1. 34-0578
UO3*0.16CO2*1.91H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
7.3800 7.3913 -.0113 1 1 0
5.0800 5.0786 .0014 0 2 1
4.3200 4.3219 -.0019 2 1 1
3.5800 3.5798 .0002 0 1 3
3.4900 3.4914 -.0014 -2 0 2
3.2200 3.2194 .0006 3 0 1
3.1660 3.1664 -.0004 2 0 3
2.5320 2.5325 -.0005 0 2 4
2.0430 2.0430 -.0000 -1 5 2
1.9670 1.9670 .0000 2 5 2
1.7900 1.7899 .0001 0 2 6
1.7440 1.7440 -.0000 2 2 6
a= 9.80 b=11.366 c= 11.3944 beta= 83.2
da=.01 db=.001 dc= .0005 dbeta= .1
V= 1260
Triklin
Dexp Dcal d(D) h k l
7.3800 7.3781 .0019 0 1 1
5.0800 5.0797 .0003 0 -1 1
4.3200 4.3200 -.0000 1 1 0
3.5800 3.5800 .0000 -1 -1 1
3.4900 3.4900 -.0000 2 0 1
3.2200 3.2201 -.0001 -2 2 2
3.1660 3.1662 -.0002 0 0 3
2.5320 2.5321 -.0001 -2 -1 1
2.0430 2.0430 .0000 2 1 4
1.9670 1.9670 .0000 -3 4 3
1.7900 1.7900 .0000 -2 -2 2
1.7440 1.7440 .0000 0 -2 4
A= 8.1004 DA= .0004
B= 9.1024 DB= .0003
C= 10.2332 DC= .0006
GAMMA=116.757 DGAMMA= .002
BETA = 94.075 DBETA = .002
ALPHA= 69.0241 DALPHA= .0005
V= 625.41
2. 34-0630
U{OH}O2{NO3}*2H2O
Triklin
Dexp Dcal d(D) h k l
9.2500 9.2258 .0242 0 0 1
8.0100 8.0072 .0028 0 -2 1
7.6900 7.6931 -.0031 -1 1 0
6.6300 6.6336 -.0036 0 -3 1
5.5700 5.5723 -.0023 -1 2 1
5.2600 5.2572 .0028 1 -2 1
4.9300 4.9271 .0029 1 4 0
4.7900 4.7861 .0039 1 -3 1
4.6100 4.6129 -.0029 0 0 2
4.2500 4.2484 .0016 -1 -5 1
4.0700 4.0702 -.0002 -2 -1 1
3.9100 3.9084 .0016 -1 2 2
A= 8.39187 DA= .0009
B= 24.428 DB= .002
C= 9.560 DC= .005
GAMMA= 86.04 DGAMMA= .01
BETA =101.62 DBETA = .02
ALPHA=100.44 DALPHA= .01
V= 1887
3. 34-0904
UF4{SO3}4
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
4.3700 4.3723 -.0023 2 1 0
4.1000 4.1025 -.0025 2 1 1
3.6400 3.6406 -.0006 -2 0 1
3.2200 3.2195 .0005 3 0 0
2.7300 2.7298 .0002 3 2 0
2.1200 2.1199 .0001 3 3 2
1.9800 1.9801 -.0001 1 3 3
1.7900 1.7900 .0000 1 1 4
1.7300 1.7300 .0000 2 4 3
a= 9.90 b=10.297 c=7.275 beta=77.38
da=.01 db=.006 dc=.002 dbeta=.03
V= 723.6
Triklin
Dexp Dcal d(D) h k l
4.3700 4.3698 .0002 1 0 0
4.1000 4.1000 .0000 -1 1 0
3.6400 3.6402 -.0002 -1 0 1
3.2200 3.2202 -.0002 -1 -1 1
2.7300 2.7301 -.0001 1 -2 1
2.1200 2.1200 -.0000 -2 0 1
1.9800 1.9800 .0000 0 4 0
1.7900 1.7900 .0000 -1 -3 2
1.7300 1.7300 .0000 -1 -1 3
A= 4.44866 DA= .00001
B= 8.03108 DB= .00008
C= 5.54230 DC= .00003
GAMMA= 98.3002 DGAMMA= .0003
BETA = 96.3211 DBETA = .0001
ALPHA= 93.749 DALPHA= .001
V= 194.09
4. 34-1244
UO2H{PO3}3
Triklin
Dexp Dcal d(D) h k l
6.6300 6.6336 -.0036 1 0 0
6.2700 6.2681 .0019 0 -1 1
5.2000 5.2046 -.0046 1 0 1
4.6200 4.6104 .0096 -1 1 0
4.4400 4.4382 .0018 1 -1 1
4.1500 4.1485 .0015 0 -1 2
3.8900 3.8877 .0023 1 1 1
3.2100 3.2110 -.0010 -1 -2 1
3.1100 3.1103 -.0003 1 2 0
3.0000 2.9992 .0008 -2 -1 1
2.9100 2.9112 -.0012 -2 1 0
2.7800 2.7803 -.0003 0 0 3
A= 6.647 DA= .001
B= 7.150 DB= .002
C= 8.737 DC= .001
GAMMA= 86.334 DGAMMA= .008
BETA = 90.83 DBETA = .02
ALPHA=107.33 DALPHA= .01
V= 395.6
5. 34-1255
{UO2}2P6O17
Triklin
Dexp Dcal d(D) h k l
7.8000 7.7990 .0010 1 0 0
5.8000 5.7959 .0041 1 1 0
4.4000 4.3971 .0029 0 1 1
3.9000 3.8995 .0005 2 0 0
3.6300 3.6322 -.0022 0 2 1
3.5300 3.5307 -.0007 1 1 1
3.4200 3.4195 .0005 -2 2 0
3.3500 3.3502 -.0002 0 -2 1
2.9100 2.9094 .0006 0 3 1
2.6300 2.6305 -.0005 -3 1 0
2.6000 2.5997 .0003 3 0 0
2.5500 2.5499 .0001 2 -2 1
A= 8.019 DA= .003
B= 10.68 DB= .01
C= 4.743 DC= .004
GAMMA=100.68 DGAMMA= .05
BETA = 99.20 DBETA = .08
ALPHA= 83.79 DALPHA= .01
V= 393.0
6. 34-1258
UO2{PO3}2
Triklin
Dexp Dcal d(D) h k l
4.3900 4.3990 -.0090 -1 1 1
4.1100 4.1062 .0038 -1 -1 1
3.9200 3.9216 -.0016 1 1 0
3.6500 3.6556 -.0056 1 0 1
3.5800 3.5805 -.0005 -1 0 2
3.5300 3.5313 -.0013 0 2 1
3.4300 3.4272 .0028 -1 2 1
3.3800 3.3812 -.0012 -1 -1 2
2.6400 2.6403 -.0003 -1 3 1
2.6100 2.6098 .0002 -1 0 3
2.4400 2.4395 .0005 2 0 0
2.3700 2.3696 .0004 1 1 2
A= 5.191 DA= .006
B= 9.370 DB= .007
C= 8.1774 DC= .0002
GAMMA=100.07 DGAMMA= .02
BETA =104.93 DBETA = .01
ALPHA=100.21 DALPHA= .1
V= 368.1
7. 34-1330
KUO2{PO3}3
Triklin
Dexp Dcal d(D) h k l
7.4500 7.5053 -.0553 0 2 1
6.5000 6.5178 -.0178 -1 1 0
5.5000 5.4997 .0003 1 1 1
5.4700 5.4696 .0004 1 -1 1
5.1000 5.0995 .0005 1 -2 1
4.9300 4.9298 .0002 -1 0 1
4.8000 4.7946 .0054 -1 2 1
4.5500 4.5495 .0005 0 5 1
4.3000 4.2988 .0012 0 0 2
4.2000 4.1982 .0018 1 4 1
4.1000 4.0999 .0001 0 -5 1
4.0200 4.0212 -.0012 -1 -3 1
A= 6.68816 DA= .00007
B= 25.1119 DB= .0002
C= 8.73084 DC= .00002
GAMMA= 93.5500 DGAMMA= .0001
BETA = 82.68639 DBETA = .00003
ALPHA= 83.66232 DALPHA= .00003
V= 1441.2
8. 34-1477
NaUO2{PO3}3
Triklin
Dexp Dcal d(D) h k l
8.3000 8.2720 .0280 0 1 0
6.8000 6.8143 -.0143 0 -1 2
6.3000 6.2963 .0037 -1 0 1
6.0000 6.0194 -.0194 1 0 1
5.8000 5.7928 .0072 -1 0 2
5.5000 5.5011 -.0011 0 1 3
5.3500 5.3421 .0079 1 -1 1
5.1000 5.1040 -.0040 -1 1 2
4.9000 4.9023 -.0023 1 -1 2
4.7000 4.6964 .0036 1 0 3
4.6500 4.6500 .0000 -1 -1 1
4.5000 4.4999 .0001 1 1 1
A= 6.5171 DA= .0007
B= 8.410 DB= .001
C= 22.908 DC= .007
GAMMA=100.211 DGAMMA= .002
BETA = 94.679 DBETA = .005
ALPHA= 91.202 DALPHA= .007
V= 1231
9. 34-1646
C18H25BU
Triklin
Dexp Dcal d(D) h k l
11.0510 11.0546 -.0036 0 0 1
7.1950 7.1934 .0016 1 0 0
6.3700 6.3699 .0001 0 -2 1
5.1250 5.1245 .0005 -1 1 1
4.7450 4.7453 -.0003 1 -2 2
4.1900 4.1903 -.0003 -1 -2 1
3.8010 3.8004 .0006 2 -1 1
3.5330 3.5330 .0000 0 -2 3
3.0580 3.0582 -.0002 2 -2 3
2.5350 2.5350 .0000 1 3 3
1.9770 1.9770 -.0000 0 6 2
1.9170 1.9170 .0000 -3 -3 1
1.6100 1.6100 .0000 -4 -2 1
1.5650 1.5650 .0000 2 -7 6
A= 7.61214 DA= .00002
B= 14.267 DB= .001
C= 11.7422 DC= .0001
GAMMA=103.001 DGAMMA= .005
BETA = 73.4693 DBETA = .0006
ALPHA=103.901 DALPHA= .008
V= 1169.86
10. 34-1647
C18H21BrU
GRUPA 3
Dexp. Dcal. d(D) h k l
6.9590 6.9338 .0252 -1 0 1
5.2610 5.2665 -.0055 0 0 2
3.9300 3.9347 -.0047 2 0 0
3.9300 3.9259 .0041 -2 0 1
3.4860 3.4851 .0009 2 0 1
2.6140 2.6142 -.0002 -2 1 3
2.1070 2.1066 .0004 0 0 5
2.1070 2.1071 -.0001 2 2 2
1.8690 1.8689 .0001 -4 1 2
1.8490 1.8490 .0000 3 1 3
1.6430 1.6430 .0000 1 2 5
a= 8.0012 b=6.1100 c=10.709 beta=100.409
da=.0006 db=.0007 dc=.001 dbet=.006
V= 515
Triklin
Dexp. Dcal. d(D) h k l
6.9590 6.9590 .0000 -1 -1 0
5.2610 5.2609 .0001 0 -1 1
3.9300 3.9300 .0000 -4 -1 0
3.4860 3.4860 .0000 5 0 0
3.4860 3.4840 .0020 -4 0 1
2.6140 2.6140 .0000 -6 0 1
2.1070 2.1070 .0000 -8 -1 1
2.1070 2.1062 .0008 5 0 2
1.8690 1.8690 .0000 -8 1 1
1.8490 1.8490 .0000 -2 2 2
A= 17.60282 DA= .00005
B= 7.71600 DB= .00005
C= 5.80268 DC= .00002
GAMMA= 82.3830 DGAMMA= .0001
BETA = 94.9213 DBETA = .0007
ALPHA=109.418 DALPHA= .001
V= 736.0
11. 34-1648
C18H21ClU
Triklin
Dexp. Dcal. d(D) h k l
7.0810 7.0810 .0000 2 0 0
6.2800 6.2800 .0000 1 -2 0
5.4470 5.4477 -.0007 0 0 1
5.0050 5.0046 .0004 -1 0 1
3.9910 3.9910 .0000 0 -3 0
3.4860 3.4857 .0003 -3 0 1
2.6380 2.6385 -.0005 2 -2 2
2.3250 2.3246 .0004 -5 3 1
2.1040 2.1040 .0000 -4 1 2
1.9500 1.9508 -.0008 5 -6 0
1.9500 1.9496 .0004 6 -2 2
1.7590 1.7590 .0000 3 -3 3
1.6050 1.6048 .0002 -6 4 2
A= 15.0259 DA= .0006
B= 12.843 DB= .001
C= 5.544 DC= .001
GAMMA=109.343 DGAMMA= .002
BETA = 84.04 DBETA = .02
ALPHA=100.34 DALPHA= .02
V= 992
Triklin
Dexp Dcal d(D) h k l
7.0810 7.0803 .0007 -1 0 1
6.2800 6.2815 -.0015 0 1 1
5.4470 5.4443 .0027 1 0 1
5.0050 5.0029 .0021 0 -1 1
3.9910 3.9926 -.0016 2 1 1
3.4860 3.4875 -.0015 -1 2 1
2.6380 2.6385 -.0005 -1 0 3
2.3250 2.3249 .0001 1 0 3
2.1040 2.1040 .0000 2 4 0
1.9500 1.9499 .0001 2 3 3
1.7590 1.7590 .0000 -5 -2 3
1.6050 1.6050 -.0000 6 3 1
A= 10.95 DA= .01
B= 8.554 DB= .009
C= 8.013 DC= .002
GAMMA= 74.72 DGAMMA= .08
BETA =102.38 DBETA = .09
ALPHA= 81.11 DALPHA= .09
V= 689.1
12. 34-1649
C3H7NO*UO2C2O4
Triklin
Dexp Dcal d(D) h k l
7.5800 7.5785 .0015 1 1 0
7.0800 7.0741 .0059 -1 0 1
6.7000 6.7001 -.0001 -1 -2 1
6.4400 6.4385 .0015 -1 1 0
5.8300 5.8240 .0060 -1 1 1
4.8700 4.8800 -.0100 0 -1 2
4.7400 4.7370 .0030 -1 0 2
4.3500 4.3455 .0045 -1 -4 1
4.1800 4.1774 .0026 0 -4 1
4.0800 4.0825 -.0025 0 -3 2
3.8300 3.8289 .0011 0 2 2
3.6300 3.6309 -.0009 -1 2 2
A= 8.356 DA= .001
B= 17.97086 DB= .00004
C= 10.484 DC= .003
GAMMA= 72.78 DGAMMA= .01
BETA =110.98 DBETA = .02
ALPHA=106.99 DALPHA= .02
V= 1373
13. 34-1650
C5H7NO7U
Triklin
Dexp Dcal d(D) h k l
7.6400 7.6220 .0180 0 1 1
7.1400 7.1199 .0201 0 -1 1
5.8700 5.8766 -.0066 -1 -1 1
5.4400 5.4435 -.0035 1 0 1
5.0200 5.0113 .0087 0 -2 1
4.9600 4.9670 -.0070 1 -1 1
4.3700 4.3631 .0069 0 1 2
4.2100 4.2067 .0033 0 3 0
4.1100 4.1104 -.0004 -2 0 1
3.8400 3.8390 .0010 2 1 0
3.6100 3.6071 .0029 1 0 2
3.5600 3.5600 .0000 0 -2 2
A= 8.423 DA= .003
B= 12.674 DB= .002
C= 9.366 DC= .005
GAMMA= 93.32 DGAMMA= .06
BETA =104.20 DBETA = .07
ALPHA= 85.21 DALPHA= .01
V= 965