1. 32-0251
CsNi{ClO4}3
Rombik
Groupa 26,28,51
Dexp. Dcal. d(D) h k l
4.4803 4.4794 .0009 0 1 0
3.6602 3.6600 .0002 1 1 0
3.3903 3.3902 .0001 1 1 1
3.1703 3.1741 -.0039 0 1 2
2.9902 2.9933 -.0031 2 0 1
2.5902 2.5898 .0003 2 1 0
2.3201 2.3197 .0004 1 1 3
2.2402 2.2397 .0005 0 2 0
2.1802 2.1799 .0003 2 0 3
2.0602 2.0599 .0003 3 0 1
2.0061 2.0049 .0012 0 2 2
1.6941 1.6951 -.0010 2 2 2
1.5871 1.5871 .0001 0 2 4
1.4961 1.4959 .0002 4 1 0
a= 6.348 b= 4.479 c= 8.997
da= .002 db= .002 dc= .006
v= 255.8
Triklin
Dexp Dcal d(D) h k l
4.4803 4.4804 -.0001 1 0 0
3.6602 3.6589 .0013 0 1 0
3.3903 3.3883 .0020 -1 0 1
3.1703 3.1695 .0008 0 -1 1
2.9902 2.9895 .0007 -1 1 0
2.5902 2.5899 .0002 1 1 1
2.3201 2.3200 .0002 1 -1 2
2.2402 2.2402 -.0000 2 0 0
2.1802 2.1800 .0002 1 1 2
2.0602 2.0604 -.0003 -1 1 2
2.0061 2.0065 -.0004 2 -1 1
1.6941 1.6941 -.0000 -2 0 2
1.5871 1.5872 -.0001 0 2 2
1.4961 1.4960 .0001 1 2 2
A= 4.5796 DA= .0006
B= 3.6792 DB= .0007
C= 6.469 DC= .001
GAMMA= 96.02 DGAMMA= .03
BETA = 79.62 DBETA = .02
ALPHA= 90.99 DALPHA= .05
V= 106.6
2. 32-0691
Ni{ClO4}2
Triklin
Dexp Dcal d(D) h k l
7.3106 7.3097 .0009 1 0 0
3.5803 3.5806 -.0003 1 1 1
2.4402 2.4395 .0007 3 -1 1
2.3702 2.3709 -.0007 1 2 1
2.2601 2.2597 .0004 2 1 2
1.9891 1.9889 .0003 0 -3 1
1.9731 1.9736 -.0004 2 -3 1
1.8411 1.8411 .0001 3 1 2
1.7461 1.7463 -.0002 -4 0 1
1.7011 1.7011 .0000 3 2 0
1.6581 1.6581 -.0000 -3 1 3
1.5121 1.5122 -.0000 -4 2 2
1.4881 1.4881 -.0000 2 -4 2
1.4471 1.4471 .0000 -5 1 1
1.3731 1.3730 .0001 -3 4 1
A= 7.5704 DA= .0008
B= 6.2303 DB= .0003
C= 7.590 DC= .007
GAMMA=104.51 DGAMMA= .01
BETA = 83.96 DBETA = .03
ALPHA= 98.13 DALPHA= .04
V= 342.2
3. 32-0697
Ni{ReO4}2*2H2O
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
5.3203 5.3213 -.0010 0 0 2
3.4903 3.4989 -.0086 2 0 2
3.4002 3.3947 .0055 1 1 0
2.8202 2.8191 .0011 2 0 3
2.4502 2.4527 -.0025 1 1 3
2.1502 2.1494 .0007 0 1 4
1.9601 1.9587 .0014 4 1 0
1.8301 1.8299 .0002 5 0 1
1.7101 1.7093 .0009 2 1 5
1.7101 1.7147 -.0046 4 1 3
1.5401 1.5391 .0010 3 0 6
1.5201 1.5204 -.0003 0 0 7
1.4401 1.4413 -.0012 4 1 5
a= 9.288 b= 3.6470 c=10.643
da= .003 db= .0006 dc= .002
V= 360.5
4. 32-0703
Ni{TeO4}2
Triklin
Dexp Dcal d(D) h k l
3.7703 3.7718 -.0015 1 0 0
2.8102 2.8109 -.0007 1 1 1
2.5701 2.5697 .0005 -1 -1 1
2.2601 2.2603 -.0001 1 2 0
2.0502 2.0502 -.0000 0 -2 2
1.8901 1.8910 -.0009 -1 1 1
1.7601 1.7604 -.0003 0 1 2
1.6201 1.6199 .0003 -2 1 0
1.5701 1.5700 .0001 0 3 0
1.4001 1.4000 .0001 1 1 3
1.3601 1.3601 -.0000 1 -3 3
1.3101 1.3101 .0000 -1 -2 3
A= 4.157 DA= .001
B= 5.124 DB= .001
C= 5.1188 DC= .0003
GAMMA= 84.08 DGAMMA= .03
BETA = 69.311 DBETA = .008
ALPHA=108.61 DALPHA= .01
V= 93.8
5. 32-0705
C4H4NiO2S*3H2O
Triklin
Dexp Dcal d(D) h k l
7.4404 7.4323 .0081 1 0 0
6.9909 6.9903 .0005 1 1 0
5.8905 5.8966 -.0061 1 0 1
5.7303 5.7352 -.0049 -1 -1 1
4.8804 4.8833 -.0029 0 1 1
4.6103 4.6224 -.0121 -1 -2 1
4.3804 4.3562 .0242 0 2 0
3.8904 3.8982 -.0078 0 0 2
3.7104 3.7162 -.0058 2 0 0
3.6003 3.5973 .0029 2 0 1
3.5103 3.5108 -.0004 2 1 1
3.3403 3.3416 -.0014 -1 -3 1
A= 7.937 DA= .007
B= 10.096 DB= .007
C= 8.5851 DC= .0006
GAMMA= 71.79 DGAMMA= .05
BETA = 88.56 DBETA = .05
ALPHA=112.9 DALPHA= .1
V= 593.5
6. 32-0714
NiTeO3
Tetrag
Groupa 105,112,131
Dexp. Dcal. d(D) h k l
4.7313 4.7174 .0138 2 0 0
3.8692 3.8699 -.0007 1 1 2
3.1662 3.1672 -.0011 0 0 3
2.8762 2.8612 .0151 1 1 3
2.7302 2.7300 .0002 2 2 2
2.5212 2.5228 -.0017 3 2 1
2.5212 2.5330 -.0118 2 1 3
2.1112 2.1097 .0015 4 2 0
2.0171 2.0173 -.0002 3 2 3
1.8861 1.8870 -.0008 5 0 0
1.7251 1.7242 .0009 5 1 2
1.5611 1.5618 -.0007 1 0 6
1.4621 1.4619 .0002 4 1 5
a= 9.435 c= 9.50
da= .006 dc= .01
v= 845.8
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
4.7313 4.7309 .0004 1 1 0
3.8692 3.8678 .0014 0 2 1
3.1662 3.1663 -.0001 -1 2 1
2.8762 2.8751 .0012 0 3 0
2.7302 2.7312 -.0011 0 3 1
2.5212 2.5207 .0005 1 1 3
2.1112 2.1111 .0000 2 2 2
2.0171 2.0165 .0007 2 3 0
1.8861 1.8860 .0002 3 0 0
1.7251 1.7251 .0001 0 5 0
1.5611 1.5613 -.0003 3 3 1
1.4621 1.4622 -.0001 -2 4 3
a= 5.663 b= 8.625 c= 8.752 beta= 87.6
da=.001 db=.006 dc=.05 dbeta=.1
V= 427.1
7. 32-0715
NiTeO3
Rombik
Groupa 30,53
Dexp. Dcal. d(D) h k l
4.1402 4.1679 -.0277 1 1 0
3.9053 3.9116 -.0063 4 0 0
3.7903 3.7845 .0057 2 1 0
3.3203 3.3288 -.0086 3 1 0
3.2003 3.2063 -.0061 0 1 1
2.9692 2.9668 .0024 2 1 1
2.9032 2.9008 .0024 4 1 0
2.5992 2.6077 -.0085 6 0 0
2.4872 2.4797 .0075 4 1 1
2.1692 2.1722 -.0030 3 0 2
1.7821 1.7820 .0001 8 1 0
1.5141 1.5134 .0007 8 0 2
a=15.65 b= 4.324 c= 4.78
da= .02 db= .004 dc= .01
V= 323.3
Triklin
Dexp Dcal d(D) h k l
4.1402 4.1397 .0005 -1 1 1
3.9053 3.9107 -.0055 0 1 1
3.7903 3.7882 .0021 0 -1 1
3.3203 3.3227 -.0025 1 -1 1
3.2003 3.2011 -.0008 -2 1 1
2.9692 2.9695 -.0003 0 2 0
2.9032 2.9027 .0005 1 1 1
2.5992 2.5968 .0024 0 2 1
2.4872 2.4878 -.0006 1 -2 1
2.1692 2.1691 .0000 2 -2 1
1.7821 1.7821 .0000 -4 1 1
1.5141 1.5140 .0001 1 -1 3
A= 7.168 DA= .001
B= 6.3019 DB= .0009
C= 5.2278 DC= .0005
GAMMA=109.46 DGAMMA= .01
BETA =104.80 DBETA = .02
ALPHA= 83.435 DALPHA= .005
V= 215.2
8. 32-0932
RbNi{ClO4}3
Rombik
Groupa 32,55
Dexp. Dcal. d(D) h k l
6.1904 6.1996 -.0092 1 1 0
4.4102 4.4200 -.0098 1 1 2
4.2904 4.2920 -.0016 2 0 0
4.2303 4.2227 .0076 0 2 1
3.9903 3.9728 .0175 1 2 0
3.8702 3.8711 -.0009 2 1 0
3.7903 3.7891 .0012 1 2 1
3.6503 3.6525 -.0023 0 2 2
3.5602 3.5477 .0126 2 0 2
3.3002 3.2987 .0015 2 1 2
3.1502 3.1517 -.0015 0 0 4
3.0902 3.0998 -.0096 2 2 0
a= 8.584 b= 8.9632 c=12.61
da= .001 db= .0008 dc= .01
V= 970
Triklin
Dexp Dcal d(D) h k l
6.1904 6.1789 .0114 1 2 0
4.4102 4.4132 -.0030 0 1 1
4.2904 4.2906 -.0002 0 -1 1
4.2303 4.2295 .0008 1 0 1
3.9903 3.9896 .0007 0 -2 1
3.8702 3.8684 .0018 -2 2 0
3.7903 3.7917 -.0014 -1 5 0
3.6503 3.6525 -.0022 1 3 1
3.5602 3.5590 .0013 1 -3 1
3.3002 3.3025 -.0023 2 0 1
3.1502 3.1508 -.0007 2 -2 1
3.0902 3.0895 .0008 2 4 0
A= 8.257 DA= .003
B= 20.759 DB= .006
C= 4.5287 DC= .00073
GAMMA= 93.33038 DGAMMA= .01
BETA = 80.060 DBETA = .003
ALPHA= 86.72 DALPHA= .01
V=761.4
9. 32-0931
Rb2Ni3{P2O7}2*10H2O
Triklin
Dexp Dcal d(D) h k l
8.0009 7.9972 .0038 0 1 1
6.9804 6.9692 .0112 -1 0 1
6.5304 6.5293 .0010 0 -1 1
5.7503 5.7517 -.0014 1 0 1
4.7104 4.7091 .0014 -1 1 2
4.0403 4.0374 .0029 -2 1 1
3.9302 3.9311 -.0008 -2 1 0
3.5203 3.5198 .0005 2 0 1
3.3503 3.3464 .0039 0 1 3
3.2802 3.2800 .0002 1 2 2
2.9302 2.9324 -.0022 -1 -1 3
2.8302 2.8298 .0004 -1 -3 1
A= 8.370 DA= .001
B= 10.6890 DB= .0003
C= 10.374 DC= .002
GAMMA= 99.27 DGAMMA= .01
BETA =102.88 DBETA = .04
ALPHA= 76.796 DALPHA= .001
V= 874.95
10. 32-1788
C7H5Cl2NNiS
Rombik
Groupa 26,28,51
Dexp. Dcal. d(D) h k l
11.6009 11.6620 -.0611 1 0 0
7.5402 7.5574 -.0172 1 0 1
5.8503 5.8310 .0193 2 0 0
4.8603 4.8672 -.0069 2 1 0
3.8132 3.8149 -.0017 1 2 1
3.3503 3.3495 .0007 3 1 1
2.9532 2.9462 .0070 0 3 0
2.5202 2.5158 .0044 3 2 2
1.9561 1.9565 -.0003 1 0 5
1.7601 1.7610 -.0009 4 4 0
1.7211 1.7213 -.0002 1 5 1
a=11.662 b= 8.839 c= 9.92
da= .009 db= .005 dc= .02
V=1023
11. 32-1790
C16H24cl2N2Ni
Triklin
Dexp Dcal d(D) h k l
6.9206 6.9213 -.0006 1 1 0
5.2205 5.2224 -.0019 -1 0 1
4.1503 4.1496 .0006 -1 -2 1
3.5102 3.5114 -.0012 1 -2 1
3.1603 3.1432 .0171 0 -3 1
2.9202 2.9211 -.0009 -1 3 0
2.7102 2.7110 -.0008 2 2 1
2.4902 2.4898 .0004 -1 3 1
2.3602 2.3601 .0001 -2 -3 2
2.2201 2.2201 .0000 3 2 1
1.9601 1.9608 -.0006 -4 -3 1
1.9201 1.9201 .0001 4 1 1
A= 8.76926 DA= .00004
B= 10.1319 DB= .0003
C= 6.16452 DC= .00003
GAMMA= 80.503 DGAMMA= .002
BETA = 99.4287 DBETA = .0004
ALPHA=103.060 DALPHA= .002
V=521.7
12. 32-1791
C6H9Cl2N3NiO9
Rombiku
Groupa 31,59
Dexp. Dcal. d(D) h k l
6.8704 6.8686 .0018 1 0 1
5.8503 5.8381 .0122 1 1 0
5.2205 5.2125 .0079 2 0 0
4.9305 4.9186 .0119 1 1 1
4.5804 4.5652 .0152 0 0 2
3.8013 3.8086 -.0073 2 1 1
3.3393 3.3379 .0014 1 2 0
2.9212 2.9215 -.0003 1 0 3
2.6272 2.6283 -.0011 2 0 3
2.2741 2.2748 -.0007 0 3 1
a=10.42 b= 7.047 c= 9.13
da= .01 db= .005 dc= .02
V= 670.7
13. 32-1793
C12H12N4Ni
Triklin
Dexp Dcal d(D) h k l
12.8003 12.7728 .0275 1 0 0
6.4606 6.4533 .0073 -1 1 0
5.8304 5.8222 .0082 -2 0 1
4.6203 4.6474 -.0271 2 1 0
4.3303 4.3257 .0046 -1 0 2
4.2303 4.2415 -.0112 -3 0 1
3.7373 3.7346 .0026 1 0 2
3.5883 3.5855 .0027 -3 -1 1
3.4253 3.4208 .0045 1 2 0
3.2072 3.2079 -.0007 1 -2 1
3.1193 3.1190 .0002 -2 2 1
3.0572 3.0581 -.0009 3 1 1
A= 13.196 DA= .006
B= 7.2338 DB= .0002
C= 8.685 DC= .001
GAMMA= 93.163 DGAMMA= .009
BETA =104.15 DBETA = .02
ALPHA= 90.72 DALPHA= .03
V=803.6
14. 32-1794
C12H12I10.97N4Ni
Triklin
Dexp Dcal d(D) h k l
10.3003 10.3501 -.0499 0 0 1
6.1906 6.1976 -.0070 0 1 1
5.2803 5.2878 -.0074 0 -2 1
5.0905 5.0904 .0001 -1 -1 1
4.6203 4.6137 .0065 -1 1 1
4.1903 4.1903 .0000 -1 -1 2
4.0802 4.0823 -.0021 1 -2 1
3.8002 3.7914 .0088 1 0 2
3.6763 3.6810 -.0048 0 -1 3
3.5883 3.5928 -.0045 1 -2 2
3.4512 3.4500 .0012 0 0 3
3.4002 3.3959 .0043 0 -3 2
A= 6.1893 DA= .0003
B= 10.6977 DB= .0003
C= 11.07055 DC= .00004
GAMMA= 92.816 DGAMMA= .007
BETA = 94.0363 DBETA = .0006
ALPHA=110.126 DALPHA= .009
V=684.1
15. 32-1795
C12H12I5.79N4Ni
Triklin
Dexp Dcal d(D) h k l
9.4010 9.4159 -.0149 1 0 0
7.4008 7.4128 -.0120 0 1 0
5.5402 5.5403 -.0001 1 0 2
4.9804 4.9775 .0029 1 -1 2
4.4803 4.4627 .0177 2 0 2
4.1102 4.1133 -.0031 2 -1 2
4.0403 4.0425 -.0022 1 1 2
3.4383 3.4425 -.0042 0 0 3
3.3252 3.3259 -.0006 3 0 2
3.2532 3.2503 .0029 1 2 1
2.9972 2.9908 .0064 1 -2 3
2.9482 2.9485 -.0003 -2 0 2
A= 10.259 DA= .001
B= 7.611 DB= .009
C= 11.528 DC= .001
GAMMA= 93.09 DGAMMA= .05
BETA = 66.71 DBETA = .04
ALPHA=102.92 DALPHA= .05
V=803.1
16. 32-1796
C12H12I12.57N4Ni
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
12.6000 13.0171 -.4171 1 0 0
8.1909 8.1705 .0204 1 1 0
5.2405 5.2478 -.0073 0 2 0
4.7203 4.7200 .0003 2 1 1
4.0202 4.0187 .0015 2 0 2
3.9322 3.9169 .0154 -3 0 2
3.7683 3.7678 .0005 -2 0 3
3.2073 3.2078 -.0006 1 3 1
3.1632 3.1629 .0003 -4 1 1
3.0572 3.0569 .0003 -2 3 1
2.9392 2.9394 -.0002 -1 1 4
2.5622 2.5623 -.0001 4 1 2
2.5142 2.5143 -.0001 -5 1 2
2.1951 2.1952 -.0001 -2 2 5
1.9721 1.9721 .0000 4 4 1
a= 13.30 b= 10.496 c= 12.252 beta= 101.81
da=.01 db=.002 dc=.007 dbeta=.04
V= 1673.9
Triklin
Dexp Dcal d(D) h k l
12.6000 12.5673 .0327 0 1 0
8.1909 8.2092 -.0182 0 0 1
5.2405 5.2419 -.0014 -1 1 0
4.7203 4.7180 .0023 0 -2 1
4.0202 4.0193 .0009 1 3 0
3.9322 3.9319 .0003 0 3 1
3.7683 3.7676 .0006 0 -1 2
3.2073 3.2091 -.0018 -2 1 1
3.1632 3.1633 -.0001 1 4 0
3.0572 3.0573 -.0002 -2 -3 1
2.9392 2.9396 -.0003 1 2 2
2.5622 2.5622 .0000 -2 1 3
2.5142 2.5135 .0007 0 5 0
2.1951 2.1948 .0003 -3 1 1
1.9721 1.9724 -.0002 0 -6 1
A= 7.236 DA= .001
B= 13.005 DB= .002
C= 8.921 DC= .002
GAMMA= 76.830 DGAMMA= .002
BETA =112.008 DBETA = .005
ALPHA= 88.55 DALPHA= .01
V= 752.2
17. 32-1797
C22H20N6NiS2
Monoklin
grupa 3
Dexp Dcal d(D) h k l
8.1004 8.0928 .0076 1 1 0
7.1208 7.1190 .0018 1 0 2
6.7205 6.7090 .0115 -1 1 1
5.8303 5.8303 -.0000 -1 0 2
5.3704 5.3703 .0002 2 1 0
4.7704 4.7649 .0055 -2 1 1
4.3304 4.3312 -.0009 0 2 2
4.0002 4.0011 -.0008 -2 1 2
3.8003 3.8012 -.0009 1 0 4
3.5602 3.5595 .0008 2 0 4
a= 12.757 b= 10.660 c= 15.250 beta=77.062
da= .001 db=.002 dc=.0005 dbet=.007
V=2022
Triklin
Dexp Dcal d(D) h k l
8.1004 8.1001 .0002 1 0 0
7.1208 7.1206 .0002 1 -1 1
6.7205 6.7212 -.0007 1 0 1
5.8303 5.8301 .0002 0 0 2
5.3704 5.3701 .0003 0 -1 2
4.7704 4.7701 .0003 -1 -1 1
4.3304 4.3301 .0002 2 -1 1
4.0002 4.0003 -.0001 -1 -1 2
3.8003 3.8004 -.0000 -2 0 1
3.5602 3.5603 -.0001 2 -2 2
A= 8.9444 DA= .0001
B= 9.80241 DB= .00002
C= 11.988 DC= .001
GAMMA=115.074 DGAMMA= .001
BETA = 83.280 DBETA = .003
ALPHA=103.382 DALPHA= .005
V= 926.0
18. 32-1798
C15H10N2NiO2S
Monoklin
grupa 3
Dexp Dcal d(D) h k l
4.5103 4.5124 -.0021 -1 1 1
4.2904 4.2939 -.0035 1 0 2
3.9413 3.9425 -.0012 2 0 1
3.5563 3.5569 -.0006 -2 1 1
3.2603 3.2614 -.0011 -2 1 2
3.0412 3.0410 .0002 -3 0 2
2.7262 2.7246 .0016 -3 0 3
2.5662 2.5688 -.0026 -1 2 1
2.2030 2.2045 -.0015 0 0 5
1.9951 1.9956 -.0005 2 1 4
1.8421 1.8431 -.0010 3 0 4
1.7441 1.7447 -.0006 3 1 4
a= 9.5874 b=5.412 c= 11.3800 beta=104.394
da=.0007 db=.001 dc=.0001 dbet=.003
V=571.6