C4H8Pb2O6*H2O
TRiklin
Dexp Dcal d(D) h k l
13.0000 13.0021 -.0021 1 0 0
3.3800 3.3801 -.0001 2 1 1
3.0500 3.0510 -.0010 -4 -1 1
2.8800 2.8802 -.0002 -3 1 1
2.7300 2.7294 .0006 -3 -1 2
2.6000 2.5999 .0001 -5 0 1
2.4800 2.4796 .0004 -4 1 1
2.2400 2.2398 .0002 -5 0 2
2.0700 2.0706 -.0006 -4 -2 2
1.9500 1.9496 .0004 -4 -1 3
1.8800 1.8797 .0003 -6 1 0
1.8100 1.8087 .0013 2 3 0
A= 13.6320 DA= .0006
B= 5.480 DB= .001
C= 6.4268 DC= .0002
GAMMA= 77.19 DGAMMA= .01
BETA =103.17 DBETA = .01
ALPHA= 96.86 DALPHA= .01
V= 454.6
2. 1-0028
Pb{C2H3O2}2*3H2O
Triklin
Dexp Dcal d(D) h k l
11.7000 11.8601 -.1601 1 0 0
7.7000 7.6829 .0171 0 0 1
4.9000 4.9003 -.0003 -2 0 1
4.3600 4.3591 .0009 0 -2 1
4.2400 4.2350 .0050 2 -1 1
3.5000 3.4989 .0011 -2 1 1
3.3600 3.3570 .0030 -2 0 2
2.9000 2.9004 -.0004 4 1 0
2.8100 2.8120 -.0020 -2 -2 3
2.6900 2.6904 -.0004 4 0 1
2.6200 2.6219 -.0019 -2 1 2
2.5300 2.5297 .0003 -2 2 1
A= 12.162 DA= .002
B= 8.9081 DB= .0006
C= 8.942 DC= .001
GAMMA= 78.162 DGAMMA= .002
BETA =100.13 DBETA = .01
ALPHA=120.428 DALPHA= .004
V=814.8
3. 1-0236
PbSiF6*2H2O
Triklin
Dexp Dcal d(D) h k l
8.8000 8.8015 -.0015 0 1 1
7.9000 7.8968 .0032 0 -1 1
6.3000 6.3000 .0000 1 1 0
5.7000 5.6971 .0029 -1 -1 1
5.1000 5.1002 -.0002 1 0 2
4.2500 4.2507 -.0007 1 2 1
3.8600 3.8561 .0039 2 0 0
3.5500 3.5514 -.0014 0 0 4
3.4300 3.4293 .0007 1 -2 2
3.2400 3.2393 .0007 0 -3 1
2.9200 2.9201 -.0001 2 0 3
2.7500 2.7493 .0007 1 3 3
A= 7.7278 DA= .0006
B= 10.326 DB= .001
C= 14.3128 DC= .0008
GAMMA= 87.743 DGAMMA= .005
BETA = 92.574 DBETA = .008
ALPHA= 83.582 DALPHA= .002
V= 1132.6
4. 1-0249
CN3Pb
Triklin
Dexp Dcal d(D) h k l
4.9900 4.9896 .0004 -1 0 1
4.0100 4.0045 .0055 0 1 1
3.6500 3.6517 -.0017 2 1 0
3.1900 3.1862 .0038 -2 1 0
3.0600 3.0582 .0018 -2 -1 1
2.9200 2.9171 .0029 -2 1 1
2.7800 2.7799 .0001 -1 0 2
2.6800 2.6758 .0042 1 0 2
2.6000 2.6020 -.0020 0 1 2
2.4600 2.4615 -.0015 -3 1 0
2.2500 2.2489 .0011 -2 1 2
2.1000 2.0998 .0002 3 2 0
A= 9.1784 DA= .0003
B= 5.183 DB= .003
C= 5.7507 DC= .0002
GAMMA= 82.47 DGAMMA= .07
BETA = 93.13 DBETA = .03
ALPHA= 85.05 DALPHA= .03
V= 269.6
5. 1-0279
Na2PbO3*3H2O
Triklin
Dexp Dcal d(D) h k l
4.8000 4.8032 -.0032 -1 1 1
4.6200 4.6188 .0012 -1 -1 1
4.1500 4.1506 -.0006 1 0 1
3.0000 3.0013 -.0013 -2 0 2
2.9000 2.9008 -.0008 -2 1 0
2.5300 2.5302 -.0002 0 3 0
1.8500 1.8500 -.0000 -2 3 0
1.7300 1.7297 .0003 -4 1 2
1.6200 1.6201 -.0001 0 3 4
1.4200 1.4201 -.0001 -5 0 3
1.3900 1.3900 .0000 -1 3 5
1.2600 1.2600 .0000 -3 -2 5
A= 7.4443 DA= .0001
B= 7.961 DB= .003
C= 7.390 DC= .003
GAMMA= 81.64 DGAMMA= .01
BETA =108.189 DBETA = .009
ALPHA= 78.159 DALPHA= .005
V= 396.7
6. 1-0285
C2PbO4
Triklin
Dexp Dcal d(D) h k l
4.7700 4.7723 -.0023 0 -1 2
4.5000 4.4919 .0081 -2 1 0
4.2500 4.2487 .0013 2 -1 1
3.7600 3.7608 -.0008 -2 0 2
3.3900 3.3883 .0017 2 1 0
3.2800 3.2785 .0015 0 1 3
3.0000 2.9995 .0005 0 0 4
2.7500 2.7504 -.0004 -2 2 2
2.6200 2.6191 .0009 -3 2 1
2.5300 2.5297 .0003 2 -1 4
2.4000 2.3996 .0004 0 0 5
2.3200 2.3199 .0001 4 0 0
A= 9.71096 DA= .00002
B= 7.1149 DB= .0001
C= 12.08211 DC= .00008
GAMMA=106.926 DGAMMA= .001
BETA = 90.9046 DBETA = .0007
ALPHA= 96.157 DALPHA= .003
V=793.3
7. 1-0590
Pb2{SbO4}2
Triklin
Dexp Dcal d(D) h k l
5.8000 5.8025 -.0025 -1 0 1
4.5500 4.5483 .0017 0 1 0
4.3500 4.3278 .0222 -1 0 3
3.8800 3.8797 .0003 1 0 3
3.4800 3.4782 .0018 -1 1 1
3.2000 3.1968 .0032 0 -1 4
3.0000 3.0018 -.0018 0 1 4
2.8200 2.8152 .0048 0 0 6
2.6500 2.6512 -.0012 -1 -1 5
2.0800 2.0809 -.0009 -1 -2 3
1.8700 1.8706 -.0006 0 1 8
1.8200 1.8203 -.0003 -3 -1 3
A= 5.979 DA= .001
B= 4.562 DB= .003
C= 17.03 DC= .01
GAMMA= 87.28 DGAMMA= .01
BETA = 96.43 DBETA = .02
ALPHA= 93.899 DALPHA= .006
V=460.2
8. 1-0608
PbI2
Rombik
Groupa 17
Dexp. Dcal. d(D) h k l
7.0000 6.9857 .0143 0 0 1
3.9500 3.9387 .0113 0 2 0
3.4300 3.4309 -.0009 0 2 1
2.6200 2.6258 -.0058 0 3 0
2.2700 2.2714 -.0014 1 3 0
2.1600 2.1601 -.0001 1 3 1
2.0000 2.0027 -.0027 1 1 3
1.9000 1.8996 .0004 2 0 2
1.7100 1.7145 -.0045 2 3 0
1.6300 1.6260 .0040 1 3 3
1.5000 1.5007 -.0007 2 2 3
1.4500 1.4499 .0001 3 1 1
a= 4.5272 b= 7.87737 c= 6.986
da= .0006 db= .00002 dc= .006
V= 249.1
Triklin
Dexp Dcal d(D) h k l
7.0000 6.9976 .0024 1 1 0
3.9500 3.9500 .0000 -1 0 1
3.4300 3.4303 -.0003 -1 -2 1
2.6200 2.6204 -.0004 -1 -4 1
2.2700 2.2702 -.0002 0 -1 2
2.1600 2.1600 .0000 -1 1 2
2.0000 1.9999 .0001 1 6 1
1.9000 1.8997 .0003 4 1 1
1.7100 1.7100 .0000 1 8 0
1.6300 1.6301 -.0001 4 5 0
1.5000 1.5001 -.0001 1 1 3
1.4500 1.4500 .0000 -5 -3 1
A= 8.4086 DA= .0006
B= 14.2256 DB= .0002
C= 4.58853 DC= .00009
GAMMA= 94.180 DGAMMA= .001
BETA = 87.448 DBETA = .001
ALPHA= 91.496 DALPHA= .001
V= 546.72
9. 1-0635
PbHAsO4
Triklin
Dexp Dcal d(D) h k l
6.7000 6.7000 .0000 1 0 0
4.8800 4.8801 -.0001 0 1 0
4.4300 4.4291 .0009 0 1 1
3.3900 3.3902 -.0002 1 1 2
3.1700 3.1717 -.0017 2 0 1
2.9300 2.9313 -.0013 0 -1 2
2.5600 2.5550 .0050 1 0 3
2.4200 2.4194 .0006 2 2 1
2.2000 2.1998 .0002 -2 -2 1
1.9500 1.9512 -.0012 0 1 4
1.7800 1.7805 -.0005 2 -1 3
1.6800 1.6798 .0002 2 3 2
A= 7.1822 DA= .0009
B= 5.2609 DB= .0009
C= 8.1836 DC= .0009
GAMMA= 69.24 DGAMMA= .02
BETA = 83.11 DBETA = .04
ALPHA= 80.83 DALPHA= .03
V= 284.76
10. 1-0654
Pb3O4
Rombik
Groupa 17
Dexp. Dcal. d(D) h k l
3.3500 3.3499 .0001 0 2 2
2.8800 2.8726 .0074 1 1 2
2.7600 2.7676 -.0076 0 3 0
2.6200 2.6213 -.0013 1 0 3
1.9500 1.9493 .0007 0 4 2
1.8900 1.8905 -.0005 0 0 6
1.8200 1.8196 .0004 0 4 3
1.7400 1.7395 .0005 1 3 4
1.6200 1.6204 -.0004 0 0 7
1.5800 1.5803 -.0003 1 3 5
1.5100 1.5095 .0005 0 2 7
1.4100 1.4102 -.0002 2 3 3
a= 3.637 b= 8.303 c=11.343
da= .003 db= .001 dc= .002
V= 342.6
11. 1-0687
2PbCO3*Pb{OH}2
Rombik
Groupa 30,53
Dexp. Dcal. d(D) h k l
4.4500 4.4482 .0018 1 1 1
4.2400 4.2251 .0149 2 0 0
3.6100 3.6092 .0008 2 1 0
3.2800 3.2870 -.0070 2 1 1
2.6200 2.6159 .0041 0 2 2
2.2300 2.2319 -.0019 1 3 0
2.1100 2.1090 .0010 3 2 1
2.0300 2.0296 .0004 2 3 0
1.8600 1.8606 -.0006 3 1 3
1.6900 1.6900 -.0000 5 0 0
a= 8.450 b= 6.942 c= 7.96
da= .001 db= .004 dc= .02
v= 466.9
12. 2-0141
Pb{ClO2}2
Triklin
Dexp Dcal d(D) h k l
5.8000 5.8007 -.0007 -1 1 0
3.0000 3.0001 -.0001 1 3 0
2.0900 2.0895 .0005 3 0 1
2.0200 2.0193 .0007 2 -3 1
1.6700 1.6697 .0003 0 -5 1
1.6000 1.5998 .0002 1 6 1
1.5200 1.5207 -.0007 -4 0 1
1.3500 1.3499 .0001 2 -4 2
1.3000 1.3002 -.0002 -5 3 0
1.2300 1.2292 .0008 -3 -3 2
1.1400 1.1400 .0000 -6 2 0
1.1000 1.1001 -.0001 3 -2 3
A= 7.031 DA= .001
B= 10.201 DB= .002
C= 3.8427 DC= .0005
GAMMA= 90.25 DGAMMA= .03
BETA = 83.65 DBETA = .01
ALPHA= 80.941 DALPHA= .004
V= 270.4
13. 2-0317
2Bi2S3*PbS
Triklin
Dexp Dcal d(D) h k l
5.8000 5.8191 -.0191 1 0 0
3.0000 2.9985 .0015 -1 0 1
2.0900 2.0899 .0001 0 -2 1
2.0200 2.0200 -.0000 1 -2 1
1.6700 1.6699 .0001 -2 3 0
1.6000 1.6001 -.0001 0 -3 1
1.5200 1.5200 -.0000 -1 3 2
1.3500 1.3500 .0000 -2 4 0
1.3000 1.3000 -.0000 4 2 0
1.2300 1.2300 .0000 1 5 1
1.1400 1.1385 .0015 5 1 0
1.1000 1.1000 .0000 5 2 1
A= 5.8632 DA= .0003
B= 6.2734 DB= .0001
C= 3.94333 DC= .00009
GAMMA= 89.219 DGAMMA= .004
BETA = 83.074 DBETA = .009
ALPHA= 74.082 DALPHA= .001
V=138.5
14. 2-0457
Bi2PbAg2S5
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
3.4200 3.4167 .0033 0 2 0
3.2800 3.2799 .0001 1 0 1
2.9500 2.9569 -.0069 1 1 1
2.8200 2.8171 .0029 1 2 0
2.0800 2.0818 -.0018 0 0 2
2.0000 1.9983 .0017 0 3 1
1.7800 1.7821 -.0021 -2 2 1
1.7100 1.7084 .0016 0 4 0
1.6400 1.6400 .0000 2 0 2
1.4800 1.4785 .0015 -3 1 1
1.4100 1.4085 .0015 2 4 0
1.3600 1.3601 -.0001 0 1 3
a= 4.985 b= 6.833 c= 4.169 beta= 87.0
da=.006 db=.005 dc=.003 dbeta=.1
V= 141.8
15. 2-0495
Sb6Pb2S11
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
3.8200 3.8162 .0038 -1 1 1
3.6100 3.6063 .0037 -1 1 2
3.3800 3.3783 .0017 -2 0 3
3.2300 3.2310 -.0010 0 0 5
2.9300 2.9319 -.0019 -1 1 4
2.7400 2.7415 -.0015 2 1 1
2.4700 2.4715 -.0015 3 0 0
2.2300 2.2290 .0010 2 0 5
2.1400 2.1397 .0003 -1 2 1
2.0000 2.0002 -.0002 2 0 6
1.8900 1.8891 .0009 -4 0 2
1.7500 1.7500 .0000 2 2 3
1.6900 1.6905 -.0005 -4 1 4
a= 7.561 b= 4.4759 c= 16.47 beta= 101.292
da= .001 db=.0005 dc=.01 dbeta=.003
V= 546.7
16. 2-0503
Sb6Pb2S11
Triklin
Dexp Dcal d(D) h k l
3.6000 3.5974 .0026 0 1 1
3.2200 3.2194 .0006 0 -1 1
3.0100 3.0103 -.0003 -1 1 0
2.8500 2.8503 -.0003 1 -1 1
2.7400 2.7401 -.0001 2 0 2
2.6300 2.6293 .0007 -1 1 1
2.1800 2.1820 -.0020 2 -1 1
2.0500 2.0533 -.0033 3 1 1
1.9700 1.9697 .0003 0 2 1
1.9200 1.9191 .0009 3 0 0
1.8000 1.7987 .0013 0 2 2
1.7300 1.7309 -.0009 2 0 4
A= 6.457 DA= .002
B= 4.148 DB= .002
C= 7.234 DC= .007
GAMMA= 74.83 DGAMMA= .02
BETA = 65.32 DBETA = .03
ALPHA= 77.389 DALPHA= .02
V= 168.6
17. 2-0538
Pb3As2S6
Triklin
Dexp Dcal d(D) h k l
4.8000 4.8050 -.0050 -2 1 0
4.4000 4.4033 -.0033 1 1 1
4.2000 4.1961 .0039 0 -1 1
3.6900 3.6854 .0046 2 -1 1
3.5300 3.5308 -.0008 -2 2 0
3.3700 3.3685 .0015 3 0 1
3.1900 3.1875 .0025 -2 1 1
3.0500 3.0464 .0036 -1 -2 1
2.8900 2.8875 .0025 4 0 0
2.7900 2.7882 .0018 4 1 0
2.7100 2.7112 -.0012 -2 -2 1
2.5800 2.5784 .0016 4 -1 1
A= 11.81802 DA= .00001
B= 9.23632 DB= .00007
C= 4.95328 DC= .00001
GAMMA= 86.9823 DGAMMA= .0002
BETA = 78.0066 DBETA = .0001
ALPHA= 86.5099 DALPHA= .0002
V=527.
18. 2-0627
{Pb,Au,Te}S
Triklin
Dexp Dcal d(D) h k l
3.6200 3.6213 -.0013 0 1 1
3.4000 3.4003 -.0003 0 -1 1
3.0200 3.0181 .0019 -1 0 2
2.8300 2.8288 .0012 -1 1 0
2.6500 2.6480 .0020 -1 1 2
2.4300 2.4351 -.0051 1 0 3
2.0900 2.0905 -.0005 -1 1 4
1.8400 1.8399 .0001 1 -1 4
1.7900 1.7897 .0003 1 0 5
1.7200 1.7201 -.0001 -2 1 1
1.5200 1.5204 -.0004 1 2 0
1.4800 1.4793 .0007 0 1 7
A= 3.573 DA= .002
B= 3.803 DB= .001
C= 10.8953 DC= .0004
GAMMA=101.554 DGAMMA= .005
BETA = 94.72 DBETA = .03
ALPHA= 83.318 DALPHA= .004
V= 143.8
19. 2-0639
2PbS*As2S3
Monoklin
Grupa 14
Dexp Dcal d(D) h k l
3.3600 3.3586 .0014 1 1 1
3.2000 3.2011 -.0011 2 2 0
3.0100 3.0124 -.0024 3 0 0
2.8400 2.8400 .0000 2 1 1
2.3200 2.3195 .0005 1 3 1
2.2000 2.1996 .0004 1 4 0
2.0900 2.0913 -.0013 -3 2 1
1.9100 1.9113 -.0013 -1 4 1
1.8600 1.8588 .0012 -3 3 1
1.5300 1.5297 .0003 -5 2 1
1.4500 1.4502 -.0002 3 5 1
1.4200 1.4200 .0000 4 2 2
1.2200 1.2199 .0001 1 7 1
a= 9.040 b= 9.0710 c= 3.904 beta= 88.580
da= .001 db=.0001 dc=.001 dbet=.002
V= 320.0
20. 2-0661
3{Ag2Pb}S*2Bi2S3
Triklin
Dexp Dcal d(D) h k l
3.6700 3.6703 -.0003 0 1 2
3.0000 2.9998 .0002 1 0 2
2.8200 2.8196 .0004 0 -1 2
2.7600 2.7572 .0028 2 1 0
2.5800 2.5762 .0038 1 2 0
2.4400 2.4431 -.0031 0 -2 1
2.3200 2.3219 -.0019 1 2 2
2.2200 2.2200 .0000 2 0 2
2.1200 2.1183 .0017 3 0 0
2.0300 2.0304 -.0004 -3 1 2
1.8900 1.8890 .0010 0 3 0
1.8300 1.8285 .0015 -3 0 3
A= 6.521 DA= .002
B= 5.9172 DB= .0007
C= 8.142 DC= .001
GAMMA= 94.36 DGAMMA= .08
BETA =102.96 DBETA = .03
ALPHA= 73.302 DALPHA= .002
V=193.1
21. 2-0665
PbO*PbBr2
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
3.9100 3.9101 -.0001 2 1 0
2.9900 2.9910 -.0010 -1 2 1
2.8900 2.8907 -.0007 3 1 1
2.1700 2.1705 -.0005 -1 1 3
2.0700 2.0698 .0002 -4 0 1
1.7400 1.7397 .0003 -3 0 3
1.7100 1.7097 .0003 1 2 4
1.6900 1.6899 .0001 2 4 1
1.5000 1.4999 .0001 0 0 5
1.4500 1.4501 -.0001 4 4 1
1.3600 1.3600 -.0000 7 0 2
1.3100 1.3101 -.0001 -2 1 5
1.3000 1.2999 .0001 5 4 0
a= 9.5712 b= 7.299 c= 7.7509 beta= 75.36
da= .00015 db= .001 dc=.0009 dbeta=.02
V= 523.9
22. 2-0757
Bi2O3*6PbO*3CO2
Triklin
Dexp Dcal d(D) h k l
6.7000 6.7011 -.0011 0 1 1
3.6700 3.6717 -.0017 2 -1 1
3.5300 3.5301 -.0001 0 3 1
3.3900 3.3899 .0001 2 1 1
3.1700 3.1712 -.0012 -2 -1 2
2.9000 2.9005 -.0005 2 -3 1
2.7000 2.7077 -.0077 3 -1 1
2.6900 2.6888 .0012 -2 4 0
2.5200 2.5206 -.0006 2 3 1
2.3500 2.3498 .0002 -4 1 1
2.2600 2.2602 -.0002 0 5 1
2.1200 2.1193 .0007 4 -1 1
A= 9.4385 DA= .0003
B= 11.963 DB= .001
C= 8.3697 DC= .0003
GAMMA= 99.68 DGAMMA= .02
BETA =101.39 DBETA = .01
ALPHA= 88.703 DALPHA= .006
V=913.7
23. 2-0763
Pb6Sb2Sn6S21
Rombik
Groupa 33,49, 62
Dexp. Dcal. d(D) h k l
3.4500 3.4485 .0015 0 2 0
3.1500 3.1507 -.0007 3 1 0
2.8900 2.8926 -.0026 2 2 0
2.0300 2.0309 -.0009 5 1 0
1.8100 1.8092 .0008 5 2 0
1.4600 1.4599 .0001 1 2 2
1.2900 1.2901 -.0001 2 3 2
a=10.6256 b= 6.897 c= 3.2606
da= .0004 db= .001 dc= .0005
V= 238.95
24. 2-0765
Pb5Sb2Sn2S12
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
3.4300 3.4448 -.0148 0 0 1
3.1500 3.1502 -.0002 1 0 1
2.8800 2.8801 -.0001 2 1 0
2.2200 2.2192 .0008 3 1 0
2.0600 2.0639 -.0039 1 2 0
1.8200 1.8181 .0019 0 2 1
1.4400 1.4400 -.0000 4 2 0
1.3000 1.2999 .0001 1 3 1
a= 7.785 b= 4.28105 c= 3.445
da= .001 db= .00004 dc= .003
V= 114.8
25. 2-0775
2PbS*{Bi,Sb}2S3
Triklin
Dexp Dcal d(D) h k l
4.2500 4.2402 .0098 -1 1 1
4.0000 3.9969 .0031 0 1 1
3.7800 3.7874 -.0074 0 -1 1
3.5500 3.5449 .0051 -1 -1 1
3.3800 3.3824 -.0024 -1 0 2
3.2700 3.2776 -.0076 1 -1 1
3.1400 3.1445 -.0045 0 0 2
2.9800 2.9783 .0017 -1 1 2
2.8600 2.8616 -.0016 2 0 1
2.7200 2.7228 -.0028 0 1 2
2.6000 2.5984 .0016 1 0 2
2.3100 2.3083 .0017 1 -1 2
A= 8.5152 DA= .0006
B= 5.0523 DB= .0002
C= 6.824 DC= .002
GAMMA=101.32 DGAMMA= .02
BETA =112.63 DBETA = .03
ALPHA= 82.791 DALPHA= .007
V=266.3
26. 2-1246
3PbO*SO3
Triklin
Dexp Dcal d(D) h k l
3.3300 3.3272 .0028 1 0 1
3.2000 3.2003 -.0003 0 1 1
2.9500 2.9488 .0012 0 -1 1
2.9200 2.9181 .0019 1 -1 1
2.4900 2.4916 -.0016 -1 2 1
2.4400 2.4397 .0003 -2 -1 1
2.2900 2.2915 -.0015 1 2 1
2.2600 2.2588 .0012 1 -2 1
2.0600 2.0616 -.0016 4 0 1
1.9900 1.9896 .0004 -3 3 0
1.9200 1.9207 -.0007 -5 2 0
1.8700 1.8698 .0002 0 3 1
A= 10.469 DA= .001
B= 6.441 DB= .001
C= 3.5395 DC= .0002
GAMMA=103.47 DGAMMA= .09
BETA = 91.41 DBETA = .01
ALPHA= 84.36 DALPHA= .02
V= 231.1
27. 2-1276
Pb5SO8
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
3.6100 3.6011 .0089 -1 1 1
3.2000 3.1986 .0014 -2 0 2
3.1000 3.0962 .0038 -1 1 2
2.8900 2.8934 -.0034 2 0 2
2.7000 2.7038 -.0038 2 1 1
2.5800 2.5784 .0016 -2 1 2
2.1700 2.1708 -.0008 0 1 4
1.9800 1.9886 -.0086 -1 0 5
1.9500 1.9483 .0017 3 1 2
1.9100 1.9105 -.0005 -4 0 1
1.8900 1.8898 .0002 1 0 5
1.8400 1.8390 .0010 4 0 1
a= 7.6710 b= 4.357 c= 10.0690 beta= 95.944
da=.0008 db=.002 dc=.0001 dbet=.007
V= 334.7
Triklin
Dexp Dcal d(D) h k l
3.6100 3.6094 .0006 0 -1 1
3.2000 3.1999 .0001 0 -3 1
3.1000 3.0978 .0022 -1 4 0
2.8900 2.8919 -.0019 1 4 0
2.7000 2.7004 -.0004 0 -5 1
2.5800 2.5835 -.0035 0 6 1
2.1700 2.1694 .0006 0 8 1
1.9800 1.9795 .0005 1 -5 1
1.9500 1.9508 -.0008 -1 2 2
1.9100 1.9111 -.0011 -2 -1 1
1.8900 1.8899 .0001 1 -6 1
1.8400 1.8391 .0009 -1 -3 2
A= 3.9342 DA= .0009
B= 20.873 DB= .004
C= 3.9672 DC= .0004
GAMMA= 95.4770 DGAMMA= .0001
BETA =111.237 DBETA = .005
ALPHA= 85.64 DALPHA= .01
V= 302.0
28. 2-1376
Pb4SO7
Monoklin
Grupa 4,11
Dexp Dcal d(D) h k l
9.7800 9.7699 .0101 0 0 1
3.2500 3.2481 .0019 0 1 1
2.7400 2.7407 -.0007 1 1 2
2.5200 2.5170 .0030 2 1 2
2.4600 2.4583 .0017 3 0 3
2.3300 2.3280 .0020 1 1 3
2.1900 2.1914 -.0014 2 1 3
2.1000 2.0997 .0003 4 1 0
1.9900 1.9923 -.0023 0 1 4
1.9400 1.9395 .0005 1 0 5
1.8900 1.8912 -.0012 2 1 4
1.8400 1.8395 .0005 -2 1 4
a= 10.610 b= 3.444 c=9.7830 beta= 87.033
da= .001 db= .001 dc=.0001 dbet=.007
V= 357.0