1. 45-0224
K2NiF4*2H2O
Triklin
Dexp Dcal d(D) h k l
3.3602 3.3585 .0017 0 -1 1
3.2002 3.2035 -.0033 0 -2 1
3.0802 3.0773 .0029 -1 1 0
3.0102 3.0111 -.0009 1 1 0
2.9502 2.9523 -.0021 0 -3 1
2.8302 2.8240 .0062 1 2 0
2.6702 2.6676 .0026 0 -4 1
2.5802 2.5843 -.0041 1 -2 1
2.5502 2.5557 -.0055 0 6 0
2.1601 2.1589 .0013 0 5 1
2.1201 2.1236 -.0035 1 5 0
2.0301 2.0298 .0004 -1 6 0
A= 3.21350 DA= .00004
B= 15.47005 DB= .00001
C= 3.4938 DC= .0001
GAMMA= 94.8143 DGAMMA= .0001
BETA = 75.444 DBETA = .002
ALPHA= 96.894 DALPHA= .001
V=166.5
2. 45-0225
KNiF3*H2O
Rombik
Groupa 27
Dexp. Dcal. d(D) h k l
4.0002 3.9962 .0041 1 1 0
2.8402 2.8376 .0027 2 1 0
2.3102 2.3100 .0002 0 0 2
2.0901 2.0874 .0027 0 1 2
1.7901 1.7914 -.0013 2 1 2
1.6401 1.6393 .0008 3 0 2
a= 6.980 b= 4.874 c= 4.620
da= .001 db= .001 dc= .001
V= 157.17
3. 45-0741
C8H16O8*NiF2
Triklin
Dexp Dcal d(D) h k l
4.7603 4.7629 -.0026 1 0 0
4.4303 4.4282 .0021 -1 1 1
3.7203 3.7200 .0003 -1 -1 1
3.5203 3.5189 .0014 -1 1 2
3.0902 3.0894 .0008 1 -1 1
2.9502 2.9506 -.0003 0 3 1
2.6502 2.6483 .0019 1 1 2
2.4402 2.4394 .0008 -2 1 1
2.2502 2.2505 -.0003 -1 3 3
2.1601 2.1606 -.0005 -1 -1 3
2.1002 2.1005 -.0003 2 0 1
1.9501 1.9501 .0000 -2 3 1
A= 4.9704 DA= .0002
B= 8.8973 DB= .0001
C= 8.071 DC= .003
GAMMA= 95.18 DGAMMA= .03
BETA =106.61 DBETA = .05
ALPHA= 69.574 DALPHA= .002
V= 320.5
4. 45-0762
NiAu2{CN}4
Triklin
Dexp Dcal d(D) h k l
10.1306 10.1213 .0094 1 0 0
7.6209 7.6245 -.0036 0 1 0
5.8706 5.8661 .0046 0 -1 1
5.1006 5.1044 -.0038 2 -1 1
4.6705 4.6701 .0004 -2 1 0
3.8304 3.8300 .0004 -1 2 0
3.4034 3.4014 .0020 3 0 2
3.2163 3.2184 -.0020 -1 2 1
3.1104 3.1084 .0019 -1 -1 2
3.0363 3.0382 -.0019 2 0 3
2.9494 2.9499 -.0006 3 -2 2
2.8193 2.8195 -.0002 4 -1 1
A= 11.480 DA= .009
B= 7.904 DB= .003
C= 9.369 DC= .005
GAMMA=104.71 DGAMMA= .01
BETA = 64.16 DBETA = .03
ALPHA=100.05 DALPHA= .03
V= 738.0
5. 45-0962
Fe5Ni23S16Ti56
Triklin
Dexp Dcal d(D) h k l
4.1072 4.1066 .0006 0 1 0
3.5063 3.5064 -.0001 0 -1 2
3.2122 3.2114 .0008 -1 -1 2
2.5692 2.5693 -.0001 0 -1 4
2.4272 2.4293 -.0021 -1 -1 4
2.1961 2.1964 -.0002 -1 1 2
2.1322 2.1335 -.0014 -1 -2 2
2.0051 2.0044 .0008 -1 -2 3
1.7891 1.7878 .0013 2 0 3
1.6851 1.6856 -.0005 1 2 5
1.6411 1.6410 .0001 -2 0 4
1.5041 1.5041 -.0000 1 0 8
A= 4.283 DA= .001
B= 4.533 DB= .003
C= 12.9016 DC= .0001
GAMMA= 64.99 DGAMMA= .03
BETA = 88.874 DBETA = .008
ALPHA= 90.92 DALPHA= .01
V= 226.9
6. 45-1226
Ni{BiF6}2
Triklin
Dexp Dcal d(D) h k l
4.6704 4.6711 -.0007 0 1 1
4.2103 4.2143 -.0039 0 -1 1
3.7503 3.7517 -.0014 -1 1 1
3.6803 3.6823 -.0020 1 -1 1
2.7702 2.7695 .0007 -1 1 2
2.7402 2.7397 .0004 2 0 0
2.5502 2.5477 .0025 0 -2 1
2.3872 2.3886 -.0014 -1 -1 2
2.3572 2.3530 .0042 1 2 0
2.2522 2.2520 .0002 0 1 3
2.2412 2.2440 -.0028 2 0 2
2.1892 2.1890 .0001 -2 2 0
A= 5.5866 DA= .0009
B= 5.822 DB= .004
C= 7.082 DC= .004
GAMMA=100.40 DGAMMA= .04
BETA = 86.76 DBETA = .01
ALPHA= 84.68 DALPHA= .01
V= 224.9
7. 45-1731
C14H12N2NiO4
Triklin
Dexp Dcal d(D) h k l
12.9900 12.9753 .0147 1 0 0
6.7006 6.6977 .0029 1 1 0
4.4003 4.4005 -.0001 2 1 1
4.0002 3.9997 .0006 2 -1 1
3.7603 3.7595 .0008 3 1 1
3.4002 3.4010 -.0007 0 2 0
3.3002 3.3006 -.0003 -3 0 1
2.7602 2.7601 .0001 -2 2 0
2.3602 2.3600 .0002 -2 -2 2
2.2502 2.2503 -.0001 -5 0 1
2.0901 2.0903 -.0002 3 -1 3
1.8501 1.8501 .0000 3 2 3
A= 13.648 DA= .001
B= 7.0081 DB= .0001
C= 6.8888 DC= .0009
GAMMA= 77.732 DGAMMA= .002
BETA = 77.80 DBETA = .04
ALPHA= 93.76 DALPHA= .02
V= 625.07
8. 45-1792
C8H24Cl2N4Ni
Triklin
Dexp Dcal d(D) h k l
7.6104 7.6047 .0058 -1 1 1
6.5003 6.4928 .0075 0 -1 1
6.1004 6.0953 .0051 1 -1 1
5.9702 5.9767 -.0064 0 0 2
5.3303 5.3290 .0013 -1 2 1
4.1504 4.1564 -.0060 0 1 3
3.9903 3.9922 -.0019 2 0 1
3.9104 3.9126 -.0022 -2 0 1
3.8602 3.8598 .0004 -2 1 2
3.7602 3.7618 -.0015 -1 2 3
3.6203 3.6240 -.0037 -1 -1 2
3.6002 3.6027 -.0025 2 -2 1
A= 9.241 DA= .004
B= 10.919 DB= .003
C= 12.635 DC= .004
GAMMA=114.95 DGAMMA= .02
BETA = 96.23 DBETA = .05
ALPHA= 71.18 DALPHA= .01
V= 1093.6
9. 45-1794
C32H12N12NiO8
Triklin
Dexp Dcal d(D) h k l
14.4920 14.5660 -.0740 0 1 0
13.8111 13.7993 .0119 1 0 0
10.2811 10.2727 .0084 1 1 0
9.9409 9.9563 -.0154 1 0 1
6.4606 6.4796 -.0189 -1 -1 1
5.1904 5.1899 .0005 1 1 2
5.0204 5.0185 .0019 1 -1 2
4.6203 4.6204 -.0001 2 -1 2
4.5103 4.5113 -.0009 -1 3 0
4.0202 4.0201 .0002 -1 3 1
3.5903 3.5907 -.0004 4 1 1
3.3902 3.3897 .0005 -3 -2 1
3.0602 3.0601 .0001 -4 2 0
2.9802 2.9801 .0001 -2 -4 1
A= 14.6153 DA= .0004
B= 14.601 DB= .001
C= 10.922 DC= .002
GAMMA= 86.44 DGAMMA= .01
BETA = 70.97 DBETA = .01
ALPHA= 87.21 DALPHA= .01
V=2198.4
10. 45-1810
C12H26F6N6NiO4
Triklin
Dexp Dcal d(D) h k l
8.4906 8.5073 -.0167 0 0 1
7.3005 7.3249 -.0244 0 1 1
6.9006 6.9011 -.0005 0 -1 1
6.4034 6.3825 .0209 -1 -1 1
6.4503 6.4547 -.0044 0 2 0
6.4103 6.3825 .0278 -1 -1 1
5.8204 5.8383 -.0179 -1 1 1
5.3704 5.3708 -.0004 1 0 1
5.2705 5.2768 -.0063 1 1 1
5.0004 4.9889 .0115 0 -2 1
4.5203 4.5101 .0102 1 2 1
4.2204 4.2229 -.0026 -2 -1 1
A= 8.8787 DA= .0002
B= 13.164 DB= .001
C= 8.780 DC= .001
GAMMA= 79.333 DGAMMA= .003
BETA =103.851 DBETA = .002
ALPHA= 89.004 DALPHA= .005
V=977.2
11. 45-1811
C12H26F6N6NiO4
Triklin
Dexp Dcal d(D) h k l
8.4204 8.3870 .0334 0 1 1
7.1807 7.1823 -.0016 0 -1 1
5.7505 5.7541 -.0036 1 1 0
5.5303 5.5382 -.0079 1 0 1
5.4303 5.4306 -.0004 1 1 1
4.8203 4.8097 .0106 1 2 1
4.4803 4.4716 .0087 0 1 2
4.1903 4.1935 -.0032 0 2 2
4.0703 4.0707 -.0004 0 -1 2
3.9503 3.9490 .0014 0 4 0
3.6703 3.6690 .0013 -1 3 1
3.5902 3.5911 -.0009 0 -2 2
A= 6.269 DA= .005
B= 16.072 DB= .002
C= 9.140 DC= .004
GAMMA= 87.77 DGAMMA= .01
BETA = 79.564 DBETA = .007
ALPHA= 79.38 DALPHA= .03
V= 890.1
12. 46-0926
Zn0.7Mn0.04Ni7Fe3.2B3.6O17.94
Triklin
Dexp Dcal d(D) h k l
5.0765 5.0770 -.0006 0 1 1
4.5844 4.5856 -.0012 1 1 1
3.7063 3.7038 .0025 2 -1 1
3.3322 3.3295 .0028 1 1 2
3.0372 3.0374 -.0002 -1 1 2
2.9602 2.9592 .0010 -1 2 0
2.7662 2.7671 -.0010 1 2 1
2.6792 2.6788 .0004 1 2 0
2.5532 2.5539 -.0007 3 1 2
2.5102 2.5119 -.0017 2 -2 1
2.4492 2.4501 -.0009 -4 1 0
2.3362 2.3366 -.0005 0 0 3
A= 10.3856 DA= .0001
B= 6.0565 DB= .0001
C= 7.3963 DC= .0001
GAMMA= 97.584 DGAMMA= .003
BETA = 76.299 DBETA = .001
ALPHA= 79.610 DALPHA= .003
V=437.2
13. 46-1546
C32H12N12NiO8
Rombik
Grupa 17
Dexp. Dcal. d(D) h k l
10.5305 10.4560 .0745 0 0 1
7.5008 7.5870 -.0862 0 1 0
6.2405 6.2314 .0091 1 0 1
4.8003 4.8154 -.0151 1 1 1
3.4102 3.4081 .0021 1 2 0
3.2402 3.2403 -.0001 1 2 1
a= 7.760 b= 7.5870 c=10.456
da= .001 db= .0003 dc= .001
V= 615.6
14. 46-1581
C24H28N6NiO6
Rombik
Groupa 17
Dexp. Dcal. d(D) h k l
11.0411 11.0020 .0391 0 1 0
7.1403 7.1045 .0357 0 0 1
6.1305 6.1715 -.0410 1 1 0
5.9003 5.9683 -.0680 0 1 1
5.1503 5.1431 .0073 1 0 1
3.6703 3.6673 .0030 0 3 0
3.3002 3.3007 -.0005 2 0 1
2.5802 2.5805 -.0003 1 4 0
2.3302 2.3296 .0006 2 2 2
a= 7.45 b=11.002 c= 7.105
da= .02 db= .008 dc= .005
V= 583
15. 6-1582
C24H28N6NiO6
Triklin
Dexp Dcal d(D) h k l
11.4805 11.4820 -.0015 0 0 1
9.1403 9.1608 -.0206 1 0 0
7.6303 7.6087 .0215 0 1 0
7.0107 7.0045 .0062 -1 0 1
6.6006 6.5907 .0100 0 -1 1
5.5303 5.5335 -.0032 -1 1 0
3.7303 3.7300 .0003 -2 1 0
3.5903 3.5912 -.0009 1 0 3
3.4703 3.4698 .0004 -2 1 1
3.1802 3.1810 -.0008 -1 -2 2
3.0602 3.0603 .0000 0 2 2
2.7602 2.7598 .0004 0 -1 4
2.2702 2.2701 .0001 4 1 0
A= 9.235 DA= .002
B= 7.687 DB= .005
C= 11.53 DC= .02
GAMMA= 83.25 DGAMMA= .01
BETA = 87.89 DBETA = .05
ALPHA= 94.322 DALPHA= .009
V= 809.4
16. 46-1583
C24H28N6NiO6
Monoklin
Grupa 14
Dexp Dcal d(D) h k l
11.4213 11.3610 .0603 1 0 0
7.5905 7.5937 -.0032 1 1 1
6.7305 6.7142 .0163 0 0 2
6.0403 6.0309 .0093 0 2 1
5.2205 5.2214 -.0009 -1 2 1
4.1202 4.1195 .0007 -2 0 2
3.7303 3.7304 -.0001 0 2 3
3.4703 3.4702 .0001 2 3 1
3.3203 3.3200 .0002 1 0 4
a= 11.430 b= 13.500 c= 13.510 beta= 83.693
da= .001 db=.001 dc=.001 dbet=.004
V= 2072
17. 46-1584
C22H22Cl2N6NiO6
Monoklin
Grupa 4,11
Dexp Dcal d(D) h k l
14.3301 14.6198 -.2897 1 0 0
11.5209 11.5361 -.0152 0 0 1
8.3003 8.3013 -.0010 1 1 0
3.6803 3.6804 -.0001 -4 0 1
3.4302 3.4303 -.0001 3 0 2
3.3602 3.3605 -.0003 1 1 3
3.2002 3.2000 .0002 -4 1 2
a= 14.863000 b= 10.0847 c= 11.7280 beta=100.374
da=.0008 db=.0004 dc=.0003 dbet=.001
V= 1729
18. 46-1585
C22H22Cl2N6NiO6
Monoklin
Grupa 4,11
Dexp Dcal d(D) h k l
14.3301 14.3394 -.0093 0 0 1
11.5209 11.5531 -.0323 1 0 1
8.1704 8.1685 .0019 1 1 0
5.7805 5.7766 .0039 2 0 2
5.4204 5.4189 .0016 -2 0 1
4.1302 4.1315 -.0012 2 2 1
3.6303 3.6303 .0000 2 0 4
3.4302 3.4291 .0011 2 2 3
3.3602 3.3585 .0017 3 2 0
3.1903 3.1898 .0004 4 0 3
a= 13.810 b= 10.400 c= 15.005 beta= 72.862
da=.001 db=.001 dc=.0004 dbet=.006
V= 2059
19. 46-1586
C20H20N6NiO6
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
11.0411 10.8900 .1511 0 1 0
10.2007 10.1416 .0591 1 0 0
7.1806 7.1788 .0019 0 1 1
5.4303 5.4450 -.0147 0 2 0
4.9705 4.9562 .0143 2 0 1
4.5902 4.5969 -.0066 2 1 0
3.6603 3.6652 -.0049 2 2 1
3.3802 3.3805 -.0003 3 0 0
3.3002 3.2967 .0035 1 3 1
3.1903 3.1911 -.0008 2 2 2
2.9502 2.9516 -.0014 2 3 0
a= 10.400 b= 10.890 c= 9.790 beta=77.192
da=.001 db=.001 dc=.001 dbet=.007
V= 1081
20. 46-1587
C20H20N6NiO6
Triklin
Dexp Dcal d(D) h k l
10.2007 10.1933 .0074 1 0 0
7.1806 7.1731 .0076 0 1 1
5.4204 5.4136 .0069 0 -1 1
4.9705 4.9659 .0046 -2 1 0
4.5902 4.5935 -.0033 0 2 0
4.2003 4.2015 -.0012 2 -1 1
3.9203 3.9154 .0049 1 1 2
3.6303 3.6389 -.0085 -1 0 2
3.3602 3.3598 .0004 -2 -1 1
3.2802 3.2822 -.0020 2 1 2
3.1703 3.1699 .0003 -1 -2 1
3.0302 3.0289 .0013 -2 2 2
A= 10.498 DA= .001
B= 9.762 DB= .001
C= 8.536 DC= .005
GAMMA=101.74 DGAMMA= .02
BETA = 85.99 DBETA = .02
ALPHA= 75.20795 DALPHA= .00002
V= 821.2
21. 46-1588
C20H20N6NiO6
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
10.2007 10.2253 -.0246 0 0 1
7.5905 7.6090 -.0185 1 1 0
6.6405 6.6534 -.0129 -1 1 1
5.6605 5.6721 -.0116 1 1 1
5.2205 5.2150 .0055 1 2 0
4.9705 4.9668 .0037 -1 0 2
4.8403 4.8173 .0230 2 0 0
4.7504 4.7585 -.0081 -2 0 1
4.1302 4.1348 -.0046 0 3 0
3.6603 3.6617 -.0014 -1 3 1
3.4102 3.4084 .0018 0 0 3
3.3203 3.3221 -.0018 -1 1 3
2.9502 2.9519 -.0017 1 4 0
2.6002 2.5981 .0021 -2 4 1
a= 9.85 b= 12.404 c= 10.457 beta= 102.07
da=.05 db=.007 dc=.001 dbeta=.003
V= 1250
Triklin
Dexp Dcal d(D) h k l
10.2007 10.1886 .0121 1 0 0
7.5905 7.5815 .0090 -1 1 0
6.6405 6.6394 .0012 -1 0 1
5.6605 5.6523 .0082 -1 -1 1
5.2205 5.2274 -.0070 1 0 1
4.9705 4.9856 -.0151 -1 1 1
4.8403 4.8298 .0106 0 1 1
4.7504 4.7335 .0169 -2 0 1
4.1302 4.1323 -.0021 -2 -1 1
3.6603 3.6616 -.0013 -1 -1 2
3.4102 3.4131 -.0029 -3 0 1
3.3203 3.3197 .0006 -2 0 2
2.9502 2.9499 .0004 3 -1 1
2.6002 2.6001 .0001 -4 1 1
A= 10.688 DA= .004
B= 9.3157 DB= .0009
C= 7.559 DC= .003
GAMMA=100.06 DGAMMA= .08
BETA =101.14 DBETA = .01
ALPHA=104.98 DALPHA= .04
V= 693.1
22. 46-1650
C16H20N6NiO4S2
Triklin
Dexp Dcal d(D) h k l
17.3012 17.2798 .0214 0 0 1
7.9005 7.8816 .0190 1 0 0
6.8104 6.8120 -.0016 0 1 1
6.2383 6.2389 -.0006 0 -1 1
5.8843 5.8780 .0063 1 -1 1
4.9123 4.9055 .0068 1 -1 2
4.7343 4.7270 .0074 -1 0 3
4.4144 4.4072 .0073 1 1 1
4.1503 4.1530 -.0027 -2 1 0
3.7663 3.7662 .0001 -1 2 0
3.5393 3.5406 -.0014 2 0 2
3.4363 3.4385 -.0022 -1 -1 3 1
A= 8.513 DA= .007
B= 7.643 DB= .004
C= 17.48 DC= .01
GAMMA=112.14 DGAMMA= .01
BETA = 94.992 DBETA = .004
ALPHA= 81.46 DALPHA= .04
V= 1041.4
23. 46-1651
C6H18N6NiO6S2
Triklin
Dexp Dcal d(D) h k l
7.4504 7.4547 -.0043 1 0 0
6.2014 6.2144 -.0130 1 1 0
5.0554 5.0594 -.0040 -1 -1 1
4.8213 4.8248 -.0035 1 0 1
4.5004 4.5083 -.0080 0 1 1
3.6743 3.6783 -.0040 -1 1 1
3.0442 3.0464 -.0022 2 1 1
2.9362 2.9401 -.0039 1 0 2
2.7082 2.7088 -.0006 0 -3 1
2.6492 2.6460 .0031 1 1 2
2.5922 2.5918 .0004 2 2 1
2.4862 2.4849 .0013 3 0 0
A= 7.6942 DA= .0005
B= 8.5019 DB= .0004
C= 6.7074 DC= .0003
GAMMA= 75.747 DGAMMA= .005
BETA = 95.110 DBETA = .005
ALPHA=105.185 DALPHA= .007
V=410.0
24. 46-1711
C18H22Cl2N6NiO6*H2O
Rombik
Groupa 54
Dexp. Dcal. d(D) h k l
3.4602 3.4589 .0013 1 0 2
3.3403 3.3378 .0025 1 1 1
3.2702 3.2785 -.0083 2 0 0
2.9902 2.9915 -.0013 0 1 2
2.6302 2.6311 -.0009 2 1 0
a= 6.557 b= 4.410 c= 8.143
da= .001 db= .001 dc= .001
V= 235.5
25. 46-1713
C28H32Cl2N8Ni*2H2O
Triklin
Dexp Dcal d(D) h k l
7.1503 7.1559 -.0056 -1 1 0
6.9204 6.9231 -.0027 0 1 1
6.7105 6.7161 -.0056 1 0 1
6.3904 6.3996 -.0092 0 -1 1
4.8204 4.8275 -.0072 0 0 2
4.4303 4.4338 -.0035 1 0 2
4.2804 4.2707 .0097 0 2 1
3.9303 3.9282 .0021 -1 0 2
3.7003 3.7033 -.0030 -2 1 1
3.3802 3.3790 .0012 -1 -1 2
3.2902 3.2923 -.0021 -2 2 1
3.1602 3.1589 .0013 -1 3 0
A= 8.5741 DA= .001
B= 9.536 DB= .003
C= 9.757 DC= .008
GAMMA=105.47 DGAMMA= .01
BETA = 83.048 DBETA = .006
ALPHA= 87.55 DALPHA= .03
V= 760.8
26. 47-0770
K6NiSiW11O39*14H2O
Triklin
Dexp Dcal d(D) h k l
10.0252 10.0388 -.0136 0 0 1
9.3494 9.3308 .0186 1 0 0
6.2196 6.2177 .0019 0 -2 1
5.6803 5.6839 -.0036 0 2 0
5.2835 5.2877 -.0042 1 -2 1
5.0334 5.0194 .0140 0 0 2
4.6662 4.6654 .0008 2 0 0
4.5024 4.4979 .0045 -2 0 1
4.4534 4.4508 .0026 -1 -2 2
4.2343 4.2301 .0042 0 2 1
3.9173 3.9198 -.0025 -1 1 2
3.7703 3.7717 -.0014 -2 -1 2
A= 9.4621 DA= .0008
B= 12.6107 DB= .0008
C= 11.1733 DC= .0008
GAMMA= 94.0433 DGAMMA= .0008
BETA = 96.167 DBETA = .01
ALPHA=114.6612 DALPHA= .0001
V=1195.2
27. 47-0771
K6NiSiW11O39
Triklin
Dexp Dcal d(D) h k l
6.3604 6.3613 -.0008 1 0 0
5.9404 5.9427 -.0024 0 1 1
3.8053 3.8011 .0042 0 -1 1
3.6305 3.6309 -.0004 -2 1 0
3.1622 3.1600 .0023 0 2 0
3.1143 3.1170 -.0027 -2 2 0
2.9723 2.9714 .0009 0 2 2
2.5802 2.5795 .0007 -2 1 2
2.3702 2.3703 -.0001 1 -3 0
2.1111 2.1109 .0003 -2 2 3
1.9852 1.9858 -.0007 -1 0 3
1.8261 1.8260 .0001 0 -1 3
A= 7.31854 DA= .00005
B= 7.965 DB= .001
C= 7.206 DC= .002
GAMMA=119.073 DGAMMA= .008
BETA = 97.019 DBETA = .009
ALPHA= 64.97 DALPHA= .01
V= 330.8
28. 47-1335
Ni6Sb2S
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
4.5004 4.5005 -.0002 -2 1 1
3.1002 3.1000 .0002 3 1 1
2.9502 2.9500 .0002 0 1 3
2.6702 2.6701 .0001 -3 0 3
2.6502 2.6506 -.0003 -1 3 1
1.8401 1.8402 -.0000 -6 1 2
1.8101 1.8102 -.0000 -5 0 4
1.7001 1.7001 .0000 -4 4 1
1.6801 1.6801 -.0000 4 0 4
1.6301 1.6301 .0000 -6 0 4
a= 11.6089 b= 8.4264 c= 9.600 beta= 100.185
da=.007 db=.003 dc=.001 dbet=.007
V= 924.2
29. 47-1915
C20H16N6NiO6
Triklin
Dexp Dcal d(D) h k l
9.8942 9.9270 -.0328 1 0 0
9.6549 9.6793 -.0244 1 1 0
6.0436 6.0437 -.0001 0 2 0
5.2013 5.2039 -.0026 1 -1 1
4.9782 4.9758 .0024 0 1 1
4.8393 4.8397 -.0004 2 2 0
4.5813 4.5768 .0045 -1 -2 1
4.3542 4.3580 -.0038 2 0 1
3.8952 3.8922 .0030 2 -1 1
3.7603 3.7623 -.0020 0 -3 1
3.5162 3.5181 -.0019 3 2 0
3.3203 3.3204 -.0001 -1 3 0
A= 10.8698 DA= .0007
B= 13.215 DB= .006
C= 6.2778 DC= .0001
GAMMA= 69.799 DGAMMA= .007
BETA = 80.73 DBETA = .02
ALPHA= 98.71 DALPHA= .04
V=814.3
30. 47-2001
C26H22CuN7NiO8
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
13.0015 13.0318 -.0303 0 1 0
9.0011 9.0025 -.0014 1 1 0
8.0009 8.0003 .0006 1 0 1
4.8003 4.7992 .0011 -1 2 2
4.1003 4.1015 -.0012 1 3 0
3.9003 3.9005 -.0002 1 0 3
3.5003 3.5005 -.0002 3 2 0
3.3002 3.2996 .0006 2 3 1
2.1002 2.1004 -.0003 -2 5 4
a= 13.200 b= 13.03 c=14.571 beta= 109.38
da=.004 db=.01 dc=.006 dbeta=.04
V= 2364
31. 47-2063
C44H58Cl2N6NiO2
Triklin
Dexp Dcal d(D) h k l
11.2055 11.1912 .0143 1 0 0
6.1025 6.0980 .0045 -1 -1 1
5.8026 5.8040 -.0015 -1 0 1
5.0021 5.0022 -.0002 -2 -1 1
4.6021 4.6020 .0001 0 1 1
4.3019 4.3034 -.0015 1 1 1
3.9017 3.9015 .0003 3 1 0
3.5015 3.5015 .0000 -2 1 1
3.3014 3.3001 .0013 0 2 1
3.2014 3.2021 -.0008 1 3 0
3.1014 3.1015 -.0001 -2 2 0
3.0013 3.0011 .0002 -3 -3 1
A= 12.1942 DA= .0002
B= 10.131 DB= .001
C= 6.5600 DC= .0002
GAMMA= 68.5485 DGAMMA= .0001
BETA =105.209 DBETA = .008
ALPHA=108.401 DALPHA= .009
V= 705.8
32. 47-2070
C34H28Cl4N10NiS2
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
6.1830 6.1628 .0202 0 0 1
5.1557 5.1548 .0009 1 0 1
4.3811 4.3889 -.0078 1 1 1
4.1856 4.1843 .0013 0 2 0
4.0998 4.0996 .0002 2 1 0
a= 9.4051 b= 8.369 c= 6.16
da= .0009 db= .002 dc= .01
V= 485.1
33. 47-2159
C28H18N2NiO2
Triklin
Dexp Dcal d(D) h k l
12.4404 12.4263 .0141 0 1 0
10.6112 10.6422 -.0310 1 0 0
7.8809 7.8769 .0040 -1 1 0
6.2105 6.2131 -.0027 0 2 0
5.6106 5.6201 -.0094 0 -1 1
5.3305 5.3211 .0094 2 0 0
4.8903 4.8910 -.0007 -1 0 1
4.3004 4.3019 -.0015 2 -1 1
4.1403 4.1421 -.0018 0 3 0
3.7903 3.7919 -.0016 -1 3 0
3.4843 3.4824 .0019 0 -3 1
3.3723 3.3739 -.0016 3 1 1
3.1872 3.1867 .0005 -2 3 0
2.4882 2.4853 .0029 0 5 0
A= 10.982 DA= .002
B= 12.4445 DB= .0004
C= 6.430 DC= .001
GAMMA= 87.12 DGAMMA= .02
BETA = 76.05 DBETA = .05
ALPHA= 90.40 DALPHA= .01
V=850.5
34. 47-2239
C10H8NiO6*30H2O
Triklin
Dexp Dcal d(D) h k l
12.8003 12.7855 .0148 1 0 0
11.7005 11.7039 -.0034 1 1 0
6.6006 6.5966 .0040 0 1 1
6.4002 6.4007 -.0004 1 0 1
6.2005 6.2002 .0003 1 1 1
5.7003 5.6913 .0089 -2 -1 1
5.3004 5.3010 -.0006 -2 0 1
4.8003 4.8013 -.0010 0 2 1
4.7003 4.6991 .0012 3 1 0
4.5004 4.4892 .0112 1 3 0
4.4003 4.4046 -.0043 2 3 0
4.2003 4.1989 .0014 -3 -2 1
A= 14.3032 DA= .0003
B= 13.611 DB= .009
C= 8.016 DC= .001
GAMMA= 64.23 DGAMMA= .02
BETA = 98.28 DBETA = .04
ALPHA= 94.64 DALPHA= .04
V= 1390.3
35. 47-2243
C10H8NiO6*16H2O
Triklin
Dexp Dcal d(D) h k l
17.7029 17.7204 -.0175 0 1 0
11.8003 11.7314 .0689 0 0 1
8.6004 8.6138 -.0134 1 1 0
7.2004 7.2000 .0004 0 -2 1
6.1003 6.1003 -.0001 -1 1 1
5.7003 5.7076 -.0073 -1 -2 1
5.3004 5.3018 -.0014 1 0 2
5.2004 5.1988 .0016 0 3 1
4.8003 4.8095 -.0092 0 2 2
4.7003 4.7056 -.0053 -1 3 0
4.5004 4.5032 -.0028 2 0 1
4.4003 4.3983 .0021 -1 1 2
A= 9.355 DA= .003
B= 17.867 DB= .001
C= 11.857 DC= .002
GAMMA= 82.98 DGAMMA= .04
BETA = 81.94 DBETA = .03
ALPHA= 91.11 DALPHA= .02
V=1944
36. 47-2247
C10H8NiO6*24H2O
Triklin
Dexp Dcal d(D) h k l
11.7005 11.6893 .0112 1 0 0
5.7003 5.7014 -.0011 1 1 1
5.2004 5.2097 -.0093 -1 -1 1
5.1004 5.0973 .0030 1 0 2
4.9002 4.9043 -.0040 2 1 0
4.6004 4.5959 .0044 2 -1 1
4.3002 4.3000 .0002 -2 0 1
4.2003 4.2017 -.0014 3 0 1
4.0002 3.9962 .0040 -2 -1 1
3.9003 3.9010 -.0007 -1 0 2
3.7002 3.6984 .0018 0 2 0
3.4002 3.4020 -.0018 -1 2 0
A= 12.6625 DA= .0001
B= 7.4899 DB= .0001
C= 10.2413 DC= .0004
GAMMA= 85.031 DGAMMA= .004
BETA = 68.58630 DBETA = .00001
ALPHA= 95.194 DALPHA= .004
V=893.5
37. 47-2275
C8H3NNiO6*H2O
Rombik
Groupa 32,55
Dexp. Dcal. d(D) h k l
9.8306 9.8500 -.0194 0 0 1
6.1103 6.1197 -.0094 1 1 0
5.7903 5.7889 .0013 0 2 1
4.9002 4.9176 -.0174 1 2 0
3.9003 3.8993 .0010 1 3 0
3.4803 3.4799 .0004 1 2 2
a= 6.770 b=14.310 c= 9.850
da= .001 db= .001 dc= .001
V= 954.3
38. 47-2387
C48H64Cl2N12NiO8
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
13.7042 13.6168 .0874 0 1 0
9.5406 9.5238 .0168 1 1 0
6.8208 6.8084 .0124 0 2 0
6.6724 6.6627 .0097 2 0 0
6.2200 6.2140 .0060 -1 0 1
6.0592 6.0629 -.0037 1 2 0
5.9899 5.9847 .0052 2 1 0
5.4952 5.4886 .0066 1 0 1
5.0882 5.0907 -.0025 1 1 1
4.7630 4.7619 .0011 2 2 0
4.5455 4.5389 .0066 0 3 0
4.2932 4.2965 -.0033 1 3 0
4.2206 4.2228 -.0022 3 1 0
4.1125 4.1123 .0001 2 1 1
3.7127 3.7151 -.0024 0 3 1
a= 13.493 b= 13.617 c= 6.548 beta= 99.04
da= .009 db=.008 dc=.009 dbet=.09
V= 1188
39. 47-2457
C10H12Li2N2NiO8*4Al{OH}3*4H2O
Triklin
Dexp Dcal d(D) h k l
14.7309 14.7015 .0294 1 0 0
8.4610 8.4589 .0020 0 1 0
7.6904 7.6787 .0117 0 0 1
7.3603 7.3626 -.0023 0 -1 1
6.6405 6.6366 .0039 -1 1 0
5.0402 5.0531 -.0128 -2 0 1
4.9104 4.9111 -.0006 2 -1 1
4.3703 4.3716 -.0013 1 2 0
4.3002 4.3033 -.0031 -1 1 1
3.8602 3.8572 .0030 3 1 1
3.6803 3.6803 .0000 -2 1 1
3.1703 3.1711 -.0008 -1 -3 1
A= 15.204 DA= .002
B= 9.518 DB= .002
C= 8.401 DC= .004
GAMMA= 76.472 DGAMMA= .004
BETA = 89.95 DBETA = .03
ALPHA=113.22 DALPHA= .04
V= 1080.4