1. 28-0086
C8H16N4O16U*6H2O
Triklin
Dexp Dcal d(D) h k l
8.0800 8.0701 .0099 0 1 1
7.3900 7.4011 -.0111 0 -1 1
6.1100 6.1091 .0009 1 1 0
5.7500 5.7602 -.0102 0 2 0
5.4700 5.4733 -.0033 1 0 1
5.1200 5.1081 .0119 -1 1 0
4.8900 4.8960 -.0060 0 1 2
3.9600 3.9548 .0052 -1 0 2
3.8400 3.8401 -.0001 0 3 0
3.1600 3.1607 -.0007 2 0 0
3.0500 3.0494 .0006 2 0 1
2.9400 2.9409 -.0009 1 2 3
A= 6.4734 DA= .0007
B= 11.849 DB= .01
C= 10.438 DC= .001
GAMMA= 77.68 DGAMMA= .01
BETA = 87.167 DBETA = .005
ALPHA= 84.54 DALPHA= .01
V= 777.4
2. 28-0164
BaU6.24O19.7
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
7.4500 7.4749 -.0249 0 0 2
3.7400 3.7412 -.0012 -1 1 1
3.5700 3.5663 .0037 0 1 2
3.5000 3.5038 -.0038 -1 1 2
3.2200 3.2194 .0006 -3 0 3
3.1700 3.1723 -.0023 2 0 3
3.1100 3.1068 .0032 -2 1 2
2.5800 2.5797 .0003 -1 0 6
2.5500 2.5495 .0005 -4 0 3
2.5000 2.4993 .0007 2 1 3
2.0730 2.0750 -.0020 -4 1 4
2.0350 2.0352 -.0002 5 0 0
2.0000 2.0002 -.0002 3 0 5
1.9650 1.9654 -.0004 -4 1 5
1.7860 1.7860 .0000 1 1 7
a= 10.537 b=4.0580 c= 15.480 beta= 105.035
da= .001 db=.0004 dc=.003 dbeta= .006
V= 639.2
Triklin
Dexp Dcal d(D) h k l
7.4500 7.4565 -.0065 1 0 1
3.7400 3.7390 .0010 -1 1 0
3.5700 3.5706 -.0006 1 -1 2
3.5000 3.5011 -.0011 -1 -1 1
3.2200 3.2205 -.0005 1 -1 3
3.1700 3.1698 .0002 1 1 2
3.1100 3.1104 -.0004 -1 1 2
2.5800 2.5793 .0007 -2 -1 2
2.5500 2.5507 -.0007 -3 0 1
2.5000 2.5007 -.0007 1 1 4
2.0730 2.0729 .0001 -3 1 2
2.0350 2.0351 -.0001 3 1 3
2.0000 1.9999 .0001 4 0 2
1.9650 1.9648 .0002 1 1 6
1.7860 1.7860 -.0000 -3 1 4
A= 8.089 DA= .001
B= 4.151 DB= .001
C= 14.628 DC= .003
GAMMA= 93.98 DGAMMA= .02
BETA = 81.21 DBETA = .01
ALPHA= 96.79 DALPHA= .03
V= 481.4
3. 28-0351
Cs2UOCl4
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
6.5500 6.5503 -.0003 1 1 1
5.8800 5.8825 -.0025 0 -1 2
5.4300 5.4370 -.0070 2 0 0
4.4600 4.4613 -.0013 2 1 1
4.0900 4.0866 .0034 1 0 3
3.8100 3.8083 .0017 2 1 2
3.5000 3.5007 -.0007 1 -3 0
3.1900 3.1906 -.0006 2 -1 3
3.1100 3.1097 .0003 -2 2 3
2.9300 2.9284 .0016 -3 -1 3
2.8600 2.8597 .0003 2 2 3
2.6900 2.6891 .0009 1 4 0
A= 10.953 DA= .003
B= 11.098 DB= .004
C= 13.989 DC= .001
GAMMA= 89.94 DGAMMA= .01
BETA = 96.888 DBETA = .007
ALPHA= 89.93 DALPHA= .03
V= 1688.1
Triklin
Dexp Dcal d(D) h k l
6.5500 6.5522 -.0022 1 0 0
5.8800 5.8818 -.0018 -1 1 1
5.4300 5.4271 .0029 -1 -1 1
4.4600 4.4621 -.0021 -1 2 0
4.0900 4.0811 .0089 0 0 2
3.8100 3.8131 -.0031 -1 -1 2
3.5000 3.5017 -.0017 -2 0 1
3.1900 3.1905 -.0005 0 -2 2
3.1100 3.1093 .0007 -2 2 1
2.9300 2.9287 .0013 2 2 0
2.8600 2.8616 -.0016 1 2 2
2.6900 2.6898 .0002 0 4 2
A= 7.0160 DA= .0002
B= 12.627 DB= .002
C= 8.8487 DC= .0005
GAMMA= 92.01811 DGAMMA= .00007
BETA =110.915 DBETA = .004
ALPHA= 80.792 DALPHA= .007
V= 722.7
4. 28-0459
UMo12H6O42*18H2O
Monoklin
Grupa 4,11
Dexp Dcal d(D) h k l
10.6000 10.6003 -.0003 1 1 0
8.0600 8.0587 .0013 0 2 0
7.0300 7.0315 -.0015 2 0 0
4.5000 4.5003 -.0003 3 -1 0
4.0200 4.0237 -.0037 -3 1 1
3.4900 3.4902 -.0002 2 3 1
3.3300 3.3274 .0026 -4 0 1
3.2200 3.2216 -.0016 4 -2 0
3.1600 3.1598 .0002 1 1 2
3.1500 3.1504 -.0004 0 -2 2
2.9600 2.9599 .0001 4 0 1
2.9300 2.9294 .0006 2 -5 0
A= 14.210 DA= .008
B= 16.117 DB= .004
C= 6.918 DC= .003
BETA = 98.24935 DBETA = .07396
V= 1567
5. 28-0543
Pb2U5O17*3H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
6.3000 6.3000 -.0000 1 2 0
4.3800 4.3797 .0003 2 2 0
3.9700 3.9697 .0003 1 1 1
3.6800 3.6797 .0003 1 4 0
3.5000 3.5003 -.0003 2 1 1
3.2300 3.2298 .0002 1 3 1
3.1400 3.1404 -.0004 0 5 0
2.9200 2.9198 .0002 3 3 0
2.6200 2.6201 -.0001 3 4 0
2.5800 2.5799 .0001 3 3 1
2.5000 2.5000 .0000 4 2 0
2.1000 2.1000 -.0000 3 6 0
A= 10.748 DA= .001
B= 15.702 DB= .004
C= 4.1867 DC= .0005
BETA = 79.015 DBETA = .008
V= 694
Triklin
Dexp Dcal d(D) h k l
6.3000 6.2890 .0110 1 0 0
4.3800 4.3783 .0017 0 1 1
3.9700 3.9703 -.0003 0 -1 1
3.6800 3.6799 .0001 1 1 1
3.5000 3.5012 -.0012 -1 -1 1
3.2300 3.2297 .0003 1 -1 1
3.1400 3.1445 -.0045 2 0 0
2.9200 2.9161 .0039 2 0 1
2.6200 2.6197 .0003 -2 0 2
2.5800 2.5796 .0004 -2 -1 1
2.5000 2.5009 -.0009 2 0 2
2.1000 2.1001 -.0001 1 2 2
A= 6.3142 DA= .0002
B= 4.7660 DB= .0006
C= 8.8667 DC= .0007
GAMMA= 85.726 DGAMMA= .006
BETA = 92.304 DBETA = .001
ALPHA= 83.482 DALPHA= .002
V= 264
6. 28-601
Li2U1.75O6.25
Monoklin
Dexp Dcal d(D) h k l
5.5800 5.5816 -.0016 1 0 2
5.4600 5.4570 .0030 1 1 0
3.4200 3.4214 -.0014 -2 0 2
3.3100 3.3097 .0003 1 0 4
3.2400 3.2407 -.0007 2 0 3
3.1300 3.1265 .0035 0 1 4
3.0400 3.0387 .0013 1 2 2
2.8480 2.8476 .0004 -1 1 4
2.7720 2.7726 -.0006 0 0 5
2.7280 2.7285 -.0005 2 2 0
2.6500 2.6497 .0003 -1 2 3
2.5840 2.5835 .0005 3 1 0
2.5030 2.5043 -.0013 0 2 4
a= 8.332 b= 7.245 c= 13.924 beta= 84.639
da=.008 db=.008 dc=.005 dbeta= .008
V= 837
7. 28-0602
Li2U2O7
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.6200 5.6201 -.0001 1 1 0
3.3000 3.2996 .0004 1 2 1
3.2300 3.2307 -.0007 0 2 2
3.0600 3.0624 -.0024 2 0 5
2.9200 2.9205 -.0005 3 1 1
2.8300 2.8309 -.0009 -2 1 3
2.6800 2.6810 -.0010 2 2 3
2.5900 2.5914 -.0014 -1 1 5
2.5200 2.5190 .0010 -2 2 2
2.3300 2.3304 -.0004 0 3 1
2.1700 2.1694 .0006 0 1 7
1.9900 1.9899 .0001 1 1 8
1.9500 1.9502 -.0002 -2 2 5
a= 9.66 b= 7.0668 c= 16.63 beta= 73.6
da=.01 db= .0005 dc= .01 dbeta=.01
V= 1089
8. 28-0602
Li2U2O7
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.6200 5.6201 -.0001 1 1 0
3.3000 3.2996 .0004 1 2 1
3.2300 3.2307 -.0007 0 2 2
3.0600 3.0624 -.0024 2 0 5
2.9200 2.9205 -.0005 3 1 1
2.8300 2.8309 -.0009 -2 1 3
2.6800 2.6810 -.0010 2 2 3
2.5900 2.5914 -.0014 -1 1 5
2.5200 2.5190 .0010 -2 2 2
2.3300 2.3304 -.0004 0 3 1
2.1700 2.1694 .0006 0 1 7
1.9900 1.9899 .0001 1 1 8
1.9500 1.9502 -.0002 -2 2 5
a= 9.662 b= 7.0668 c= 16.63 beta= 73.6
da=.01 db= .0005 dc=.01 dbeta= .01
V= 1089
Triklin
Dexp Dcal d(D) h k l
5.6200 5.6216 -.0016 1 0 0
3.3000 3.2986 .0014 -1 1 1
3.2300 3.2298 .0002 1 -1 1
3.0600 3.0599 .0001 1 0 2
2.9200 2.9194 .0006 0 -2 1
2.8300 2.8293 .0007 -2 0 1
2.6800 2.6781 .0019 -1 0 3
2.5900 2.5903 -.0003 0 -2 2
2.5200 2.5187 .0013 2 0 1
2.3300 2.3298 .0002 -1 2 0
2.1700 2.1691 .0009 -2 -2 3
1.9900 1.9902 -.0002 -2 -3 1
1.9500 1.9507 -.0007 -2 -1 4
A= 6.112 DA= .001
B= 6.3682 DB= .0002
C= 8.620 DC= .004
GAMMA= 69.510 DGAMMA= .008
BETA =104.588 DBETA = .009
ALPHA=103.00 DALPHA= .02
V= 300.7
9. 28-0603
Li2U2O7
Triklin
Dexp Dcal d(D) h k l
5.8300 5.8355 -.0055 0 1 1
5.5500 5.5519 -.0019 0 -1 1
5.4300 5.4329 -.0029 1 -1 1
5.1700 5.1718 -.0018 1 1 1
5.1100 5.1117 -.0017 -1 1 1
4.7200 4.7171 .0029 0 1 2
3.7600 3.7617 -.0017 3 0 1
3.4100 3.4096 .0004 2 -1 3
3.3800 3.3800 .0000 3 -1 1
3.3100 3.3100 -.0000 0 0 4
3.2400 3.2402 -.0002 2 0 4
3.1500 3.1497 .0003 0 2 0
A= 11.341 DA= .008
B= 6.344 DB= .001
C= 13.754 DC= .002
GAMMA= 95.71 DGAMMA= .05
BETA = 74.72 DBETA = .03
ALPHA= 87.98 DALPHA= .06
V= 948
10. 28-0604
Li2U6O19
Romb
Groupa 31, 59
Dexp. Dcal. d(D) h k l
7.9800 7.9699 .0101 2 0 0
5.2200 5.2114 .0086 1 2 1
4.6800 4.6829 -.0029 3 0 1
4.1500 4.1477 .0023 3 2 0
3.6200 3.6241 -.0041 3 0 2
2.4400 2.4410 -.0010 2 5 1
3.2500 3.2486 .0014 1 4 0
3.1000 3.0998 .0002 5 1 0
2.6480 2.6472 .0008 0 3 3
2.6050 2.6050 .0000 6 1 0
2.0740 2.0739 .0001 6 4 0
2.0040 2.0040 .0000 1 6 2
a=15.9398 b=13.273 c= 9.91
da= .0004 db= .001 dc= .01
V=2097
Monoklin
Grupa 4,11
Dexp Dcal d(D) h k l
7.9800 7.9885 -.0085 1 1 0
5.2200 5.2146 .0054 0 2 0
4.6800 4.6763 .0037 2 1 1
4.1500 4.1483 .0017 1 2 1
3.6200 3.6190 .0010 0 0 2
2.4400 2.4391 .0009 2 3 2
3.2500 3.2524 -.0024 2 1 2
3.1000 3.0997 .0003 1 3 1
2.6480 2.6484 -.0004 4 2 1
2.6050 2.6044 .0006 3 3 1
2.0740 2.0742 -.0002 2 4 2
2.0040 2.0043 -.0003 0 5 1
a= 12.66 b= 10.429 c= 7.373 beta=79.03
da=.01 db=.004 dc=.004 dbeta=.06
V= 955
Triklin
Dexp Dcal d(D) h k l
7.9800 7.9819 -.0019 1 0 0
5.2200 5.2208 -.0008 -1 1 1
4.6800 4.6798 .0002 1 -1 1
4.1500 4.1538 -.0038 -1 2 0
3.6200 3.6198 .0002 -2 1 1
2.4400 2.4400 -.0000 1 -2 2
3.2500 3.2498 .0002 -1 1 2
3.1000 3.1008 -.0008 1 2 1
2.6480 2.6485 -.0005 0 3 1
2.6050 2.6052 -.0002 -3 1 1
2.0740 2.0740 .0000 4 -1 1
2.0040 2.0038 .0002 0 4 1
A= 8.5892 DA= .0007
B= 8.56946 DB= .00005
C= 7.141 DC= .001
GAMMA=110.590 DGAMMA= .008
BETA = 87.911 DBETA = .007
ALPHA= 77.833 DALPHA= .007
V= 477.5
11. 28-0639
MgUF7
Triklin
Dexp Dcal d(D) h k l
4.9000 4.8990 .0010 0 1 1
4.3600 4.3650 -.0050 0 -1 1
4.0000 4.0004 -.0004 -1 0 1
2.9700 2.9687 .0013 1 2 1
2.7300 2.7326 -.0026 0 -2 1
2.6300 2.6301 -.0001 1 -1 2
2.5430 2.5430 .0000 -1 -2 1
2.4600 2.4602 -.0002 -2 0 1
2.3900 2.3892 .0008 1 -2 1
2.3230 2.3234 -.0004 2 2 0
2.2100 2.2102 -.0002 0 1 3
2.0400 2.0395 .0005 -1 -2 2
A= 5.91001 DA= .00003
B= 6.46163 DB= .00006
C= 6.99017 DC= .00000
GAMMA= 78.1491 DGAMMA= .0004
BETA = 77.6716 DBETA = .0003
ALPHA= 81.1433 DALPHA= .0004
V= 253.5
12. 28-0640
MgU2F12
Triklin
Dexp Dcal d(D) h k l
6.9500 6.9574 -.0074 1 1 0
5.2100 5.2030 .0070 1 0 2
4.8600 4.8561 .0039 -1 -1 2
4.2500 4.2502 -.0002 2 1 0
3.9700 3.9667 .0033 1 0 3
3.8700 3.8659 .0041 0 -2 1
3.7400 3.7390 .0010 1 2 2
3.6100 3.6121 -.0021 2 1 2
3.4000 3.4026 -.0026 2 2 1
3.3500 3.3503 -.0003 -2 -2 1
3.1700 3.1704 -.0004 1 1 4
2.9000 2.9020 -.0020 1 -2 2
A= 8.729 DA= .001
B= 8.681 DB= .001
C= 14.095 DC= .005
GAMMA= 73.81 DGAMMA= .02
BETA = 92.19 DBETA = .01
ALPHA= 84.83 DALPHA= .04
V= 1020
13. 28-0971
Rb{UO2}2F5
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.8800 5.8842 -.0042 0 1 0
4.3600 4.3616 -.0016 5 0 0
4.2500 4.2530 -.0030 -5 0 1
4.0000 3.9992 .0008 4 1 0
3.7200 3.7208 -.0008 -1 0 3
3.6700 3.6697 .0003 2 1 2
3.4800 3.4809 -.0009 -3 0 3
3.1000 3.0985 .0015 -2 1 3
3.0200 3.0199 .0001 -5 0 3
2.9160 2.9157 .0003 1 2 0
2.7320 2.7315 .0005 -8 0 1
2.5610 2.5614 -.0004 1 2 2
a= 21.998 b= 5.884 c=11.17 beta= 97.54
da=.004 db= .002 dc= .01 dbeta=.06
V= 1433
Triklin
Dexp Dcal d(D) h k l
5.8800 5.8830 -.0030 0 -1 1
4.3600 4.3585 .0015 0 -3 1
4.2500 4.2515 -.0015 1 0 0
4.0000 3.9978 .0022 1 2 0
3.7200 3.7186 .0014 0 -4 1
3.6700 3.6762 -.0062 1 3 0
3.4800 3.4820 -.0020 0 5 1
3.1000 3.0993 .0007 -1 -2 1
3.0200 3.0204 -.0004 0 6 1
2.9160 2.9155 .0005 -1 3 1
2.7320 2.7299 .0021 1 -1 2
2.5610 2.5593 .0017 0 -4 2
A= 4.342 DA= .002
B= 19.763 DB= .001
C= 6.496 DC= .001
GAMMA= 85.15 DGAMMA= .01
BETA = 78.874 DBETA = .002
ALPHA= 83.93 DALPHA= .01
V= 543.2
14. 28-0974
Rb5{UO2}2F9
Triklin
Dexp Dcal d(D) h k l
7.1800 7.1810 -.0010 0 1 1
6.4900 6.4905 -.0005 -1 -1 1
6.0300 6.0298 .0002 0 -1 1
5.1500 5.1527 -.0027 1 1 1
4.7200 4.7219 -.0019 -2 -1 1
4.4800 4.4814 -.0014 2 2 0
4.3000 4.2985 .0015 -2 -2 1
4.0600 4.0575 .0025 1 3 1
3.6800 3.6815 -.0015 -2 -3 1
3.5000 3.5001 -.0001 -2 -1 2
3.3100 3.3099 .0001 -2 2 0
3.1900 3.1901 -.0001 -1 -4 1
A= 10.007 DA= .001
B= 14.735 DB= .002
C= 7.995 DC= .001
GAMMA= 74.301 DGAMMA= .004
BETA =108.82 DBETA = .01
ALPHA= 84.12 DALPHA= .02
V= 1051
15. 28-1066
{Na,Ca}UO4-x
Romb.
Groupa 36,40,63
Dexp. Dcal. d(D) h k l
4.0500 4.0794 -.0294 0 1 1
2.8800 2.8803 -.0003 1 1 1
2.0400 2.0397 .0003 0 2 2
1.8200 1.8200 .0000 2 1 1
1.6800 1.6798 .0002 1 3 1
1.6500 1.6498 .0002 1 1 3
1.4400 1.4401 -.0001 2 2 2
1.2300 1.2300 .0000 3 2 0
a= 4.0672 b= 5.849 c= 5.6927
da= .0003 db= .001 dc= .0004
V= 135.42
16. 28-1067
{Na,Ca}UO4-x
Romb
Groupa 19
Dexp. Dcal. d(D) h k l
4.1000 4.0988 .0012 2 0 1
2.9000 2.8995 .0005 3 1 0
2.4000 2.3990 .0010 3 0 2
2.3500 2.3462 .0038 2 2 0
2.2100 2.2094 .0006 0 0 3
2.0500 2.0494 .0006 4 0 2
1.8500 1.8507 -.0007 4 2 0
1.6900 1.6909 -.0009 0 2 3
1.6500 1.6505 -.0005 6 1 0
1.4500 1.4498 .0002 6 2 0
1.4200 1.4201 -.0001 4 3 1
1.3000 1.2999 .0001 3 2 4
a=10.4309 b= 5.254 c= 6.6283
da= .0002 db= .001 dc= .0005
V= 363.2
17. 28-1068
Na0.5Ca0.5UO3.75
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.8100 5.8002 .0098 0 0 1
4.7000 4.7032 -.0032 1 1 0
3.3400 3.3389 .0011 1 1 1
3.1600 3.1591 .0009 -2 1 1
2.9000 2.9001 -.0001 0 0 2
2.4200 2.4217 -.0017 1 2 1
2.0300 2.0309 -.0009 0 3 0
1.9600 1.9584 .0016 1 3 0
1.8500 1.8497 .0003 4 0 0
1.6900 1.6901 -.0001 -1 3 2
1.6400 1.6398 .0002 3 0 2
1.4500 1.4500 -.0000 0 0 4
1.4300 1.4303 -.0003 4 2 1
1.3000 1.2999 .0001 3 1 3
a= 7.801 b= 6.093 c= 6.115 beta= 108.47
da=.006 db=.003 dc=.00 dbeta= .05
V= 275.7
18. 28-1158
alfa-Na2UO4
Triklin
Dexp Dcal d(D) h k l
4.9000 4.9040 -.0040 0 0 1
3.4900 3.4855 .0045 0 -2 1
2.8500 2.8508 -.0008 -1 -1 1
2.4700 2.4691 .0009 -2 1 0
2.4300 2.4299 .0001 0 -2 2
2.2300 2.2304 -.0004 2 -3 1
2.1900 2.1896 .0004 2 -1 2
2.0000 2.0001 -.0001 -1 -1 2
1.8600 1.8600 .0000 1 -2 3
1.7500 1.7502 -.0002 2 -2 3
1.6600 1.6601 -.0001 -1 -3 2
1.6200 1.6199 .0001 0 -3 3
A= 5.322 DA= .003
B= 8.184 DB= .002
C= 5.5856 DC= .0006
GAMMA=112.41 DGAMMA= .02
BETA = 68.451 DBETA = .001
ALPHA=115.08 DALPHA= .01
V= 197.5
19. 28-1159
NaU2O7
Triklin
Dexp Dcal d(D) h k l
6.7200 6.7165 .0035 0 1 1
6.5500 6.5434 .0066 0 -1 1
5.9600 5.9666 -.0066 1 0 1
5.1300 5.1244 .0056 1 0 2
5.0500 5.0548 -.0048 1 1 0
4.9800 4.9805 -.0005 1 1 1
4.4900 4.4850 .0050 1 1 2
4.1800 4.1727 .0073 0 -1 3
3.7600 3.7599 .0001 -1 1 2
3.6600 3.6612 -.0012 0 2 0
3.5400 3.5377 .0023 0 -2 1
3.4800 3.4803 -.0003 1 -1 3
A= 6.262 DA= .004
B= 7.396 DB= .001
C= 15.715 DC= .002
GAMMA= 82.169 DGAMMA= .006
BETA = 83.23 DBETA = .01
ALPHA= 87.17 DALPHA= .01
V= 715
20. 28-1160
Na2U7.6O23.8
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
7.2500 7.2515 -.0015 1 1 0
3.6400 3.6397 .0003 -2 0 2
3.5500 3.5499 .0001 0 0 3
3.4800 3.4800 -.0000 2 1 2
3.2000 3.1993 .0007 -3 0 1
3.1400 3.1402 -.0002 1 3 1
2.5500 2.5498 .0002 2 2 3
2.5200 2.5200 .0000 1 4 0
2.0780 2.0782 -.0002 -1 0 5
2.0430 2.0430 -.0000 0 5 1
2.0100 2.0105 -.0005 4 3 1
1.9570 1.9568 .0002 2 3 4
a= 10.109 b= 10.409 c= 10.651 beta= 89.167
da=.003 db=.002 dc=.0003 dbeta= .006
V= 1121
Triklin
Dexp Dcal d(D) h k l
7.2500 7.2424 .0076 1 0 0
3.6400 3.6397 .0003 -1 0 2
3.5500 3.5488 .0012 0 -1 1
3.4800 3.4788 .0012 0 0 2
3.2000 3.2016 -.0016 -1 -1 1
3.1400 3.1404 -.0004 -2 1 1
2.5500 2.5495 .0005 -2 -1 1
2.5200 2.5199 .0001 2 -1 1
2.0780 2.0781 -.0001 3 0 1
2.0430 2.0431 -.0001 -3 0 3
2.0100 2.0101 -.0001 2 -1 2
1.7870 1.7869 .0001 -4 1 0
A= 7.8399 DA= .0002
B= 4.2847 DB= .0001
C= 7.4042 DC= .0002
GAMMA=101.8680 DGAMMA= .0002
BETA =109.9528 DBETA = .0003
ALPHA= 84.572 DALPHA= .002
V= 228.74
21. 22-1161
Na6U7O24
Triklin
Dexp Dcal d(D) h k l
12.5000 12.5117 -.0117 -1 1 0
11.8600 11.8436 .0164 -1 0 1
10.1500 10.1379 .0121 -1 -2 1
9.7600 9.7485 .0115 -1 1 1
9.3400 9.3416 -.0016 -1 2 0
7.9800 7.9791 .0009 -1 -1 2
7.6400 7.6426 -.0026 -1 -2 2
7.3100 7.3121 -.0021 -2 -1 1
7.1900 7.1898 .0002 -2 0 1
7.0300 7.0302 -.0002 1 -3 1
6.9100 6.9089 .0011 1 -1 2
6.7000 6.7014 -.0014 -1 1 2
A= 15.247 DA= .001
B= 26.67 DB= .01
C= 17.22 DC= .01
GAMMA= 83.198 DGAMMA= .003
BETA = 99.538 DBETA = .009
ALPHA=108.12 DALPHA= .04
V= 6543
22. 28-1162
NaUVO5+x
Triklin
Dexp Dcal d(D) h k l
6.4800 6.4852 -.0052 0 1 1
6.2400 6.2397 .0003 0 -1 1
5.1700 5.1691 .0009 1 1 0
4.1800 4.1801 -.0001 -1 -1 2
3.9900 3.9921 -.0021 -1 0 3
3.8900 3.8878 .0022 0 0 4
3.2600 3.2601 -.0001 1 2 1
3.2100 3.2099 .0001 1 1 4
3.1200 3.1198 .0002 0 -2 2
2.9380 2.9384 -.0004 -1 1 4
2.7980 2.7958 .0022 -2 1 0
2.7540 2.7559 -.0019 2 -1 1
A= 6.6056 DA= .0001
B= 7.06125 DB= .00006
C= 15.58641 DC= .00003
GAMMA= 81.167 DGAMMA= .001
BETA = 87.5552 DBETA = .0002
ALPHA= 86.7038 DALPHA= .0005
V= 716.8
23. 28-1163
Na3UV3O11
Triklin
Dexp Dcal d(D) h k l
12.5000 12.4875 .0125 1 0 0
5.9500 5.9513 -.0013 -1 1 1
5.8500 5.8527 -.0027 1 -1 1
5.0500 5.0480 .0020 -1 2 0
3.9000 3.9009 -.0009 -3 1 1
3.5800 3.5814 -.0014 -1 1 2
3.4600 3.4595 .0005 -3 2 1
3.2900 3.2913 -.0013 -4 1 0
3.2100 3.2094 .0006 2 -1 2
3.1400 3.1406 -.0006 -2 -2 1
3.0500 3.0497 .0003 -1 2 2
2.9780 2.9770 .0010 -4 0 1
A= 13.1968 DA= .0004
B= 10.1233 DB= .0002
C= 7.75507 DC= .00004
GAMMA=108.352 DGAMMA= .001
BETA = 93.940 DBETA = .001
ALPHA= 91.077 DALPHA= .001
V= 980.2
24. 28-1164
Na4UV4O14
Triklin
Dexp Dcal d(D) h k l
6.6000 6.6020 -.0020 0 1 1
6.0800 6.0737 .0063 -1 1 0
5.8400 5.8390 .0010 0 -1 1
5.0100 5.0061 .0039 0 2 0
4.8300 4.8306 -.0006 2 0 0
4.3800 4.3816 -.0016 1 -1 1
3.5800 3.5782 .0018 2 2 1
3.2700 3.2714 -.0014 1 3 1
3.2200 3.2204 -.0004 3 0 0
3.1400 3.1400 .0000 -2 1 2
3.1000 3.0998 .0002 -1 2 2
2.9880 2.9880 -.0000 -2 -2 2
A= 10.342 DA= .001
B= 10.554 DB= .008
C= 8.067 DC= .006
GAMMA= 72.99 DGAMMA= .01
BETA =100.68 DBETA = .02
ALPHA= 86.34 DALPHA= .01
V= 821
25. 28-1166
NaUO2VO4
Triklin
Dexp Dcal d(D) h k l
7.7600 7.7439 .0161 0 1 1
6.3900 6.3939 -.0039 1 0 0
5.8500 5.8476 .0024 0 -1 1
5.1200 5.1150 .0050 1 1 1
4.6100 4.6110 -.0010 -1 1 0
4.3700 4.3671 .0029 0 2 1
4.1200 4.1183 .0017 -1 1 2
3.9700 3.9714 -.0014 1 2 0
3.3700 3.3701 -.0001 -1 0 3
3.2000 3.2004 -.0004 -1 2 0
3.1800 3.1804 -.0004 0 2 3
2.9700 2.9698 .0002 0 -1 3
A= 6.6323 DA= .0005
B= 8.9615 DB= .0005
C= 11.1170 DC= .0007
GAMMA= 79.1422 DGAMMA= .0006
BETA = 97.754 DBETA = .004
ALPHA= 75.665 DALPHA= .007
V= 617.2
26. 28-1167
Na{UO2}{VO3}3}
Triklin
Dexp Dcal d(D) h k l
13.0000 13.0049 -.0049 1 0 0
6.5000 6.5024 -.0024 2 0 0
5.9900 5.9967 -.0067 -1 0 1
5.4200 5.4134 .0066 1 1 0
4.3200 4.3202 -.0002 0 -1 1
3.4400 3.4385 .0015 -2 -1 1
3.3200 3.3202 -.0002 0 0 2
3.0400 3.0398 .0002 3 1 1
2.9760 2.9758 .0002 -4 1 1
2.8990 2.8987 .0003 1 2 1
2.7060 2.7067 -.0007 2 2 0
2.4500 2.4501 -.0001 -5 0 1
A= 13.26899 DA= .00005
B= 6.69623 DB= .00009
C= 6.73467 DC= .00001
GAMMA=101.296 DGAMMA= .001
BETA = 93.715 DBETA = .001
ALPHA= 80.6049 DALPHA= .0008
V= 578.61
27. 28-1343
TiUF5
Monoklin
Grupa 4,11
Dexp Dcal d(D) h k l
6.9000 6.9235 -.0235 0 1 0
3.9900 3.9842 .0058 2 1 0
3.8300 3.8317 -.0017 -1 0 3
3.5000 3.4995 .0005 2 -1 2
3.4600 3.4617 -.0017 0 2 0
3.3500 3.3510 -.0010 -1 -1 3
3.2600 3.2605 -.0005 1 -2 0
3.2400 3.2413 -.0013 0 0 4
3.1600 3.1563 .0037 1 0 4
3.0300 3.0322 -.0022 2 -1 3
2.7060 2.7071 -.0011 3 0 3
2.6330 2.6317 .0013 2 -2 2
A= 9.770 DA= .005
B= 6.923 DB= .002
C= 13.0116 DC= .0005
BETA = 85.16 DBETA = .03
V= 877
Triklin
Dexp Dcal d(D) h k l
6.9000 6.9017 -.0017 -1 1 0
3.9900 3.9900 .0000 -1 2 0
3.8300 3.8309 -.0009 -2 1 1
3.5000 3.4999 .0001 0 -2 1
3.4600 3.4613 -.0013 -2 0 1
3.3500 3.3500 .0000 -2 1 2
3.2600 3.2600 -.0000 -2 2 1
3.2400 3.2395 .0005 2 0 1
3.1600 3.1591 .0009 -2 0 2
3.0300 3.0287 .0013 2 -2 2
2.7060 2.7059 .0001 1 -1 4
2.6330 2.6337 -.0007 2 -2 3
A= 8.023 DA= .001
B= 8.048 DB= .002
C= 11.6919 DC= .0007
GAMMA=118.651 DGAMMA= .009
BETA = 92.3924 DBETA = .0008
ALPHA= 97.420 DALPHA= .008
V= 652.3
28. 28-1344
TiU3F13
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.5300 5.5165 .0135 1 1 0
4.6000 4.5943 .0057 -1 1 1
4.2600 4.2600 .0000 1 0 2
3.7600 3.7620 -.0020 1 1 2
3.6800 3.6859 -.0059 2 0 1
3.5400 3.5461 -.0061 1 2 0
3.3900 3.3881 .0019 -2 0 1
3.3500 3.3490 .0010 2 1 1
3.2600 3.2609 -.0009 -1 2 1
3.1200 3.1209 -.0009 -2 1 1
2.9210 2.9195 .0015 1 2 2
2.7150 2.7134 .0016 2 2 1
a= 7.6586 b= 8.018 c= 9.546 beta= 83.0
da=.0008 db= .003 dc= .003 dbet= .1
V= 582
Triklin
Dexp Dcal d(D) h k l
5.5300 5.5349 -.0049 0 1 0
4.6000 4.5890 .0110 0 -1 2
4.2600 4.2451 .0149 -1 0 2
3.7600 3.7634 -.0034 -1 1 0
3.6800 3.6815 -.0015 -1 1 1
3.5400 3.5354 .0046 0 0 4
3.3900 3.3911 -.0011 -1 1 2
3.3500 3.3463 .0037 -1 -1 2
3.2600 3.2572 .0028 1 -1 2
3.1200 3.1234 -.0034 1 0 3
2.9210 2.9206 .0004 1 1 2
2.7150 2.7182 -.0032 -1 -1 4
A= 4.8159 DA= .0009
B= 5.5768 DB= .0005
C= 14.357 DC= .001
GAMMA= 93.989 DGAMMA= .001
BETA = 98.0972 DBETA = .0004
ALPHA= 95.167 DALPHA= .001
V= 378.9
29. 28-1345
Ti4UF5
Romb
Groupa 19
Dexp. Dcal. d(D) h k l
3.5700 3.5659 .0041 2 2 1
3.3500 3.3450 .0050 0 3 1
3.3100 3.3089 .0011 4 0 0
3.2400 3.2430 -.0030 1 3 1
3.2000 3.1936 .0064 4 1 0
3.0500 3.0514 -.0014 0 4 0
2.9960 2.9909 .0051 3 3 0
2.8520 2.8565 -.0045 0 1 2
2.6480 2.6473 .0007 0 2 2
2.4610 2.4579 .0031 2 2 2
2.3650 2.3677 -.0027 5 1 1
2.3060 2.3079 -.0019 3 4 1
a=13.24 b=12.205 c= 5.876
da= .01 db= .001 dc= .001
V= 949
Triklin
Dexp Dcal d(D) h k l
3.5700 3.5718 -.0018 3 0 0
3.3500 3.3504 -.0004 0 4 0
3.3100 3.3096 .0004 0 -1 1
3.2400 3.2410 -.0010 3 1 0
3.2000 3.1987 .0013 0 1 1
3.0500 3.0508 -.0008 2 3 0
2.9960 2.9961 -.0001 -2 1 1
2.8520 2.8496 .0024 3 2 0
2.6480 2.6489 -.0009 -1 -3 1
2.4610 2.4607 .0003 0 -4 1
2.3650 2.3639 .0011 3 -1 1
2.3060 2.3072 -.0012 3 0 1
A= 11.191 DA= .008
B= 13.927 DB= .005
C= 3.38142 DC= .00008
GAMMA=105.26 DGAMMA= .02
BETA = 96.19 DBETA = .01
ALPHA= 92.36 DALPHA= .01
V= 504
30. 28-1404
N2H4UF4
Triklin
Dexp Dcal d(D) h k l
7.9300 7.9333 -.0033 1 0 0
7.1600 7.1478 .0122 0 1 0
5.5700 5.5696 .0004 -1 0 1
5.3000 5.2994 .0006 0 -1 1
4.5000 4.4974 .0026 1 1 0
4.2000 4.1977 .0023 0 1 2
4.0300 4.0294 .0006 2 -1 1
3.6900 3.6864 .0036 -1 2 1
3.5100 3.5170 -.0070 0 2 1
3.4300 3.4358 -.0058 -2 0 1
3.3100 3.3132 -.0032 2 -1 2
3.1800 3.1811 -.0011 0 -2 1
A= 8.715 DA= .006
B= 7.815 DB= .006
C= 9.495 DC= .002
GAMMA=112.34 DGAMMA= .02
BETA = 82.52 DBETA = .05
ALPHA= 84.982 DALPHA= .001
V= 586.4
31. 28-1407
beta-C4H6O6U
Triklin
Dexp Dcal d(D) h k l
6.4800 6.4803 -.0003 1 1 0
6.3700 6.3632 .0068 0 1 1
6.0400 6.0428 -.0028 0 -1 1
5.1600 5.1595 .0005 1 1 1
4.8600 4.8602 -.0002 1 -1 1
3.7700 3.7663 .0037 -2 -1 1
3.7000 3.6974 .0026 -1 1 2
3.5800 3.5799 .0001 1 1 2
3.5000 3.5003 -.0003 2 -1 1
3.2400 3.2401 -.0001 2 2 0
3.1800 3.1816 -.0016 0 2 2
2.8020 2.8031 -.0011 1 -2 2
A= 9.093 DA= .003
B= 8.897 DB= .001
C= 8.684 DC= .003
GAMMA= 87.80 DGAMMA= .02
BETA = 93.80 DBETA = .05
ALPHA= 87.202 DALPHA= .002
V= 699.5
32. 28-1409
gamma-C4H6O6U
Triklin
Dexp Dcal d(D) h k l
6.4100 6.4040 .0060 0 1 1
6.3300 6.3357 -.0057 0 -1 1
5.9600 5.9581 .0019 -1 1 0
5.6000 5.6046 -.0046 0 2 0
4.9100 4.9026 .0074 -1 -1 1
4.5200 4.5151 .0049 0 -2 1
4.2000 4.1902 .0098 -1 2 0
3.7900 3.7941 -.0041 1 0 2
3.7200 3.7213 -.0013 1 3 0
3.6700 3.6714 -.0014 0 1 2
3.5600 3.5581 .0019 -2 1 0
3.5000 3.4962 .0038 1 3 1
A= 8.4704 DA= .0004
B= 11.516 DB= .004
C= 7.9087 DC= .0001
GAMMA= 76.76 DGAMMA= .06
BETA = 78.19 DBETA = .01
ALPHA= 86.69 DALPHA= .04
V= 735
33. 28-1410
C2H8N2O6U
Romb
Groupa 27
Dexp. Dcal. d(D) h k l
9.2000 9.1871 .0129 1 0 0
6.6600 6.6635 -.0035 0 1 0
3.8600 3.8522 .0078 1 1 2
3.5800 3.5767 .0033 2 1 1
3.1300 3.1322 -.0022 1 2 0
2.6200 2.6195 .0005 2 2 1
2.3600 2.3606 -.0006 2 0 4
2.1300 2.1303 -.0003 4 1 1
2.0200 2.0199 .0001 4 1 2
a= 9.187 b= 6.664 c=11.007
da= .008 db= .002 dc= .009
v= 674
34. 28-1411
UO2F2x{OH}x*2H2O
Triklin
Dexp Dcal d(D) h k l
7.6700 7.6673 .0027 0 1 1
7.5000 7.4851 .0149 -1 0 1
6.0800 6.0866 -.0066 0 -1 1
5.9700 5.9656 .0044 1 0 1
5.3100 5.3122 -.0022 1 1 1
4.9300 4.9363 -.0063 -2 2 0
4.6000 4.6005 -.0005 1 2 0
4.5000 4.5078 -.0078 -1 1 2
4.3200 4.3193 .0007 0 -2 1
4.1900 4.1844 .0056 -1 0 2
4.1100 4.1105 -.0005 0 0 2
3.9100 3.9093 .0007 -3 1 0
A= 12.4876 DA= .0001
B= 13.333 DB= .0028
C= 9.01890 DC= .00001
GAMMA=114.423 DGAMMA= .001
BETA =110.059 DBETA = .001
ALPHA= 69.612 DALPHA= .003
V= 1246.4
35. 28-1412
UO2HF3*2H2O
Romb
Groupa 19
Dexp. Dcal. d(D) h k l
7.7500 7.7130 .0370 0 1 1
7.6300 7.6000 .0300 2 0 0
4.6700 4.6688 .0012 2 0 2
4.6700 4.6577 .0123 3 0 1
3.8500 3.8485 .0015 3 0 2
3.8000 3.8000 -.0000 4 0 0
3.7400 3.7381 .0019 1 2 2
3.5600 3.5596 .0004 4 1 0
3.5000 3.5011 -.0011 2 0 3
3.4300 3.4346 -.0046 3 2 1
3.0700 3.0687 .0013 3 2 2
2.8400 2.8407 -.0007 0 1 4
2.5220 2.5217 .0003 1 2 4
a=15.200 b=10.170 c=11.8339
da= .003 db= .001 dc= .0008
V=1829.3
Triklin
Dexp Dcal d(D) h k l
7.7500 7.7272 .0228 0 0 1
7.6300 7.6165 .0135 1 0 0
4.6700 4.6717 -.0017 0 -2 1
3.8500 3.8485 .0015 -2 -1 1
3.8000 3.7985 .0015 -1 -2 2
3.7400 3.7441 -.0041 0 -2 2
3.5600 3.5608 -.0008 -1 0 2
3.5000 3.5008 -.0008 -2 -2 1
3.4300 3.4311 -.0011 -1 2 0
3.0700 3.0707 -.0007 2 -1 1
2.8400 2.8398 .0002 -1 1 2
2.5220 2.5212 .0008 1 -3 2
A= 7.97619 DA= .00007
B= 9.8788 DB= .0004
C= 8.6456 DC= .0008
GAMMA= 73.318 DGAMMA= .009
BETA =101.25 DBETA = .01
ALPHA=116.30 DALPHA= .01
V= 583.3
36. 28-1413
{UO2}H2F4*4H2O
Triklin
Dexp Dcal d(D) h k l
12.6000 12.5980 .0020 1 0 0
11.5000 11.5001 -.0001 -1 1 0
8.5100 8.5100 .0000 0 0 1
6.9100 6.9102 -.0002 0 -2 1
5.7000 5.6989 .0011 -1 3 0
5.2200 5.2197 .0003 -1 2 1
5.1300 5.1290 .0010 2 0 1
4.2600 4.2600 .0000 -1 3 1
3.7700 3.7700 -.0000 3 -3 1
3.5000 3.5001 -.0001 -1 5 0
3.2800 3.2801 -.0001 2 1 2
2.8450 2.8450 .0000 1 -3 3
A= 13.012 DA= .006
B= 18.111 DB= .008
C= 8.8043 DC= .0005
GAMMA=104.41 DGAMMA= .03
BETA = 84.928 DBETA = .006
ALPHA=104.79 DALPHA= .01
V= 1942
37. 28-1414
{UO2}3H4{SO4}5**H2O
Triklin
Dexp Dcal d(D) h k l
17.2000 17.1752 .0248 1 0 0
12.7000 12.6951 .0049 -1 1 1
10.7000 10.6940 .0060 1 -1 1
9.8400 9.8382 .0018 -1 0 2
8.4200 8.4145 .0055 -1 2 0
7.7300 7.7300 -.0000 -2 1 2
7.4000 7.4032 -.0032 2 -1 1
7.2300 7.2395 -.0095 -2 2 0
6.9100 6.9139 -.0039 -2 -1 1
6.6300 6.6285 .0015 2 1 0
6.3900 6.3903 -.0003 -2 -1 2
5.5100 5.5115 -.0015 1 -1 3
5.3500 5.3470 .0030 2 -2 2
5.2500 5.2503 -.0003 0 -2 3
4.8900 4.8897 .0003 -3 3 1
4.8400 4.8400 -.0000 0 -3 2
4.8000 4.7991 .0009 -4 1 1
A= 19.2891 DA= .0001
B= 16.939 DB= .001
C= 20.298 DC= .009
GAMMA=109.98 DGAMMA= .02
BETA =107.78 DBETA = .03
ALPHA= 89.251 DALPHA= .007
V= 5905
38. 28-1415
UO2{OH}2
Triklin
Dexp Dcal d(D) h k l
8.0700 8.0819 -.0119 0 1 1
7.3700 7.3715 -.0015 -1 0 1
6.8300 6.8261 .0039 0 -1 1
5.0800 5.0837 -.0037 -1 -2 1
4.9500 4.9549 -.0049 1 0 1
4.4600 4.4608 -.0008 -1 0 2
4.0500 4.0496 .0004 -1 -3 1
3.8600 3.8616 -.0016 -2 2 1
3.7500 3.7486 .0014 -2 -2 1
3.7000 3.7011 -.0011 2 2 0
3.6100 3.6109 -.0009 -1 -2 2
3.5000 3.5008 -.0008 -2 2 2
A= 8.7526 DA= .0002
B= 16.0509 DB= .0009
C= 9.1900 DC= .0003
GAMMA= 90.701 DGAMMA= .001
BETA =111.911 DBETA = .002
ALPHA= 78.947 DALPHA= .007
V= 1173.2
39. 28-1418
alfa-UO2SO4*H2O
Triklin
Dexp Dcal d(D) h k l
9.1400 9.1615 -.0215 0 1 1
8.4500 8.4513 -.0013 -1 1 1
7.9600 7.9358 .0242 0 -1 1
7.5700 7.5500 .0200 0 0 2
7.1100 7.1175 -.0075 -1 -1 1
5.9400 5.9400 -.0000 -2 1 1
5.8300 5.8284 .0016 -2 0 2
5.6700 5.6779 -.0079 0 -1 2
5.3300 5.3299 .0001 2 0 1
5.1300 5.1270 .0030 0 2 0
5.0200 5.0212 -.0012 -1 2 1
4.8200 4.8204 -.0004 0 1 3
A= 13.495 DA= .007
B= 10.442 DB= .003
C= 16.114 DC= .003
GAMMA= 96.40 DGAMMA= .05
BETA =108.51 DBETA = .01
ALPHA= 79.6395 DALPHA= .0007
V= 2114
40. 28-1419
{UO2}U5 O15SO4*18H2O
Triklin
Dexp Dcal d(D) h k l
18.6000 18.6074 -.0074 1 0 0
16.7000 16.7612 -.0612 0 1 0
14.9000 14.9399 -.0399 -1 0 1
14.6000 14.6008 -.0008 1 0 1
13.8000 13.7975 .0025 -1 1 0
12.4000 12.3866 .0134 0 1 1
11.3000 11.3031 -.0031 0 -1 2
9.2500 9.2451 .0049 -1 -1 2
8.6500 8.6485 .0015 2 -1 1
8.1500 8.1506 -.0006 0 -1 3
8.0400 8.0399 .0001 -2 1 1
7.3000 7.3004 -.0004 2 0 2
A= 18.945 DA= .002
B= 17.65 DB= .01
C= 25.121 DC= .003
GAMMA=100.76 DGAMMA= .01
BETA = 88.5575 DBETA = .0001
ALPHA=104.877 DALPHA= .002
V= 7973
41. 28-1420
{UO2}2U3O9SO4*23H2O
Triklin
Dexp Dcal d(D) h k l
14.1000 14.1080 -.0080 1 0 0
13.9000 13.9173 -.0173 -1 1 0
12.4000 12.3445 .0555 -1 0 1
12.3000 12.2897 .0103 -1 1 1
8.5400 8.5401 -.0001 1 0 1
8.4700 8.4729 -.0029 1 -1 1
8.1100 8.1086 .0014 -1 -1 1
8.0600 8.0620 -.0020 -1 2 1
6.9600 6.9587 .0013 -2 2 0
6.7400 6.7400 .0000 -2 1 2
6.1700 6.1723 -.0023 -2 0 2
6.0800 6.0800 .0000 -1 -1 2
A= 17.237 DA= .001
B= 17.3293 DB= .0003
C= 15.255 DC= .003
GAMMA=119.003 DGAMMA= .007
BETA =113.54 DBETA = .01
ALPHA= 78.449 DALPHA= .005
V= 3654.6
42. 28-1421
C14H18Br0.99N9.01O10.03U
Triklin
Dexp Dcal d(D) h k l
10.1000 10.0826 .0174 0 0 1
7.9100 7.9119 -.0019 -1 -1 1
6.7000 6.6997 .0003 0 -2 1
6.5500 6.5496 .0004 1 -2 1
5.9800 5.9838 -.0038 -1 -2 1
5.6400 5.6418 -.0018 3 0 1
5.4400 5.4388 .0012 0 -1 2
5.2500 5.2488 .0012 2 2 0
4.9100 4.9154 -.0054 2 0 2
4.8000 4.8035 -.0035 2 -2 2
4.1260 4.1278 -.0018 0 -3 2
3.9000 3.9000 .0000 2 3 0
A= 17.8966 DA= .0001
B= 13.971 DB= .001
C= 11.250 DC= .001
GAMMA= 94.06 DGAMMA= .01
BETA = 75.250 DBETA = .005
ALPHA=112.36 DALPHA= .02
V= 2514.8
43. 28-1422
C4H18Br0.765N9.235O10.705
Triklin
Dexp Dcal d(D) h k l
9.8500 9.8463 .0037 1 0 0
7.6000 7.5916 .0084 0 1 1
6.4900 6.4968 -.0068 0 -1 1
5.8700 5.8717 -.0017 2 1 1
5.6500 5.6486 .0014 1 -1 1
5.2700 5.2753 -.0053 1 2 1
4.8000 4.7981 .0019 0 1 2
4.6900 4.6968 -.0068 2 0 2
4.0900 4.0955 -.0055 2 -1 1
3.9500 3.9478 .0022 -2 1 0
3.6200 3.6183 .0017 3 0 1
3.4300 3.4290 .0010 3 1 3
A= 11.931 DA= .008
B= 10.639 DB= .002
C= 11.894 DC= .003
GAMMA= 66.46 DGAMMA= .01
BETA = 59.52 DBETA = .01
ALPHA= 71.05 DALPHA= .01
V= 1178
44. 28-1423
C4H18Br0.39N9.61O11.83U
Triklin
Dexp Dcal d(D) h k l
9.8800 9.8842 -.0042 0 -1 1
7.6400 7.6444 -.0044 -1 -1 1
6.5600 6.5568 .0032 0 -2 1
5.9600 5.9588 .0012 -1 1 1
5.7600 5.7611 -.0011 -1 2 0
5.4100 5.4134 -.0034 -2 0 1
5.2700 5.2678 .0022 -2 -1 1
4.7800 4.7800 .0000 2 -2 1
4.7000 4.7005 -.0005 1 -2 2
4.0200 4.0197 .0003 3 -1 1
3.6000 3.6001 -.0001 2 2 1
3.4900 3.4898 .0002 -2 1 2
A= 12.926 DA= .002
B= 13.561 DB= .008
C= 10.790 DC= .001
GAMMA= 94.567 DGAMMA= .001
BETA = 88.49 DBETA = .01
ALPHA=113.447 DALPHA= .005
V=1730
45. 28-1424
C4H18Cl0.5N9.5O11.5U
Triklin
Dexp Dcal d(D) h k l
9.9600 9.9149 .0452 0 1 1
7.5300 7.5290 .0010 -1 0 1
7.3000 7.2891 .0109 0 -1 1
6.1100 6.1145 -.0045 1 0 1
5.9200 5.9166 .0034 -1 0 2
5.4300 5.4345 -.0045 0 2 1
4.9500 4.9510 -.0010 1 2 1
4.8300 4.8337 -.0037 0 1 3
4.6200 4.6236 -.0036 1 0 2
4.4800 4.4806 -.0006 -1 0 3
4.0500 4.0491 .0009 -1 2 1
3.8900 3.8876 .0024 1 1 3
A= 8.122 DA= .003
B= 11.199 DB= .006
C= 14.861 DC= .006
GAMMA= 76.532 DGAMMA= .001
BETA = 99.65 DBETA = .02
ALPHA= 74.96 DALPHA= .03
V= 1231
46. 28-1424
C4H18Cl0.5N9.5O11.5U
Triklin
Dexp Dcal d(D) h k l
9.9600 9.9149 .0452 0 1 1
7.5300 7.5290 .0010 -1 0 1
7.3000 7.2891 .0109 0 -1 1
6.1100 6.1145 -.0045 1 0 1
5.9200 5.9166 .0034 -1 0 2
5.4300 5.4345 -.0045 0 2 1
4.9500 4.9510 -.0010 1 2 1
4.8300 4.8337 -.0037 0 1 3
4.6200 4.6236 -.0036 1 0 2
4.4800 4.4806 -.0006 -1 0 3
4.0500 4.0491 .0009 -1 2 1
3.8900 3.8876 .0024 1 1 3
A= 8.122 DA= .003
B= 11.199 DB= .006
C= 14.861 DC= .006
GAMMA= 76.532 DGAMMA= .001
BETA = 99.65 DBETA = .02
ALPHA= 74.96 DALPHA= .03
V= 1231
47. 28-1425
C4H24ClN5O10U
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
18.9000 18.8662 .0338 0 0 1
16.5000 16.4712 .0288 1 1 0
12.6000 12.5731 .0269 1 1 1
9.6000 9.5920 .0080 2 0 1
8.9500 8.9604 -.0104 2 1 1
6.2600 6.2605 -.0005 0 3 2
5.9900 5.9874 .0026 -1 0 3
5.6200 5.6227 -.0027 0 2 3
4.9300 4.9295 .0005 1 3 3
4.7500 4.7491 .0009 2 4 2
4.1400 4.1402 -.0002 2 2 4
4.0200 4.0202 -.0002 -3 5 1
a= 21.837 b= 25.11 c= 18.8777 beta= 87.99
da= .006 db=.01 dc=.0007 dbeta=.03
V= 10344
48. 28-1426
C4H24I0.36N9.64O11.92U
Triklin
Dexp Dcal d(D) h k l
9.9600 9.9556 .0044 1 0 0
7.5500 7.5537 -.0037 -1 1 2
6.5800 6.5724 .0076 1 1 0
6.0200 6.0196 .0004 -1 2 1
5.6500 5.6521 -.0021 -1 2 2
5.5100 5.5056 .0044 0 2 0
5.2600 5.2580 .0020 -2 0 1
4.8200 4.8209 -.0009 0 0 3
4.6700 4.6690 .0010 -2 1 3
4.1100 4.1115 -.0015 -1 -2 1
3.7600 3.7615 -.0015 -3 1 2
3.5800 3.5793 .0007 -3 1 3
A= 11.340 DA= .003
B= 12.244 DB= .002
C= 16.3901 DC= .0001
GAMMA=111.95 DGAMMA= .05
BETA =114.484 DBETA = .05
ALPHA= 68.81 DALPHA= .01
V= 1863
49. 28-1427
C4H24I1.1N8.9O9.7U
Triklin
Dexp Dcal d(D) h k l
10.1000 10.1013 -.0013 1 0 0
7.6600 7.6573 .0027 -1 0 1
6.6300 6.6265 .0035 1 -2 1
6.0900 6.0934 -.0034 -1 2 0
5.9000 5.9001 -.0001 0 -2 1
5.7000 5.6980 .0020 2 -1 1
5.4900 5.4947 -.0047 -2 1 0
5.3500 5.3491 .0009 -1 0 2
5.2300 5.2298 .0002 0 1 2
4.9600 4.9597 .0003 2 0 1
4.7500 4.7511 -.0011 0 -1 3
4.6600 4.6584 .0016 -2 1 1
A= 11.482 DA= .003
B= 13.3983 DB= .0007
C= 14.967 DC= .005
GAMMA=117.42 DGAMMA= .03
BETA = 73.41 DBETA = .02
ALPHA=112.4395 DALPHA= .0007
V= 1872
50. 28-1428
C4H24N10O13U
Triklin
Dexp Dcal d(D) h k l
9.7700 9.7866 -.0166 1 -1 0
7.3600 7.3779 -.0179 0 2 0
6.4700 6.4597 .0103 0 0 1
5.9400 5.9472 -.0072 -2 1 0
5.6100 5.6194 -.0094 1 0 1
5.4700 5.4757 -.0057 0 -2 1
5.1900 5.1857 .0043 -1 1 1
4.7200 4.7194 .0006 -2 -1 1
4.6200 4.6178 .0022 -1 3 0
4.0800 4.0768 .0032 2 -2 1
3.7400 3.7415 -.0015 -3 2 0
3.5600 3.5601 -.0001 -1 4 0
A= 12.952 DA= .008
B= 15.106 DB= .006
C= 6.629 DC= .001
GAMMA= 89.91 DGAMMA= .08
BETA = 94.03 DBETA = .02
ALPHA=102.34 DALPHA= .02
V= 1264
51. 28-1823
C9H15NaO8U*xH2O
Triklin
Dexp Dcal d(D) h k l
9.7100 9.6834 .0266 0 1 1
8.4900 8.4840 .0060 0 -1 1
7.7300 7.7371 -.0071 -1 1 0
7.0700 7.0779 -.0079 1 -1 1
6.3300 6.3304 -.0004 1 1 1
6.1100 6.1092 .0008 1 -1 2
5.9200 5.9175 .0025 1 1 2
5.6400 5.6413 -.0013 0 -1 3
5.5300 5.5354 -.0054 0 1 4
5.3000 5.3004 -.0004 -1 -1 2
5.0400 5.0360 .0040 -1 1 4
4.8000 4.8016 -.0016 -2 0 1
4.7100 4.7113 -.0013 -1 2 2
4.3300 4.3288 .0012 2 -1 2
A= 10.042 DA= .004
B= 10.1376 DB= .0005
C= 24.08 DC= .02
GAMMA=101.42 DGAMMA= .02
BETA = 91.19 DBETA = .01
ALPHA= 79.24 DALPHA= .02
V= 2360
52. 28-1949
C36H30Cl4S3U
Triklin
Dexp Dcal d(D) h k l
10.4000 10.4367 -.0367 0 1 1
10.0000 9.9935 .0065 0 -1 1
8.2100 8.2108 -.0008 1 0 1
7.9900 8.0022 -.0122 1 1 0
7.5200 7.5426 -.0226 0 2 0
6.5100 6.5077 .0023 0 -2 1
6.3500 6.3444 .0056 -1 0 1
6.2700 6.2702 -.0002 1 0 2
6.1700 6.1732 -.0032 -1 -1 1
5.5700 5.5697 .0003 -1 1 1
5.0300 5.0284 .0016 0 3 0
4.8300 4.8285 .0015 1 3 1
A= 8.878 DA= .007
B= 15.536 DB= .003
C= 14.56 DC= .01
GAMMA= 76.39 DGAMMA= .02
BETA = 72.35 DBETA = .02
ALPHA= 83.59 DALPHA= .02
V= 1858.4
53. 28-1950
C48H40Cl4O4S4U
Triklin
Dexp Dcal d(D) h k l
10.8000 10.8013 -.0013 -1 0 1
9.8600 9.8856 -.0256 0 1 1
9.4800 9.4652 .0148 0 -1 1
9.0200 9.0145 .0055 1 0 1
7.2100 7.2099 .0001 -1 1 0
6.6500 6.6471 .0029 -1 1 2
5.5900 5.5923 -.0023 -2 0 1
5.4900 5.4889 .0011 -1 0 4
5.2100 5.2086 .0014 -2 -1 1
4.8000 4.8001 -.0001 2 1 1
4.7100 4.7101 -.0001 -1 -2 2
4.1400 4.1404 -.0004 -1 -1 5
A= 11.2615 DA= .0002
B= 10.8205 DB= .0002
C= 22.883 DC= .001
GAMMA= 83.393 DGAMMA= .006
BETA =102.82 DBETA = .01
ALPHA= 88.388 DALPHA= .003
V= 2697
54. 28-1951
C22H48CrN24O32U*5H2O
Triklin
Dexp Dcal d(D) h k l
8.3200 8.3130 .0070 1 0 0
7.3300 7.3309 -.0009 0 1 0
6.5900 6.5907 -.0007 0 1 1
6.0700 6.0751 -.0051 0 -1 1
5.3600 5.3621 -.0021 -1 1 1
4.5400 4.5414 -.0014 0 -1 2
4.0700 4.0703 -.0003 -2 1 0
3.6400 3.6399 .0001 -2 1 1
3.3600 3.3598 .0002 -1 0 3
3.1300 3.1303 -.0003 1 2 1
2.9800 2.9802 -.0002 2 -2 2
2.6900 2.6898 .0002 2 -2 3
A= 8.890 DA= .005
B= 7.5655 DB= .0001
C= 12.962 DC= .009
GAMMA=103.30 DGAMMA= .03
BETA = 74.74 DBETA = .07
ALPHA= 88.48 DALPHA= .01
V= 815
55. 28-1952
C20H24U
Triklin
Dexp Dcal d(D) h k l
7.8200 7.8189 .0011 -1 0 1
6.9900 6.9954 -.0054 0 1 1
6.0400 6.0309 .0091 0 -1 1
5.8000 5.7908 .0092 0 0 2
5.2700 5.2689 .0011 -1 0 2
4.9000 4.9035 -.0035 1 -1 1
4.7000 4.7005 -.0005 -1 1 2
3.8100 3.8089 .0011 -2 -1 1
3.3800 3.3803 -.0003 -1 2 2
3.2800 3.2802 -.0002 1 1 3
2.9300 2.9297 .0003 -2 2 2
2.8300 2.8304 -.0004 -2 -1 3
A= 9.387 DA= .001
B= 7.887 DB= .006
C= 11.862 DC= .006
GAMMA= 91.81 DGAMMA= .02
BETA = 98.54 DBETA = .01
ALPHA= 80.69 DALPHA= .04
V= 857
Triklin
Dexp Dcal d(D) h k l
7.8200 7.8267 -.0067 1 0 0
6.9900 6.9745 .0155 1 1 0
6.0400 6.0378 .0022 1 0 1
5.8000 5.7965 .0035 0 1 1
5.2700 5.2754 -.0054 1 -1 1
4.9000 4.8909 .0091 0 -1 2
4.7000 4.6996 .0004 1 2 0
3.8100 3.8109 -.0009 -2 -1 1
3.3800 3.3794 .0006 -2 1 0
3.2800 3.2812 -.0012 0 -1 3
2.9300 2.9300 -.0000 2 -1 2
2.8300 2.8301 -.0001 1 3 1
A= 8.06357 DA= .00005
B= 10.877 DB= .001
C= 9.8737 DC= .0001
GAMMA= 76.150 DGAMMA= .003
BETA = 93.68 DBETA = .01
ALPHA=110.95 DALPHA= .03
V= 785.4
56. 28-1954
C64H32N16U
Triklin
Dexp Dcal d(D) h k l
12.7000 12.6815 .0185 1 0 0
11.2000 11.2124 -.0124 0 1 0
8.5700 8.5634 .0066 0 1 1
7.8200 7.8215 -.0015 1 -1 1
7.2200 7.2225 -.0025 -1 0 1
5.5200 5.5114 .0086 1 0 2
5.2100 5.2090 .0010 0 1 2
4.8800 4.8790 .0010 -2 0 1
4.5200 4.5164 .0036 1 2 0
3.9200 3.9218 -.0018 -1 3 1
3.7500 3.7503 -.0003 0 3 1
3.5900 3.5896 .0004 0 1 3
A= 14.168 DA= .004
B= 12.223 DB= .001
C= 11.175 DC= .008
GAMMA=111.04 DGAMMA= .01
BETA = 76.51 DBETA = .02
ALPHA= 85.19 DALPHA= .02
V= 1726
57. 28-1955
C6H12Cl4O2P2U
Triklin
Dexp Dcal d(D) h k l
8.0300 8.0262 .0038 1 0 0
7.5600 7.5484 .0116 0 1 1
6.8600 6.8622 -.0022 0 -1 1
5.7300 5.7429 -.0129 0 0 2
5.5300 5.5289 .0011 -1 1 0
5.0600 5.0651 -.0051 1 1 2
4.6700 4.6717 -.0017 0 -1 2
4.2500 4.2463 .0037 -1 0 2
3.9800 3.9793 .0007 2 1 0
3.8000 3.7981 .0019 1 0 3
3.5500 3.5513 -.0013 -2 0 1
3.4900 3.4897 .0003 2 2 1
A= 8.451 DA= .005
B= 9.492 DB= .005
C= 11.9097 DC= .0006
GAMMA= 76.90 DGAMMA= .03
BETA = 75.70 DBETA = .02
ALPHA= 81.50 DALPHA= .03
V= 897.4
58. 28-1955
C6H12Cl4O2P2U
Triklin
Dexp Dcal d(D) h k l
8.0300 8.0262 .0038 1 0 0
7.5600 7.5484 .0116 0 1 1
6.8600 6.8622 -.0022 0 -1 1
5.7300 5.7429 -.0129 0 0 2
5.5300 5.5289 .0011 -1 1 0
5.0600 5.0651 -.0051 1 1 2
4.6700 4.6717 -.0017 0 -1 2
4.2500 4.2463 .0037 -1 0 2
3.9800 3.9793 .0007 2 1 0
3.8000 3.7981 .0019 1 0 3
3.5500 3.5513 -.0013 -2 0 1
3.4900 3.4897 .0003 2 2 1
A= 8.451 DA= .005
B= 9.492 DB= .005
C= 11.9097 DC= .0006
GAMMA= 76.90 DGAMMA= .03
BETA = 75.70 DBETA = .02
ALPHA= 81.50 DALPHA= .03
V= 897.4
59. 28-1956
C6H12Cl4O2P2U
Triklin
Dexp Dcal d(D) h k l
7.0900 7.0907 -.0007 0 1 1
6.4900 6.4812 .0088 0 -1 1
4.8100 4.8054 .0046 -1 -1 1
4.7200 4.7217 -.0017 1 1 1
4.1100 4.1073 .0027 -1 1 1
4.0200 4.0212 -.0012 1 0 2
3.9600 3.9597 .0003 1 1 2
3.6400 3.6399 .0001 1 2 0
3.5700 3.5709 -.0009 -1 0 3
3.1300 3.1304 -.0004 -1 -2 2
3.0900 3.0896 .0004 0 1 4
2.8150 2.8154 -.0004 -1 2 2
A= 5.7331 DA= .0005
B= 8.184 DB= .002
C= 12.961 DC= .002
GAMMA= 77.72 DGAMMA= .01
BETA = 94.49 DBETA = .02
ALPHA= 85.36 DALPHA= .02
V= 589.4
60. 28-1957
C9H18Cl4O3P3U
Triklin
Dexp Dcal d(D) h k l
7.9900 8.0038 -.0138 -1 0 1
7.3800 7.3817 -.0017 0 1 1
7.0300 7.0391 -.0091 0 -1 1
6.7000 6.6824 .0176 0 2 0
5.4300 5.4314 -.0014 -1 -2 1
5.2800 5.2711 .0089 -2 0 1
4.8700 4.8732 -.0032 -1 2 1
4.5900 4.5929 -.0029 2 2 0
4.2200 4.2230 -.0030 -1 1 2
4.1400 4.1365 .0035 0 1 2
4.0700 4.0714 -.0014 1 -2 1
3.8700 3.8691 .0009 0 -3 1
A= 11.2374 DA= .0003
B= 13.6610 DB= .0009
C= 9.0428 DC= .0003
GAMMA= 78.43028 DGAMMA= .00007
BETA =108.72 DBETA = .01
ALPHA= 90.914 DALPHA= .006
V= 1286
61. 28-1958
C14H10O6*2H2O
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
18.7000 18.6185 .0815 0 0 1
9.1800 9.1906 -.0106 2 0 1
6.9100 6.9854 -.0754 2 0 2
6.5900 6.5892 .0008 3 0 1
6.2100 6.2062 .0038 0 0 3
5.2900 5.2839 .0061 4 0 0
5.0600 5.0665 -.0065 1 1 3
4.6700 4.6673 .0027 0 2 1
4.2000 4.1960 .0040 1 2 2
3.9600 3.9679 -.0079 2 2 2
3.5000 3.4981 .0019 4 2 1
3.4300 3.4277 .0023 1 1 5
a=21.13562 b= 9.643 c=18.62
da= .00008 db= .007 dc= .03
V=3794
Triklin
Dexp Dcal d(D) h k l
18.7000 18.6807 .0193 1 0 0
9.1800 9.2061 -.0261 1 1 0
6.9100 6.9069 .0031 0 -1 1
6.5900 6.6046 -.0146 -2 0 1
6.2100 6.2045 .0055 2 0 1
5.2900 5.2800 .0100 2 1 1
5.0600 5.0599 .0001 -3 -1 1
4.6700 4.6702 -.0002 4 0 0
4.2000 4.1995 .0005 -1 -1 2
3.9600 3.9593 .0007 -4 1 0
3.5000 3.5011 -.0011 -1 -2 2
3.4300 3.4289 .0011 -2 -2 2
A= 18.998 DA= .002
B= 9.8638 DB= .0004
C= 8.8658 DC= .0002
GAMMA= 80.15 DGAMMA= .02
BETA = 94.78 DBETA = .01
ALPHA= 97.42 DALPHA= .05
V= 1620
62. 28-1959
C6H10O6U
Triklin
Dexp Dcal d(D) h k l
7.4300 7.4383 -.0083 1 0 0
7.0200 7.0084 .0116 0 1 1
6.6000 6.5977 .0023 0 -1 1
4.1700 4.1693 .0007 1 2 0
3.9300 3.9303 -.0003 0 3 0
3.6900 3.6899 .0001 -1 3 1
3.5400 3.5420 -.0020 -2 2 0
3.0000 2.9998 .0002 2 1 1
2.9700 2.9705 -.0005 -1 -3 1
2.7600 2.7610 -.0010 2 -3 1
2.6700 2.6696 .0004 1 -3 2
2.6300 2.6292 .0008 -2 4 0
A= 7.727 DA= .001
B= 12.184 DB= .001
C= 8.412 DC= .002
GAMMA=104.14 DGAMMA= .01
BETA = 98.032 DBETA = .008
ALPHA= 84.522 DALPHA= .005
V= 758.8
63. 28-1960
C6H10O6U*2H2O
Triklin
Dexp Dcal d(D) h k l
7.3100 7.3100 -.0000 0 -1 1
6.9700 6.9705 -.0005 -1 1 1
5.6400 5.6396 .0004 1 -1 1
5.4700 5.4688 .0012 1 0 1
5.2100 5.2099 .0001 0 -2 1
4.2100 4.2105 -.0005 -1 3 0
3.7300 3.7291 .0009 2 0 1
3.5600 3.5602 -.0002 -3 1 0
3.3000 3.3016 -.0016 2 2 0
3.1500 3.1500 .0000 0 2 2
3.0700 3.0702 -.0002 1 1 2
2.9600 2.9596 .0004 3 1 0
A= 11.329 DA= .001
B= 12.6544 DB= .0007
C= 8.797 DC= .001
GAMMA=108.534 DGAMMA= .008
BETA =109.06 DBETA = .06
ALPHA= 92.1595 DALPHA= .0004
V= 1116.1