3 0
3.1800 3.1794 .0006 2 3 0
2.8600 2.8606 -.0006 -3 1 0
2.6150 2.6159 -.0009 -1 3 0
2.1860 2.1872 -.0012 0 2 1
2.0580 2.0584 -.0004 -2 -2 1
1.9850 1.9843 .0007 -3 0 1
1.9290 1.9284 .0006 3 5 0
1.8980 1.8985 -.0005 1 5 0
1.8730 1.8718 .0012 -3 1 1
1.8480 1.8479 .0001 4 5 0
1.8070 1.8071 -.0001 2 -2 1
A= 11.188 DA= .005
B= 9.7670 DB= .0006
C= 2.4192 DC= .0004
GAMMA= 67.16 DGAMMA= .04
BETA = 89.01 DBETA = .06
ALPHA= 86.12 DALPHA= .05
V=243.0
128. 18-0694
Pb3Ge2O7
Triklin
Dexp Dcal d(D) h k l
7.4600 7.4571 .0029 -1 0 1
3.7100 3.7078 .0022 0 1 1
3.3600 3.3611 -.0011 0 -1 1
3.3100 3.3111 -.0011 -1 0 3
3.2100 3.2096 .0004 1 -1 1
2.9590 2.9543 .0047 -2 0 3
2.9310 2.9331 -.0021 1 0 3
2.8490 2.8477 .0013 1 1 2
2.0800 2.0785 .0015 -4 1 0
2.0270 2.0262 .0008 2 -1 3
2.0020 2.0019 .0001 -4 1 3
1.9370 1.9381 -.0011 4 -1 1
A= 9.439 DA= .003
B= 3.8611 DB= .0008
C= 10.245 DC= .001
GAMMA= 99.38 DGAMMA= .01
BETA =102.26 DBETA = .02
ALPHA= 79.84 DALPHA= .01
V= 356.1
129. 18-0694
Pb3Ge2O7
Triklin
Dexp Dcal d(D) h k l
7.0800 7.0861 -.0061 -1 1 0
4.1000 4.1073 -.0073 3 0 0
3.8800 3.8800 .0000 1 3 0
3.7500 3.7488 .0012 2 3 0
3.6500 3.6546 -.0046 0 3 0
3.5500 3.5430 .0070 -2 2 0
3.4400 3.4439 -.0039 1 -1 1
3.3500 3.3509 -.0009 3 3 0
3.2400 3.2394 .0006 0 -2 1
3.1300 3.1256 .0044 -2 -1 1
3.0600 3.0595 .0005 -1 1 1
3.0000 3.0031 -.0031 -2 0 1
A= 13.11608 DA= .00005
B= 11.72155 DB= .00003
C= 3.67566 DC= .00001
GAMMA= 70.76166 DGAMMA= .00007
BETA = 86.72180 DBETA = .00003
ALPHA= 96.27826 DALPHA= .00007
V=527.1
130. 18-0696
PbGeO3
Triklin
Dexp Dcal d(D) h k l
6.5600 6.5586 .0014 0 1 0
5.9500 5.9567 -.0067 1 0 1
4.4000 4.3956 .0044 0 -1 2
3.6300 3.6316 -.0016 1 2 0
3.4300 3.4359 -.0059 2 1 1
3.3300 3.3320 -.0020 1 0 3
3.1600 3.1633 -.0033 2 0 1
3.1200 3.1176 .0024 2 1 2
3.0500 3.0494 .0006 1 1 3
2.9880 2.9874 .0006 2 2 0
2.9400 2.9365 .0035 2 2 1
2.8850 2.8871 -.0021 1 2 2
ram.:
A= 6.960 DA= .008
B= 7.325 DB= .001
C= 10.473 DC= .005
GAMMA= 65.505 DGAMMA= .001
BETA = 78.33 DBETA = .06
ALPHA= 94.30 DALPHA= .04
V= 468.2
131. 18-0697
Pb4GeO6
Triklin
Dexp Dcal d(D) h k l
7.5000 7.5002 -.0002 0 1 1
3.2800 3.2794 .0006 0 -2 2
3.1800 3.1787 .0013 -2 2 0
3.1200 3.1199 .0001 -1 4 0
3.0700 3.0691 .0009 -1 -2 2
2.9500 2.9497 .0003 -2 3 2
2.8940 2.8956 -.0016 -2 3 0
2.7710 2.7719 -.0009 0 -3 2
2.6830 2.6822 .0008 1 -4 1
2.6370 2.6374 -.0004 -2 1 3
2.5080 2.5081 -.0001 0 5 1
2.4300 2.4302 -.0002 0 -2 3
A= 7.061 DA= .003
B= 13.265 DB= .003
C= 9.0543 DC= .0004
GAMMA=106.89 DGAMMA= .01
BETA =110.369 DBETA = .009
ALPHA= 76.681 DALPHA= .005
V=753.3
132. 18-0701
PbO*4H2O
Triklin
Dexp Dcal d(D) h k l
6.1000 6.1028 -.0028 0 1 1
5.7000 5.7015 -.0015 1 1 0
4.6500 4.6473 .0027 0 -1 1
3.6000 3.6018 -.0018 2 1 0
3.3700 3.3694 .0006 1 1 2
3.0500 3.0514 -.0014 0 2 2
2.9000 2.9005 -.0005 2 2 1
2.8500 2.8507 -.0007 2 2 0
2.6300 2.6291 .0009 0 3 0
2.5400 2.5397 .0003 3 1 0
2.4500 2.4486 .0014 2 -2 1
2.4200 2.4204 -.0004 -3 0 1
A= 7.986 DA= .001
B= 8.200 DB= .005
C= 7.276 DC= .005
GAMMA= 86.74 DGAMMA= .02
BETA = 85.11 DBETA = .02
ALPHA= 74.26 DALPHA= .05
V=456.7
133. 18-1031
K4Pb5O12
Triklin
Dexp Dcal d(D) h k l
8.9000 8.9061 -.0062 0 1 0
5.3000 5.3020 -.0020 -2 1 0
3.0900 3.0925 -.0025 -2 1 1
3.0100 3.0095 .0005 -2 -1 1
2.8710 2.8708 .0002 -2 3 0
2.4180 2.4186 -.0006 -4 0 1
1.8910 1.8906 .0004 -6 2 0
1.8020 1.8020 .0000 -2 5 0
1.7600 1.7603 -.0003 0 -1 2
1.7180 1.7183 -.0003 -6 -1 1
1.6380 1.6379 .0001 -2 2 2
1.5670 1.5672 -.0002 3 -5 1
A= 11.793 DA= .003
B= 9.0846 DB= .0002
C= 3.5868 DC= .0001
GAMMA=100.596 DGAMMA= .004
BETA = 98.39 DBETA = .01
ALPHA= 92.532 DALPHA= .008
V=372.6
134. 18-1055
3K2PbO3*4H2O
Triklin
Dexp Dcal d(D) h k l
7.4800 7.4760 .0040 1 0 0
6.5300 6.5253 .0047 0 1 0
4.7000 4.7031 -.0031 -1 0 1
3.3800 3.3803 -.0003 0 -1 2
3.2800 3.2779 .0021 -1 -2 1
3.1000 3.1049 -.0049 1 2 1
2.8640 2.8635 .0005 -2 -2 1
2.7160 2.7180 -.0020 3 1 0
2.5300 2.5285 .0015 3 0 1
2.4920 2.4920 .0000 3 0 0
2.4270 2.4269 .0001 -2 1 1
2.2930 2.2913 .0017 3 0 2
A= 8.273 DA= .005
B= 7.1406 DB= .0006
C= 7.385 DC= .005
GAMMA= 67.700 DGAMMA= .003
BETA = 80.33 DBETA = .05
ALPHA= 94.52 DALPHA= .02
V= 393.1
135. 18-1056
3K2PbO3*2H2O
Triklin
Dexp Dcal d(D) h k l
9.1600 9.1598 .0002 -1 1 0
6.6400 6.6402 -.0002 0 1 1
5.4700 5.4721 -.0021 0 -1 1
3.8800 3.8804 -.0004 1 2 1
3.8000 3.8008 -.0008 2 -2 1
3.3400 3.3401 -.0001 -3 1 1
3.1800 3.1809 -.0009 2 -1 2
3.1300 3.1305 -.0005 2 2 1
2.8910 2.8911 -.0001 -2 0 2
2.8160 2.8163 -.0003 -1 3 2
2.7650 2.7643 .0007 0 3 2
2.6980 2.6978 .0002 4 -2 1
A= 11.66130 DA= .00006
B= 10.7831 DB= .0002
C= 7.6564 DC= .0008
GAMMA=110.258 DGAMMA= .003
BETA = 85.6011 DBETA = .0004
ALPHA= 80.839 DALPHA= .002
V= 882.6
136. 18-1236
Na4PbO4
Triklin
Dexp Dcal d(D) h k l
5.5700 5.5705 -.0005 1 1 0
5.3200 5.3179 .0021 0 1 1
4.7200 4.7189 .0011 0 -1 1
4.7000 4.7019 -.0019 -1 1 0
4.3000 4.3026 -.0026 2 1 0
3.9800 3.9811 -.0011 0 1 2
3.7300 3.7299 .0001 -2 -1 1
3.3800 3.3832 -.0032 -1 -1 2
3.2300 3.2296 .0004 1 -1 2
2.9100 2.9071 .0029 -2 1 2
2.7940 2.7957 -.0017 2 2 1
2.7200 2.7204 -.0004 -1 -2 1
A= 10.537 DA= .009
B= 6.024 DB= .004
C= 9.728 DC= .004
GAMMA= 78.16 DGAMMA= .09
BETA = 85.18 DBETA = .06
ALPHA= 81.50 DALPHA= .02
V= 596.7
137. 18-1620
C3H6Cl2N2PbS
Triklin
Dexp Dcal d(D) h k l
4.3200 4.3198 .0002 2 0 0
4.0000 3.9972 .0028 2 -1 0
3.6800 3.6819 -.0019 0 -1 2
3.4800 3.4777 .0023 -1 -2 2
3.2300 3.2290 .0010 2 0 1
3.1400 3.1450 -.0050 2 -1 1
2.8300 2.8343 -.0043 2 -2 1
2.7800 2.7786 .0014 3 -1 0
2.6600 2.6608 -.0008 -2 -1 3
2.5100 2.5099 .0001 1 -4 0
2.4700 2.4701 -.0001 -2 1 3
2.2800 2.2772 .0028 -2 -4 2
A= 9.399 DA= .006
B= 10.622 DB= .004
C= 8.183 DC= .001
GAMMA= 86.5 DGAMMA= .1
BETA =113.192 DBETA = .002
ALPHA= 99.23 DALPHA= .05
V=741.6
138. 18-1738
C2H6O4Pb
Triklin
Dexp Dcal d(D) h k l
11.9000 11.7433 .1567 1 0 0
9.7500 9.7581 -.0081 1 2 0
6.9300 6.9364 -.0064 0 1 1
6.7200 6.7188 .0012 0 -1 1
6.1600 6.1588 .0012 1 1 1
6.1000 6.0963 .0037 1 0 1
5.8900 5.8936 -.0036 1 2 1
5.8200 5.8158 .0042 2 2 0
5.7300 5.7333 -.0033 1 -1 1
5.3700 5.3587 .0113 -1 2 1
5.2600 5.2417 .0183 -1 4 0
5.1800 5.1895 -.0095 0 5 0
A= 12.0024 DA= .0003
B= 26.5700 DB= .0001
C= 7.0906 DC= .0002
GAMMA= 78.104 DGAMMA= .002
BETA = 88.456 DBETA = .003
ALPHA= 86.166 DALPHA= .003
V=2209.3
139. 18-1739
C12H18O12Pb3*PbO*H2O
Triklin
Dexp Dcal d(D) h k l
12.2000 11.8645 .3355 0 0 1
6.7900 6.7892 .0008 1 0 0
6.1600 6.1772 -.0172 1 1 0
5.9600 5.9793 -.0193 1 0 1
5.8100 5.8096 .0004 -1 0 1
5.3100 5.3097 .0003 0 -1 1
5.2500 5.2375 .0125 -1 -1 1
4.5500 4.5485 .0015 1 1 2
3.9600 3.9548 .0052 0 0 3
3.8000 3.7991 .0009 1 -1 0
3.7800 3.7863 -.0063 2 1 0
3.5200 3.5199 .0001 1 1 3
A= 7.640 DA= .001
B= 6.994 DB= .002
C= 11.9469 DC= .0001
GAMMA= 62.762 DGAMMA= .006
BETA = 85.36 DBETA = .02
ALPHA= 83.55 DALPHA= .01
V=563.4
140. 18-1740
C4H6O4Pb*2PbO*H2O
Triklin
Dexp Dcal d(D) h k l
12.7000 12.4557 .2443 1 0 0
7.1500 7.1527 -.0027 -1 1 1
6.7800 6.7883 -.0083 0 1 1
5.7400 5.7421 -.0021 0 -1 1
5.2200 5.2167 .0033 1 1 1
4.4300 4.4298 .0002 -1 1 2
4.3800 4.3742 .0058 0 0 2
4.3100 4.3069 .0031 -3 1 1
4.2800 4.2814 -.0014 -2 2 1
4.2000 4.2039 -.0039 0 1 2
4.1500 4.1519 -.0019 3 0 0
4.1000 4.1020 -.0020 -2 -1 1
A= 13.399 DA= .005
B= 9.414 DB= .009
C= 9.159 DC= .001
GAMMA=108.811 DGAMMA= .008
BETA =104.422 DBETA = .005
ALPHA= 76.57 DALPHA= .06
V=1044.5
141. 18-1741
C24H72N12O9P6*Pb{ClO4}2
Triklin
Dexp Dcal d(D) h k l
11.8000 11.7977 .0023 1 1 0
9.8200 9.8376 -.0176 0 1 1
7.6200 7.6204 -.0004 1 2 0
5.9800 5.9814 -.0014 0 0 2
5.6400 5.6416 -.0016 1 0 2
4.6700 4.6670 .0030 2 1 2
4.2900 4.2888 .0012 3 2 1
3.8100 3.8102 -.0002 2 4 0
3.5500 3.5498 .0002 -2 0 3
3.3100 3.3106 -.0006 4 1 2
2.8900 2.8900 -.0000 -1 1 4
a= 16.14 b= 17.29 c= 11.965 beta= 88.97
da=.02 db=.02 dc=.003 dbeta=.01
V= 3338.5
142. 18-1741
C24H72N12O9P6*Pb{ClO4}2
Monoklin
Grupa 4,11
Dexp Dcal d(D) h k l
11.8000 11.7973 .0027 0 1 1
9.8200 9.8378 -.0178 1 1 0
7.6200 7.6204 -.0004 0 2 1
5.9800 5.9815 -.0015 2 0 0
5.6400 5.6418 -.0018 2 0 1
4.6700 4.6671 .0029 2 1 2
4.2900 4.2887 .0013 1 2 3
3.8100 3.8102 -.0002 0 4 2
3.5500 3.5497 .0003 -3 0 2
3.3100 3.3105 -.0005 2 1 4
2.8900 2.8905 -.0005 3 4 1
a= 11.9650 b= 17.290 c= 16.140 beta= 88.963
da=.0004 db=.001 dc=.001 dbet=.002
V= 3338.4
143. 19-0679
Pb5B8O17
Triklin
Dexp Dcal d(D) h k l
10.1000 10.1055 -.0055 0 1 1
9.8200 9.8273 -.0073 0 -1 1
8.3400 8.3529 -.0129 1 0 0
5.2400 5.2456 -.0056 1 -2 1
5.1700 5.1760 -.0060 -1 -2 1
4.9200 4.9136 .0064 0 -2 2
4.8500 4.8473 .0027 0 -3 1
4.6000 4.5992 .0008 1 1 2
4.1200 4.1218 -.0018 -2 1 0
3.9600 3.9618 -.0018 2 1 0
3.7800 3.7798 .0002 -2 2 1
3.6500 3.6505 -.0005 -2 1 2
A= 8.427 DA= .003
B= 15.963 DB= .001
C= 12.862 DC= .005
GAMMA= 94.8224 DGAMMA= .0003
BETA = 96.08 DBETA = .01
ALPHA= 87.87 DALPHA= .01
V= 1713.8
144. 19-0681
Pb3O2CO3
Triklin
Dexp Dcal d(D) h k l
7.0600 7.0535 .0065 -1 0 1
5.5600 5.5621 -.0021 1 1 0
4.5400 4.5398 .0002 -1 -1 2
4.4500 4.4446 .0054 2 0 0
3.9900 3.9872 .0028 0 -1 3
3.5100 3.5041 .0059 -1 1 2
3.3600 3.3643 -.0043 -2 1 0
2.9990 2.9988 .0002 1 -1 4
2.9340 2.9343 -.0003 2 -1 3
2.8690 2.8686 .0004 3 1 0
2.7770 2.7775 -.0005 -1 -2 3
2.6330 2.6326 .0004 1 -2 3
A= 9.031 DA= .002
B= 6.4598 DB= .0001
C= 13.374 DC= .001
GAMMA= 81.282 DGAMMA= .003
BETA = 86.701 DBETA = .007
ALPHA=101.599 DALPHA= .003
V= 752.3
145. 19-0682
Pb2OCO3
Triklin
Dexp Dcal d(D) h k l
6.4700 6.4976 -.0276 1 0 1
4.6200 4.6192 .0008 1 1 1
4.4600 4.4610 -.0010 -1 -1 1
4.1300 4.1313 -.0013 0 0 2
4.0200 4.0231 -.0031 -1 1 1
3.3800 3.3799 .0001 0 1 2
3.2500 3.2488 .0012 2 0 2
3.2200 3.2144 .0056 -2 1 1
3.1800 3.1733 .0067 2 -1 1
2.9320 2.9311 .0009 -2 -1 2
2.8550 2.8545 .0005 1 2 0
2.7310 2.7304 .0006 1 2 1
A= 10.68 DA= .02
B= 5.7219 DB= .0005
C= 8.269 DC= .008
GAMMA= 77.67 DGAMMA= .03
BETA = 89.20 DBETA = .09
ALPHA= 87.83 DALPHA= .03
V= 493.4
146. 19-0685
Pb{Cr19Mo11}O4
Triklin
Dexp Dcal d(D) h k l
4.8900 4.8880 .0020 2 0 0
4.7200 4.7190 .0010 1 1 1
4.3300 4.3357 -.0057 1 -1 1
3.4400 3.4396 .0004 -1 0 2
3.2200 3.2249 -.0049 0 2 0
3.1200 3.1202 -.0002 -1 2 0
3.0100 3.0101 -.0001 -1 2 1
2.6680 2.6678 .0002 -2 2 1
2.5470 2.5457 .0013 2 -2 1
2.4020 2.4033 -.0013 -1 0 3
2.3660 2.3660 -.0000 -3 2 0
2.3540 2.3540 .0000 -2 -2 1
A= 9.83484 DA= .00001
B= 6.53092 DB= .00000
C= 7.74541 DC= .00000
GAMMA= 92.72475 DGAMMA= .00002
BETA = 84.81181 DBETA = .00004
ALPHA= 81.68027 DALPHA= .00002
V=489.3
147. 19-0686
alfa-Pb4BF11
Triklin
Dexp Dcal d(D) h k l
9.7000 9.6946 .0054 1 0 0
6.2000 6.2137 -.0137 -1 1 0
4.8300 4.8294 .0006 -1 -1 2
4.4500 4.4493 .0007 -2 -1 1
4.0500 4.0511 -.0011 0 -2 1
3.6200 3.6188 .0012 1 -2 1
3.4100 3.4091 .0009 -3 0 1
3.2900 3.2907 -.0007 0 -1 3
3.1600 3.1596 .0004 -2 0 3
3.0300 3.0303 -.0003 -3 1 0
2.6300 2.6302 -.0002 2 -2 2
2.4200 2.4194 .0006 1 1 3
A= 10.246 DA= .002
B= 8.183 DB= .002
C= 10.506 DC= .002
GAMMA= 86.7754 DGAMMA= .0007
BETA =108.75 DBETA = .01
ALPHA=106.80 DALPHA= .01
V= 797.9
148. 19-0687
beta-Pb4BF11
Monoklin
Grupa 14
Dexp Dcal d(D) h k l
6.2000 6.2110 -.0110 1 1 0
4.1600 4.1542 .0058 -2 1 1
3.6700 3.6709 -.0009 2 0 2
3.6100 3.6076 .0024 1 2 0
3.3100 3.3117 -.0017 2 1 2
3.1600 3.1561 .0039 0 2 2
3.1100 3.1086 .0014 1 1 3
3.0300 3.0308 -.0008 -2 2 1
2.6300 2.6273 .0027 1 0 4
2.4900 2.4923 -.0023 3 2 1
2.4100 2.4106 -.0006 -3 2 2
2.2710 2.2771 -.0061 -3 0 4
a= 10.610 b= 7.676 c= 11.1350 beta= 94.959
da= .001 db=.001 dc= .0003 dbet= .004
V= 903.4
Triklin
Dexp Dcal d(D) h k l
6.2000 6.1983 .0017 1 0 0
4.1600 4.1588 .0012 -1 1 1
3.6700 3.6720 -.0020 1 -1 1
3.6100 3.6150 -.0050 0 0 2
3.3100 3.3167 -.0067 -1 -1 2
3.1600 3.1550 .0050 -1 2 0
3.1100 3.1116 -.0016 -2 0 1
3.0300 3.0294 .0006 -2 -1 1
2.6300 2.6299 .0001 -2 -1 2
2.4900 2.4909 -.0009 0 -3 1
2.4100 2.4100 -.0000 0 0 3
2.2710 2.2705 .0005 0 1 3
A= 6.408 DA= .001
B= 7.882 DB= .006
C= 7.440 DC= .003
GAMMA= 82.98 DGAMMA= .02
BETA =103.3515 DBETA = .0005
ALPHA= 94.46 DALPHA= .01
V= 362.4
149. 19-0688
Pb2BF7
Triklin
Dexp Dcal d(D) h k l
9.2000 9.2153 -.0153 1 1 0
5.7500 5.7563 -.0063 1 2 0
4.4200 4.4247 -.0047 -1 0 1
4.2200 4.2226 -.0026 -1 2 0
3.9200 3.9171 .0029 1 3 0
3.6600 3.6602 -.0002 0 3 0
3.6100 3.6139 -.0039 0 -2 1
3.5700 3.5694 .0006 3 1 0
3.3000 3.3015 -.0015 -2 -2 1
3.2600 3.2563 .0037 -1 2 1
3.1500 3.1514 -.0014 1 3 1
3.1000 3.1004 -.0004 -1 3 0
A= 10.730 DA= .003
B= 11.7657 DB= .0006
C= 4.9758 DC= .0001
GAMMA= 69.073 DGAMMA= .002
BETA = 88.185 DBETA = .005
ALPHA= 87.241 DALPHA= .006
V=585.4
150. 19-1954
C16H36N2O10Pb
Rombik
Groupa 54
Dexp. Dcal. d(D) h k l
8.7000 8.7412 -.0412 0 0 2
6.9000 6.9150 -.0150 0 1 2
5.0000 4.9902 .0098 1 0 2
4.7500 4.7464 .0036 0 2 2
3.9500 3.9423 .0077 1 1 3
3.7700 3.7682 .0018 0 3 0
3.3700 3.3745 -.0045 1 2 3
3.1500 3.1502 -.0002 1 3 1
2.8700 2.8705 -.0005 2 0 2
a= 6.078 b=11.304 c=17.48
da= .009 db= .001 dc= .03
v=1201