1. 2-1353
FeO{Nb,Ta}2O5*5IiO2
Rombik
Groupa 56
Dexp. Dcal. d(D) h k l
3.2700 3.2707 -.0007 1 1 0
2.5000 2.5041 -.0041 3 0 2
2.3100 2.3095 .0005 1 1 3
2.1900 2.1898 .0002 3 1 1
1.7000 1.7022 -.0022 1 2 1
1.6300 1.6301 -.0001 4 0 4
1.4800 1.4802 -.0002 0 1 6
1.4300 1.4304 -.0004 0 2 4
1.3700 1.3693 .0007 3 2 3
1.3600 1.3595 .0005 2 2 4
1.0500 1.0501 -.0001 4 2 6
.8950 .8950 .0000 1 3 7
.8810 .8810 .0000 6 3 3
a= 8.7446 b= 3.5266 c= 9.7848
da= .0009 db= .0006 dc= .0008
V= 301.7
2-1380
Ñì.Ñîåäèíåíèÿ U
2. 3-0514
Nb2O5
Rombik
Groupa 27
Dexp. Dcal. d(D) h k l
4.0400 4.0404 -.0004 3 0 0
3.1700 3.1657 .0043 0 4 0
2.4800 2.4790 .0010 1 5 0
1.9700 1.9701 -.0001 0 0 2
1.8100 1.8090 .0010 0 7 0
1.6700 1.6703 -.0003 7 2 0
1.6500 1.6511 -.0011 3 7 0
1.5700 1.5695 .0005 1 8 0
1.4600 1.4594 .0006 6 6 0
1.3400 1.3393 .0007 9 1 0
1.2300 1.2308 -.0008 8 6 0
1.1800 1.1800 .0000 8 2 2
a=12.121 b=12.663 c= 3.9401
da= .001 db= .001 dc= .0008
V=604.8
3-0652
Cì. ñîåäèíåíèÿ U
3. 3-0857
NbC
Rombik
Groupa 41,64
Dexp. Dcal. d(D) h k l
2.5500 2.5499 .0001 1 2 0
2.2000 2.2073 -.0073 2 2 0
1.5600 1.5597 .0003 4 2 0
1.3300 1.3299 .0001 5 2 0
1.2700 1.2698 .0002 2 2 2
1.1000 1.1003 -.0003 4 2 2
1.0100 1.0099 .0001 5 2 2
.9860 .9860 .0000 6 3 1
.9000 .9001 -.0001 8 2 0
.8490 .8491 -.0001 7 4 0
.7800 .7799 .0001 8 4 0
a= 7.63592 b= 5.410 c= 3.1047
da= .00001 db= .001 dc= .0007
V= 128.26
4. 3-0905
Nb
Triklin
Dexp Dcal d(D) h k l
4.2300 4.2290 .0010 1 0 1
2.9600 2.9591 .0009 0 1 0
2.4200 2.4197 .0003 0 -1 2
2.0900 2.0901 -.0001 2 1 1
1.8800 1.8806 -.0006 -2 -1 1
1.7100 1.7096 .0004 2 1 3
1.4900 1.4902 -.0002 3 1 2
1.4000 1.4004 -.0004 -2 1 1
1.2700 1.2700 .0000 1 2 3
1.2100 1.2099 .0001 0 -2 4
1.1700 1.1702 -.0002 2 0 6
1.1300 1.1297 .0003 4 1 3
A= 4.657 DA= .001
B= 3.1218 DB= .0001
C= 7.2567 DC= .0009
GAMMA= 73.1463 DGAMMA= .0009
BETA = 74.34 DBETA = .01
ALPHA= 92.801 DALPHA= .006
V= 96.29
5. 3-1138
{Ca,Ge,Na}{NbTi}O3
Rombik
Groupa 17
Dexp. Dcal. d(D) h k l
2.7400 2.7403 -.0003 0 1 0
1.9300 1.9331 -.0031 0 0 3
1.5800 1.5796 .0004 0 1 3
1.3700 1.3701 -.0001 0 2 0
1.2200 1.2196 .0004 5 0 2
1.1600 1.1599 .0001 0 0 5
1.1200 1.1202 -.0002 6 0 0
1.0300 1.0300 -.0000 3 0 5
.9100 .9100 .0000 3 2 4
a= 6.721 b= 2.7403 c= 5.7993
da= .002 db= .0002 dc= .0004
V= 106.81
Triklin
Dexp Dcal d(D) h k l
2.7400 2.7399 .0001 1 0 0
1.9300 1.9299 .0001 -1 1 1
1.5800 1.5800 .0000 1 -1 1
1.3700 1.3700 .0000 0 1 2
1.2200 1.2200 -.0000 -2 1 0
1.1600 1.1600 .0000 -2 1 2
1.1200 1.1200 .0000 -1 2 2
1.0300 1.0300 .0000 -1 1 3
.9100 .9100 .0000 1 -3 2
A= 3.2336 DA= .0001
B= 4.3741 DB= .0001
C= 3.7198 DC= .0001
GAMMA= 69.8782 DGAMMA= .0009
BETA =119.9110 DBETA = .0007
ALPHA=110.215 DALPHA= .002
V= 41.84
6. 5-0352
Ni2O5
Triklin
Dexp Dcal d(D) h k l
4.3290 4.3267 .0023 0 1 1
3.9310 3.9327 -.0017 0 -1 1
3.4840 3.4827 .0013 -1 0 1
3.1400 3.1410 -.0010 1 -1 1
2.8550 2.8553 -.0003 -1 0 2
2.7280 2.7252 .0028 1 1 1
2.5900 2.5875 .0025 1 0 3
2.4470 2.4470 -.0000 0 -1 3
2.1200 2.1175 .0025 1 0 4
1.9620 1.9610 .0010 2 0 0
1.9080 1.9093 -.0013 -1 1 4
1.8250 1.8253 -.0003 1 2 0
A= 4.0190 DA= .0003
B= 4.69957 DB= .00009
C= 9.478 DC= .003
GAMMA=100.91 DGAMMA= .03
BETA = 84.87 DBETA = .02
ALPHA= 84.21 DALPHA= .01
V= 173.8
7. 5-0427
NbPO5
Triklin
Dexp Dcal d(D) h k l
4.5020 4.5015 .0005 0 1 1
3.4510 3.4511 -.0001 0 -1 1
3.1960 3.1962 -.0002 1 -1 1
3.0350 3.0363 -.0013 1 1 1
2.3470 2.3472 -.0002 0 -2 1
2.2520 2.2517 .0003 -2 3 0
2.0170 2.0163 .0007 -4 2 1
1.8800 1.8799 .0001 -2 4 1
1.8080 1.8085 -.0005 2 0 2
1.7260 1.7255 .0005 0 -2 2
1.6610 1.6613 -.0003 0 2 3
1.6230 1.6234 -.0004 -4 3 3
A= 8.074 DA= .003
B= 7.575 DB= .003
C= 5.663 DC= .001
GAMMA=123.17 DGAMMA= .06
BETA =113.57 DBETA = .04
ALPHA= 65.05 DALPHA= .03
V= 256.3
8. 8-0215
NbO2
Triklin
Dexp Dcal d(D) h k l
3.4900 3.4874 .0026 -1 2 0
3.4100 3.4137 -.0037 0 1 1
3.3500 3.3472 .0028 0 -1 1
3.2100 3.2077 .0023 -1 3 0
2.5900 2.5908 -.0008 -1 1 1
2.5400 2.5389 .0011 -1 -2 1
2.4900 2.4881 .0019 1 2 1
2.4200 2.4229 -.0029 1 3 1
2.2500 2.2480 .0020 0 7 1
2.1700 2.1710 -.0010 -1 5 1
1.9800 1.9804 -.0004 0 10 0
1.9300 1.9300 .0000 2 1 0
A= 3.86318 DA= .00003
B= 19.9056 DB= .0007
C= 3.4388 DC= .0005
GAMMA= 85.30 DGAMMA= .01
BETA = 92.246 DBETA = .009
ALPHA= 86.86 DALPHA= .01
V=263.1
9. 9-0258
Nb2TiO7
Triklin
Dexp Dcal d(D) h k l
10.2000 10.1519 .0481 0 0 1
9.4000 9.4172 -.0172 1 0 0
5.1300 5.1348 -.0048 1 1 0
5.0600 5.0697 -.0097 0 1 1
3.7100 3.7075 .0025 0 -1 2
3.6100 3.6140 -.0040 2 0 2
3.4200 3.4195 .0005 -1 1 2
3.3800 3.3840 -.0040 0 0 3
3.3100 3.3101 -.0001 -2 0 2
3.2800 3.2776 .0024 1 0 3
3.1400 3.1391 .0009 3 0 0
2.9500 2.9488 .0012 1 1 3
A= 9.51736 DA= .00004
B= 5.7440 DB= .0001
C= 10.20733 DC= .00006
GAMMA= 83.376 DGAMMA= .001
BETA = 84.6361 DBETA = .0008
ALPHA= 86.7992 DALPHA= .0007
V=550.6
10. 10-0398
{Y,Er}{Nb,Ia}2O6
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
4.0300 4.0297 .0003 -2 1 2
3.5900 3.5894 .0006 -2 2 1
3.2300 3.2300 .0000 -2 1 3
3.1300 3.1309 -.0009 2 0 3
2.9800 2.9790 .0010 1 3 0
2.9200 2.9200 -.0000 4 0 1
2.8100 2.8123 -.0023 -3 2 2
2.7500 2.7508 -.0008 2 3 0
2.6400 2.6396 .0004 1 1 4
2.5900 2.5888 .0012 2 2 3
2.5200 2.5204 -.0004 4 1 2
2.4500 2.4511 -.0011 0 2 4
a= 12.485 b= 9.206 c= 11.651 beta= 96.17
da=.004 db=.001 dc=.003 dbeta=.04
V= 1331.4
Triklin
Dexp Dcal d(D) h k l
4.0300 4.0253 .0047 -2 1 1
3.5900 3.5898 .0002 -2 0 1
3.2300 3.2308 -.0008 0 -1 1
3.1300 3.1268 .0032 1 -1 1
2.9800 2.9824 -.0024 -1 -1 1
2.9200 2.9192 .0008 0 2 0
2.8100 2.8089 .0011 1 2 1
2.7500 2.7481 .0019 -3 0 1
2.6400 2.6417 -.0017 -3 2 1
2.5900 2.5898 .0002 0 0 2
2.5200 2.5211 -.0011 3 1 0
2.4500 2.4506 -.0006 1 0 2
A= 9.711 DA= .005
B= 6.77 DB= .01
C= 5.880 DC= .003
GAMMA=106.15 DGAMMA= .06
BETA =100.99 DBETA = .06
ALPHA= 62.020 DALPHA= .009
V=327.1
11. 11-0260
{Ce,Ca<Fe,Th}{Ti,Nb}2O6
Triklin
Dexp Dcal d(D) h k l
5.4300 5.4417 -.0117 -2 1 0
4.3900 4.3931 -.0031 -1 2 0
4.3300 4.3303 -.0003 1 2 0
4.0200 4.0192 .0008 -3 1 0
3.7400 3.7478 -.0078 2 2 0
3.3200 3.3106 .0094 4 0 0
3.0800 3.0794 .0006 0 3 0
3.0100 3.0064 .0036 0 0 1
2.9400 2.9405 -.0005 1 0 1
2.7900 2.7927 -.0027 0 -1 1
2.6600 2.6618 -.0018 4 2 0
2.5700 2.5688 .0012 1 2 1
A= 13.247 DA= .004
B= 9.271 DB= .001
C= 3.0167 DC= .0004
GAMMA= 91.27 DGAMMA= .03
BETA = 89.33 DBETA = .02
ALPHA= 85.35 DALPHA= .01
V=369.1
12. 12-0093
NbJ5
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
6.0900 6.0846 .0054 1 0 1
5.5700 5.5798 -.0098 1 1 0
3.4700 3.4704 -.0004 1 2 0
3.2400 3.2463 -.0063 1 2 1
3.0700 3.0715 -.0015 -2 0 1
3.0400 3.0423 -.0023 2 0 2
2.4000 2.3981 .0019 -2 2 1
2.3600 2.3587 .0013 1 3 1
2.0200 2.0199 .0001 4 0 2
1.8600 1.8599 .0001 3 3 0
1.8300 1.8302 -.0002 1 4 1
1.7300 1.7276 .0024 -2 0 3
a= 8.515 b=7.6763 c= 6.90 beta=72.581
da=.002 db=.0007 dc=.01 dbeta=.008
V= 430.6
13. 12-0095
Nb2O5
Triklin
Dexp Dcal d(D) h k l
3.7700 3.7702 -.0002 -2 -1 1
3.7100 3.7092 .0008 2 -1 1
3.6300 3.6340 -.0040 -1 1 2
3.5600 3.5615 -.0015 2 0 3
3.4900 3.4880 .0020 0 1 3
3.3600 3.3606 -.0006 -1 2 0
3.1600 3.1604 -.0004 0 -2 2
2.8200 2.8198 .0002 0 0 4
2.7700 2.7696 .0004 -2 1 2
2.7000 2.6998 .0002 3 -1 2
2.5700 2.5721 -.0021 4 1 2
2.5500 2.5498 .0002 0 -3 1
A= 10.310 DA= .003
B= 8.366 DB= .002
C= 12.137 DC= .001
GAMMA= 72.71 DGAMMA= .03
BETA = 68.64 DBETA = .02
ALPHA= 80.48 DALPHA= .03
V=931.2
14. 12-0104
Nb2O5
Triklin
Dexp. Dcal. d(D) h k l
5.5820 5.5820 .0000 0 2 0
5.5340 5.5340 .0000 2 -2 0
4.3920 4.3841 .0079 3 -2 0
4.1780 4.1780 .0000 3 0 0
4.1390 4.1352 .0038 -2 1 1
3.6840 3.6893 -.0053 3 -3 0
3.5130 3.5129 .0001 2 -1 1
3.2250 3.2231 .0019 -2 -1 1
2.6790 2.6801 -.0011 -2 -2 1
2.3830 2.3849 -.0019 1 -5 0
2.3760 2.3765 -.0005 4 -3 1
2.2200 2.2203 -.0003 0 -4 1
A= 14.100 DA= .004
B= 12.698 DB= .006
C= 4.649 DC= .001
GAMMA=117.00 DGAMMA= .03
BETA = 99.05 DBETA = .02
ALPHA= 77.613 DALPHA= .003
V= 722.7
15. 13-0331
Na3NbO4
Triklin
Dexp Dcal d(D) h k l
8.3200 8.2299 .0901 1 0 1
6.6000 6.6201 -.0201 0 -1 1
5.4800 5.4934 -.0134 2 0 1
5.2400 5.2412 -.0012 2 0 0
4.1900 4.1844 .0056 2 -1 1
4.1100 4.1149 -.0049 2 0 2
4.0400 4.0379 .0021 -2 -1 1
3.9400 3.9403 -.0003 2 2 0
3.7890 3.7874 .0016 3 0 1
3.4630 3.4594 .0036 -2 -2 1
3.4010 3.3992 .0018 0 1 2
3.0680 3.0696 -.0016 -2 1 1
A= 11.84 DA= .01
B= 8.765 DB= .005
C= 9.033 DC= .003
GAMMA= 73.78 DGAMMA= .08
BETA = 70.171 DBETA = .004
ALPHA= 96.27 DALPHA= .04
V=823.0
16. 13-0472
Zn3Nb2O8
Triklin
Dexp Dcal d(D) h k l
4.2400 4.2403 -.0003 -2 1 0
3.2700 3.2693 .0007 0 4 0
3.1600 3.1611 -.0011 2 2 0
2.6900 2.6891 .0009 2 3 0
2.5700 2.5694 .0006 3 1 0
2.5400 2.5398 .0002 0 1 1
2.3600 2.3595 .0005 1 -2 1
2.2320 2.2319 .0001 0 -3 1
2.2130 2.2135 -.0005 1 -3 1
2.0010 2.0008 .0002 2 5 0
1.8910 1.8911 -.0001 3 -1 1
1.8680 1.8681 -.0001 -1 5 1
A= 8.507 DA= .001
B= 13.478 DB= .001
C= 2.59205 DC= .00003
GAMMA=104.01 DGAMMA= .01
BETA = 91.290 DBETA = .006
ALPHA= 89.948 DALPHA= .002
V=288.5
17. 13-0473
ZnNb2O6
Monoklin
GRUPA 3
Dexp. Dcal. d(D) h k l
3.6100 3.6123 -.0023 2 1 0
3.5300 3.5358 -.0058 1 2 0
2.9300 2.9331 -.0031 3 0 2
2.8400 2.8390 .0010 1 0 3
2.4700 2.4734 -.0034 1 3 1
2.3500 2.3497 .0003 3 2 2
2.1880 2.1875 .0005 4 1 2
2.0610 2.0608 .0002 4 1 3
1.8830 1.8834 -.0004 3 3 0
1.8150 1.8158 -.0008 3 3 3
1.7630 1.7634 -.0004 5 0 1
1.7190 1.7181 .0009 2 0 5
a= 9.1421 b= 7.852 c= 8.624 beta= 62.869
da= .007 db=.007 dc= .005 dbet=.004
V=550.4
18. 14-0258
Na2{Nb,Ti}2Si2O9*xH2O
Triklin
Dexp Dcal d(D) h k l
7.1300 7.1324 -.0024 1 0 0
6.1100 6.1026 .0074 1 1 0
5.3000 5.3003 -.0003 1 1 1
4.3300 4.3298 .0002 -1 1 1
3.9500 3.9465 .0035 -1 -1 1
3.7500 3.7475 .0025 2 1 0
3.1200 3.1187 .0013 -2 -1 1
2.9700 2.9702 -.0002 -1 2 1
2.8700 2.8726 -.0026 -2 1 1
2.7200 2.7209 -.0009 -1 -2 1
2.6000 2.6008 -.0008 -2 0 2
2.3900 2.3897 .0003 3 1 1
A= 7.626 DA= .004
B= 8.02 DB= .01
C= 7.367 DC= .004
GAMMA= 70.72 DGAMMA= .06
BETA = 88.44 DBETA = .05
ALPHA= 64.48 DALPHA= .06
V= 380.2
19. 14-0279
{NaCa}2{Ti,Nb}Si{O,F}6
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
10.1000 10.0054 .0946 1 0 0
6.8600 6.8651 -.0051 1 1 0
5.6000 5.5922 .0078 1 1 1
5.0800 5.0703 .0097 -1 0 2
4.3200 4.3307 -.0107 0 2 1
4.1000 4.0981 .0019 1 1 2
3.9400 3.9437 -.0037 2 1 1
3.5700 3.5684 .0016 0 2 2
3.4500 3.4541 -.0041 -1 2 2
3.3400 3.3371 .0029 -1 1 3
3.2600 3.2579 .0021 2 1 2
3.1400 3.1393 .0007 -2 0 3
a=10.09 b= 9.44 c= 11.00 beta=97.37
da=.01 db= .03 dc=.01 dbeta=.03
V= 1039
Triklin
Dexp Dcal d(D) h k l
10.1000 10.0907 .0093 1 0 0
6.8600 6.8596 .0004 -1 0 1
5.6000 5.6005 -.0005 1 1 1
5.0800 5.0815 -.0015 1 2 0
4.3200 4.3174 .0026 0 0 2
4.1000 4.0994 .0006 -1 0 2
3.9400 3.9301 .0099 -2 -2 1
3.5700 3.5781 -.0081 1 -1 2
3.4500 3.4516 -.0016 3 1 0
3.3400 3.3402 -.0002 -3 -1 1
3.2600 3.2592 .0008 0 -3 1
3.1400 3.1399 .0001 -2 -3 1
A= 10.459 DA= .001
B= 10.593 DB= .001
C= 8.713 DC= .002
GAMMA= 75.56 DGAMMA= .01
BETA = 96.25 DBETA = .03
ALPHA= 95.90 DALPHA= .05
V=926.7
20. 14-0623
NbOI3
Rombik
Groupa 31,59
Dexp. Dcal. d(D) h k l
3.7400 3.7419 -.0019 1 2 0
3.3500 3.3560 -.0060 0 1 1
3.0800 3.0758 .0042 5 1 0
2.8800 2.8780 .0020 3 1 1
2.2900 2.2888 .0012 7 1 0
2.2600 2.2608 -.0008 6 2 0
2.1100 2.1104 -.0004 0 3 1
1.7500 1.7497 .0003 7 3 0
1.6700 1.6697 .0003 1 2 2
1.5300 1.5300 .0000 9 2 1
1.3100 1.3098 .0002 12 0 1
1.2200 1.2202 -.0002 13 0 1
1.2000 1.1989 .0011 14 0 0
a=16.785 b= 7.6770 c= 3.731
da= .004 db= .0001 dc= .001
v= 480.8
Triklin
Dexp Dcal d(D) h k l
3.7400 3.7371 .0029 0 1 1
3.3500 3.3496 .0004 0 -1 1
3.0800 3.0813 -.0013 -1 0 1
2.8800 2.8825 -.0025 -1 1 0
2.2900 2.2910 -.0010 0 0 2
2.2600 2.2582 .0018 0 -2 1
2.1100 2.1091 .0009 1 1 1
1.7500 1.7510 -.0010 1 2 1
1.6700 1.6703 -.0003 -1 3 0
1.5300 1.5298 .0002 -2 -1 1
1.3100 1.3099 .0001 -1 3 3
1.2200 1.2199 .0001 1 1 3
1.2000 1.2001 -.0001 -1 0 4
A= 3.3630 DA= .0006
B= 5.6213 DB= .0007
C= 4.8645 DC= .0001
GAMMA= 98.38 DGAMMA= .01
BETA =108.606 DBETA = .003
ALPHA= 81.351 DALPHA= .003
V=85.73
21. 15-0162
NbI3.2
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
2.9500 2.9469 .0031 0 4 0
2.3100 2.3092 .0008 2 3 0
2.1300 2.1331 -.0031 0 1 2
2.0300 2.0275 .0025 1 0 2
1.9500 1.9471 .0029 1 5 1
1.8800 1.8785 .0015 3 1 0
1.8100 1.8107 -.0007 3 2 0
1.6700 1.6703 -.0003 1 4 2
1.5700 1.5698 .0002 0 7 1
1.5000 1.4999 .0001 3 4 1
1.4800 1.4807 -.0007 3 5 0
1.4500 1.4503 -.0003 2 7 0
a= 5.708322 b=11.787640 c= 4.337732
da= .000690 db= .006255 dc= .000462
V= 291.9
Triklin
Dexp Dcal d(D) h k l
2.9500 2.9498 .0002 1 0 1
2.3100 2.3105 -.0005 -2 1 2
2.1300 2.1297 .0003 -2 1 0
2.0300 2.0301 -.0001 -1 1 3
1.9500 1.9499 .0001 1 0 2
1.8800 1.8798 .0002 2 0 1
1.8100 1.8099 .0001 1 2 2
1.6700 1.6704 -.0004 0 0 3
1.5700 1.5698 .0002 -3 0 2
1.5000 1.4999 .0001 -2 2 4
1.4800 1.4801 -.0001 -2 -2 1
1.4500 1.4499 .0001 -3 -1 1
A= 5.088 DA= .008
B= 5.377 DB= .006
C= 6.151 DC= .001
GAMMA=104.8 DGAMMA= .1
BETA =114.00 DBETA = .06
ALPHA= 59.76 DALPHA= .04
V= 132.5
22. 15-0459
Co0.97Nb0.03
Triklin
Dexp Dcal d(D) h k l
5.6200 5.6208 -.0008 -1 0 1
4.8300 4.8359 -.0059 1 1 0
3.5500 3.5519 -.0019 1 0 3
3.1100 3.1092 .0008 0 -1 3
3.0040 3.0089 -.0049 0 2 0
2.9320 2.9330 -.0010 -2 -1 1
2.7350 2.7321 .0029 -2 1 1
2.5710 2.5728 -.0018 0 -2 2
2.4070 2.4064 .0006 1 -1 4
2.2940 2.2928 .0012 -2 -2 1
2.2470 2.2457 .0013 3 1 0
2.2080 2.2082 -.0002 -3 0 1
A= 7.0410 DA= .0001
B= 6.096 DB= .001
C= 11.663 DC= .004
GAMMA= 82.398 DGAMMA= .006
BETA = 81.938 DBETA = .009
ALPHA= 83.88 DALPHA= .02
V=489.1
23. 15-0465
Co0.967Nb0.033
Triklin
Dexp Dcal d(D) h k l
3.3900 3.3846 .0054 1 0 2
2.9520 2.9502 .0018 1 2 1
2.8250 2.8227 .0023 1 -2 2
2.5480 2.5493 -.0013 2 0 2
2.3970 2.3952 .0018 1 2 2
2.2840 2.2847 -.0007 1 -3 2
2.2240 2.2247 -.0007 -2 -1 1
2.0860 2.0866 -.0006 2 0 3
2.0230 2.0240 -.0010 2 2 2
1.9780 1.9796 -.0016 -2 2 1
1.9200 1.9188 .0012 3 0 1
1.3900 1.3898 .0002 -2 2 3
A= 5.782 DA= .005
B= 8.10 DB= .01
C= 7.212 DC= .003
GAMMA= 94.86 DGAMMA= .06
BETA = 71.477 DBETA = .005
ALPHA= 99.33 DALPHA= .03
V=316.4
24. 15-0493
Nb2O5
Triklin
Dexp Dcal d(D) h k l
5.1810 5.1852 -.0042 0 1 0
5.0490 5.0613 -.0123 1 0 2
4.6780 4.6656 .0124 0 -1 2
4.0810 4.0822 -.0012 -1 -1 1
3.9550 3.9557 -.0007 0 1 3
3.7810 3.7767 .0043 -1 1 0
3.7030 3.6976 .0054 -1 1 1
3.5710 3.5749 -.0039 -1 -1 3
3.4550 3.4621 -.0071 0 1 4
3.3900 3.3853 .0047 1 1 3
3.3220 3.3176 .0044 -1 0 5
3.2160 3.2193 -.0033 1 0 5
A= 6.081 DA= .005
B= 5.212 DB= .003
C= 19.44 DC= .01
GAMMA= 84.84 DGAMMA= .01
BETA = 92.15 DBETA = .08
ALPHA= 92.89 DALPHA= .02
V= 612.60
25. 15-0710
NbTe2
Rombik
Groupa 30, 53
Dexp. Dcal. d(D) h k l
6.6100 6.2922 .3178 0 0 2
3.3100 3.3146 -.0046 4 0 2
2.9200 2.9177 .0023 2 0 4
2.8500 2.8448 .0052 0 1 1
2.6700 2.6726 -.0026 2 1 1
2.5500 2.5462 .0038 3 1 0
2.2940 2.2910 .0030 2 1 3
2.2170 2.2152 .0018 5 0 4
2.0580 2.0641 -.0061 2 1 4
1.8520 1.8520 .0000 2 1 5
1.8180 1.8184 -.0004 7 0 4
1.6570 1.6573 -.0003 8 0 4
1.6190 1.6189 .0001 3 1 6
1.5440 1.5436 .0004 7 1 4
a=15.598 b= 2.920 c=12.584
da= .002 db= .003 dc= .005
V=573.2
Triklin
Dexp Dcal d(D) h k l
6.6100 6.6264 -.0164 0 1 0
3.3100 3.3118 -.0018 0 -1 2
2.9200 2.9177 .0023 1 -1 1
2.8500 2.8513 -.0013 0 -2 2
2.6700 2.6691 .0009 -1 0 2
2.5500 2.5497 .0003 0 2 1
2.2940 2.2939 .0001 1 -1 2
2.2170 2.2138 .0032 0 -1 3
2.0580 2.0584 -.0004 0 0 3
1.8520 1.8523 -.0003 -2 1 0
1.8180 1.8179 .0001 -2 -3 1
1.6570 1.6566 .0004 0 4 0
1.6190 1.6192 -.0002 0 -4 3
1.5440 1.5442 -.0002 0 3 2
A= 4.3128 DA= .0006
B= 7.443 DB= .004
C= 6.877 DC= .006
GAMMA= 73.69 DGAMMA= .02
BETA =104.55 DBETA = .07
ALPHA=114.68 DALPHA= .06
V= 190.2
26. 15-0928
C10H10Cl4N2Nb
Triklin
Dexp Dcal d(D) h k l
8.2000 8.1893 .0107 0 1 1
6.5000 6.5077 -.0077 -1 1 0
6.1200 6.1231 -.0031 0 -1 1
5.7600 5.7677 -.0077 -1 0 1
5.3700 5.3653 .0047 0 1 2
5.1600 5.1596 .0004 1 0 2
4.1500 4.1480 .0020 2 0 1
3.8300 3.8303 -.0003 2 -1 1
3.7100 3.7133 -.0033 2 1 1
3.1600 3.1595 .0005 1 -1 3
2.8100 2.8094 .0006 2 2 0
2.6900 2.6903 -.0003 1 2 4
A= 8.373 DA= .003
B= 9.471 DB= .003
C= 11.600 DC= .003
GAMMA= 94.41 DGAMMA= .03
BETA = 76.47 DBETA = .01
ALPHA= 74.90 DALPHA= .01
V= 854.2
27. 15-0929
C10H10I4N2Nb
Triklin
Dexp Dcal d(D) h k l
6.7600 6.7570 .0030 1 0 0
5.5800 5.5818 -.0018 0 1 1
4.3500 4.3548 -.0048 0 -1 1
4.0700 4.0650 .0050 0 2 1
3.9400 3.9446 -.0046 -1 0 1
3.8500 3.8560 -.0060 1 -1 1
3.4700 3.4710 -.0010 2 1 1
3.3100 3.3081 .0019 2 0 1
2.7900 2.7909 -.0009 0 2 2
2.5700 2.5688 .0012 0 -1 2
2.2600 2.2599 .0001 -2 2 1
2.2000 2.2000 -.0000 0 -4 0
A= 7.20675 DA= .00006
B= 9.4151 DB= .0006
C= 6.3524 DC= .0005
GAMMA= 75.74 DGAMMA= .01
BETA = 71.87 DBETA = .01
ALPHA= 71.334 DALPHA= .007
V=382.9
28. 15-0930
C10H10Br4N2Nb
Triklin
Dexp Dcal d(D) h k l
6.6200 6.6208 -.0008 0 1 0
6.2700 6.2712 -.0012 0 -1 1
5.3000 5.3068 -.0068 -1 -1 1
4.2100 4.2118 -.0018 1 1 1
4.0400 4.0351 .0049 -1 -2 1
3.8800 3.8805 -.0005 0 1 1
3.6900 3.6917 -.0017 0 -2 1
3.2700 3.2689 .0011 -2 -2 1
3.1400 3.1356 .0044 0 -2 2
2.8500 2.8483 .0017 1 2 1
2.7800 2.7793 .0007 1 -2 1
2.7100 2.7105 -.0005 1 1 2
A= 7.73 DA= .01
B= 8.280 DB= .002
C= 7.3515 DC= .0002
GAMMA= 63.32 DGAMMA= .07
BETA = 89.75 DBETA = .08
ALPHA=113.4 DALPHA= .1
V= 376.2