1. 32-0535
PbSmHfNbO7
Rombik
Groupa 27
Dexp. Dcal. d(D) h k l
3.1800 3.1802 -.0002 0 3 0
3.0600 3.0600 .0000 1 0 2
2.6500 2.6512 -.0012 2 3 0
1.8800 1.8812 -.0012 1 4 2
1.6000 1.6000 -.0000 6 0 0
1.5300 1.5300 .0000 2 0 4
1.3290 1.3287 .0003 6 4 0
1.2200 1.2203 -.0003 7 2 2
1.1890 1.1889 .0001 7 4 0
1.1640 1.1641 -.0001 1 8 1
1.0840 1.0835 .0005 3 7 3
1.0680 1.0680 .0000 4 8 0
1.0220 1.0221 -.0001 2 9 1
.9900 .9903 -.0003 3 7 4
a= 9.6002 b= 9.5407 c= 6.4567
da= .0002 db= .0001 dc= .0006
V= 591.38
Triklin
Dexp Dcal d(D) h k l
3.1800 3.1797 .0003 0 1 1
3.0600 3.0596 .0004 0 -1 1
2.6500 2.6485 .0015 -1 0 1
1.8800 1.8804 -.0004 1 1 1
1.6000 1.6000 .0000 -1 3 1
1.5300 1.5298 .0002 0 -2 2
1.3290 1.3290 .0000 2 2 0
1.2200 1.2200 -.0000 1 5 0
1.1890 1.1891 -.0001 0 -5 1
1.1640 1.1640 -.0000 -1 2 3
1.0840 1.0838 .0002 -1 -3 3
1.0680 1.0679 .0001 0 6 0
1.0220 1.0220 -.0000 -2 2 3
.9900 .9901 -.0001 -1 -4 3
A= 2.9470 DA= .0001
B= 6.4544 DB= .0005
C= 3.77974 DC= .00007
GAMMA= 83.592 DGAMMA= .001
BETA =109.064 DBETA = .009
ALPHA= 89.662 DALPHA= .008
V= 67.46
2. 32-0586
Li0.4K0.6NbO
Triklin
Dexp Dcal d(D) h k l
8.2600 8.2622 -.0022 1 0 0
7.9600 7.9559 .0041 0 1 1
5.5600 5.5612 -.0012 0 -1 1
5.1000 5.1003 -.0003 -1 1 0
3.7980 3.7980 .0000 2 1 2
3.5300 3.5300 -.0000 -1 -1 2
3.2380 3.2409 -.0029 1 3 2
3.1850 3.1851 -.0001 -2 1 1
3.1280 3.1273 .0007 2 3 1
2.9480 2.9483 -.0003 3 1 0
2.8580 2.8572 .0008 3 2 2
2.6530 2.6520 .0010 0 3 3
A= 9.0999 DA= .0008
B= 10.021 DB= .005
C= 10.736 DC= .001
GAMMA= 65.62 DGAMMA= .01
BETA = 76.60 DBETA = .01
ALPHA= 66.25 DALPHA= .02
V= 813.5
3. 32-0587
Li0.2K0.6Na0.2NbO3
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
8.3400 8.3460 -.0060 1 1 0
7.9600 7.9614 -.0014 0 1 1
5.6800 5.6786 .0014 2 1 0
3.7700 3.7704 -.0004 1 1 3
3.6500 3.6499 .0001 -1 0 3
3.2600 3.2613 -.0013 -1 3 1
3.1400 3.1396 .0004 2 3 0
3.0560 3.0552 .0008 0 3 2
2.6340 2.6340 .0000 5 0 2
a= 13.647 b= 10.657 c= 12.178 beta= 79.55
da=.004 db=.006 dc=.00 dbeta=.05
V= 1742
Triklin
Dexp Dcal d(D) h k l
8.3400 8.3391 .0009 1 0 0
7.9600 7.9578 .0022 0 1 1
5.6800 5.6795 .0005 0 -1 1
3.7700 3.7700 -.0000 2 1 2
3.6500 3.6500 .0000 2 0 2
3.2600 3.2600 -.0000 0 3 0
3.1400 3.1400 .0000 1 2 3
3.0560 3.0560 .0000 -1 3 1
2.6340 2.6340 .0000 -1 1 3
A= 8.839 DA= .001
B= 10.4155 DB= .0005
C= 9.8589 DC= .0002
GAMMA= 83.52 DGAMMA= .01
BETA = 70.647 DBETA = .008
ALPHA= 69.889 DALPHA= .003
V= 804.1
4. 32-0594
Li0.6Na0.4NbO3
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
3.8300 3.8312 -.0012 -1 0 2
2.7590 2.7579 .0011 0 4 0
2.6520 2.6530 -.0010 -1 3 2
2.5890 2.5895 -.0005 2 1 0
2.2940 2.2937 .0003 2 0 2
2.1770 2.1777 -.0007 -2 0 3
1.9120 1.9120 .0000 -1 5 2
1.7380 1.7380 -.0000 1 6 0
1.6870 1.6870 .0000 -3 2 1
1.6160 1.6157 .0003 -1 5 4
1.5510 1.5510 .0000 2 1 5
1.5330 1.5332 -.0002 1 6 3
a= 5.342 b=11.03171 c=10.2453 beta= 94.22
da=.001 db=.00006 dc=.0006 dbeta=.05
V= 602.1
Triklin
Dexp Dcal d(D) h k l
3.8300 3.8302 -.0002 -1 -1 1
2.7590 2.7583 .0007 -1 -1 2
2.6520 2.6518 .0002 -1 1 0
2.5890 2.5893 -.0003 0 -2 1
2.2940 2.2941 -.0001 0 -2 2
2.1770 2.1770 -.0000 -2 -1 1
1.9120 1.9129 -.0009 -2 -1 2
1.7380 1.7373 .0007 2 2 1
1.6870 1.6864 .0006 0 -3 2
1.6160 1.6162 -.0002 2 3 0
1.5510 1.5512 -.0002 0 -1 4
1.5330 1.5334 -.0004 -1 -2 4
A= 4.4564 DA= .0005
B= 5.726 DB= .002
C= 6.2951 DC= .0002
GAMMA= 65.234 DGAMMA= .001
BETA = 99.476 DBETA = .009
ALPHA=111.68 DALPHA= .01
V= 135.5
5. 32-0710
Nb2O5
Rombik
Groupa 32,55
Dexp. Dcal. d(D) h k l
3.9000 3.8996 .0004 1 1 0
3.1200 3.1212 -.0012 0 0 3
2.7120 2.7142 -.0022 0 2 1
2.4270 2.4268 .0002 2 1 0
2.1020 2.0990 .0030 0 2 3
1.9550 1.9549 .0001 1 2 3
a= 5.370 b= 5.672 c= 9.364
da= .001 db= .001 dc= .001
V= 285.2
6. 32-0711
Nb2O5
Triklin
Dexp Dcal d(D) h k l
4.8700 4.8669 .0031 0 1 1
3.7500 3.7506 -.0006 0 -1 1
3.5700 3.5692 .0008 -1 1 0
3.3700 3.3665 .0035 1 1 0
2.7900 2.7919 -.0019 0 1 2
2.5100 2.5062 .0038 1 -1 1
2.3200 2.3185 .0015 0 -1 2
2.0600 2.0593 .0007 -1 3 2
1.9100 1.9112 -.0012 2 1 0
1.7800 1.7793 .0007 -2 1 3
1.7000 1.6997 .0003 0 4 1
1.6800 1.6805 -.0005 -1 4 1
A= 4.447 DA= .003
B= 6.915 DB= .002
C= 6.160 DC= .001
GAMMA=100.241 DGAMMA= .008
BETA =113.34 DBETA = .01
ALPHA= 72.275 DALPHA= .003
V= 165.3
7. 32-0823
KNb0.25Ta0.75O3
Triklin
11.3000 11.3110 -.0110 1 0 0
5.8300 5.8303 -.0003 0 1 1
5.6800 5.6816 -.0016 0 -1 1
5.4300 5.4244 .0056 2 2 0
5.2800 5.2812 -.0012 -1 -1 1
4.3300 4.3290 .0010 -1 -2 1
3.8300 3.8314 -.0014 2 -1 1
3.2600 3.2593 .0007 2 1 2
3.1400 3.1402 -.0002 4 2 1
3.0900 3.0914 -.0014 1 -1 2
2.9300 2.9304 -.0004 3 4 1
2.7460 2.7459 .0001 3 0 2
A= 13.040 DA= .003
B= 12.695 DB= .009
C= 6.863 DC= .0014
GAMMA= 61.62 DGAMMA= .02
BETA = 78.23 DBETA = .03
ALPHA= 82.99 DALPHA= .03
V= 978.1
8. 32-0842
K0.4Na0.6NbO3
Rombik
Groupa 33,49,62
Dexp. Dcal. d(D) h k l
8.5500 8.6050 -.0550 1 1 0
5.5300 5.5290 .0010 1 2 0
3.8300 3.8316 -.0016 2 0 1
3.2700 3.2664 .0036 2 2 1
3.2070 3.2055 .0015 0 3 1
3.1290 3.1245 .0045 0 4 0
2.9660 2.9664 -.0004 4 0 0
2.2850 2.2850 .0000 1 2 2
2.2360 2.2374 -.0014 0 5 1
a=11.8654 b=12.498 c= 5.019
da= .0006 db= .007 dc= .001
V= 744.2
9. 32-0932
alfa-RbNbO3
Triklin
Dexp Dcal d(D) h k l
8.8500 8.8512 -.0012 1 0 0
7.6300 7.6359 -.0059 0 0 1
4.3700 4.3702 -.0002 0 -2 1
4.1500 4.1514 -.0014 2 -1 1
3.8400 3.8411 -.0011 1 0 2
3.6300 3.6297 .0003 0 -1 2
3.5340 3.5348 -.0008 2 -2 1
3.3880 3.3864 .0016 -2 1 1
3.2270 3.2260 .0010 1 -2 2
3.0890 3.0904 -.0014 -1 -1 2
3.0180 3.0177 .0003 0 2 2
2.8850 2.8857 -.0007 -2 3 0
A= 9.166 DA= .003
B= 10.458 DB= .001
C= 7.863 DC= .002
GAMMA= 97.18 DGAMMA= .04
BETA = 76.372 DBETA = .003
ALPHA= 93.88 DALPHA= .02
V= 726.2
10. 32-0934
Rb6Nb16O43
Triklin
Dexp Dcal d(D) h k l
7.1200 7.1026 .0174 1 0 0
6.4700 6.4731 -.0031 0 1 1
6.2600 6.2708 -.0108 0 -1 1
5.5900 5.5852 .0048 1 1 0
4.1600 4.1593 .0007 1 2 0
3.6400 3.6414 -.0014 1 2 1
3.6100 3.6094 .0006 0 1 2
3.3600 3.3608 -.0008 -1 1 2
3.3410 3.3402 .0008 -2 1 1
3.2500 3.2511 -.0011 -2 0 1
3.1210 3.1217 -.0007 -1 -1 2
3.0540 3.0539 .0001 -2 3 0
A= 7.317 DA= .002
B= 12.5349 DB= .0005
C= 7.488 DC= .001
GAMMA=103.788 DGAMMA= .004
BETA = 92.519 DBETA = .003
ALPHA= 87.430 DALPHA= .008
V= 665.9
11. 33-0546
EuNb4O11
Triklin
Dexp Dcal d(D) h k l
5.5100 5.5080 .0020 2 0 0
3.9200 3.9190 .0010 -1 0 2
3.8000 3.8008 -.0008 0 1 2
3.6700 3.6720 -.0020 3 0 0
3.5700 3.5721 -.0021 -2 -1 2
3.5000 3.5003 -.0003 -1 -2 2
3.4300 3.4298 .0002 -2 0 2
3.3200 3.3203 -.0003 1 2 2
3.1800 3.1797 .0003 -1 3 0
3.0900 3.0899 .0001 4 2 0
3.0500 3.0496 .0004 -3 -1 2
3.0000 3.0001 -.0001 -2 -3 2
A= 12.453 DA= .008
B= 12.837 DB= .001
C= 8.109 DC= .003
GAMMA= 62.84 DGAMMA= .03
BETA = 96.81 DBETA = .09
ALPHA= 92.94 DALPHA= .08
V=1142
12. 33-0964
NbCl5
Rombik
Groupa 54
Dexp. Dcal. d(D) h k l
4.4600 4.4677 -.0077 0 0 4
4.3100 4.3035 .0065 1 0 2
3.9400 3.9448 -.0048 1 1 1
3.5600 3.5659 -.0059 0 2 0
3.3000 3.3046 -.0046 1 0 4
2.6800 2.6782 .0018 1 1 5
2.5970 2.5968 .0002 1 2 3
2.5470 2.5466 .0004 1 0 6
2.3780 2.3773 .0007 0 3 0
a= 4.910545 b= 7.131898 c=17.870750
da= .001923 db= .004389 dc= .002927
V= 625.8
13. 33-1033
C6K3NbO12*2H2O
Triklin
Dexp Dcal d(D) h k l
10.9000 10.9369 -.0369 0 1 1
7.8100 7.7741 .0359 0 -1 1
7.2400 7.2496 -.0096 1 0 0
6.4300 6.4095 .0205 0 2 0
6.2700 6.2658 .0042 0 0 2
5.9400 5.9664 -.0264 1 1 1
5.6400 5.6550 -.0150 1 0 1
5.5300 5.5262 .0038 -1 0 2
5.2000 5.1929 .0071 1 2 1
5.0100 5.0162 -.0062 0 -1 2
4.8700 4.8885 -.0185 -1 -1 2
4.4270 4.4255 .0015 -1 2 2
A= 7.63048 DA= .00005
B= 13.76816 DB= .00003
C= 13.55716 DC= .00001
GAMMA= 80.3574 DGAMMA= .0004
BETA =101.8360 DBETA = .0003
ALPHA= 73.5738 DALPHA= .0002
V=1298
14. 33-1122
beta-Rb6O17
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
9.6500 9.6524 -.0024 0 0 1
4.9800 4.9800 .0000 2 1 0
4.5500 4.5515 -.0015 -2 0 2
4.1900 4.1913 -.0013 0 1 2
3.8700 3.8719 -.0019 0 2 1
3.4400 3.4365 .0035 -3 1 2
3.3020 3.3070 -.0050 -2 0 3
3.2200 3.2175 .0025 0 0 3
3.1000 3.0973 .0027 -2 2 2
3.0280 3.0282 -.0002 -4 1 1
2.8940 2.8950 -.0010 4 1 0
2.7060 2.7050 .0010 0 3 1
a= 12.9739 b= 8.4538 c= 10.1601 beta= 108.19
da=.0005 db=.0008 dc=.005 dbeta=.03
V= 1059
Triklin
Dexp Dcal d(D) h k l
9.6500 9.6698 -.0198 0 0 1
4.9800 4.9808 -.0008 0 -2 1
4.5500 4.5496 .0004 1 1 0
4.1900 4.1812 .0088 -1 1 0
3.8700 3.8759 -.0059 1 -1 2
3.4400 3.4381 .0019 -1 1 1
3.3020 3.3020 .0000 1 2 1
3.2200 3.2213 -.0013 -1 -1 2
3.1000 3.1015 -.0015 -1 0 2
3.0280 3.0280 .0000 1 0 3
2.8940 2.8935 .0005 1 -2 3
2.7060 2.7052 .0008 1 1 3
A= 5.025 DA= .002
B= 10.125 DB= .003
C= 10.453 DC= .004
GAMMA= 88.17 DGAMMA= .05
BETA = 78.05 DBETA = .01
ALPHA=108.16 DALPHA= .08
V= 491.7
15. 33-1784
C10H10Br12Cl6Nb6
Geksag.
Grupa 143
Dexp. Dcal. d(D) h k l p
9.5900 9.5777 .0123 1 0 1 0
6.8900 6.8856 .0044 2 0 0 0
6.6700 6.6646 .0054 0 0 2 0
4.7900 4.7888 .0012 2 0 2 0
4.3400 4.3402 -.0002 3 0 1 0
4.2300 4.2285 .0015 1 0 3 1
3.9800 3.9754 .0046 2 2 0 4
3.8100 3.8096 .0004 2 2 1 0
3.4400 3.4428 -.0028 4 0 0 5
3.3400 3.3334 .0066 4 0 1 13
3.2400 3.2388 .0012 1 0 4 2
3.1900 3.1926 -.0026 3 0 3 6
a= 15.90 c= 13.33
da= .01 dc= .0009
V= 3370
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
9.5900 9.5889 .0011 1 1 0
6.8900 6.8914 -.0014 -1 1 1
6.6700 6.6670 .0030 1 1 1
4.7900 4.7889 .0011 0 0 2
4.3400 4.3391 .0009 1 3 0
4.2300 4.2287 .0013 1 1 2
3.9800 3.9807 -.0007 -2 0 2
3.8100 3.8103 -.0003 -1 2 2
3.4400 3.4406 -.0006 0 4 0
3.3400 3.3399 .0001 -3 0 2
3.2400 3.2397 .0003 -1 3 2
3.1900 3.1896 .0004 3 0 2
a= 13.38 b= 13.763 c= 9.588 beta= 92.64
da=.01 db= .004 dc=.001 dbeta=.05
V= 1764
Triklin
Dexp Dcal d(D) h k l
9.5900 9.5846 .0054 1 0 0
6.8900 6.8915 -.0015 1 0 1
6.6700 6.6669 .0031 0 -1 1
4.7900 4.7901 -.0001 0 2 0
4.3400 4.3405 -.0005 0 1 2
4.2300 4.2300 .0000 0 -2 1
3.9800 3.9797 .0003 1 1 2
3.8100 3.8106 -.0006 -1 -1 2
3.4400 3.4379 .0021 -2 2 0
3.3400 3.3401 -.0001 2 2 0
3.2400 3.2398 .0002 2 -1 2
3.1900 3.1899 .0001 -2 1 2
A= 9.594 DA= .001
B= 9.589 DB= .001
C= 9.58902 DC= .00008
GAMMA= 91.60 DGAMMA= .01
BETA = 88.1430 DBETA = .0006
ALPHA= 88.21 DALPHA= .01
V= 880.9
16. 33-1785
C10H10Cl18N2Nb6
Rombik
Groupa 26,28,51
Dexp. Dcal. d(D) h k l
9.4200 9.3888 .0312 1 0 1
6.7600 6.7577 .0023 0 1 0
6.5300 6.5268 .0032 2 0 1
5.4900 5.4847 .0053 1 1 1
5.2400 5.2421 -.0021 3 0 0
4.7000 4.6947 .0053 2 1 1
4.2500 4.2584 -.0084 1 1 2
3.9100 3.9047 .0053 3 1 1
3.8600 3.8554 .0046 2 1 2
3.7300 3.7269 .0031 4 0 1
3.3800 3.3808 -.0008 3 1 2
3.2600 3.2635 -.0035 4 1 1
a=15.73 b= 6.7577 c=11.70
da= .01 db= .0004 dc= .01
V=1244
Triklin
Dexp Dcal d(D) h k l
9.4200 9.4178 .0022 1 0 0
6.7600 6.7582 .0018 -1 1 0
6.5300 6.5312 -.0012 -1 0 1
5.4900 5.4896 .0004 1 -1 1
5.2400 5.2398 .0002 -1 -1 1
4.7000 4.7009 -.0009 0 0 2
4.2500 4.2530 -.0030 -1 2 0
3.9100 3.9107 -.0007 2 -1 1
3.8600 3.8605 -.0005 1 -1 2
3.7300 3.7303 -.0003 -2 -1 1
3.3800 3.3791 .0009 -2 2 0
3.2600 3.2597 .0003 0 -2 2
A= 9.4294 DA= .0004
B= 9.3834 DB= .0007
C= 9.4144 DC= .0007
GAMMA= 91.863 DGAMMA= .004
BETA = 87.905 DBETA = .003
ALPHA= 87.980 DALPHA= .003
V=831.2