1. 32-0181
Ca2U{TeO3}5
Triklin
Dexp. Dcal. d(D) h k l
5.4300 5.4300 .0000 2 0 0
4.8200 4.8185 .0015 -1 -3 0
4.7700 4.7700 .0000 -2 -2 0
4.5700 4.5653 .0047 0 -2 1
4.0000 4.0000 .0000 -2 -3 0
3.8700 3.8672 .0028 0 -3 1
3.7900 3.7932 -.0032 1 2 1
3.7100 3.7103 -.0003 -1 -4 0
3.6300 3.6287 .0013 2 0 1
3.5700 3.5666 .0034 -2 1 1
3.3600 3.3585 .0015 1 -4 0
3.2800 3.2815 -.0015 -1 -4 1
A= 11.05189 DA= .00021
B= 15.27199 DB= .00298
C= 5.25462 DC= .00422
GAMMA= 80.01753 DGAMMA= .00670
BETA = 95.27975 DBETA = .00802
ALPHA= 98.90135 DALPHA= .04819
V= 861.0
2. 32-0183
Ca3{UO2}{TeO3}4
Triklin
Dexp Dcal d(D) h k l
6.3000 6.2901 .0099 0 2 0
5.5300 5.5226 .0074 -1 2 0
5.1600 5.1689 -.0089 1 2 0
4.8100 4.8039 .0061 -2 1 0
4.5700 4.5656 .0044 2 1 0
4.0800 4.0836 -.0036 -2 2 0
3.9600 3.9606 -.0006 1 0 1
3.8000 3.8001 -.0001 2 2 0
3.3600 3.3614 -.0014 3 0 0
3.3000 3.2999 .0001 -1 2 1
3.2500 3.2499 .0001 2 -1 1
3.1900 3.1895 .0005 3 1 0
A= 10.20278 DA= .00002
B= 12.67847 DB= .00003
C= 4.11780 DC= .00003
GAMMA= 93.3998 DGAMMA= .0007
BETA = 82.344 DBETA = .001
ALPHA= 84.243 DALPHA= .001
V= 523.8
3. 32-0866
K2U7O22*xH2O
Triklin
Dexp Dcal d(D) h k l
7.4500 7.4496 .0004 1 0 0
3.6900 3.6894 .0006 -1 1 1
3.5700 3.5679 .0021 1 -1 1
3.5100 3.5103 -.0003 2 1 1
3.2100 3.2094 .0006 -2 0 1
3.1800 3.1769 .0031 1 1 3
2.8000 2.8012 -.0012 -2 1 0
2.5600 2.5601 -.0001 3 0 1
2.5450 2.5472 -.0022 1 2 0
2.4600 2.4596 .0004 3 0 2
2.3050 2.3047 .0003 -1 2 0
2.0470 2.0471 -.0001 2 2 4
A= 7.8958 DA= .0005
B= 5.396 DB= .003
C= 10.169 DC= .001
GAMMA= 76.634 DGAMMA= .007
BETA = 72.981 DBETA = .007
ALPHA= 73.707 DALPHA= .009
V= 392.3
4. 32-0964
Rb2{UO2}4O2{OH}2Br4*2H2O
Triklin
Dexp Dcal d(D) h k l
10.2800 10.2881 -.0081 1 0 0
9.8000 9.8045 -.0045 -1 1 0
6.6100 6.6122 -.0022 -1 1 1
6.0800 6.0824 -.0024 1 1 0
5.6600 5.6599 .0001 1 0 2
4.9300 4.9297 .0003 2 -1 2
4.4400 4.4395 .0005 -2 0 1
4.3100 4.3094 .0006 1 1 2
3.9860 3.9863 -.0003 1 0 3
3.8370 3.8369 .0001 1 -3 0
3.5150 3.5150 .0000 -1 0 3
3.4400 3.4401 -.0001 2 1 2
A= 11.993 DA= .003
B= 12.049 DB= .001
C= 12.692 DC= .001
GAMMA=119.20 DGAMMA= .02
BETA = 73.24 DBETA = .01
ALPHA=105.80 DALPHA= .02
V= 1513.9
5. 32-0965
Pb{UO2}4O2{Oh}2Cl4*2H2O
Triklin
Dexp Dcal d(D) h k l
10.2000 10.2116 -.0116 1 0 0
9.4500 9.4714 -.0214 1 1 0
6.5600 6.5567 .0033 0 0 1
6.0700 6.0695 .0005 -1 -1 1
5.5900 5.5967 -.0067 2 1 0
5.0400 5.0439 -.0039 -1 1 1
4.7400 4.7357 .0043 2 2 0
4.3300 4.3305 -.0005 -2 -2 1
3.8670 3.8664 .0006 -2 1 1
3.7380 3.7382 -.0002 1 3 0
3.8670 3.8664 .0006 -2 1 1
3.7380 3.7382 -.0002 1 3 0
A= 11.817 DA= .001
B= 11.29306 DB= .00007
C= 6.9087 DC= .00040
GAMMA= 65.2370 DGAMMA= .0003
BETA =108.02 DBETA = .01
ALPHA= 94.26 DALPHA= .01
V= 794.6
Dexp Dcal d(D) h k l
10.2000 10.1948 .0052 1 0 0
9.4500 9.4770 -.0270 0 1 0
6.5600 6.5549 .0051 -1 -1 1
6.0700 6.0735 -.0035 1 1 0
5.5900 5.5923 -.0023 0 -1 2
5.0400 5.0395 .0005 -1 0 2
4.7400 4.7385 .0015 0 2 0
4.3300 4.3282 .0018 1 -2 2
3.8670 3.8672 -.0002 1 2 0
3.7380 3.7390 -.0010 0 -1 3
3.3830 3.3825 .0005 0 0 3
3.2900 3.2903 -.0003 2 -3 1
A= 10.789 DA= .004
B= 10.813 DB= .002
C= 11.337 DC= .004
GAMMA=103.55 DGAMMA= .01
BETA = 96.85 DBETA = .02
ALPHA=112.96 DALPHA= .01
V= 1151.2
6. 32-0966
Rb4{UO2}4O2Cl8
Triklin
Dexp Dcal d(D) h k l
10.2000 10.2124 -.0124 0 1 1
8.2700 8.2662 .0038 0 -1 1
7.5200 7.5193 .0007 -1 1 1
6.0600 6.0675 -.0075 1 0 1
5.9800 5.9817 -.0017 -1 2 0
5.5400 5.5360 .0040 0 3 0
4.9300 4.9277 .0023 -1 2 2
4.6700 4.6685 .0015 1 3 0
4.1500 4.1520 -.0020 0 4 0
3.8400 3.8399 .0001 2 2 0
3.6800 3.6806 -.0006 -1 0 3
3.4800 3.4794 .0006 1 -2 2
A= 8.945 DA= .004
B= 17.083 DB= .002
C= 11.530 DC= .004
GAMMA= 93.28 DGAMMA= .02
BETA =104.80 DBETA = .04
ALPHA= 76.46 DALPHA= .04
V= 1656
7. 32-1091
Na0.5{UO2}0.25*2H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
9.1100 9.1141 -.0041 1 1 0
5.3000 5.3003 -.0003 -2 0 1
4.5200 4.5190 .0010 2 0 2
4.3700 4.3699 .0001 3 0 0
3.5000 3.4997 .0003 1 1 3
3.3900 3.3906 -.0006 2 0 3
2.9900 2.9899 .0001 2 2 3
2.9400 2.9400 .0000 -1 4 1
a= 13.2414 b=12.6797 c=11.0273 beta= 81.90
da=.0007 db=.0008 dc=.0007 dbeta=.01
V= 1833.0
8. 32-1131
Na6UMo4O18
Triklin
Dexp Dcal d(D) h k l
13.1000 13.0823 .0177 1 0 0
9.4000 9.4101 -.0101 0 1 1
8.7500 8.7585 -.0085 0 -1 1
7.0900 7.0875 .0025 -1 -1 2
6.8300 6.8314 -.0014 0 1 2
5.9800 5.9800 -.0000 -1 1 2
5.5800 5.5798 .0002 2 0 1
5.5300 5.5259 .0041 1 2 1
5.0700 5.0701 -.0001 0 1 3
4.9200 4.9221 -.0021 2 2 1
4.8000 4.7996 .0004 -2 1 0
4.7800 4.7799 .0001 3 1 0
A= 14.8775 DA= .0008
B= 11.901 DB= .002
C= 17.181 DC= .002
GAMMA= 66.12 DGAMMA= .02
BETA =105.455 DBETA = .003
ALPHA= 92.245 DALPHA= .001
V= 2672.6
9. 32-1191
Na{UO2}2F5*4H2O
Triklin
Dexp Dcal d(D) h k l
7.8400 7.8411 -.0011 0 -1 1
6.2900 6.2902 -.0002 1 -1 1
4.1400 4.1403 -.0003 0 -3 1
4.0400 4.0414 -.0014 -1 -2 1
4.0000 4.0019 -.0019 1 -3 1
3.7500 3.7502 -.0002 -2 1 0
3.5900 3.5895 .0005 2 1 1
3.5300 3.5301 -.0001 0 3 2
3.4800 3.4799 .0001 -1 2 2
3.4000 3.4000 .0000 0 4 1
3.3100 3.3100 .0000 1 0 3
3.2800 3.2799 .0001 -2 1 1
A= 7.772 DA= .002
B= 14.258 DB= .001
C= 10.1571 DC= .0006
GAMMA= 96.751 DGAMMA= .004
BETA = 76.92 DBETA = .01
ALPHA= 87.71 DALPHA= .01
V= 1086.1
10. 32-1192
Na3{UO2}2F7*2H2O
Triklin
Dexp Dcal d(D) h k l
7.4400 7.4302 .0098 -1 0 1
6.2300 6.2279 .0021 0 1 1
5.9100 5.9073 .0027 0 -1 1
5.5600 5.5506 .0094 -1 -1 1
5.3700 5.3910 -.0210 1 0 1
4.3000 4.2855 .0145 -2 1 0
4.0400 4.0321 .0079 -1 2 1
3.7800 3.7807 -.0007 0 1 2
3.7400 3.7434 -.0034 -1 -1 2
3.4300 3.4352 -.0052 -2 2 1
3.3800 3.3828 -.0028 2 -1 1
3.2300 3.2300 .0000 2 2 0
A= 10.035 DA= .007
B= 9.152 DB= .001
C= 8.5626 DC= .0007
GAMMA= 93.36 DGAMMA= .03
BETA =108.49 DBETA = .05
ALPHA= 86.057 DALPHA= .001
V= 743.5
Triklin
Dexp Dcal d(D) h k l
7.4400 7.4424 -.0024 2 1 0
6.2300 6.2339 -.0039 3 0 0
5.9100 5.9067 .0033 1 0 1
5.5600 5.5575 .0025 -2 1 1
5.3700 5.3695 .0005 2 2 0
4.3000 4.3043 -.0043 4 1 0
4.0400 4.0380 .0020 2 3 0
3.7800 3.7807 -.0007 -4 2 1
3.7400 3.7403 -.0003 5 0 0
3.4300 3.4280 .0020 -2 4 0
3.3800 3.3797 .0003 -4 3 1
3.2300 3.2313 -.0013 -2 -3 1
A= 18.909 DA= .003
B= 14.510 DB= .004
C= 6.5489 DC= .0006
GAMMA= 97.18 DGAMMA= .02
BETA = 95.93 DBETA = .01
ALPHA= 78.397 DALPHA= .003
V= 1741
11. 32-1194
NaUO2P2O7*5H2O
Triklin
Dexp Dcal d(D) h k l
7.4400 7.4364 .0036 0 1 1
6.2300 6.2302 -.0002 0 -1 1
5.9100 5.9099 .0001 -1 0 1
5.5600 5.5575 .0025 -1 1 1
5.3700 5.3710 -.0010 0 2 0
4.3000 4.3028 -.0028 0 1 2
4.0400 4.0424 -.0024 -2 1 0
3.7800 3.7794 .0006 -1 1 2
3.7400 3.7391 .0009 2 1 1
3.4300 3.4293 .0007 -2 2 0
3.3800 3.3800 -.0000 -1 -1 2
3.2300 3.2301 -.0001 2 2 1
A= 8.576 DA= .003
B= 10.9268 DB= .0004
C= 8.842 DC= .002
GAMMA= 92.24 DGAMMA= .04
BETA = 86.84 DBETA = .01
ALPHA= 79.84 DALPHA= .02
V= 813.2
12. 32-1195
Na2UO2P2O7*5H2O
Triklin
Dexp Dcal d(D) h k l
5.7900 5.7820 .0080 0 1 1
5.3700 5.3742 -.0042 -1 2 0
5.1700 5.1619 .0081 0 -1 1
4.1400 4.1400 .0000 1 0 1
4.0800 4.0837 -.0037 -1 3 0
3.4800 3.4784 .0016 1 -2 1
3.1100 3.1086 .0014 0 4 1
3.0900 3.0889 .0011 -2 3 0
3.0800 3.0794 .0006 -1 0 2
2.9900 2.9908 -.0008 1 -3 1
2.8900 2.8910 -.0010 0 2 2
2.8100 2.8101 -.0001 -2 1 2
A= 7.93 DA= .01
B= 13.72 DB= .01
C= 6.3407 DC= .0003
GAMMA=101.5 DGAMMA= .1
BETA =107.74 DBETA = .04175
ALPHA= 78.36 DALPHA= .01
V= 635.4
13. 32-1346
Ti10U{PW11O39}2*21H2O
Triklin
Dexp. Dcal. d(D) h k l
5.6500 5.6500 .0000 -1 -2 0
4.9700 4.9695 .0005 1 -1 1
4.7600 4.7600 .0000 3 0 0
4.5000 4.5007 -.0007 1 -2 1
4.3000 4.3000 .0000 -2 -2 0
4.1400 4.1409 -.0009 -1 -3 0
3.8500 3.8510 -.0010 1 -3 1
3.5200 3.5197 .0003 -2 -2 1
3.3800 3.3802 -.0002 3 -3 1
3.2500 3.2499 .0001 1 -4 1
3.1800 3.1812 -.0012 -3 4 1
3.1100 3.1103 -.0003 0 -4 1
A= 15.831 DA= .003
B= 16.289 DB= .006
C= 5.498 DC= .001
GAMMA=115.01 DGAMMA= .02
BETA = 95.235 DBETA = .007
ALPHA= 89.65 DALPHA= .02
V= 1279
14. 32-1396
H0.1{UO2}0.95*5.8H2O
Triklin
Dexp Dcal d(D) h k l
10.5000 10.4855 .0145 1 0 0
6.8000 6.8124 -.0124 0 1 1
6.2300 6.2400 -.0100 0 -1 1
5.9000 5.9016 -.0016 1 1 0
5.2100 5.2099 .0001 -2 1 0
5.0100 5.0158 -.0058 -2 0 1
4.5100 4.5062 .0038 -1 2 0
4.3900 4.3857 .0043 -1 2 1
4.0800 4.0754 .0046 -2 1 2
3.9800 3.9842 -.0042 -2 2 1
3.6300 3.6290 .0010 -3 1 0
3.4700 3.4711 -.0011 -2 2 2
A= 11.226 DA= .003
B= 9.190 DB= .001
C= 10.091 DC= .008
GAMMA=108.266 DGAMMA= .003
BETA =102.50 DBETA = .04
ALPHA= 81.406 DALPHA= .006
V= 961.2
15. 32-1404
U*SiO4
Triklin
Dexp Dcal d(D) h k l
7.6700 7.6716 -.0016 1 0 0
6.6000 6.5934 .0066 -1 1 0
4.9800 4.9805 -.0005 -1 0 1
4.7300 4.7305 -.0005 1 1 0
3.8300 3.8298 .0002 1 -1 2
3.3700 3.3703 -.0003 2 -1 2
3.2200 3.2203 -.0003 1 2 1
3.1400 3.1400 .0000 -2 0 1
2.9780 2.9780 .0000 -2 2 1
2.9030 2.9029 .0001 0 0 3
2.7100 2.7102 -.0002 -1 3 0
2.1280 2.1279 .0001 3 -2 3
A= 8.468 DA= .001
B= 8.188 DB= .002
C= 9.320 DC= .002
GAMMA=105.67 DGAMMA= .02
BETA = 73.021 DBETA = .005
ALPHA= 83.26 DALPHA= .02
V= 581.4
16. 32-1408
UO2SO4*2H2O
Triklin
Dexp Dcal d(D) h k l
9.2100 9.2187 -.0087 0 1 1
8.5800 8.5857 -.0057 0 -1 1
7.1300 7.1206 .0094 1 1 0
5.6400 5.6494 -.0094 0 -1 2
5.1500 5.1502 -.0002 1 0 2
4.7900 4.7886 .0014 -1 -2 1
4.5500 4.5512 -.0012 -1 -1 2
4.5300 4.5324 -.0024 1 2 2
4.3300 4.3297 .0003 1 -1 2
4.2700 4.2661 .0039 0 1 3
4.0400 4.0404 -.0004 -1 2 0
3.8600 3.8572 .0028 -1 2 1
A= 7.550 DA= .001
B= 12.522 DB= .002
C= 13.48 DC= .01
GAMMA= 72.56 DGAMMA= .01
BETA = 82.62 DBETA = .02
ALPHA= 83.91 DALPHA= .04
V= 1202.8
17. 32-1521
C27H49CoNO24U3*6H2O
Triklin
Dexp. Dcal. d(D) h k l
8.2500 8.2500 .0000 3 0 0
7.9200 7.9231 -.0031 2 0 1
7.4300 7.4300 .0000 -2 -1 1
7.2200 7.2237 -.0037 2 -1 1
6.9800 6.9839 -.0039 -3 0 1
6.7500 6.7552 -.0052 3 -1 0
6.3700 6.3697 .0003 -3 -1 0
6.2000 6.2000 -.0000 -3 -1 1
5.2600 5.2612 -.0012 -2 -1 2
5.0500 5.0503 -.0003 3 1 1
4.9500 4.9500 .0000 5 0 0
4.8700 4.8656 .0044 -3 0 2
A= 24.8893 DA= .0008
B= 11.210 DB= .002
C= 11.677 DC= .005
GAMMA= 92.045 DGAMMA= .002
BETA = 94.97 DBETA = .01
ALPHA=105.34 DALPHA= .06
V= 3124
18. 32-1522
C27H49MnNO24U3*6H2O
Triklin
Dexp Dcal d(D) h k l
8.2900 8.2977 -.0077 0 0 1
7.9700 7.9545 .0155 1 1 0
7.5600 7.5474 .0126 0 -2 1
7.2400 7.2444 -.0044 1 0 1
7.0200 7.0360 -.0160 1 -2 1
6.8300 6.8280 .0020 1 1 1
6.5000 6.4901 .0099 1 -3 1
6.3600 6.3585 .0015 0 5 0
5.9200 5.9234 -.0034 0 -4 1
5.3000 5.2987 .0013 0 6 0
5.1100 5.1132 -.0032 -1 1 1
5.0500 5.0503 -.0003 -1 -1 1
A= 9.1031 DA= .0004
B= 32.2482 DB= .0004
C= 8.84067 DC= .00001
GAMMA= 99.000 DGAMMA= .002
BETA = 70.1137 DBETA = .0003
ALPHA= 96.318 DALPHA= .001
V= 2406
19. 32-1523
C27H49NNiO24U3*7H2O
Triklin
Dexp Dcal d(D) h k l
8.2200 8.2289 -.0089 0 1 1
7.8800 7.8872 -.0072 -1 1 0
7.4000 7.3990 .0010 1 0 3
7.1900 7.1894 .0006 0 -1 2
6.9400 6.9337 .0063 1 -1 2
6.7300 6.7243 .0057 -1 1 3
6.4100 6.4078 .0022 1 0 4
6.3600 6.3672 -.0072 -1 0 4
6.2300 6.2270 .0030 1 -1 3
5.2600 5.2599 .0001 1 1 2
5.0700 5.0698 .0002 -1 -1 2
4.9400 4.9402 -.0002 -2 1 2
A= 10.475 DA= .004
B= 8.9404 DB= .0003
C= 33.957 DC= .007
GAMMA=111.35 DGAMMA= .05
BETA = 91.66 DBETA = .03
ALPHA= 84.53 DALPHA= .01287
V= 2948
20. 32-1524
C27H49NO24U3*8H2O
Triklin
Dexp Dcal d(D) h k l
8.3000 8.3311 -.0311 0 2 0
7.9300 7.9365 -.0065 1 1 0
7.4500 7.4629 -.0129 -1 0 1
6.9700 6.9870 -.0170 -1 -2 1
6.7500 6.7429 .0071 -1 1 0
6.5000 6.5063 -.0063 1 2 0
6.3300 6.3204 .0096 0 2 1
6.2300 6.2178 .0122 1 1 1
5.2600 5.2509 .0091 -1 -3 2
5.0900 5.0916 -.0016 1 3 0
4.9400 4.9434 -.0034 0 -2 3
4.2900 4.2905 -.0005 1 3 1
A= 8.4566 DA= .0008
B= 18.424 DB= .005
C= 15.650 DC= .001
GAMMA= 74.40 DGAMMA= .01
BETA =102.624 DBETA = .002
ALPHA=112.468 DALPHA= .001
V= 2151
21. 32-1963
C40H24F12O8U
Triklin
Dexp Dcal d(D) h k l
10.3000 10.2999 .0001 1 0 0
8.9000 8.8967 .0033 0 1 0
6.8000 6.7985 .0015 -1 0 1
6.3000 6.2905 .0095 1 0 1
5.7000 5.7071 -.0071 1 1 0
5.4000 5.4140 -.0140 -2 1 1
4.6000 4.6013 -.0013 -1 1 2
4.4500 4.4484 .0016 0 2 0
4.2200 4.2216 -.0016 0 0 2
4.0800 4.0809 -.0009 2 -1 1
3.9800 3.9768 .0032 -2 1 2
3.7400 3.7387 .0013 -3 1 0
A= 11.595 DA= .005
B= 10.6597 DB= .0006
C= 9.3187 DC= .0005
GAMMA=116.99 DGAMMA= .02
BETA =104.68 DBETA = .01
ALPHA= 65.36 DALPHA= .01
V= 929.9
22. 32-1964
C32H28N4O4U
Triklin
Dexp Dcal d(D) h k l
12.8000 12.8528 -.0528 0 0 1
7.0300 7.0259 .0041 1 0 0
6.5100 6.5105 -.0005 0 -2 1
6.1900 6.1868 .0032 -1 1 0
5.8700 5.8613 .0087 1 0 1
5.3500 5.3431 .0069 1 -1 1
5.1300 5.1275 .0025 -1 -2 1
4.8000 4.7990 .0010 1 2 1
4.4900 4.4872 .0028 1 -2 1
4.3300 4.3232 .0068 -1 -2 2
4.1400 4.1390 .0010 -1 -3 1
3.9500 3.9525 -.0025 -1 3 0
A= 7.106 DA= .005
B= 15.196 DB= .003
C= 12.957 DC= .008
GAMMA= 85.401 DGAMMA= .004
BETA = 97.26 DBETA = .04
ALPHA= 90.30 DALPHA= .06
V= 1383
23. 32-1966
CH3NO4U*0.5H2O
Triklin
Dexp Dcal d(D) h k l
10.6000 10.6112 -.0112 1 1 0
7.4900 7.4891 .0009 -1 1 0
6.7400 6.7404 -.0004 -1 1 2
6.5900 6.5930 -.0030 0 2 2
5.7800 5.7812 -.0012 1 1 2
4.8100 4.8133 -.0033 -1 0 3
4.2000 4.2013 -.0013 2 2 2
3.9450 3.9452 -.0002 -1 3 0
3.8350 3.8323 .0027 -1 1 4
3.7990 3.7985 .0005 3 1 0
3.5570 3.5555 .0015 -2 -3 2
3.4980 3.4981 -.0001 -2 1 4
A= 11.6908 DA= .0006
B= 16.658 DB= .003
C= 15.529 DC= .003
GAMMA= 75.25 DGAMMA= .01
BETA =101.20 DBETA = .02
ALPHA= 69.526 DALPHA= .003
V= 2602.2
24. 32-1967
C36H40F20O8U
Triklin
Dexp Dcal d(D) h k l
10.6000 10.6095 -.0095 1 1 0
9.6000 9.6034 -.0034 2 0 0
8.5000 8.5083 -.0083 1 0 1
8.2000 8.1972 .0028 -1 -1 1
7.5000 7.5046 -.0046 2 1 0
6.6000 6.5987 .0013 -1 2 0
6.4000 6.4023 -.0023 3 0 0
6.1500 6.1527 -.0027 2 -1 1
5.9500 5.9498 .0002 0 -2 1
5.7200 5.7199 .0001 -1 -2 1
5.4000 5.3994 .0006 -3 -1 1
5.0500 5.0478 .0022 3 0 1
A= 19.616 DA= .002
B= 13.673 DB= .004
C= 10.630 DC= .005
GAMMA= 94.606 DGAMMA= .008
BETA =100.3589 DBETA = .0007
ALPHA= 94.57 DALPHA= .03
V= 2782
25. 32-1968
C32H40F12O8U
Triklin
Dexp Dcal d(D) h k l
10.3000 10.3191 -.0191 -1 1 1
9.0000 8.9752 .0248 0 1 1
8.6000 8.6010 -.0010 0 -1 1
6.9500 6.9510 -.0010 -1 -1 1
6.7500 6.7625 -.0125 -1 0 2
6.4000 6.3982 .0018 2 0 0
6.3500 6.3535 -.0035 -1 2 1
6.0000 5.9937 .0063 -2 1 2
5.8000 5.8001 -.0001 0 1 2
5.6000 5.5961 .0039 0 -1 2
5.1300 5.1311 -.0011 1 0 2
5.0000 5.0008 -.0008 -3 1 1
A= 15.030 DA= .002
B= 13.23336 DB= .00006
C= 14.030 DC= .001
GAMMA=115.42 DGAMMA= .02
BETA =112.41 DBETA = .02
ALPHA= 78.516 DALPHA= .006
V= 2329
26. 32-1969
C32H16F12O8U
Triklin
Dexp Dcal d(D) h k l
9.5000 9.5003 -.0003 1 0 0
8.8000 8.8266 -.0266 0 1 0
8.4000 8.4014 -.0014 1 0 1
6.5000 6.4873 .0127 1 0 2
5.7500 5.7533 -.0033 0 1 2
5.4000 5.4057 -.0057 1 -1 1
5.1000 5.1061 -.0061 2 1 0
4.8500 4.8406 .0094 -1 -2 1
4.6000 4.6009 -.0009 2 0 1
4.4300 4.4272 .0028 -1 1 2
4.1500 4.1500 -.0000 2 2 0
4.0700 4.0722 -.0022 -1 -2 3
A= 10.355 DA= .002
B= 9.759 DB= .004
C= 17.821 DC= .01
GAMMA= 66.581 DGAMMA= .005
BETA = 93.35 DBETA = .08
ALPHA=100.25 DALPHA= .09
V= 1625.7
27. 32-1523
C27H49NNiO24U3*7H2O
Triklin
Dexp Dcal d(D) h k l
8.2200 8.2199 .0001 0 1 1
7.8800 7.8838 -.0038 0 -1 1
7.4000 7.3978 .0022 1 0 0
7.1900 7.1831 .0069 -1 1 0
6.9400 6.9437 -.0037 1 2 0
6.7300 6.7343 -.0043 -1 2 0
6.4100 6.4128 -.0028 1 3 0
6.3600 6.3631 -.0031 -1 0 1
6.2300 6.2263 .0037 -1 -1 1
5.2600 5.2593 .0007 1 5 0
5.0700 5.0699 .0001 0 6 1
4.9400 4.9396 .0004 1 1 1
A= 7.6453 DA= .0001
B= 35.959 DB= .004
C= 8.5652 DC= .0002
GAMMA= 88.853 DGAMMA= .001
BETA =104.419 DBETA = .001
ALPHA= 85.004 DALPHA= .007
V= 2270.0
28. 32-1524
C27H49NO24U3Zn*8H2O
Triklin
Dexp Dcal d(D) h k l
8.3000 8.2950 .0050 3 0 0
7.9300 7.9294 .0006 0 0 1
7.4500 7.4444 .0056 -2 1 0
6.9700 6.9685 .0015 2 1 0
6.7500 6.7469 .0031 -2 0 1
6.5000 6.4930 .0070 0 -1 1
6.3300 6.3378 -.0078 1 -1 1
6.2300 6.2289 .0011 -1 -1 1
5.2600 5.2597 .0003 -4 1 0
5.0900 5.0901 -.0001 -2 1 1
4.9400 4.9416 -.0016 -4 0 1
4.2900 4.2904 -.0004 1 2 0
A= 24.947 DA= .002
B= 8.9793 DB= .0003
C= 8.056 DC= .006
GAMMA= 93.879 DGAMMA= .003
BETA = 90.43 DBETA = .03
ALPHA=100.11 DALPHA= .01
V= 1772.5
Triklin
Dexp Dcal d(D) h k l
8.3000 8.2651 .0349 1 1 0
7.9300 7.9235 .0065 0 2 0
7.4500 7.4611 -.0111 0 0 1
6.9700 6.9880 -.0180 -1 1 0
6.7500 6.7554 -.0054 -1 0 1
6.5000 6.5005 -.0005 1 2 0
6.3300 6.3188 .0112 -1 1 1
6.2300 6.2361 -.0061 0 -1 1
5.2600 5.2600 -.0000 -1 2 1
5.0900 5.0991 -.0091 1 1 1
4.9400 4.9286 .0114 1 0 1
4.2900 4.2912 -.0012 2 0 0
A= 9.111 DA= .002
B= 16.4174 DB= .0009
C= 7.964 DC= .008
GAMMA= 81.96 DGAMMA= .01
BETA =106.05 DBETA = .02
ALPHA= 80.02 DALPHA= .05
V= 1105.7
29. 32-1963
C40H24F12*O8U
Triklin
Dexp Dcal d(D) h k l
10.3000 10.2973 .0027 1 0 0
8.9000 8.8968 .0032 0 1 0
6.8000 6.7983 .0017 -1 0 1
6.3000 6.2893 .0107 1 0 1
5.7000 5.7056 -.0056 1 1 0
5.4000 5.4143 -.0143 -2 1 1
4.6000 4.6012 -.0012 -1 1 2
4.4500 4.4484 .0016 0 2 0
4.2200 4.2215 -.0015 0 0 2
4.0800 4.0809 -.0009 2 -1 1
3.9800 3.9768 .0032 -2 1 2
3.7400 3.7384 .0016 -3 1 0
A= 11.59 DA= .01
B= 10.661 DB= .004
C= 9.3179 DC= .0003
GAMMA=117.02 DGAMMA= .08
BETA =104.69 DBETA = .04
ALPHA= 65.37 DALPHA= .02
V= 929.6
30. 32-1964
C32H28N4O4U
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
12.8000 12.9871 -.1871 1 0 0
7.0300 7.0154 .0146 1 1 0
6.5100 6.4936 .0164 2 0 0
6.1900 6.1926 -.0026 0 0 2
5.8700 5.8729 -.0029 -1 0 2
5.3500 5.3439 .0061 1 0 2
5.1300 5.1228 .0072 2 1 0
4.8000 4.8011 -.0011 -1 1 2
4.4900 4.4989 -.0089 1 1 2
4.3300 4.3290 .0010 3 0 0
4.1400 4.1466 -.0066 -2 1 2
3.9500 3.9504 -.0004 0 2 1
a= 13.0835 b=8.336 c= 12.48 beta= 96.95
da=.0007 db=.002 dc=.012 dbeta=.07
V= 1351
Triklin
Dexp Dcal d(D) h k l
12.8000 12.8752 -.0752 0 0 1
7.0300 7.0193 .0107 1 0 0
6.5100 6.5141 -.0041 0 -2 1
6.1900 6.1810 .0090 1 1 0
5.8700 5.8618 .0082 -1 0 1
5.3500 5.3429 .0071 -1 -1 1
5.1300 5.1266 .0034 1 -2 1
4.8000 4.7998 .0002 -1 2 1
4.4900 4.4867 .0033 -1 -2 1
4.3300 4.3247 .0053 1 -2 2
4.1400 4.1389 .0011 1 -3 1
3.9500 3.9501 -.0001 1 3 0
A= 7.098 DA= .003
B= 15.195 DB= .003
C= 12.98 DC= .01
GAMMA= 94.64 DGAMMA= .02
BETA = 82.80 DBETA = .01
ALPHA= 90.32 DALPHA= .05
V= 1384
31. 32-1970
C12H12Cl4N2O2U
Triklin
Dexp Dcal d(D) h k l
9.2300 9.2330 -.0030 -1 1 0
8.7200 8.6968 .0232 0 -1 1
8.5200 8.5188 .0012 -1 0 1
7.4400 7.4358 .0042 -1 1 1
7.3000 7.3069 -.0069 1 1 1
6.8900 6.8811 .0089 1 -1 1
5.6500 5.6484 .0016 1 2 1
5.5100 5.5012 .0088 -2 0 1
5.2300 5.2252 .0048 -1 0 2
4.2200 4.2221 -.0021 -1 -3 1
4.0700 4.0712 -.0012 1 -3 1
3.9690 3.9684 .0006 2 1 2
A= 12.26 DA= .01
B= 14.778 DB= .008
C= 11.307 DC= .002
GAMMA= 87.867 DGAMMA= .007
BETA = 92.92 DBETA = .08
ALPHA= 86.57 DALPHA= .02
V= 2041
32. 32-1971
C24H22Cl4O2U
Triklin
Dexp Dcal d(D) h k l
7.7400 7.7426 -.0026 1 0 0
7.5100 7.5068 .0032 1 1 0
6.8000 6.8046 -.0046 0 2 1
6.3900 6.3849 .0051 1 0 1
5.9700 5.9654 .0046 1 2 1
5.3500 5.3569 -.0069 -1 1 1
4.9500 4.9435 .0065 0 3 1
4.7800 4.7761 .0039 1 3 1
4.6400 4.6474 -.0074 0 2 2
4.5700 4.5749 -.0049 1 3 0
4.3000 4.2999 .0001 1 0 2
4.0200 4.0289 -.0089 1 3 2
A= 8.037 DA= .004
B= 15.7407 DB= .0007
C= 10.151 DC= .001
GAMMA= 75.79 DGAMMA= .03
BETA = 79.72 DBETA = .01
ALPHA= 72.09 DALPHA= .01
V= 1176.8
33. 32-1973
C8.25H8.25F2N1.65O2U
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
12.1000 12.1097 -.0097 1 0 1
7.2900 7.2769 .0131 2 0 0
6.4100 6.4058 .0042 0 1 0
6.0500 6.0548 -.0048 2 0 2
5.7300 5.7281 .0019 0 0 4
5.5800 5.5791 .0009 0 -1 2
4.7800 4.7774 .0026 -3 0 1
4.6900 4.6879 .0021 -1 1 3
4.6400 4.6349 .0051 1 1 3
4.3900 4.3896 .0004 2 -1 2
4.3300 4.3311 -.0011 1 0 5
4.1100 4.1119 -.0019 -2 1 3
A= 14.56 DA= .02
B= 6.406 DB= .006
C= 22.92 DC= .01
GAMMA= 89.9 DGAMMA= .1
BETA = 91.8 DBETA = .1
ALPHA= 89.7 DALPHA= .2
V= 2138
Triklin
Dexp Dcal d(D) h k l
12.1000 12.1051 -.0051 1 0 0
7.2900 7.2892 .0008 2 1 1
6.4100 6.4097 .0003 0 -1 1
6.0500 6.0525 -.0025 2 0 0
5.7300 5.7323 -.0023 1 2 0
5.5800 5.5762 .0038 0 1 2
4.7800 4.7795 .0005 3 1 1
4.6900 4.6875 .0025 2 2 0
4.6400 4.6405 -.0005 2 3 2
4.3900 4.3904 -.0004 2 2 3
4.3300 4.3301 -.0001 0 -2 1
4.1100 4.1106 -.0006 -2 -1 1
A= 14.63 DA= .01
B= 14.43 DB= .01
C= 13.23 DC= .01
GAMMA= 64.25 DGAMMA= .07
BETA = 57.48 DBETA = .09
ALPHA= 56.02 DALPHA= .07
V= 1915.6
34. 32-1974
C3.55H3.55F2N0.71O2U
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
8.5500 8.5675 -.0175 2 0 0
7.6200 7.6547 -.0347 -1 0 1
7.1000 7.0760 .0240 0 1 0
6.5300 6.5403 -.0103 1 1 0
5.3500 5.3574 -.0074 0 1 1
4.8800 4.8855 -.0055 -3 0 1
4.6700 4.6601 .0099 -2 1 1
4.4400 4.4444 -.0044 3 1 0
4.2800 4.2838 -.0038 4 0 0
4.1000 4.1005 -.0005 0 0 2
3.8300 3.8274 .0026 -2 0 2
3.5400 3.5380 .0020 0 2 0
a= 17.20 b=7.076 c= 8.23 beta=94.9
da=.03 db=.004 dc=.01 dbeta=.1
V= 998
Triklin
Dexp Dcal d(D) h k l
8.5500 8.5447 .0053 1 0 0
7.6200 7.6137 .0063 0 1 1
7.1000 7.0921 .0079 0 -1 1
6.5300 6.5383 -.0083 -1 2 0
5.3500 5.3447 .0053 0 -2 1
4.8800 4.8766 .0034 -1 3 0
4.6700 4.6733 -.0033 -1 3 1
4.4400 4.4385 .0015 -2 1 1
4.2800 4.2795 .0005 -1 1 2
4.1000 4.1052 -.0052 0 -3 1
3.8300 3.8292 .0008 1 3 0
3.5400 3.5393 .0007 -1 -3 1
A= 9.203 DA= .005
B= 15.513 DB= .008
C= 8.7948 DC= .0001
GAMMA=107.58 DGAMMA= .02
BETA =105.10 DBETA = .01
ALPHA= 81.14 DALPHA= .01
V= 1151.8
35. 32-1976
C8H4O6U
Triiklin
Dexp Dcal d(D) h k l
8.4600 8.4719 -.0119 1 0 0
6.6500 6.6414 .0086 1 1 1
5.3000 5.3048 -.0048 1 2 0
5.0900 5.0848 .0052 1 -1 2
4.8600 4.8545 .0055 1 2 1
4.5400 4.5360 .0040 -1 1 1
4.4300 4.4292 .0008 0 0 2
4.3600 4.3617 -.0017 0 -3 1
4.3000 4.2984 .0016 -1 -2 1
4.2200 4.2218 -.0018 2 0 2
4.0600 4.0603 -.0003 2 1 0
3.9700 3.9735 -.0035 0 1 2
A= 9.6649 DA= .0001
B= 13.752 DB= .001
C= 10.3172 DC= .0001
GAMMA= 95.20 DGAMMA= .01
BETA = 61.251 DBETA = .001
ALPHA=102.716 DALPHA= .007
V= 1172.5