1. 33-0380
CsUO2{PO3}3
Rombik
Groupa 17
Dexp. Dcal. d(D) h k l
6.4000 6.4224 -.0224 0 0 3
5.7000 5.7026 -.0026 0 1 0
5.5000 5.4681 .0319 0 1 1
5.4500 5.4681 -.0181 0 1 1
5.4000 5.3934 .0066 1 1 0
4.8000 4.7992 .0008 3 0 2
4.2000 4.1927 .0073 3 0 3
4.1500 4.1512 -.0012 4 0 0
3.8500 3.8534 -.0034 0 0 5
3.4900 3.4863 .0037 4 0 3
3.3800 3.3780 .0020 3 1 3
3.3500 3.3561 -.0061 4 1 0
a=16.60 b= 5.703 c=19.27
da= .02 db= .003 dc= .01
V=1824
Triklin
Dexp Dcal d(D) h k l
6.4000 6.3988 .0012 0 3 0
5.7000 5.6966 .0034 -1 0 1
5.5000 5.5025 -.0025 1 2 0
5.4500 5.4483 .0017 0 2 1
5.4000 5.4029 -.0029 -1 2 0
4.8000 4.7991 .0009 0 4 0
4.2000 4.1982 .0018 0 -4 1
4.1500 4.1495 .0005 1 1 1
3.8500 3.8508 -.0008 -1 4 0
3.4900 3.4908 -.0008 -1 -2 2
3.3800 3.3798 .0002 -2 0 1
3.3500 3.3503 -.0003 1 5 0
A= 6.8989 DA= .0004
B= 19.3363 DB= .0003
C= 7.46978 DC= .00001
GAMMA= 87.0457 DGAMMA= .0002
BETA =106.1871 DBETA = .0001
ALPHA= 96.8117 DALPHA= .0008
V= 950.1
2. 33-0836
LiVUO6
Rombik
Grupa 16
Dexp. Dcal. d(D) h k l
8.1500 8.1333 -.0167 2 1 0
6.5500 6.5566 .0066 2 2 0
6.4000 6.3974 -.0026 0 3 0
5.2300 5.2103 -.0197 2 3 0
4.3800 4.3717 -.0083 4 1 0
4.1000 4.1073 .0073 1 2 1
3.8200 3.8186 -.0014 2 2 1
3.7900 3.7864 -.0036 0 3 1
3.7300 3.7439 .0139 3 4 0
3.3000 3.2995 -.0005 1 4 1
3.2000 3.1987 -.0013 0 6 0
3.2000 3.2000 .0000 3 3 1
a= 17.96 b= 19.19 c= 4.70
da=.03 db=4.28 dc= .01
V= 1619
Triklin
Dexp Dcal d(D) h k l
8.1500 8.1513 -.0013 1 0 0
6.5500 6.5524 -.0024 0 1 0
6.4000 6.4002 -.0002 -1 0 1
5.2300 5.2383 -.0083 0 0 2
4.3800 4.3854 -.0054 -1 0 2
4.1000 4.0988 .0012 2 1 0
3.8200 3.8188 .0012 -1 -1 2
3.7900 3.7847 .0053 -2 0 1
3.7300 3.7327 -.0027 -2 -1 1
3.3000 3.3052 -.0052 1 -1 2
3.2000 3.2001 -.0001 -2 0 2
3.1300 3.1274 .0026 -2 -1 2
A= 8.612 DA= .007
B= 6.950 DB= .004
C= 10.53 DC= .02
GAMMA= 71.20 DGAMMA= .02
BETA = 87.6 DBETA = .1
ALPHA= 84.32 DALPHA= .08
V= 593.6
3. 35-1135
RbUO2{PO3}3
Triklin
Dexp Dcal d(D) h k l
8.5000 8.5087 -.0087 -1 0 1
7.8000 7.8006 -.0006 0 1 1
7.5000 7.5065 -.0065 0 -1 1
6.7000 6.6925 .0075 -1 -1 1
6.5000 6.5037 -.0037 -1 2 1
5.6000 5.6049 -.0049 0 -2 1
5.3000 5.3054 -.0054 -2 1 1
5.1000 5.0984 .0016 -2 0 1
4.9500 4.9444 .0056 -1 1 2
4.6000 4.5965 .0035 1 -2 1
4.4500 4.4518 -.0018 0 0 2
4.4000 4.4001 -.0001 -2 1 2
A= 10.66969 DA= .00001
B= 15.5847 DB= .0009
C= 10.015 DC= .001
GAMMA=106.27 DGAMMA= .02
BETA =117.14 DBETA = .02
ALPHA= 80.504 DALPHA= .003
V= 1421.5
4. 33-1300
Na3UO2F4
Triklin
Dexp Dcal d(D) h k l
4.9300 4.9293 .0007 1 1 1
4.8500 4.8508 -.0008 1 1 0
4.7600 4.7606 -.0006 1 -1 1
4.5700 4.5715 -.0015 2 0 1
4.3600 4.3608 -.0008 1 -1 2
4.1700 4.1672 .0028 1 1 3
3.6700 3.6693 .0007 -2 0 2
3.6200 3.6204 -.0004 2 1 1
3.2200 3.2197 .0003 2 -1 3
3.1500 3.1505 -.0005 0 1 5
3.1300 3.1302 -.0002 2 1 4
3.0100 3.0099 .0001 1 0 6
A= 9.1481 DA= .0006
B= 5.8264 DB= .0001
C= 18.2445 DC= .0009
GAMMA= 89.21 DGAMMA= .01
BETA = 77.151 DBETA = .004
ALPHA= 84.89 DALPHA= .01
V= 944.3
Triklin
Dexp. Dcal. d(D) h k l
4.9300 4.9203 .0097 1 -3 0
4.8500 4.8498 .0002 0 -3 0
4.7600 4.7579 .0021 2 -2 0
4.5700 4.5683 .0017 -1 0 1
4.3600 4.3606 -.0006 -2 -1 0
4.1700 4.1676 .0024 0 -2 1
3.6700 3.6689 .0011 -2 -2 0
3.6200 3.6195 .0005 -2 0 1
3.2200 3.2203 -.0003 2 1 1
3.1500 3.1508 -.0008 -1 -4 0
3.1300 3.1293 .0007 2 -3 1
3.0100 3.0093 .0007 -1 4 1
A= 10.3599 DA= .0008
B= 15.123 DB= .005
C= 5.026 DC= .002
GAMMA=105.80 DGAMMA= .04
BETA = 92.45 DBETA = .02
ALPHA= 90.341 DALPHA= .007
V= 756.9
5. 33-1412
C4H6O5U
Triklin
Dexp Dcal d(D) h k l
10.5000 10.5183 -.0183 1 0 0
9.7400 9.7493 -.0093 0 1 1
6.8400 6.8590 -.0190 0 -1 1
6.2200 6.2353 -.0153 -1 1 1
5.7200 5.7154 .0046 0 1 2
5.4400 5.4432 -.0032 2 0 1
5.4000 5.3953 .0047 2 1 1
5.3500 5.3434 .0066 -1 -1 1
5.0700 5.0767 -.0067 1 2 2
4.9900 4.9951 -.0051 -1 2 0
4.5700 4.5666 .0034 2 -1 1
4.5500 4.5492 .0008 2 0 2
A= 11.22357 DA= .00002
B= 12.528 DB= .001
C= 12.298 DC= .005
GAMMA= 80.41 DGAMMA= .03
BETA = 69.73 DBETA = .03
ALPHA= 68.23 DALPHA= .03
V= 1505
6. 33-1413
beta-{UO2}3{AsO4}2
Rombik
Groupa 32,55
Dexp. Dcal. d(D) h k l
7.2000 7.1876 .0124 1 1 0
4.9500 4.9498 .0002 1 2 0
3.6100 3.6136 -.0036 1 3 0
3.5500 3.5500 .0000 0 0 1
2.8100 2.8100 .0000 1 4 0
a= 9.052 b=11.824 c= 3.55
da= .001 db= .001 dc= .001
V=380.0
7. 33-1414
alfa-{UO2}{AsO4}2
Rombik
Grupa 16
Dexp. Dcal. d(D) h k l
7.0500 7.0477 -.0023 0 1 0
5.6000 5.6020 .0020 0 0 2
4.8500 4.8458 -.0042 1 0 1
4.2700 4.2736 .0036 1 1 0
2.8500 2.8500 -.0000 1 2 1
a= 5.375 b= 7.048 c=11.204
da=.003 db=.002 dc= .004
V= 424.4
8. 33-1415
alfa-UO2{AsO3}2
Rombik
Grupa 16
Dexp. Dcal. d(D) h k l
4.4300 4.4329 .0029 0 0 1
4.2300 4.2415 .0115 1 2 0
4.0700 4.0709 .0009 0 1 1
3.5800 3.5778 -.0022 1 1 1
3.0300 3.0300 .0000 2 2 0
a= 7.500 b=10.29 c=4.432898
da=.008 db=.02 dc=.02
V= 342.0
9. 33-1416
{UO2}2As2O7
Rombik
Grupa 16
Dexp. Dcal. d(D) h k l
8.6000 8.5823 -.0177 0 0 1
6.4000 6.4270 .0270 0 2 0
5.9000 5.8986 -.0014 1 1 0
3.6000 3.6000 .0000 1 3 0
3.4700 3.4700 .0000 1 1 2
a= 6.64 b= 12.85 c= 8.58
da=.03 db=.03 dc=.01
V= 732.4
Triklin
Dexp Dcal d(D) h k l
8.6000 8.5817 .0183 0 0 1
6.4000 6.4047 -.0047 0 2 0
5.9000 5.8976 .0024 1 1 0
3.6000 3.5999 .0001 1 -3 0
3.4700 3.4700 .0000 1 1 2
A= 6.66 DA= .01
B= 12.81 DB= .03
C= 8.582 DC= .001
GAMMA= 90.2 DGAMMA= .1
BETA = 90. DBETA = .02
ALPHA= 90. DALPHA= .00006
V= 731.6
10. 33-1417
beta-UO2{AsO3}2
Rombik
Grupa 16
Dexp. Dcal. d(D) h k l
7.0000 7.0116 .0116 2 0 0
4.1300 4.1268 -.0032 1 1 1
4.0800 4.0697 -.0103 2 1 0
3.6600 3.6583 -.0017 2 0 2
3.1700 3.1702 .0002 1 1 2
a=14.02 b= 4.998 c= 8.58
da=.02 db= .007 dc= .01
V= 601.1
11. 33-1418
{UO2}3{AsO4}2*11H2O
Rombik
Grupa 16
Dexp. Dcal. d(D) h k l
11.6000 11.5550 -.0450 0 1 0
5.7700 5.7775 .0075 0 2 0
4.6300 4.6306 .0006 0 1 2
3.5700 3.5711 .0011 1 1 0
3.5200 3.5199 -.0001 1 0 1
a=3.7549 b=11.55 c= 10.108
da=.0004 db=.04 dc=.009
V= 438.6
12. 33-1419
{UO2}3{AsO4}2*H2O
Rombik
Grupa 20
Dexp. Dcal. d(D) h k l
4.9000 4.8973 .0027 1 0 2
3.5500 3.5500 .0000 0 1 1
3.3700 3.3765 -.0065 2 0 0
3.0500 3.0502 -.0002 2 0 2
2.9000 2.9003 -.0003 0 1 3
a= 6.753 b= 3.666 c=14.225
da= .001 db= .001 dc= .001
V=352.2
13. 33-1420
UO3*0.75CO2*0.68H2O
Triklin
Dexp Dcal d(D) h k l
6.4900 6.4911 -.0011 0 1 0
4.5400 4.5400 .0000 -1 -1 2
4.2600 4.2599 .0001 0 -1 2
3.8400 3.8399 .0001 1 0 2
3.4000 3.4010 -.0010 -1 -2 1
3.2000 3.1986 .0014 0 -2 1
2.6100 2.6102 -.0002 -2 -2 3
2.4800 2.4795 .0005 0 -1 4
2.4200 2.4199 .0001 2 -1 2
2.2900 2.2897 .0003 -1 -3 1
2.1300 2.1300 .0000 0 -2 4
2.0500 2.0496 .0004 0 0 5
A= 8.316 DA= .001
B= 6.878 DB= .001
C= 10.7803 DC= .0007
GAMMA= 71.76 DGAMMA= .01
BETA =106.950 DBETA = .002
ALPHA=101.117 DALPHA= .001
V= 556.7
14. 33-1421
UO3*0.156CO2*0.36H2O
Triklin
Dexp Dcal d(D) h k l
8.6400 8.6395 .0005 1 0 1
7.0300 7.0310 -.0010 0 1 1
4.1700 4.1698 .0002 1 0 3
3.4400 3.4406 -.0006 3 -1 1
2.6400 2.6399 .0001 3 -1 4
2.0900 2.0898 .0002 1 -1 6
2.0000 2.0003 -.0003 -4 -1 1
1.9600 1.9603 -.0003 4 -4 1
1.8000 1.7985 .0015 5 -5 5
1.7790 1.7791 -.0001 3 -5 1
1.7260 1.7264 -.0004 2 3 5
1.6890 1.6889 .0001 -2 5 2
A= 10.3362 DA= .0003
B= 9.089 DB= .001
C= 12.7628 DC= .0009
GAMMA=109.241 DGAMMA= .008
BETA = 74.040 DBETA = .001
ALPHA= 95.23 DALPHA= .01
V= 1088.4
15. 33-1422
UO3*0.31CO2*0.29H2O
Triklin
Dexp Dcal d(D) h k l
8.4800 8.4792 .0008 -1 0 1
4.3800 4.3806 -.0006 0 1 1
4.1300 4.1303 -.0003 0 -1 1
3.7800 3.7807 -.0007 2 1 0
3.3200 3.3212 -.0012 -1 0 3
3.1200 3.1212 -.0012 3 0 1
2.5500 2.5495 .0005 1 1 3
2.0900 2.0900 -.0000 -3 1 4
2.0100 2.0097 .0003 5 0 1
1.7320 1.7320 .0000 1 1 5
1.6830 1.6829 .0001 -2 -2 4
1.5590 1.5590 .0000 -1 -3 1
A= 11.431 DA= .001
B= 4.7757 DB= .0003
C= 9.9749 DC= .0007
GAMMA= 85.056 DGAMMA= .001
BETA =106.124 DBETA = .003
ALPHA= 87.332 DALPHA= .004
V= 519.8
16. 33-1423
UO3*0.85CO2*0.6H2O
Triklin
Dexp Dcal d(D) h k l
6.5900 6.5932 -.0031 -1 0 1
4.4300 4.4309 -.0009 1 1 1
4.1800 4.1792 .0008 -1 -1 1
3.7700 3.7697 .0003 -1 1 2
3.3400 3.3398 .0002 0 -1 2
3.1100 3.1099 .0001 0 1 3
2.5600 2.5602 -.0002 1 2 2
2.4400 2.4399 .0001 -3 0 2
2.3700 2.3698 .0002 2 2 1
2.2500 2.2500 -.0000 -2 2 1
2.1000 2.1000 -.0000 -1 -1 4
2.0100 2.0101 -.0001 -3 -1 3
A= 7.7882 DA= .0005
B= 5.8187 DB= .0007
C= 10.045 DC= .001
GAMMA= 86.067 DGAMMA= .005
BETA = 99.107 DBETA = .006
ALPHA= 78.29 DALPHA= .01
V= 437.7
17. 33-1425
UO2Cl2*H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
8.6600 8.6453 .0147 0 0 2
5.3000 5.3079 -.0079 3 0 0
5.0100 5.0095 .0005 2 1 1
4.8400 4.8352 .0048 2 1 0
4.3700 4.3691 .0009 -2 1 1
4.2100 4.2095 .0005 3 1 1
4.0000 4.0003 -.0003 3 1 0
3.7500 3.7473 .0027 2 1 4
3.2500 3.2499 .0001 -3 1 2
3.1400 3.1379 .0021 -4 0 2
3.0500 3.0482 .0018 5 1 2
2.9300 2.9308 -.0008 5 1 4
a= 17.65 b=6.09 c=19.17 beta=64.4
da=.05 db=.01 dc=.05 dbeta=.2
V= 1858
Triklin
Dexp Dcal d(D) h k l
8.6600 8.6531 .0069 1 0 0
5.3000 5.3111 -.0111 1 1 1
5.0100 5.0170 -.0070 1 -1 1
4.8400 4.8389 .0011 0 2 0
4.3700 4.3650 .0050 2 1 0
4.2100 4.2123 -.0023 0 -2 1
4.0000 4.0071 -.0071 2 1 1
3.7500 3.7521 -.0021 0 2 1
3.2500 3.2504 -.0004 1 1 2
3.1400 3.1402 -.0002 -2 -2 1
3.0500 3.0478 .0022 2 0 2
2.9300 2.9287 .0013 1 3 1
A= 9.1040 DA= .0005
B= 10.00368 DB= .00008
C= 7.0978 DC= .0005
GAMMA= 77.110 DGAMMA= .002
BETA = 78.494 DBETA = .001
ALPHA= 94.164 DALPHA= .002
V= 612.8
18. 33-1426
UO2HAsO4*H2O
Rombik
Grupa 16
Dexp. Dcal. d(D) h k l
10.2000 10.2080 .0080 1 0 0
5.8200 5.8296 .0096 0 1 1
4.4000 4.4012 .0012 2 1 0
3.0500 3.0496 -.0004 2 2 1
2.6200 2.6200 .0000 0 0 3
a= 10.208 b= 8.691 c= 7.8600
da=.008 db=.007 dc=.0001
V= 697.3
19. 33-1427
UO2H2P2O7
Rombik
Grupa 16
Dexp. Dcal. d(D) h k l
6.7500 6.7587 .0087 0 1 1
5.7000 5.7039 .0039 0 0 2
4.7200 4.7170 -.0030 0 1 2
3.4800 3.4777 -.0023 1 2 0
3.0000 3.0000 .0000 2 0 1
a= 6.2189 b=8.39 c= 11.408
da=.0003 db=.01 dc=.007
V= 595.2
20. 33-1428
UO2HPO4*H2O
Rombik
Grupa 16
Dexp. Dcal. d(D) h k l
5.2200 5.2276 .0076 2 0 1
4.2500 4.2455 -.0045 2 0 2
4.2000 4.2008 .0008 0 0 3
3.5400 3.5390 -.0010 0 1 0
2.9800 2.9801 .0001 1 1 2
a= 11.49 b=3.5390 c= 12.602
da=.02 db= .0008 dc=.002
V= 512.5
21. 33-1430
gamma-UO2{PO3}2
Rombik
Grupa 16
Dexp. Dcal. d(D) h k l
7.9000 7.8935 -.0065 1 0 1
5.9000 5.9027 .0027 2 0 0
4.4200 4.4195 -.0005 0 1 1
3.6900 3.6897 -.0003 3 0 1
3.4300 3.4300 .0000 1 1 2
a= 11.805340 b=4.861 c=10.62
da=.001 db=.006 dc= .01
V= 609.1
22. 33-1431
beta-UO2{PO3}2
Rombik
Grupa 16
Dexp. Dcal. d(D) h k l
6.0500 6.0415 -.0085 0 1 0
5.4500 5.4570 .0070 0 1 1
4.2500 4.2389 -.0111 0 0 3
4.0500 4.0500 .0000 1 0 0
3.4700 3.4700 -.0000 0 1 3
a=4.0500 b=6.0415 c=12.717
da=.0001 db=.008 dc=.008
V= 311.15
23. 33-1435
C14H10N4O8U
Triklin
Dexp Dcal d(D) h k l
8.5300 8.5302 -.0002 1 0 0
7.8300 7.8373 -.0073 0 1 1
7.2900 7.2726 .0174 1 -1 1
7.1500 7.1570 -.0070 0 2 0
6.4900 6.4884 .0016 -1 1 1
6.3200 6.3214 -.0014 -1 2 0
6.0600 6.0515 .0085 0 0 2
5.9200 5.9195 .0005 0 -2 2
5.3100 5.3078 .0022 0 2 1
5.1000 5.1071 -.0071 1 -2 2
5.0700 5.0736 -.0036 -1 2 1
4.9700 4.9650 .0050 1 -3 1
A= 8.81 DA= .01
B= 16.01 DB= .01
C= 13.18212 DC= .00001
GAMMA=103.16 DGAMMA= .07
BETA = 90.74 DBETA = .02
ALPHA=112.514 DALPHA= .002
V= 1662
24. 33-1947
C6H16N2O6U
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.7530 5.7576 -.0046 1 1 0
3.8270 3.8248 .0022 1 0 3
3.4660 3.4643 .0017 -1 1 3
3.3310 3.3320 -.0010 1 1 3
3.2090 3.2095 -.0005 2 0 3
2.8310 2.8319 -.0009 -2 2 1
2.4420 2.4420 .0000 4 1 1
2.3650 2.3653 -.0003 0 1 5
2.3320 2.3316 .0004 2 2 3
2.2270 2.2265 .0005 0 3 1
2.0790 2.0794 -.0004 1 3 2
2.0490 2.0490 .0000 -4 2 2
a= 10.911 b= 6.786 c= 12.655 beta= 94.42
da=.001 db=.001 dc=.007 dbeta=.02
V= 934.2
Triklin
Dexp Dcal d(D) h k l
5.7530 5.7549 -.0019 -1 0 1
3.8270 3.8271 -.0001 1 2 0
3.4660 3.4659 .0001 -1 -2 1
3.3310 3.3321 -.0011 0 2 1
3.2090 3.2100 -.0010 -1 0 2
2.8310 2.8309 .0001 2 -1 2
2.4420 2.4416 .0004 -3 -1 2
2.3650 2.3649 .0001 -2 -3 1
2.3320 2.3324 -.0004 4 2 0
2.2270 2.2271 -.0001 0 -3 2
2.0790 2.0789 .0001 3 2 2
2.0490 2.0489 .0001 3 3 1
A= 11.440 DA= .003
B= 8.1868 DB= .0005
C= 6.7562 DC= .0008
GAMMA= 90.50 DGAMMA= .01
BETA = 89.07884 DBETA = .00008
ALPHA= 95.9660 DALPHA= .0005
V= 629.4
25. 33-1948
C30H19Br6N3O6U
Triklin
Dexp Dcal d(D) h k l
10.4000 10.3951 .0049 1 0 0
8.8500 8.8423 .0077 1 1 0
7.9000 7.9116 -.0116 -1 0 1
6.8600 6.8594 .0006 0 1 1
6.3000 6.3002 -.0002 -1 1 0
5.1900 5.1975 -.0075 2 0 0
4.9200 4.9162 .0038 1 -1 2
4.5300 4.5311 -.0011 1 1 2
4.3800 4.3806 -.0006 1 2 1
4.1800 4.1819 -.0019 1 -2 1
3.9900 3.9909 -.0009 2 0 2
3.7800 3.7800 .0000 2 1 2
3.6000 3.5991 .0009 -1 2 1
3.4200 3.4196 .0004 3 1 1
A= 11.056 DA= .006
B= 11.32912 DB= .00003
C= 13.0243 DC= .0003
GAMMA= 70.10 DGAMMA= .02
BETA = 95.86 DBETA = .07
ALPHA=108.85 DALPHA= .1
V= 1451.6
26. 33-1949
C21H14Br4N2O5U
Triklin
Dexp Dcal d(D) h k l
9.5400 9.5337 .0063 -1 1 0
8.8300 8.8201 .0099 0 1 1
8.2500 8.2530 -.0030 0 -1 1
6.5500 6.5493 .0007 0 2 0
5.5000 5.4988 .0012 1 -2 1
5.0200 5.0171 .0029 1 0 2
4.8200 4.8226 -.0026 1 -1 2
4.3500 4.3501 -.0001 2 1 0
3.9800 3.9798 .0002 0 -3 1
3.8300 3.8303 -.0003 1 2 2
3.6100 3.6102 -.0002 -1 3 2
3.4900 3.4899 .0001 -1 1 3
A= 10.704 DA= .002
B= 13.725 DB= .002
C= 11.252 DC= .002
GAMMA=106.97 DGAMMA= .02
BETA = 88.45 DBETA = .03
ALPHA= 86.780 DALPHA= .006
V= 1577.0
27. 33-1950
C30H19Cl6N3O6U
Triklin
Dexp Dcal d(D) h k l
9.9600 9.9606 -.0006 0 1 1
8.6100 8.6136 -.0036 0 -1 1
7.4800 7.4796 .0004 -1 -1 1
6.4500 6.4512 -.0012 1 0 1
5.4300 5.4294 .0006 1 -1 1
4.9800 4.9803 -.0003 0 2 2
4.4200 4.4199 .0001 0 -3 1
3.8500 3.8517 -.0017 0 0 3
3.7300 3.7301 -.0001 -2 1 2
3.6400 3.6400 .0000 2 3 1
3.3900 3.3900 -.0000 -1 -2 3
A= 9.4704 DA= .0001
B= 15.925 DB= .001
C= 11.8855 DC= .0004
GAMMA= 75.889 DGAMMA= .003
BETA =100.492 DBETA = .002
ALPHA= 84.3489 DALPHA= .0002
V= 1690.02
28. 33-1951
C21H14Cl4N205U
Triklin
Dexp Dcal d(D) h k l
9.9500 9.9529 -.0029 1 0 0
8.6200 8.6191 .0009 0 1 1
7.4900 7.4893 .0007 0 -1 1
5.4300 5.4299 .0001 -2 1 0
4.9600 4.9599 .0001 1 -1 2
4.7600 4.7601 -.0001 -2 2 0
4.4000 4.3999 .0001 -2 0 1
3.9000 3.9001 -.0001 0 0 3
3.6500 3.6500 -.0000 0 3 0
3.4100 3.4100 .0000 0 2 3
A= 10.900 DA= .001
B= 12.0300 DB= .0006
C= 11.8418 DC= .0008
GAMMA=113.189 DGAMMA= .007
BETA = 86.262 DBETA = .008
ALPHA= 84.1156 DALPHA= .0004
V= 1410.36
29. 33-1952
C8H20N2O6U
Triklin
Dexp Dcal d(D) h k l
7.3140 7.3119 .0021 1 1 1
7.0250 7.0252 -.0002 0 1 1
5.9850 5.9876 -.0026 0 -1 1
5.2400 5.2411 -.0011 -1 0 1
4.8010 4.8015 -.0005 -1 -1 1
4.4750 4.4735 .0015 0 2 1
4.2580 4.2580 .0000 0 1 2
3.3940 3.3938 .0002 2 -1 1
3.3560 3.3554 .0006 -2 -1 1
3.2140 3.2142 -.0002 2 3 1
3.0790 3.0790 -.0000 3 1 1
2.9710 2.9713 -.0003 -2 1 1
A= 9.2851 DA= .0002
B= 10.36598 DB= .00009
C= 9.63489 DC= .00008
GAMMA= 67.5746 DGAMMA= .0009
BETA = 67.742 DBETA = .001
ALPHA= 73.717 DALPHA= .001
V= 783.21
30. 34-1244
UO2H{PO3}3
Triklin
Dexp Dcal d(D) h k l
6.6300 6.6336 -.0036 1 0 0
6.2700 6.2681 .0019 0 -1 1
5.2000 5.2046 -.0046 1 0 1
4.6200 4.6104 .0096 -1 1 0
4.4400 4.4382 .0018 1 -1 1
4.1500 4.1485 .0015 0 -1 2
3.8900 3.8877 .0023 1 1 1
3.2100 3.2110 -.0010 -1 -2 1
3.1100 3.1103 -.0003 1 2 0
3.0000 2.9992 .0008 -2 -1 1
2.9100 2.9112 -.0012 -2 1 0
2.7800 2.7803 -.0003 0 0 3
A= 6.647 DA= .001
B= 7.150 DB= .002
C= 8.737 DC= .001
GAMMA= 86.334 DGAMMA= .009
BETA = 90.82 DBETA = .02
ALPHA=107.33 DALPHA= .01
V= 395.6