1. 29-0555
{NI,Fe,Cu}0.75Ir
TRIKLIN
Dexp Dcal d(D) h k l
5.8806 5.8880 -.0074 0 1 1
5.7003 5.7021 -.0018 0 -1 1
3.9703 3.9721 -.0018 -1 0 1
3.5202 3.5238 -.0035 1 1 0
3.3303 3.3315 -.0012 -1 1 0
3.1903 3.1916 -.0013 -1 -1 2
2.9822 2.9828 -.0006 1 -1 3
2.8942 2.8936 .0006 -1 1 3
2.7982 2.7972 .0010 0 2 3
2.5912 2.5917 -.0006 1 0 6
2.4742 2.4734 .0007 -1 -2 1
2.3671 2.3680 -.0009 1 -2 1
A= 4.1614 DA= .0001
B= 6.1154 DB= .0002
C= 18.7693 DC= .0003
GAMMA= 86.274 DGAMMA= .003
BETA = 85.0864 DBETA = .0004
ALPHA= 86.589 DALPHA= .003
v=474.1
2. 29-0862
{Mg,Ni,Fe,Al}1212Si6Al2O20{OH}16
Triklin
Dexp Dcal d(D) h k l
7.1208 7.1208 .0000 1 0 0
4.7504 4.7492 .0011 -1 -1 1
4.6054 4.6043 .0011 -1 0 1
3.5563 3.5535 .0028 2 1 0
2.8342 2.8315 .0027 2 2 0
2.6582 2.6580 .0002 1 -2 1
2.5792 2.5761 .0030 -1 -2 2
2.5481 2.5473 .0008 1 2 1
2.3932 2.3949 -.0017 -1 -3 1
2.2652 2.2648 .0004 -2 -3 1
2.0271 2.0268 .0004 -3 -2 2
2.0082 2.0082 -.0001 0 -3 2
A= 7.510 DA= .003
B= 7.233 DB= .004
C= 5.8446 DC= .0007
GAMMA= 72.38 DGAMMA= .04
BETA =100.547 DBETA = .008
ALPHA=107.600 DALPHA= .004
V= 286.9
3. 30-0864
c4H4NiO4S*3H2O
Triklin
Dexp Dcal d(D) h k l
7.1208 7.1271 -.0063 1 0 0
4.7504 4.7457 .0047 0 1 1
4.6054 4.6041 .0013 0 -1 1
3.5563 3.5581 -.0017 1 -1 1
2.8342 2.8353 -.0011 2 1 1
2.6582 2.6574 .0007 -2 1 2
2.5792 2.5805 -.0013 2 -1 1
2.5481 2.5491 -.0009 -1 -2 1
2.3932 2.3929 .0003 -1 0 4
2.2652 2.2641 .0011 -2 -2 1
2.0271 2.0274 -.0003 -1 2 3
2.0082 2.0086 -.0004 0 -2 3
A= 7.33674 DA= .00004
B= 5.4165 DB= .0001
C= 9.6401 DC= .0001
GAMMA= 83.95956 DGAMMA= .00009
BETA =102.2144 DBETA = .0005
ALPHA= 89.3252 DALPHA= .0008
V=372.1
4. 30-0958
KNiHP2O7*2H2O
Triklin
Dexp Dcal d(D) h k l
7.6303 7.6246 .0057 0 1 1
4.9603 4.9496 .0107 0 -1 1
4.7303 4.7395 -.0092 -1 1 0
3.8403 3.8429 -.0026 -1 1 2
3.4503 3.4503 -.0000 -1 2 0
3.2902 3.2900 .0002 1 0 2
3.2402 3.2426 -.0023 0 1 3
3.0402 3.0339 .0063 0 2 3
2.9202 2.9188 .0014 -1 1 3
2.7802 2.7801 .0001 1 2 2
2.7302 2.7328 -.0026 -1 -1 2
2.6102 2.6093 .0009 0 3 0
A= 5.299 DA= .003
B= 8.820 DB= .001
C= 9.828 DC= .003
GAMMA=103.31 DGAMMA= .03
BETA = 97.94 DBETA = .02
ALPHA= 64.714 DALPHA= .004
V=403.9
5. 30-0959
K2Ni{H2P2O7}2*2H2O
Triklin
Dexp Dcal d(D) h k l
7.1604 7.1570 .0034 1 0 0
6.5655 6.5655 .0001 0 1 1
5.4506 5.4424 .0081 0 -1 1
5.0103 5.0201 -.0098 0 0 2
4.8104 4.8160 -.0056 -1 1 0
4.2403 4.2471 -.0068 -1 -1 1
3.6103 3.6072 .0031 2 1 1
3.5703 3.5785 -.0082 2 0 0
3.3902 3.3912 -.0010 2 1 2
3.2502 3.2492 .0010 0 -2 1
3.2002 3.1998 .0004 -1 -1 2
3.0502 3.0494 .0008 2 -1 1
A= 7.550 DA= .005
B= 7.626 DB= .003
C= 10.702 DC= .004
GAMMA= 78.91 DGAMMA= .03
BETA = 73.02 DBETA = .01
ALPHA= 76.19 DALPHA= .04
V= 567.2
6. 30-1227
C4H4Na2NiO4S
Triklin
Dexp Dcal d(D) h k l
7.7807 7.7785 .0022 0 1 1
6.4304 6.4273 .0031 0 -1 1
5.5905 5.5902 .0003 -1 1 0
4.4503 4.4493 .0010 -1 2 0
3.9503 3.9490 .0012 0 -1 2
3.4102 3.4157 -.0055 -1 3 0
3.1902 3.1917 -.0015 1 1 2
2.8902 2.8913 -.0010 -2 2 1
2.8002 2.8028 -.0026 -1 -2 2
2.6202 2.6199 .0003 -1 -1 3
2.5202 2.5199 .0003 1 0 3
2.3902 2.3902 -.0000 -2 2 3
A= 6.0231 DA= .0003
B= 11.507 DB= .001
C= 9.513 DC= .001
GAMMA=104.196 DGAMMA= .005
BETA =102.408 DBETA = .003
ALPHA= 76.465 DALPHA= .006
V= 612.73
7. 30-1742
C2H12Cl14N6Ni*6H2O
Triklin
Dexp Dcal d(D) h k l
6.2305 6.2472 -.0166 1 1 0
5.2803 5.2998 -.0195 0 1 1
4.4503 4.4474 .0030 1 0 1
3.7002 3.7059 -.0057 0 0 2
3.5703 3.5718 -.0015 1 2 0
3.3003 3.2978 .0025 1 2 1
3.1002 3.1000 .0003 1 -1 1
2.9502 2.9463 .0039 1 0 2
2.8002 2.7998 .0004 2 0 1
2.6502 2.6544 -.0043 1 2 2
2.5302 2.5313 -.0011 -1 0 3
2.4702 2.4706 -.0004 0 0 3
A= 7.666 DA= .001
B= 7.16 DB= .01
C= 7.671 DC= .001
GAMMA= 64.34 DGAMMA= .02
BETA =101.19 DBETA = .02
ALPHA= 86.06 DALPHA= .04
V=366.6
8. 30-1826
C24H16Cl2N4NiO2*2H2O
Triklin
Dexp Dcal d(D) h k l
10.2007 10.2164 -.0157 0 1 1
8.6607 8.6938 -.0331 0 -1 1
6.4606 6.4477 .0129 1 0 0
5.8606 5.8729 -.0123 -1 1 0
5.6805 5.6747 .0058 1 0 1
5.1802 5.1907 -.0105 1 1 1
4.9203 4.9205 -.0003 -1 1 2
4.4102 4.4044 .0058 -1 -1 2
4.2504 4.2479 .0024 -1 2 2
4.1702 4.1736 -.0034 1 -2 1
4.0002 4.0020 -.0018 -1 1 3
3.8003 3.7976 .0027 1 2 2
A= 6.49341 DA= .00002
B= 12.68946 DB= .00005
C= 14.41545 DC= .00001
GAMMA= 94.32972 DGAMMA= .00001
BETA = 95.89892 DBETA = .00004
ALPHA= 80.3529 DALPHA= .0002
V=1162
9. 30-1827
C22H18N8Ni
Triklin
Dexp Dcal d(D) h k l
8.3802 8.3784 .0018 0 1 1
5.9903 5.9994 -.0091 0 -1 1
5.2704 5.2700 .0003 1 0 0
4.5004 4.5025 -.0022 1 1 1
4.2803 4.2822 -.0018 -1 0 2
4.0202 4.0199 .0003 0 -1 2
3.8302 3.8238 .0065 1 2 1
3.5603 3.5614 -.0011 1 1 2
2.7302 2.7304 -.0002 -2 -1 1
2.5602 2.5596 .0006 -1 3 1
2.3902 2.3902 -.0000 -1 -1 4
2.1502 2.1503 -.0001 2 0 2
A= 5.5218 DA= .0007
B= 9.839 DB= .003
C= 11.2728 DC= .0009
GAMMA= 80.06 DGAMMA= .02
BETA =100.66 DBETA = .01
ALPHA= 73.584 DALPHA= .009
V= 560.7
10 30-1830
C12H30Br2N2NiO2
Geksag. singonij
Grupa 143
Dexp. Dcal. d(D) h k l
8.6104 8.5835 .0269 1 0 1
6.4206 6.4135 .0071 1 1 1
4.5203 4.5211 -.0008 1 1 2
3.6803 3.6802 .0000 0 0 3
3.5102 3.5107 -.0005 3 0 2
a= 15.75838 c= 11.04074
da= .022531 dc= .000491
V= 2374
11. 30-1833
C24H60Cl2N4NiO12
Rombik
Groupa 26,28,51
Dexp. Dcal. d(D) h k l
8.8202 8.7750 .0452 2 0 0
7.8907 7.8730 .0177 0 1 0
4.4603 4.4587 .0016 1 0 1
3.8403 3.8411 -.0007 1 2 0
3.6203 3.6208 -.0005 3 0 1
3.5102 3.5100 .0002 5 0 0
a=17.550 b= 7.873 c= 4.610
da= .001 db= .004 dc= .001
v= 637.0
12. 30-1834
C12H30Cl2N2NiO2
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
8.3205 8.3098 .0107 1 1 0
7.5905 7.5873 .0033 1 1 1
6.6203 6.6190 .0013 -1 1 1
5.8205 5.8216 -.0011 0 1 2
5.4403 5.4412 -.0010 0 2 1
4.4803 4.4807 -.0003 1 0 3
3.8602 3.8640 -.0038 3 0 0
3.7002 3.6991 .0011 3 0 2
3.5203 3.5185 .0018 -3 0 1
a= 11.8587 b= 11.918 c= 13.650 beta= 77.817
da=.0001 db=.006 dc=.006 dbeta=.01
V= 1886
13. 30-1836
C12H30I2N2NiO2
Rombik
Groupa 33,49,62
Dexp. Dcal. d(D) h k l
7.8205 7.8101 .0104 1 1 0
5.9203 5.8941 .0262 2 1 0
4.4902 4.4976 -.0073 3 1 0
3.8803 3.8900 -.0097 4 0 0
3.6403 3.6381 .0022 0 1 1
3.5403 3.5397 .0005 2 0 1
a=15.560 b= 9.03 c= 3.975
da= .001 db= .01 dc= .001
V= 558.5
14. 30-1837
C36H28I6N4Ni
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
7.6508 7.6343 .0165 1 1 0
6.6703 6.6568 .0135 1 1 1
6.3903 6.3827 .0076 -1 1 1
5.3104 5.3062 .0042 0 1 2
5.1903 5.1756 .0147 -2 0 1
4.1304 4.1341 -.0038 -2 0 2
3.8502 3.8487 .0015 0 1 3
3.7003 3.6999 .0003 2 2 1
3.5202 3.5222 -.0020 2 0 3
3.4402 3.4415 -.0013 -3 1 1
3.3302 3.3284 .0018 2 2 2
3.2202 3.2189 .0013 1 3 0
3.1302 3.1323 -.0021 1 3 1
2.8102 2.8104 -.0002 -2 3 1
a= 11.78 b= 10.041 c= 12.534 beta= 85.8
da=.02 db=.003 dc=.006 dbeta=.1
V= 1479
Triklin
Dexp Dcal d(D) h k l
7.6508 7.6403 .0105 1 0 0
6.6703 6.6669 .0034 -1 1 0
6.3903 6.3849 .0053 0 -1 1
5.3104 5.3093 .0011 -1 0 1
5.1903 5.1923 -.0020 -1 1 1
4.1304 4.1317 -.0013 1 -2 1
3.8502 3.8500 .0002 2 0 1
3.7003 3.6999 .0003 2 -1 1
3.5202 3.5191 .0011 0 3 1
3.4402 3.4402 .0000 2 1 0
3.3302 3.3303 -.0001 2 0 2
3.2202 3.2202 -.0000 2 -2 1
3.1302 3.1308 -.0006 1 3 1
2.8102 2.8102 .0000 2 -2 2
A= 7.8892 DA= .0005
B= 10.841 DB= .003
C= 9.537 DC= .003
GAMMA= 96.11 DGAMMA= .01
BETA = 78.109 DBETA = .004
ALPHA= 81.06 DALPHA= .01
V= 780.3
15. 31-0061
{NH4}2Ni3{P2O7}2*10H2O
Triklin
Dexp Dcal d(D) h k l
8.1203 8.1021 .0182 0 1 1
7.0704 7.0611 .0093 0 -1 1
6.0903 6.0919 -.0016 1 0 0
5.0905 5.0785 .0120 1 1 1
5.0103 5.0015 .0088 1 1 0
4.6904 4.6855 .0049 0 1 2
3.5102 3.5122 -.0020 1 2 2
3.3403 3.3372 .0031 0 3 2
3.2302 3.2300 .0002 2 -1 1
3.1903 3.1914 -.0012 0 0 3
2.9202 2.9203 -.0001 -1 3 2
2.8302 2.8301 .0000 1 -2 3
A= 6.488 DA= .001
B= 12.5709 DB= .0001
C= 10.014 DC= .003
GAMMA=101.78 DGAMMA= .02
BETA = 74.95 DBETA = .04
ALPHA= 85.42 DALPHA= .03
V= 764.4
16. 31-0063
{NH4}4Ni{TeMo6O24}*10H2O
Triklin
Dexp Dcal d(D) h k l
9.0106 9.0032 .0074 0 1 1
8.7804 8.7751 .0053 0 -1 1
8.0904 8.0850 .0054 1 -1 1
7.2904 7.3091 -.0187 -1 0 1
5.8503 5.8509 -.0005 1 0 2
5.7204 5.7200 .0004 0 1 2
5.4003 5.4012 -.0009 -1 2 1
5.1804 5.1773 .0031 2 -1 1
3.7703 3.7696 .0008 2 -3 1
3.6102 3.6112 -.0010 2 -1 3
3.4202 3.4211 -.0008 -3 2 0
3.2602 3.2600 .0002 -1 4 0
A= 10.7369 DA= .0003
B= 13.0456 DB= .0002
C= 12.9144 DC= .0002
GAMMA=107.7004 DGAMMA= .0008
BETA = 80.073 DBETA = .002
ALPHA= 91.6307 DALPHA= .0009
V=1697
17. 31-0371
Cs2Ni3{P2O7}2*10H2O
Triklin
Dexp Dcal d(D) h k l
8.0907 8.1005 -.0099 1 0 0
7.1305 7.1300 .0005 0 1 0
5.7805 5.7826 -.0021 -1 0 1
4.6804 4.6779 .0024 -1 -1 1
4.0403 4.0412 -.0010 0 1 2
3.9402 3.9334 .0068 1 -1 1
3.5703 3.5650 .0053 0 2 0
3.3802 3.3798 .0004 0 -1 2
2.9502 2.9509 -.0007 -1 2 0
2.9302 2.9317 -.0015 -1 2 1
2.8602 2.8599 .0004 2 2 2
2.7602 2.7573 .0030 -2 -1 2
A= 8.54132 DA= .00008
B= 7.6693 DB= .0008
C= 8.7727 DC= .0002
GAMMA= 71.619 DGAMMA= .002
BETA = 84.183 DBETA = .008
ALPHA= 77.22 DALPHA= .01
V=531.5
18. 31-0731
Li2Ni2{MoO4}3
Triklin
Dexp Dcal d(D) h k l
5.1905 5.1928 -.0023 -1 2 0
4.4003 4.3874 .0129 -2 2 0
3.3803 3.3862 -.0060 -3 2 0
3.3403 3.3428 -.0025 -2 3 0
3.3002 3.3010 -.0008 3 0 0
2.9712 2.9723 -.0011 -2 1 1
2.9012 2.9030 -.0018 -2 0 1
2.8102 2.8086 .0016 0 2 1
2.5922 2.5964 -.0042 -2 4 0
2.5582 2.5584 -.0002 -3 1 1
2.5302 2.5300 .0002 1 2 1
2.4572 2.4536 .0036 -3 0 1
A= 10.72 DA= .01
B= 10.466 DB= .007
C= 3.439 DC= .003
GAMMA=112.23 DGAMMA= .05
BETA = 93.88 DBETA = .02
ALPHA= 88.19 DALPHA= .03
V=356.0
19. 31-0734
Li2NiP2O7*4H2O
Triklin
Dexp Dcal d(D) h k l
9.1810 9.1901 -.0091 1 0 0
8.3503 8.3569 -.0066 0 1 0
8.2709 8.2703 .0006 -1 0 1
5.8503 5.8501 .0002 0 0 2
5.5204 5.5192 .0012 1 1 0
4.5603 4.5482 .0122 -2 1 0
3.9603 3.9616 -.0013 2 0 1
3.6003 3.6014 -.0011 0 -2 1
3.2502 3.2499 .0003 2 0 2
3.1002 3.1011 -.0010 -2 1 4
3.0702 3.0692 .0011 0 1 4
2.8802 2.8804 -.0002 0 3 2
A= 10.1470 DA= .0005
B= 9.4010 DB= .0007
C= 13.1171 DC= .0003
GAMMA=110.983 DGAMMA= .008
BETA =110.465 DBETA = .005
ALPHA= 66.8731 DALPHA= .0009
V= 1041.3
20. 31-0894
{Ni{NH3}6}Cl2*0.5H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.8304 5.8205 .0099 0 0 1
3.5603 3.5600 .0003 1 1 0
3.0402 3.0434 -.0032 1 0 1
2.9102 2.9102 -.0001 0 0 2
2.5202 2.5202 -.0000 1 2 0
2.0601 2.0602 -.0000 0 3 0
1.9401 1.9402 -.0000 0 0 3
1.7801 1.7800 .0001 2 2 0
1.7001 1.7002 -.0001 -1 2 3
1.5901 1.5900 .0001 1 0 3
a= 4.607 b= 6.1805 c= 6.157 beta= 109.02
da= .004 db=.0005 dc=.007 dbeta=.09
V= 165.7
21. 31-0895
{Ni{NH3}6{NO3}2
Tetragon
Grupa 75
Dexp. Dcal. d(D) h k l
6.2806 6.2732 .0074 0 0 1
3.8503 3.8431 .0073 1 0 0
3.2902 3.2770 .0132 1 0 1
3.1402 3.1366 .0036 0 0 2
2.7202 2.7175 .0027 1 1 0
2.4301 2.4300 .0002 1 0 2
2.0901 2.0911 -.0009 0 0 3
1.9201 1.9215 -.0014 2 0 0
a= 3.843 c= 6.273
da= .007 dc= .004
v= 95.6
22. 31-0896
Ni{NH3}2SO4
Monoklin
GRUPA 3,6,10
Dexp. Dcal. d(D) h k l
5.5703 5.5675 .0029 0 1 1
4.9302 4.9312 -.0010 -1 0 1
3.6001 3.5987 .0014 2 0 1
3.2401 3.2414 -.0013 2 1 1
2.5901 2.5901 -.0001 2 2 1
1.9301 1.9301 .0000 -2 3 1
1.7701 1.7700 .0000 2 2 4
a= 7.3580 b= 7.4617 c= 8.576 beta= 77.172
da=.0008 db=.0006 dc=.001 dbet=.008
V=459.1
23. 31-0897
{Ni{NH3}5}SO4*H2O
Triklin
Dexp Dcal d(D) h k l
6.0703 6.0721 -.0018 1 0 0
5.6103 5.6125 -.0022 -1 1 0
5.3403 5.3403 .0001 -1 -1 1
5.1904 5.1926 -.0022 1 1 0
4.4203 4.4214 -.0011 0 -2 1
4.1903 4.1905 -.0002 -1 -2 1
4.0202 4.0209 -.0007 0 2 1
3.4703 3.4697 .0006 1 -1 1
3.1502 3.1499 .0003 1 3 0
3.0002 3.0002 .0001 -2 0 2
A= 6.976 DA= .001
B= 11.7796 DB= .0008
C= 6.9500 DC= .0008
GAMMA= 93.212 DGAMMA= .001
BETA =119.037 DBETA = .004
ALPHA= 93.192 DALPHA= .003
V=496.2
24. 31-898
Ni{NH3}2CS3
Monoklin
grupa 3
Dexp Dcal d(D) h k l
5.9404 5.9316 .0088 -1 0 2
5.6405 5.6425 -.0020 2 0 0
4.5103 4.4985 .0119 1 1 0
4.1702 4.1615 .0087 2 0 3
3.2102 3.2051 .0051 -2 1 2
3.0902 3.0888 .0014 0 0 5
2.7442 2.7434 .0008 3 1 3
2.2561 2.2570 -.0009 5 0 0
2.2561 2.2542 .0019 -2 1 5
2.1721 2.1731 -.0010 -1 1 6
2.0501 2.0504 -.0002 5 1 0
1.9013 1.9012 .0001 6 0 2
1.8776 1.8782 -.0005 2 2 5
a= 11.443000 b= 4.905 c= 15.660 beta= 80.463
da=.001 db=.002 dc= .001 dbet=.009
V=866.9
Triklin
Dexp Dcal d(D) h k l
5.9404 5.9427 -.0023 0 1 1
5.6405 5.6407 -.0002 1 0 0
4.9003 4.9035 -.0032 0 -1 1
4.5103 4.5121 -.0018 1 1 1
4.1702 4.1724 -.0021 -1 1 0
3.2102 3.2119 -.0017 0 2 0
3.0902 3.0899 .0003 -1 1 2
2.7442 2.7443 -.0001 2 1 1
2.2561 2.2560 .0001 2 2 2
2.1721 2.1723 -.0001 -1 -2 2
2.0501 2.0501 .0000 -2 -1 2
1.9013 1.9012 .0001 1 -3 1
1.8776 1.8776 .0001 -1 -3 1
A= 5.83373 DA= .00005
B= 6.589 DB= .001
C= 10.203 DC= .002
GAMMA= 85.061 DGAMMA= .006
BETA = 75.339 DBETA = .004
ALPHA= 77.28 DALPHA= .01
V= 369.9
25. 31-0907
NiP4O11
Triklin
Dexp Dcal d(D) h k l
6.2806 6.3071 -.0265 1 0 0
6.1103 6.1172 -.0069 0 -1 2
5.3705 5.3731 -.0026 -1 0 2
4.6103 4.6139 -.0036 1 1 2
4.5203 4.5175 .0028 -1 -1 2
4.3403 4.3390 .0014 -1 2 0
4.2602 4.2611 -.0008 0 -2 2
4.1302 4.1272 .0030 1 2 0
3.9302 3.9309 -.0007 0 2 4
3.9103 3.9136 -.0033 -1 -2 1
3.5003 3.4990 .0013 1 -2 2
3.3602 3.3579 .0023 1 0 4
A= 6.3708 DA= .0002
B= 11.83567 DB= .00004
C= 17.7956 DC= .0005
GAMMA= 94.762 DGAMMA= .001
BETA = 97.590 DBETA = .001
ALPHA= 74.6938 DALPHA= .0009
V=1279.9
26. 31-0908
Ni2P2O7*8H2O
Triklin
Dexp Dcal d(D) h k l
6.3405 6.3389 .0016 -1 0 1
6.0105 6.0044 .0061 0 1 1
5.6305 5.6272 .0032 0 -1 1
5.0505 5.0503 .0002 -2 0 1
4.7704 4.7712 -.0008 -1 2 1
4.5603 4.5667 -.0064 0 2 1
4.4703 4.4655 .0047 -3 1 0
4.2602 4.2687 -.0085 2 -1 1
3.9703 3.9626 .0077 1 2 1
3.7803 3.7811 -.0008 -2 3 0
3.4102 3.4135 -.0033 -2 -2 1
3.3102 3.3125 -.0023 2 2 1
A= 13.6951 DA= .0007
B= 12.11167 DB= .00001
C= 6.8140 DC= .0001
GAMMA=105.4449 DGAMMA= .0008
BETA = 99.6198 DBETA = .0005
ALPHA= 83.3645 DALPHA= .0001
V=1071.6
27. 31-0909
Ni2P4O12*10H2O
Triklin
Dexp Dcal d(D) h k l
9.9409 9.9513 -.0104 1 0 0
7.9005 7.9269 -.0264 -1 1 0
6.4002 6.3897 .0106 1 0 1
6.1103 6.0831 .0272 0 -2 1
5.8703 5.8744 -.0040 0 2 0
5.7503 5.7499 .0004 -1 1 1
5.2505 5.2544 -.0039 -1 2 0
5.0103 5.0193 -.0090 1 1 1
4.7903 4.7932 -.0029 -1 -1 2
4.5703 4.5688 .0016 -1 0 2
4.3303 4.3383 -.0080 0 2 1
4.2303 4.2327 -.0023 -2 1 1
A= 10.07833 DA= .00007
B= 12.61912 DB= .00008
C= 10.2845 DC= .0001
GAMMA= 91.6796 DGAMMA= .0003
BETA = 97.7610 DBETA = .0005
ALPHA=110.8949 DALPHA= .0001
V=1205.8
28. 31-0910
Ni4P8O24*19H2O
Triklin
Dexp Dcal d(D) h k l
8.5110 8.5041 .0069 1 0 1
8.1909 8.1981 -.0072 0 1 0
7.0306 7.0291 .0015 -1 1 0
5.4003 5.4042 -.0039 0 -1 1
5.1305 5.1331 -.0026 -2 1 0
4.8003 4.8041 -.0038 1 0 2
4.4404 4.4382 .0021 2 -1 1
3.6703 3.6695 .0008 1 -1 2
3.5102 3.5145 -.0043 -2 2 0
3.3803 3.3810 -.0007 2 2 0
3.2503 3.2499 .0003 1 0 3
3.0303 3.0296 .0006 3 -1 2
A= 12.989 DA= .001
B= 8.690 DB= .003
C= 10.340 DC= .007
GAMMA= 88.56 DGAMMA= .02
BETA = 78.68 DBETA = .02
ALPHA= 70.78 DALPHA= .04
V= 1079.6
29. 31-0915
NiTeMoO6
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
3.8503 3.8513 -.0010 -3 0 1
3.5602 3.5602 .0000 3 1 2
3.2602 3.2597 .0005 -1 2 2
3.1802 3.1803 -.0000 4 0 2
2.9782 2.9788 -.0006 -1 3 1
2.8902 2.8897 .0005 3 1 3
2.7412 2.7425 -.0013 0 2 3
2.6472 2.6480 -.0008 2 3 2
2.4902 2.4887 .0014 -3 3 1
2.4402 2.4396 .0006 -3 0 3
2.4082 2.4081 .0001 1 4 0
2.1862 2.1860 .0002 -2 0 4
2.0681 2.0678 .0004 5 3 2
a= 14.120 b= 9.7833 c=10.1930 beta= 77.103
da=.001 db=.0005 dc=.0003 dbet=.004
V=1373.0
Triklin
Dexp Dcal d(D) h k l
3.8503 3.8471 .0032 -1 1 1
3.5602 3.5583 .0019 0 -1 1
3.2602 3.2629 -.0027 1 -1 1
3.1802 3.1782 .0020 -2 1 1
2.9782 2.9771 .0011 -2 0 1
2.8902 2.8910 -.0008 -2 2 1
2.7412 2.7374 .0038 0 -2 1
2.6472 2.6459 .0013 -3 1 0
2.4902 2.4912 -.0010 -2 -1 1
2.4402 2.4392 .0010 3 0 0
2.4082 2.4086 -.0004 2 -2 1
2.1862 2.1873 -.0011 1 -3 1
2.0681 2.0682 -.0001 -1 0 2
A= 8.111 DA= .002
B= 8.345 DB= .004
C= 4.197 DC= .001
GAMMA=114.01 DGAMMA= .03
BETA =100.944 DBETA = .006
ALPHA= 83.355 DALPHA= .009
V= 254.6
30 31-1056
K2NiO3
Triklin
Dexp Dcal d(D) h k l
4.5504 4.5491 .0013 1 1 0
3.6403 3.6404 -.0002 -1 1 1
3.5102 3.5090 .0012 -1 -1 1
3.3503 3.3502 .0001 1 2 0
3.0202 3.0211 -.0009 0 -2 1
2.7102 2.7092 .0010 -2 0 1
2.1322 2.1312 .0010 -1 0 2
1.8411 1.8405 .0007 -3 1 0
1.7601 1.7603 -.0001 -3 2 0
1.7011 1.7013 -.0002 1 1 2
1.6771 1.6771 .0000 -3 3 1
1.5131 1.5131 -.0000 3 -1 1
A= 5.8457 DA= .0006
B= 8.9812 DB= .0007
C= 4.2717 DC= .0001
GAMMA= 94.819 DGAMMA= .002
BETA =107.86 DBETA = .01
ALPHA= 88.9639 DALPHA= .0008
V= 212.7
31. 31-1057
K2Ni3{P2O7}2*10H2O
Triklin
Dexp Dcal d(D) h k l
8.1508 8.1491 .0018 1 0 0
7.0107 7.0059 .0048 0 1 1
5.7704 5.7732 -.0028 0 -1 1
5.0005 4.9999 .0006 0 -2 0
4.7003 4.6992 .0011 1 0 1
3.9302 3.9278 .0024 0 -2 1
3.5102 3.5029 .0073 0 2 2
3.3302 3.3298 .0005 -2 -2 2
3.2302 3.2320 -.0018 2 1 1
3.1802 3.1817 -.0015 1 1 2
2.9202 2.9209 -.0007 -2 1 3
2.8502 2.8502 .0000 3 1 0
A= 9.68441 DA= .00007
B= 10.51358 DB= .00004
C= 9.36512 DC= .00004
GAMMA= 75.8923 DGAMMA= .0001
BETA =117.9476 DBETA = .0005
ALPHA= 86.9618 DALPHA= .0006
V=801.2
32. 31-1319
Na2Ni4Si8O20{OH}2*8H2O
Triklin
Dexp Dcal d(D) h k l
10.6014 10.5977 .0037 1 0 0
4.5403 4.5363 .0040 1 1 1
3.7202 3.7150 .0052 -1 -1 1
3.2802 3.2800 .0002 2 0 2
3.1802 3.1802 .0001 -3 0 1
3.0763 3.0780 -.0018 -2 -1 1
2.6532 2.6531 .0001 0 2 2
2.5972 2.5973 -.0001 1 1 3
2.4402 2.4402 -.0001 2 0 3
2.2521 2.2522 -.0001 -3 2 2
2.0301 2.0302 -.0000 -1 1 4
1.8901 1.8902 -.0001 5 1 0
A= 10.73479 DA= .00001
B= 5.941 DB= .002
C= 8.3081 DC= .0008
GAMMA= 98.77 DGAMMA= .01
BETA = 89.552 DBETA = .008
ALPHA= 75.90 DALPHA= .01
V= 507.3