104. 14-0122
PbSe2O5
Triklin
Dexp Dcal d(D) h k l
3.6000 3.5987 .0013 -1 2 1
3.3100 3.3087 .0013 -1 -2 1
3.1500 3.1386 .0114 -1 0 3
3.0700 3.0696 .0004 1 3 1
2.9100 2.9082 .0018 0 4 0
2.4800 2.4797 .0003 -1 -3 2
2.3400 2.3379 .0021 -1 2 5
2.2600 2.2608 -.0008 1 -4 1
2.1600 2.1598 .0002 1 -2 4
2.0800 2.0796 .0004 2 2 2
1.9300 1.9298 .0002 -1 -2 5
1.8900 1.8901 -.0001 -2 1 4
A= 4.50600 DA= .00000
B= 12.352 DB= .001
C= 13.72215 DC= .00007
GAMMA= 88.845 DGAMMA= .005
BETA = 90.476 DBETA = .003
ALPHA= 70.408 DALPHA= .003
V=719.1
105. 14-0123
Pb{HSeO3}2
Triklin
Dexp Dcal d(D) h k l
4.1500 4.1483 .0017 -1 0 1
3.7400 3.7397 .0003 0 1 3
3.3200 3.3179 .0021 1 -1 2
3.0700 3.0688 .0012 0 -1 4
2.9900 2.9882 .0018 1 -1 3
2.8900 2.8885 .0015 1 0 4
2.7200 2.7223 -.0023 -1 -1 2
2.6100 2.6066 .0034 -1 0 5
2.4500 2.4477 .0023 0 -2 1
2.3900 2.3874 .0026 1 -2 1
2.2700 2.2696 .0004 -1 2 3
2.1300 2.1306 -.0006 2 0 0
A= 4.4062 DA= .0004
B= 5.160 DB= .005
C= 16.15 DC= .01
GAMMA=104.67 DGAMMA= .06
BETA = 92.3189 DBETA = .0001
ALPHA= 86.95 DALPHA= .07
V= 354.6
106. 14-0405
PbSiO3
Triklin
Dexp Dcal d(D) h k l
6.4200 6.4225 -.0025 0 1 1
5.7900 5.7990 -.0090 0 -1 1
5.6800 5.6771 .0029 -1 1 0
5.1300 5.1305 -.0005 -1 0 1
4.3700 4.3671 .0029 1 0 1
4.0600 4.0576 .0024 1 -1 1
3.5500 3.5508 -.0008 1 2 1
3.5200 3.5196 .0004 0 1 2
3.3300 3.3322 -.0022 -1 1 2
3.2100 3.2113 -.0013 0 2 2
3.0900 3.0917 -.0017 -1 2 2
3.0400 3.0387 .0013 -2 1 1
A= 6.3703 DA= .0002
B= 11.8650 DB= .001
C= 7.270 DC= .004
GAMMA= 94.73 DGAMMA= .01
BETA = 99.77 DBETA = .02
ALPHA= 82.725 DALPHA= .003
V= 536.1
107. 14-0430
Pb2N2SeO9
Triklin
Dexp Dcal d(D) h k l
4.3000 4.2973 .0027 -1 -1 1
3.7100 3.7075 .0025 0 1 2
3.4200 3.4232 -.0032 -2 1 2
2.9500 2.9524 -.0024 -3 0 2
2.7100 2.7124 -.0024 0 -2 1
2.5200 2.5209 -.0009 1 -2 1
2.4300 2.4316 -.0016 2 2 2
2.3700 2.3705 -.0005 -4 1 0
2.1100 2.1106 -.0006 2 3 0
1.9800 1.9786 .0014 -2 3 0
1.9400 1.9395 .0005 -2 3 3
1.7300 1.7287 .0013 1 4 1
A= 10.92219 DA= .00004
B= 7.0058 DB= .0001
C= 7.89767 DC= .00005
GAMMA= 89.7858 DGAMMA= .0003
BETA =105.0616 DBETA = .0002
ALPHA= 72.2971 DALPHA= .0003
V=553.6
108. 14-0431
PbSeO4
Triklin
Dexp Dcal d(D) h k l
4.3600 4.3606 -.0006 -1 3 0
3.9100 3.9107 -.0007 0 2 1
3.5500 3.5496 .0004 3 0 0
3.4000 3.4073 -.0073 -3 2 0
3.2900 3.2913 -.0013 0 4 0
3.0700 3.0738 -.0038 -2 4 0
2.8200 2.8194 .0006 -2 3 1
2.6500 2.6497 .0003 -4 2 0
2.4600 2.4604 -.0004 0 -5 1
2.2800 2.2800 .0000 -1 -5 1
2.2300 2.2298 .0002 1 -4 2
2.1300 2.1297 .0003 5 0 0
A= 10.9845 DA= .0003
B= 13.534 DB= .002
C= 5.3518 DC= .0002
GAMMA=101.99 DGAMMA= .02
BETA = 80.944 DBETA = .005
ALPHA= 97.747 DALPHA= .009
V=763.9
109. 14-0737
C4H8Pb2O6*H2O
Triklin
Dexp. Dcal. d(D) h k l
13.0000 13.0000 .0000 1 0 0
3.3800 3.3800 .0000 3 -1 0
3.0500 3.0505 -.0005 0 1 1
2.8800 2.8808 -.0008 -1 -1 1
2.7300 2.7300 .0000 4 -1 0
2.6000 2.6000 .0000 5 0 0
2.4800 2.4800 .0000 -3 -1 1
2.2400 2.2397 .0003 -4 -3 0
2.0700 2.0697 .0003 -4 1 1
1.9500 1.9500 -.0000 6 -1 0
1.8800 1.8811 -.0011 1 4 0
1.8100 1.8099 .0001 -4 2 1
A= 13.4582 DA= .0005
B= 7.592 DB= .002
C= 3.2804 DC= .0004
GAMMA= 75.343 DGAMMA= .005
BETA = 85.87 DBETA = .02
ALPHA= 85.73 DALPHA= .02
V= 322.9
110. 14-0961
C10H10Cl2N2Pb
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
11.9000 11.7616 .1384 0 0 1
8.1000 8.0937 .0063 0 1 1
6.9000 6.8750 .0250 1 1 0
5.2000 5.2021 -.0021 0 1 2
4.8700 4.8703 -.0003 1 1 2
4.1500 4.1528 -.0028 -1 1 2
3.9100 3.9052 .0048 2 0 2
3.7100 3.7183 -.0083 0 3 0
3.5500 3.5454 .0046 0 3 1
3.2600 3.2651 -.0051 2 0 3
3.0600 3.0650 -.0050 1 3 2
2.7800 2.7802 -.0002 -2 2 2
a= 8.9160 b= 11.155 c= 12.0120 beta= 78.272
da= .0005 db=.001 dc=.0008 dbet=.004
V= 1169.8
Triklin
Dexp Dcal d(D) h k l
11.9000 11.9016 -.0016 1 0 0
8.1000 8.0941 .0059 0 1 0
6.9000 6.9002 -.0002 0 1 1
5.2000 5.2043 -.0043 2 0 1
4.8700 4.8655 .0045 0 1 2
4.1500 4.1428 .0072 -2 -1 1
3.9100 3.9091 .0009 -1 2 1
3.7100 3.7091 .0009 3 0 1
3.5500 3.5583 -.0083 0 1 3
3.2600 3.2603 -.0003 -3 1 2
3.0600 3.0602 -.0002 -3 2 0
2.7800 2.7797 .0003 -3 1 3
A= 12.037 DA= .002
B= 8.2176 DB= .0008
C= 11.420 DC= .002
GAMMA= 98.43 DGAMMA= .01
BETA = 92.6080 DBETA = .0006
ALPHA= 84.38 DALPHA= .04
V= 1111.5
111. 15-0167
Bi4PbTe7
Monoklin
Grupa 14
Dexp Dcal d(D) h k l
3.2120 3.2118 .0002 2 1 0
2.3470 2.3485 -.0015 2 1 2
2.2590 2.2588 .0002 3 1 0
2.1970 2.1981 -.0011 -2 0 2
1.9930 1.9927 .0003 3 0 2
1.9610 1.9617 -.0007 1 1 3
1.8170 1.8168 .0002 1 4 0
1.6610 1.6611 -.0001 2 4 0
1.6030 1.6029 .0001 0 4 2
1.5390 1.5388 .0002 1 0 4
1.4760 1.4743 .0017 2 0 4
1.4010 1.4008 .0002 -2 3 3
a= 7.155 b= 7.5170 c= 6.185 beta= 83.203
da= .001 db=.0007 dc=.001 dbet=.008
V= 330.3
Triklin
Dexp Dcal d(D) h k l
3.2120 3.2080 .0040 1 1 1
2.3470 2.3461 .0009 1 1 3
2.2590 2.2601 -.0011 0 -2 2
2.1970 2.1974 -.0004 -1 1 3
1.9930 1.9939 -.0009 1 -1 3
1.9610 1.9609 .0001 1 1 4
1.8170 1.8167 .0003 2 0 0
1.6610 1.6607 .0003 1 1 5
1.6030 1.6040 -.0010 2 2 2
1.5390 1.5396 -.0006 -1 -1 5
1.4760 1.4759 .0001 1 -1 5
1.4010 1.4009 .0001 2 2 4
A= 3.679 DA= .001
B= 5.914 DB= .004
C= 9.254 DC= .004
GAMMA= 81.02 DGAMMA= .02
BETA = 89.12 DBETA = .03
ALPHA= 79.93 DALPHA= .02
V=195.7
112. 15-0284
Pb3Si2O7
Triklin
Dexp Dcal d(D) h k l
6.3400 6.3406 -.0006 0 -1 1
4.5500 4.5485 .0015 -1 -1 1
4.1300 4.1292 .0008 -1 0 2
3.8700 3.8706 -.0006 1 1 3
3.4700 3.4717 -.0017 0 0 4
3.1900 3.1902 -.0002 -1 1 3
3.1400 3.1410 -.0010 -1 -1 3
3.0200 3.0176 .0024 -1 -2 2
2.9400 2.9415 -.0015 1 3 1
2.8100 2.8128 -.0028 1 3 0
2.7500 2.7509 -.0009 2 1 1
2.6600 2.6605 -.0005 2 1 2
A= 5.5185 DA= .0003
B= 9.1473 DB= .0001
C= 14.6393 DC= .0005
GAMMA= 71.355 DGAMMA= .002
BETA = 82.981 DBETA = .005
ALPHA= 71.601 DALPHA= .004
V=664.2
113. 15-0436
Pb5GeP2O12
Triklin
Dexp Dcal d(D) h k l
8.5100 8.5082 .0018 0 0 1
4.9000 4.9011 -.0011 0 -2 1
4.2500 4.2479 .0021 -1 -1 1
4.0800 4.0788 .0012 1 0 1
3.6600 3.6627 -.0027 1 1 1
3.3600 3.3589 .0011 -1 -2 2
3.2200 3.2165 .0035 0 -3 1
2.9200 2.9188 .0012 -1 -3 2
2.8400 2.8401 -.0001 1 -2 2
2.7700 2.7670 .0030 -1 2 0
2.2500 2.2513 -.0013 -2 -1 1
2.1900 2.1898 .0002 2 1 1
A= 4.606 DA= .003
B= 10.093 DB= .002
C= 9.778 DC= .002
GAMMA= 76.2414 DGAMMA= .0002
BETA = 93.03 DBETA = .02
ALPHA=119.25 DALPHA= .04
V= 384.2
114. 15-0924
C8H16Cl2O12Pb
Triklin
Dexp Dcal d(D) h k l
7.4700 7.4793 -.0093 1 0 0
6.6800 6.6801 -.0001 0 1 0
5.7700 5.7873 -.0173 1 -1 1
5.2600 5.2595 .0005 -1 0 1
4.3000 4.3016 -.0016 1 1 0
3.8700 3.8688 .0012 -1 -1 1
3.5000 3.5021 -.0021 -1 0 2
3.3400 3.3401 -.0001 0 2 0
3.2500 3.2531 -.0031 -2 0 1
3.1200 3.1196 .0004 1 -2 2
2.8900 2.8936 -.0036 2 -2 2
2.8200 2.8204 -.0004 1 0 3
A= 8.168 DA= .002
B= 7.30288 DB= .00005
C= 8.921 DC= .001
GAMMA=112.134 DGAMMA= .008
BETA = 77.179 DBETA = .008
ALPHA=103.088 DALPHA= .003
V=474.7
115. 16-0117
PbO1.5
Monoklin
Grupa 4,11
Dexp Dcal d(D) h k l
6.9600 6.9573 .0027 1 1 0
3.4800 3.4786 .0014 2 2 0
3.2400 3.2355 .0045 -3 0 1
3.2100 3.2111 -.0011 1 0 3
3.1300 3.1331 -.0031 0 3 1
3.0300 3.0312 -.0012 -2 0 3
2.9590 2.9575 .0015 1 3 1
2.8170 2.8146 .0024 -3 1 2
2.7920 2.7883 .0037 0 3 2
2.3190 2.3191 -.0001 3 3 0
2.1180 2.1177 .0003 0 0 5
1.9190 1.9190 -.0000 3 1 4
a=9.8990 b= 9.840 c= 10.654 beta= 96.354
da=.0008 db=.001 dc= .0009 dbet= .004
V= 1031.4
116. 16-0296
Pb3Si2O7
Triklin
Dexp Dcal d(D) h k l
5.5300 5.5197 .0103 -1 1 0
4.0100 4.0111 -.0011 1 -1 2
3.8300 3.8277 .0023 2 0 0
3.6200 3.6292 -.0092 -1 -1 2
3.5000 3.4976 .0024 -2 1 1
3.2600 3.2623 -.0023 -2 0 2
3.1700 3.1690 .0010 1 -1 3
3.1100 3.1125 -.0025 2 0 2
3.0400 3.0394 .0006 -1 2 1
3.0000 3.0011 -.0011 -1 -1 3
2.9500 2.9460 .0040 -2 -1 1
2.8700 2.8705 -.0005 0 0 4
A= 7.8588 DA= .0004
B= 6.5013 DB= .0009
C= 11.5114 DC= .0001
GAMMA=102.748 DGAMMA= .006
BETA = 92.210 DBETA = .001
ALPHA= 92.894 DALPHA= .002
V=572.5
117. 16-0316
PbAl2O4
Triklin
Dexp Dcal d(D) h k l
4.6200 4.6201 -.0001 0 -1 1
4.4600 4.4634 -.0034 -1 1 1
4.2300 4.2298 .0002 1 -1 1
4.0600 4.0594 .0006 -1 -1 1
3.1200 3.1195 .0005 0 -1 2
3.0700 3.0707 -.0007 -1 1 2
2.6300 2.6290 .0010 1 1 2
2.5400 2.5399 .0001 2 -1 2
2.5100 2.5083 .0017 -3 1 2
2.3900 2.3902 -.0002 -3 2 0
2.3100 2.3101 -.0001 0 -2 2
2.2300 2.2302 -.0002 -1 1 3
A= 9.7367 DA= .0003
B= 5.9079 DB= .0006
C= 7.2801 DC= .0004
GAMMA=102.122 DGAMMA= .006
BETA =100.41 DBETA = .01
ALPHA= 91.0055 DALPHA= .0008
V=402.0
118. 16-0317
Pb2GeO4
Triklin
Dexp Dcal d(D) h k l
8.8500 8.8290 .0210 1 0 0
5.4400 5.4464 -.0064 0 1 1
5.2200 5.2214 -.0015 0 -1 1
4.8500 4.8445 .0055 -1 0 1
4.6000 4.5997 .0003 -1 -1 1
4.4200 4.4145 .0055 2 0 0
3.7700 3.7725 -.0025 0 3 0
3.6800 3.6782 .0018 2 0 1
3.5300 3.5324 -.0024 -1 2 1
3.3400 3.3384 .0016 1 3 1
3.2900 3.2884 .0016 2 -1 1
3.1800 3.1769 .0031 -2 1 1
A= 9.10342 DA= .00008
B= 11.660 DB= .001
C= 6.06877 DC= .00000
GAMMA= 76.376 DGAMMA= .005
BETA = 85.543 DBETA = .001
ALPHA= 86.136 DALPHA= .001
V=622.7
119. 16-0662
Pb2MgWO6
Triklin
Dexp Dcal d(D) h k l
7.9500 7.9390 .0110 -1 0 1
7.1300 7.1187 .0113 0 1 1
5.7300 5.7273 .0027 0 -1 1
5.6600 5.6557 .0043 -1 1 0
5.0900 5.1027 -.0127 1 0 1
5.0300 5.0237 .0063 -1 0 2
4.7100 4.7312 -.0212 -1 1 2
4.6100 4.6273 -.0173 0 0 2
4.3100 4.3139 -.0039 0 2 0
4.2700 4.2773 -.0073 0 2 1
4.0100 4.0212 -.0112 2 0 0
3.9700 3.9695 .0005 -2 0 2
A= 8.8597 DA= .0005
B= 8.8340 DB= .0001
C= 10.4029 DC= .0006
GAMMA= 90.513 DGAMMA= .001
BETA =114.387 DBETA = .003
ALPHA= 78.519 DALPHA= .002
V=724.4
120. 17-0729
Pb2CO4
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
6.4800 6.4758 .0042 1 0 1
4.1400 4.1355 .0045 1 0 2
4.0200 4.0244 -.0044 1 1 1
3.4500 3.4490 .0010 0 1 2
3.3900 3.3881 .0019 2 1 0
3.2200 3.2213 -.0013 1 1 2
3.1800 3.1838 -.0038 2 1 1
2.9350 2.9338 .0012 1 0 3
2.8590 2.8597 -.0007 3 0 1
2.7370 2.7391 -.0021 2 1 2
2.6520 2.6558 -.0038 0 1 3
2.5680 2.5684 -.0004 0 2 0
a= 9.0152 b= 5.137 c= 9.3080
da= .0003 db= .003 dc= .0001
V= 431.0
121. 17-0731
Pb3CO5
Monoklin
Grupa 14
Dexp Dcal d(D) h k l
7.0700 7.0481 .0219 0 1 1
5.5500 5.5502 -.0002 0 0 2
4.5700 4.5615 .0085 0 2 0
4.4600 4.4481 .0119 -1 1 1
4.0200 4.0142 .0058 -1 0 2
3.6000 3.5960 .0040 1 1 2
3.5200 3.5240 -.0040 0 2 2
3.0100 3.0135 -.0035 -1 2 2
2.9390 2.9329 .0061 0 3 1
2.8750 2.8736 .0014 0 2 3
2.7760 2.7751 .0009 0 0 4
2.6590 2.6550 .0040 0 1 4
a= 5.6610 b= 9.1230 c= 11.1040 beta 91.459
da= .0001 db=.0009 dc=.0005 dbet=.0002
V= 573.2
Triklin
Dexp Dcal d(D) h k l
7.0700 7.0700 -.0000 0 0 1
5.5500 5.5521 -.0021 1 0 1
4.5700 4.5689 .0011 0 -2 1
4.4600 4.4569 .0031 1 -2 1
4.0200 4.0216 -.0016 1 2 1
3.6000 3.6031 -.0031 1 -3 1
3.5200 3.5163 .0037 2 0 1
3.0100 3.0087 .0013 2 -3 1
2.9390 2.9407 -.0017 2 2 0
2.8750 2.8727 .0023 -2 -1 1
2.7760 2.7760 -.0000 2 0 2
2.6590 2.6592 -.0002 2 1 2
A= 7.745 DA= .004
B= 13.434 DB= .004
C= 7.1624 DC= .0007
GAMMA=103.394 DGAMMA= .007
BETA = 82.689 DBETA = .002
ALPHA= 86.29 DALPHA= .03
V= 715.65
122. 17-0732
Pb7C4O15
Triklin
Dexp Dcal d(D) h k l
7.1200 7.1240 -.0040 0 1 1
7.0300 7.0340 -.0040 -1 1 0
6.9900 6.9878 .0022 0 -1 1
6.1900 6.1872 .0028 1 1 0
5.7200 5.7140 .0060 -2 0 2
5.1700 5.1710 -.0010 1 -1 2
4.7100 4.7077 .0023 2 0 2
4.6200 4.6210 -.0010 0 -1 3
4.4200 4.4216 -.0016 0 0 4
3.8200 3.8194 .0006 -1 2 1
3.6400 3.6381 .0019 -1 2 2
3.5400 3.5408 -.0008 1 2 0
A= 13.045 DA= .001
B= 7.7867 DB= .0001
C= 18.0892 DC= .0004
GAMMA= 98.7557 DGAMMA= .0006
BETA =102.031 DBETA = .003
ALPHA= 86.728 DALPHA= .001
V=1775
123. 17-0789
Pb4GeO6
Triklin
Dexp Dcal d(D) h k l
7.5000 7.4998 .0002 -1 1 0
3.2800 3.2801 -.0001 1 3 0
3.1800 3.1800 -.0000 -2 2 1
3.1200 3.1204 -.0004 2 2 0
3.0700 3.0712 -.0012 1 3 1
2.9500 2.9503 -.0003 2 -2 3
2.8940 2.8940 .0000 -2 -2 1
2.7710 2.7719 -.0009 -1 -1 3
2.6830 2.6835 -.0005 -1 1 3
2.6370 2.6360 .0010 3 1 1
2.5080 2.5083 -.0003 3 -1 3
2.4300 2.4293 .0007 0 0 4
A= 8.8597 DA= .0001
B= 12.1002 DB= .0003
C= 10.23173 DC= .00009
GAMMA=103.78 DGAMMA= .01
BETA = 74.0546 DBETA = .0002
ALPHA=102.204 DALPHA= .007
V=1011.8
124. 17-0790
Pb3GeO7
Triklin
Dexp Dcal d(D) h k l
7.4600 7.4573 .0027 -1 0 1
3.7100 3.7082 .0018 0 1 1
3.3600 3.3605 -.0005 0 -1 1
3.3100 3.3115 -.0015 -1 0 3
3.2100 3.2090 .0010 1 -1 1
2.9590 2.9545 .0045 -2 0 3
2.9310 2.9344 -.0034 1 0 3
2.8490 2.8491 -.0001 1 1 2
2.0800 2.0786 .0014 -4 1 0
2.0270 2.0263 .0007 2 -1 3
2.0020 2.0019 .0001 -4 1 3
1.9370 1.9382 -.0012 4 -1 1
A= 9.440 DA= .002
B= 3.86079 DB= .00003
C= 10.248 DC= .002
GAMMA= 99.36 DGAMMA= .05
BETA =102.24 DBETA = .03
ALPHA= 79.821 DALPHA= .007
V= 356.2
125. 17-0791
PbGeO3
Triklin
Dexp Dcal d(D) h k l
6.5600 6.5676 -.0076 0 1 1
5.9500 5.9527 -.0027 0 -1 1
4.4000 4.4017 -.0017 2 0 0
3.6300 3.6260 .0040 1 -2 1
3.4300 3.4300 .0000 0 -3 1
3.3300 3.3265 .0035 2 2 1
3.1600 3.1604 -.0004 -1 2 2
3.1200 3.1202 -.0002 1 4 0
3.0000 2.9994 .0006 1 2 2
5.0000 4.9957 .0043 0 2 1
2.9880 2.9866 .0014 -2 1 2
2.9400 2.9415 -.0015 -3 -1 1
A= 9.10892 DA= .00000
B= 12.6976 DB= .0001
C= 7.37616 DC= .00005
GAMMA= 80.2630 DGAMMA= .0005
BETA =100.3309 DBETA = .0002
ALPHA= 85.4669 DALPHA= .0002
V=821.7
126. 17-0792
PbGe2O5
Triklin
Dexp Dcal d(D) h k l
7.0800 7.0863 -.0063 1 1 0
4.1000 4.1016 -.0016 3 1 0
3.8800 3.8789 .0011 1 0 2
3.7500 3.7485 .0015 -2 -1 2
3.6500 3.6467 .0033 -4 1 0
3.5500 3.5532 -.0032 -1 2 1
3.4400 3.4400 .0000 0 1 2
3.3500 3.3469 .0031 -2 1 2
3.2400 3.2388 .0012 1 1 2
3.1300 3.1303 -.0003 2 -2 2
3.0600 3.0619 -.0019 -4 2 0
2.9980 2.9994 -.0014 -4 0 2
A= 15.304 DA= .003
B= 8.9700 DB= .0004
C= 8.61777 DC= .00210
GAMMA= 96.461 DGAMMA= .001
BETA = 95.99 DBETA = .01
ALPHA=103.059 DALPHA= .006
V=1134.7