1. 49-0531
Co3{AsO4}2
Triklin
Dexp Dcal d(D) h k l
5.8000 5.7999 .0001 -1 2 0
4.5470 4.5441 .0029 2 1 1
4.3700 4.3675 .0025 2 -1 1
3.9760 3.9759 .0001 1 -3 0
3.7030 3.7030 .0000 2 -3 0
3.4900 3.4825 .0075 1 3 1
3.2400 3.2388 .0012 3 -2 1
3.0680 3.0682 -.0002 -3 3 1
2.7650 2.7644 .0006 3 -3 1
2.7270 2.7287 -.0017 2 -1 2
2.7000 2.7000 .0000 0 3 2
2.6400 2.6404 -.0004 3 1 2
A= 14.5360 DA= .0001
B= 12.2597 DB= .0008
C= 6.28525 DC= .00003
GAMMA= 97.528 DGAMMA= .006
BETA = 88.685 DBETA = .001
ALPHA= 79.242 DALPHA= .003
V=1090
2. 49-0532
Co6As2O11
Triklin
Dexp Dcal d(D) h k l
9.3600 9.3618 -.0018 0 -1 1
5.1500 5.1500 .0000 0 -3 1
3.8170 3.8180 -.0010 -1 -3 2
3.5140 3.5145 -.0005 0 -4 2
3.1070 3.1072 -.0002 -1 -3 3
2.9000 2.8989 .0011 -2 0 2
2.8700 2.8704 -.0004 -1 -4 3
2.6080 2.6080 -.0000 2 -2 1
2.5300 2.5291 .0009 1 -3 3
2.3680 2.3684 -.0004 1 -6 1
2.0870 2.0868 .0002 0 2 4
2.0200 2.0203 -.0003 1 -4 4
A= 6.2756 DA= .0005
B= 15.9899 DB= .0001
C= 10.2456 DC= .0006
GAMMA= 85.244 DGAMMA= .002
BETA =105.213 DBETA = .003
ALPHA=107.856 DALPHA= .006
V= 944.37
3. 49-0658
Co0.04Al0.45Si0.06P0.44O2*0.48H2O*0.43C6H12N
Triklin
Dexp Dcal d(D) h k l
18.9000 18.5835 .3165 1 0 0
9.1100 9.2918 -.1818 2 0 0
6.0700 6.0779 -.0079 1 1 0
5.2600 5.2548 .0052 2 1 0
4.6500 4.6459 .0041 4 0 0
4.5400 4.5453 -.0053 -3 1 0
3.7300 3.7299 .0001 4 1 0
3.6800 3.6836 -.0036 0 0 2
3.5600 3.5588 .0012 -4 1 1
3.2800 3.2795 .0005 -2 1 2
3.2400 3.2387 .0013 2 1 2
2.8500 2.8506 -.0006 6 0 1
2.7600 2.7602 -.0002 4 1 2
2.5600 2.5602 -.0002 2 2 2
A= 18.5914 DA= .0009
B= 6.6009 DB= .0006
C= 7.4864 DC= .0001
GAMMA= 91.662 DGAMMA= .001
BETA = 90.553 DBETA = .001
ALPHA= 79.772 DALPHA= .002
V=904.4
4. 49-0681
Co2Mo{NH3}12{CN}8*3H2O
Triklin
Dexp Dcal d(D) h k l
6.6900 6.6960 -.0060 1 1 0
6.1300 6.1315 -.0015 0 0 1
5.7600 5.7624 -.0024 0 2 0
5.5700 5.5723 -.0023 -1 0 1
5.3000 5.3112 -.0112 -2 1 0
4.9940 4.9907 .0033 1 0 1
4.4660 4.4683 -.0023 1 2 0
4.2170 4.2170 .0000 2 1 0
4.1910 4.1897 .0013 -2 0 1
3.7530 3.7462 .0068 0 -2 1
3.4050 3.4059 -.0009 3 0 0
3.2300 3.2305 -.0005 -1 1 2
A= 11.0036 DA= .0003
B= 12.7424 DB= .0006
C= 6.505 DC= .001
GAMMA=110.64 DGAMMA= .01
BETA =102.75 DBETA = .02
ALPHA= 71.811 DALPHA= .005
V=803.3
5. 49-0691
Sr0.5CoBi0.5Ox
Triklin
Dexp Dcal d(D) h k l
14.7000 14.5637 .1363 0 0 1
7.4500 7.4470 .0030 -1 0 1
4.9700 4.9665 .0035 0 -1 1
3.7200 3.7226 -.0026 0 -1 3
3.5000 3.4980 .0020 -2 1 0
3.3200 3.3207 -.0007 -1 -1 3
3.2100 3.2112 -.0012 -2 0 3
3.1300 3.1293 .0007 0 -1 4
2.9780 2.9779 .0001 -2 -1 2
2.8780 2.8779 .0001 -3 0 1
2.7610 2.7602 .0008 -2 0 4
2.7000 2.7004 -.0004 -2 1 3
A= 8.9281 DA= .0008
B= 5.127 DB= .002
C= 14.6766 DC= .0004
GAMMA= 95.39 DGAMMA= .01
BETA = 87.038 DBETA = .006
ALPHA= 96.71 DALPHA= .02
V= 663.7
6. 49-0703
Co0.85Mn0.15HPO4*1.5H2O
Triklin
Dexp Dcal d(D) h k l
7.8000 7.8065 -.0065 0 1 0
6.7000 6.7032 -.0032 1 0 0
5.2300 5.2338 -.0038 0 -1 2
4.3000 4.3016 -.0016 1 -1 1
3.8000 3.8008 -.0008 1 1 2
3.6200 3.6188 .0012 0 -2 2
3.2700 3.2713 -.0013 -2 0 1
3.0900 3.0889 .0011 -2 -2 1
3.0100 3.0104 -.0004 -1 2 0
2.9800 2.9800 .0000 -2 0 2
2.5900 2.5903 -.0003 0 -3 2
2.5500 2.5493 .0007 2 -1 2
A= 7.071 DA= .001
B= 8.415 DB= .002
C= 12.0241 DC= .0001
GAMMA= 71.724 DGAMMA= .003
BETA = 97.392 DBETA = .005
ALPHA=103.95 DALPHA= .01
V= 658.2
7. 49-0769
{Co{NH3}6}{P4N4O8H4}3*xH2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.8000 5.8021 -.0021 -1 1 1
4.9700 4.9762 -.0062 0 2 0
4.5800 4.5844 -.0044 -1 0 2
4.1300 4.1337 -.0037 2 1 0
3.8100 3.8179 -.0079 1 1 2
3.6700 3.6706 -.0006 2 1 1
3.5700 3.5706 -.0006 -2 0 2
3.5100 3.5067 .0033 0 2 2
3.3600 3.3609 -.0009 -2 1 2
3.3100 3.3175 -.0075 0 3 0
3.1600 3.1577 .0023 2 0 2
3.0300 3.0295 .0005 3 0 0
a= 9.158 b= 9.95 c= 9.9601 beta= 97.04
da=.002 db=.01 dc=.0001 dbeta=.08
V= 900.9
Triklin
Dexp Dcal d(D) h k l
5.8000 5.8236 -.0236 0 1 1
4.9700 4.9832 -.0132 0 -1 1
4.5800 4.5881 -.0081 -1 -1 1
4.1300 4.1333 -.0033 -1 1 0
3.8100 3.8073 .0027 1 1 1
3.6700 3.6733 -.0033 0 2 1
3.5700 3.5644 .0056 0 1 2
3.5100 3.5177 -.0077 1 2 0
3.3600 3.3652 -.0052 -1 1 2
3.3100 3.3081 .0019 -1 -1 2
3.1600 3.1579 .0021 0 -1 2
3.0300 3.0277 .0023 -1 2 1
A= 5.94254 DA= .00001
B= 7.93836 DB= .00001
C= 7.89094 DC= .00001
GAMMA= 80.9309 DGAMMA= .0001
BETA =108.07830 DBETA = .00004
ALPHA= 84.47758 DALPHA= .00002
V=345.3
8. 49-1104
Co{N2H3SOO}2
Triklin
Dexp Dcal d(D) h k l
5.5900 5.6027 -.0127 1 1 0
5.2700 5.2612 .0088 0 1 1
4.8000 4.7938 .0062 0 -1 1
4.5100 4.5146 -.0046 0 2 0
4.2600 4.2588 .0012 1 -1 1
3.9200 3.9301 -.0101 -1 -1 1
3.8000 3.8006 -.0006 0 2 1
3.4500 3.4502 -.0002 0 -2 1
3.2900 3.2887 .0013 1 -2 1
2.8500 2.8471 .0029 1 0 2
2.6700 2.6740 -.0040 1 -1 2
2.6300 2.6306 -.0006 0 2 2
A= 7.8549 DA= .0002
B= 9.1288 DB= .0009
C= 6.0572 DC= .0002
GAMMA= 96.224 DGAMMA= .006
BETA = 88.424 DBETA = .001
ALPHA= 84.449 DALPHA= .002
V=429.4
9. 49-1728
AlxCo
Triklin
Dexp Dcal d(D) h k l
4.2506 4.2471 .0035 1 -1 2
3.9870 3.9844 .0026 2 0 0
2.0633 2.0630 .0003 4 -1 2
3.8581 3.8645 -.0064 -2 1 0
3.6316 3.6325 -.0009 0 3 2
3.5748 3.5745 .0003 2 0 2
3.4263 3.4284 -.0021 0 -3 2
3.4043 3.4066 -.0023 2 3 0
3.2901 3.2891 .0010 -2 3 0
3.2422 3.2419 .0003 2 -2 2
3.1872 3.1847 .0025 -2 -1 1
2.4850 2.4847 .0003 2 6 0
A= 8.467 DA= .005
B= 18.57 DB= .03
C= 9.145 DC= .001
GAMMA= 86.41 DGAMMA= .09
BETA = 70.38 DBETA = .02
ALPHA= 85.48 DALPHA= .03
V=1350
Triklin
(Ïî èíòåíñèâíûì ðåôëåêñàì)
Dexp Dcal d(D) h k l
4.2506 4.2482 .0024 1 0 1
3.8581 3.8569 .0012 0 1 1
3.6316 3.6367 -.0051 0 -1 1
3.5748 3.5749 -.0001 -1 0 1
3.4043 3.4039 .0004 1 0 2
2.1219 2.1219 .0000 -1 2 1
2.0735 2.0728 .0007 1 0 4
2.0633 2.0630 .0003 0 2 1
2.0089 2.0087 .0002 -2 0 1
1.9528 1.9528 .0000 2 -1 3
1.9377 1.9381 -.0004 0 1 4
1.9265 1.9269 -.0004 2 0 3
A= 4.7420 DA= .0001
B= 4.4595 DB= .0009
C= 8.610 DC= .003
GAMMA=110.08 DGAMMA= .02
BETA = 78.67 DBETA = .01
ALPHA= 89.98 DALPHA= .02
V= 167.23
10. 49-1901
Co{NO3}2*2HCONH2*2H2O
Triklin
Dexp Dcal d(D) h k l
8.8800 8.8722 .0078 0 1 0
5.9450 5.9440 .0010 1 -1 1
5.1430 5.1460 -.0030 0 -1 2
4.3920 4.3931 -.0011 1 0 2
4.3870 4.3867 .0003 -1 -1 1
3.9790 3.9857 -.0067 1 -2 2
3.9650 3.9657 -.0007 -1 2 0
3.6420 3.6419 .0001 -1 0 2
3.0870 3.0848 .0022 1 2 1
3.0640 3.0624 .0016 1 -3 2
3.0640 3.0624 .0016 1 -3 2
2.9550 2.9574 -.0024 0 3 0
A= 6.6903 DA= .0004
B= 9.630 DB= .002
C= 11.044 DC= .001
GAMMA=104.110 DGAMMA= .005
BETA = 74.9870 DBETA = .0004
ALPHA=110.85 DALPHA= .01
V=633.1
11. 49-1910
C26H22CoN4O2S2
Triklin
Dexp Dcal d(D) h k l
16.0860 16.0950 -.0090 0 1 0
13.9790 13.9616 .0174 1 0 0
10.5420 10.5412 .0008 1 -1 0
7.9038 7.9050 -.0012 0 -1 1
5.8346 5.8354 -.0008 0 -2 1
5.5510 5.5475 .0035 1 -2 1
5.0169 5.0154 .0015 0 3 1
4.1535 4.1513 .0022 -1 -1 2
3.9174 3.9187 -.0013 1 -2 2
3.5506 3.5521 -.0015 0 -4 1
3.3400 3.3402 -.0002 -2 4 1
2.9433 2.9434 -.0001 -2 -3 2
2.8183 2.8185 -.0002 -2 0 3
1.9738 1.9737 .0001 1 -7 2
A= 14.10 DA= .01
B= 16.261 DB= .001
C= 10.0226 DC= .0008
GAMMA= 88.806 DGAMMA= .005
BETA = 81.95 DBETA = .01
ALPHA= 81.82 DALPHA= .01
V=2253
12. 49-1921
C10H15CoN3O6
Rombik
Groupa 17
Dexp. Dcal. d(D) h k l
10.1980 10.1800 .0180 0 0 1
4.9731 4.9684 .0047 0 1 0
3.2802 3.2807 -.0005 2 0 2
2.1034 2.1035 -.0001 2 2 1
1.6932 1.6925 .0007 5 0 1
1.5316 1.5316 -.0000 5 0 3
a= 8.582 b= 4.9684 c=10.180
da= .001 db= .0001 dc= .001
V= 434.06
13. 49-1946
C14H12CoN2O4*2H2O
Triklin
Dexp Dcal d(D) h k l
9.8200 9.8320 -.0120 1 0 0
8.4500 8.4522 -.0022 0 1 1
7.8500 7.8423 .0077 0 -1 1
7.3000 7.3030 -.0030 0 0 2
6.6400 6.6545 -.0145 1 0 2
6.1000 6.1024 -.0024 1 1 2
5.6500 5.6386 .0114 0 -1 2
4.8400 4.8357 .0043 1 0 3
4.6700 4.6674 .0026 1 1 3
4.3700 4.3611 .0089 -2 0 1
4.2800 4.2837 -.0037 -1 -2 1
4.1200 4.1188 .0012 2 -1 1
A= 10.351 DA= .001
B= 10.050 DB= .007
C= 15.15 DC= .01
GAMMA= 77.67 DGAMMA= .01
BETA = 75.27 DBETA = .02
ALPHA= 82.50 DALPHA= .04
V= 1484.4
14. 49-1950
C14H12CoN2O4*C2H4O2
Triklin
Dexp Dcal d(D) h k l
6.9900 6.9923 -.0023 -1 0 1
5.2700 5.2675 .0025 1 1 1
5.0900 5.1060 -.0160 1 -1 1
4.8600 4.8729 -.0129 0 2 1
4.6700 4.6673 .0027 0 0 2
4.5300 4.5312 -.0012 -1 1 2
4.3700 4.3667 .0033 -2 1 0
4.3000 4.2974 .0026 -2 0 1
4.0700 4.0591 .0109 0 -2 1
3.9300 3.9275 .0025 1 2 1
3.7900 3.7943 -.0043 1 -2 1
3.7600 3.7572 .0028 -2 2 1
A= 9.264 DA= .003
B= 10.453 DB= .004
C= 9.72607 DC= .00003
GAMMA=101.21 DGAMMA= .05
BETA =100.53 DBETA = .03
ALPHA= 75.8373 DALPHA= .0009
V=886.8
15. 49-1967
C38H52Cl2CoN4S4
Triklin
Dexp Dcal d(D) h k l
11.7400 11.6998 .0402 1 0 0
9.0900 9.0800 .0100 0 1 0
8.2900 8.2681 .0219 0 0 1
6.5700 6.5685 .0015 -1 0 1
5.6900 5.7112 -.0212 -1 1 1
4.5400 4.5400 .0000 0 2 0
4.1900 4.1858 .0042 2 1 1
3.9700 3.9737 -.0037 1 0 2
3.4500 3.4481 .0019 -3 0 1
3.3900 3.3906 -.0006 -1 -1 2
3.2400 3.2427 -.0027 3 1 1
3.0400 3.0396 .0004 -1 3 0
2.4600 2.4595 .0005 2 1 3
A= 11.841 DA= .002
B= 9.197 DB= .003
C= 8.300 DC= .002
GAMMA= 98.18 DGAMMA= .04
BETA = 87.12 DBETA = .02
ALPHA= 86.37 DALPHA= .06
V= 891.2
16. 49-2036
C14H16Cl2CoN4O4
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
8.4249 8.3932 .0317 1 1 0
6.8255 6.8383 -.0128 2 0 0
5.9614 5.9644 -.0030 0 0 1
5.7535 5.7511 .0024 2 1 0
4.5521 4.5588 -.0067 3 0 0
4.1907 4.1898 .0009 3 1 0
3.9689 3.9682 .0007 0 2 1
3.6553 3.6585 -.0032 3 1 1
3.4217 3.4191 .0026 4 0 0
3.2549 3.2549 -.0000 4 1 0
3.1480 3.1462 .0018 2 3 0
3.0460 3.0464 -.0004 0 3 1
a= 13.81 b= 10.63 c= 6.025 beta= 81.89
da=.01 db=.01 dc=.007 dbeta=.06
V= 875.9
Triklin
Dexp Dcal d(D) h k l
8.4249 8.4035 .0214 1 0 0
6.8255 6.8257 -.0002 1 1 0
5.9614 5.9582 .0032 -1 -1 1
5.7535 5.7585 -.0050 1 0 1
4.5521 4.5507 .0014 1 -1 1
4.1907 4.1831 .0076 -1 1 1
3.9689 3.9644 .0045 -1 -1 2
3.6553 3.6538 .0015 1 0 2
3.4217 3.4230 -.0013 0 1 2
3.2549 3.2542 .0007 -2 -1 2
3.1480 3.1492 -.0012 2 -1 1
3.0460 3.0476 -.0016 -2 0 2
A= 8.825 DA= .004
B= 8.531 DB= .001
C= 8.577 DC= .003
GAMMA= 72.51 DGAMMA= .01
BETA = 96.95 DBETA = .02
ALPHA=103.11 DALPHA= .07
V= 598.9
17. 49-2117
C34H26CoO6
Triklin
Dexp Dcal d(D) h k l
12.2800 12.2990 -.0190 1 0 0
11.4600 11.4907 -.0307 0 1 1
10.0200 10.0265 -.0065 -1 0 1
8.8700 8.8831 -.0131 1 0 1
7.9200 7.9213 -.0013 0 -1 1
7.3000 7.2939 .0061 0 0 2
6.9900 6.9880 .0020 -1 -1 1
6.6400 6.6399 .0001 -1 0 2
6.2000 6.1876 .0124 1 1 2
5.5400 5.5295 .0105 -2 1 1
5.0100 5.0132 -.0032 -2 0 2
4.6900 4.6918 -.0018 0 2 3
A= 12.392 DA= .001
B= 12.7769 DB= .0007
C= 15.754 DC= .003
GAMMA= 89.549 DGAMMA= .001
BETA = 96.391 DBETA = .004
ALPHA= 68.908 DALPHA= .003
V=2309
18. 49-2120
C58H40CoN2O6
Triklin
Dexp Dcal d(D) h k l
10.2400 10.2411 -.0011 -1 0 1
9.7000 9.6972 .0028 0 1 1
8.7000 8.6945 .0055 0 -1 1
8.5400 8.5399 .0001 -1 1 0
7.5000 7.4967 .0033 1 1 1
6.5900 6.5946 -.0046 2 1 0
6.4500 6.4602 -.0102 -1 -2 1
6.0000 5.9983 .0017 -1 0 2
5.6000 5.6065 -.0065 -1 -1 2
4.9900 4.9874 .0026 2 0 1
4.7700 4.7695 .0005 0 3 1
4.6300 4.6294 .0006 2 3 0
A= 13.882 DA= .002
B= 15.606 DB= .002
C= 12.158 DC= .004
GAMMA= 74.23 DGAMMA= .01
BETA =106.355 DBETA = .007
ALPHA= 88.4537 DALPHA= .0006
V=2419
19. 49-2122
C44H30CoN2O4
Monoklin 3
Dexp Dcal d(D) h k l
10.4700 10.4449 .0251 1 1 0
7.5000 7.4938 .0062 -1 0 1
6.2800 6.2806 -.0006 1 1 1
5.5200 5.5103 .0097 0 2 1
5.5000 5.5103 -.0103 0 2 1
4.9200 4.9116 .0084 3 0 0
4.0600 4.0615 -.0015 3 0 1
3.4800 3.4816 -.0016 3 3 0
3.3900 3.3907 -.0007 -4 1 1
3.3200 3.3191 .0009 -1 4 1
3.1800 3.1796 .0004 4 1 1
2.9800 2.9801 -.0001 4 2 1
a= 14.80 b= 14.808 c= 8.284 beta= 95.2
da=.02 db=.007 dc=.001 dbeta=.1
V= 1808
Triklin
Dexp Dcal d(D) h k l
10.4700 10.4715 -.0015 1 0 0
7.5000 7.4998 .0002 -1 1 1
6.2800 6.2803 -.0003 -1 -1 1
5.5200 5.5206 -.0006 0 2 1
5.5000 5.4998 .0002 -2 1 0
4.9200 4.9202 -.0002 -2 0 1
4.0600 4.0597 .0003 0 2 2
3.4800 3.4799 .0001 0 -1 3
3.3900 3.3901 -.0001 0 1 3
3.3200 3.3200 -.0000 3 -2 1
3.1800 3.1799 .0001 -3 1 2
2.9800 2.9800 -.0000 -2 2 3
A= 11.0909 DA= .0009
B= 14.043 DB= .001
C= 10.731 DC= .002
GAMMA=108.20 DGAMMA= .03
BETA = 95.71 DBETA = .02
ALPHA= 91.07 DALPHA= .02
V= 1577.6
20. 49-2326
C5H5Br2CoNO*H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
9.0400 8.9833 .0567 0 0 1
7.1640 7.1527 .0113 1 0 0
6.3420 6.3404 .0016 1 1 0
4.0770 4.0749 .0021 -1 2 1
3.6120 3.6124 -.0004 2 0 1
3.1990 3.2001 -.0011 0 4 1
3.1640 3.1644 -.0004 2 0 2
3.0910 3.0931 -.0021 -2 0 1
3.0120 3.0120 -.0000 1 4 1
2.8370 2.8379 -.0009 -1 4 1
2.7240 2.7234 .0006 0 4 2
2.4370 2.4375 -.0005 -1 4 2
a= 7.34 b= 13.699 c= 9.217 beta= 77.05
da=.01 db=.009 dc=.003 dbeta=.03
V= 903.2
Triklin
Dexp Dcal d(D) h k l
9.0400 9.0360 .0040 0 0 1
7.1640 7.1637 .0003 1 0 0
6.3420 6.3287 .0133 1 1 1
4.0770 4.0778 -.0008 -1 -1 1
3.6120 3.6121 -.0001 2 1 2
3.1990 3.1989 .0001 -2 1 0
3.1640 3.1644 -.0004 2 2 2
3.0910 3.0908 .0002 -1 -2 1
3.0120 3.0120 .0000 0 0 3
2.8370 2.8371 -.0001 0 3 0
2.7240 2.7240 .0000 1 3 0
2.4370 2.4370 -.0000 3 2 2
A= 7.8707 DA= .0002
B= 8.932 DB= .001
C= 10.171 DC= .002
GAMMA= 78.61 DGAMMA= .01
BETA = 66.06 DBETA = .01
ALPHA= 73.11 DALPHA= .01
V= 622.7
21. 49-2327
C12H12Cl2CoF2N2
Rombik
Groupa 16
Dexp. Dcal. d(D) h k l
14.4700 14.4710 -.0010 1 0 0
10.0100 9.9820 .0280 0 0 2
8.4390 8.4390 -.0000 1 1 0
6.6510 6.6547 -.0037 0 0 3
5.6910 5.6910 .0000 2 1 1
a=14.471 b=10.388 c=19.964
da= .001 db= .001 dc= .001
V=3001.2
22. 49-2328
C12H14Cl2CoN2
Rombik
Groupa 17
Dexp. Dcal. d(D) h k l
7.9110 7.9095 .0015 0 0 2
7.3510 7.3567 -.0057 1 0 1
6.4450 6.4450 .0000 0 1 0
5.7350 5.7292 .0058 1 0 2
5.2730 5.2730 .0000 0 0 3
a= 8.310 b= 6.4450 c=15.819
da= .001 db= .0001 dc= .001
V= 847.2
23. 49-2329
c14H18Cl2CoN2
Rombik
Groupa 31,59
Dexp. Dcal. d(D) h k l
11.6130 11.6790 -.0660 1 0 0
10.0330 10.1131 -.0801 0 1 1
8.4390 8.3596 .0794 1 0 1
7.3630 7.3463 .0167 1 2 0
5.9900 5.9855 .0045 0 0 2
5.5750 5.5751 -.0001 0 3 1
a=11.679 b=18.900 c=11.971
da= .001 db= .001 dc= .001
V=2642.4
24. 49-2330
C14H18Cl2CoN2O2
Rombik
Groupa 31,59
Dexp. Dcal. d(D) h k l
7.6810 7.7000 -.0190 0 2 0
6.9860 7.0289 -.0429 1 0 1
5.2860 5.2845 .0015 2 0 0
4.9970 4.9984 -.0014 2 1 0
4.5080 4.5066 .0014 0 3 1
4.2990 4.2991 -.0001 1 0 2
a=10.569 b=15.400 c= 9.412
da= .001 db= .001 dc= .001
V=1531.9
25. 49-2374
C3.1H3.1Co0.31Pb1.18S5.18Ti2
Triklin
Dexp Dcal d(D) h k l
22.6400 22.6275 .0125 1 0 0
7.5940 7.5425 .0515 3 0 0
5.7250 5.7282 -.0032 0 1 1
4.5780 4.5780 -.0000 1 -1 1
3.8160 3.8157 .0003 0 1 2
3.2710 3.2707 .0003 0 2 0
2.8640 2.8641 -.0001 0 2 2
2.5460 2.5460 -.0000 -7 -1 1
2.2890 2.2890 -.0000 2 -2 2
1.9090 1.9090 -.0000 5 -3 1
1.5280 1.5280 .0000 -10 2 4
1.4330 1.4330 .0000 11 -2 3
A= 22.85 DA= .03
B= 6.7720 DB= .0006
C= 8.232 DC= .001
GAMMA= 97.89 DGAMMA= .05
BETA = 92.59 DBETA = .07
ALPHA= 76.985 DALPHA= .003
V= 1229
26. 50-0963
Al70Co20Ni10
Triklin
Dexp Dcal d(D) h k l
7.3110 7.3042 .0068 1 1 0
5.8140 5.8102 .0038 0 1 1
4.0490 4.0509 -.0019 0 -1 1
3.8310 3.8275 .0035 2 0 1
3.6720 3.6621 .0099 -1 1 1
3.5790 3.5768 .0022 -1 -1 1
3.5280 3.5320 -.0040 2 3 1
3.2770 3.2765 .0005 2 3 2
3.0020 3.0044 -.0024 -2 1 0
2.8100 2.8095 .0005 3 1 2
2.7820 2.7839 -.0019 -2 -1 1
2.5460 2.5464 -.0004 1 -2 1
A= 10.305 DA= .003
B= 10.816 DB= .001
C= 7.558 DC= .001
GAMMA= 52.169 DGAMMA= .009
BETA = 55.77 DBETA = .01
ALPHA= 54.410 DALPHA= .007
V=512.5
27. 50-0964
Al73Co27
Rombik
Groupa 32,55
Dexp. Dcal. d(D) h k l
3.8250 3.8240 .0010 0 0 1
3.3990 3.4025 -.0035 2 1 0
2.0430 2.0434 -.0004 3 2 0
2.0320 2.0315 .0006 4 0 0
2.0110 2.0108 .0002 1 3 0
1.7940 1.7940 -.0000 4 0 1
a= 8.126 b= 6.226 c= 3.824
da= .001 db= .004 dc= .001
V= 193.5
28. 50-0965
Al69Co25Cu6
Rombik
Groupa 34,58
Dexp. Dcal. d(D) h k l
3.8260 3.8234 .0026 1 0 1
3.4000 3.4019 -.0019 1 1 1
2.0460 2.0459 .0001 3 0 1
2.0110 2.0111 -.0001 2 3 0
1.7980 1.7980 .0000 1 4 0
a= 6.850 b= 7.453 c= 4.608
da= .001 db= .004 dc= .001
V=235.3
29. 50-0966
Al72.5Co19Ni8.5
Rombik
Groupa 32,55
Dexp. Dcal. d(D) h k l
3.7930 3.7950 -.0020 2 1 0
3.3960 3.3928 .0032 1 2 0
2.0360 2.0356 .0004 2 1 1
2.0160 2.0160 -.0000 0 2 1
1.7980 1.7980 -.0000 1 4 0
a= 8.865 b= 7.345 c= 2.412
da= .001 db= .001 dc= .001
v= 157.0
Rombik
Groupa 34,58
Dexp. Dcal. d(D) h k l
3.7930 3.7950 -.0020 2 1 0
3.3960 3.3928 .0032 1 2 0
2.0360 2.0356 .0004 2 1 2
2.0160 2.0160 -.0000 0 2 2
1.7980 1.7980 -.0000 1 4 0
a= 8.865 b= 7.345 c= 4.824
da= .001 db= .001 dc= .001
V= 314.1
30. 50-2125
C32H12CoN12O8
Groupa 27
Dexp. Dcal. d(D) h k l
14.0000 13.9500 .0500 1 0 0
6.6200 6.7500 -.1300 0 1 0
6.0700 6.0761 -.0061 1 1 0
3.4700 3.4700 .0000 0 0 2
3.2800 3.2804 -.0004 1 2 0
a=13.950 b= 6.750 c= 6.940
da= .001 db= .001 dc= .001
V= 653.5
31. 50-2151
C4H12CoN4O4
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
9.1200 9.1200 -.0000 1 0 1
8.1200 8.1062 .0138 -1 0 1
5.4100 5.4097 .0003 -2 0 1
4.8000 4.8017 -.0017 -2 1 1
4.0400 4.0401 -.0001 3 1 0
3.4500 3.4488 .0012 2 0 3
3.2800 3.2792 .0008 -3 0 2
3.0600 3.0602 -.0002 -4 0 1
2.9200 2.9185 .0015 3 1 3
2.5500 2.5497 .0003 5 1 0
2.4800 2.4812 -.0012 -1 4 1
2.3900 2.3905 -.0005 2 4 1
a= 13.241 b= 10.425 c= 11.377 beta= 83.18
da= .002 db=.003 dc=.005 dbeta=.04
V= 1559
Triklin
Dexp Dcal d(D) h k l
9.1200 9.1123 .0077 1 0 0
8.1200 8.1198 .0002 0 1 0
5.4100 5.4076 .0024 0 1 1
4.8000 4.8008 -.0008 -1 0 1
4.0400 4.0385 .0015 -1 2 0
3.4500 3.4481 .0019 1 2 0
3.2800 3.2809 -.0009 3 -1 1
3.0600 3.0595 .0005 2 1 2
2.9200 2.9211 -.0011 -1 -2 1
2.5500 2.5499 .0001 0 3 1
2.4800 2.4798 .0002 -3 0 1
2.3900 2.3899 .0001 1 1 3
A= 10.0460 DA= .0006
B= 8.3206 DB= .0007
C= 7.64171 DC= .00001
GAMMA=102.54 DGAMMA= .02
BETA = 68.117 DBETA = .006
ALPHA= 93.34 DALPHA= .01
V= 578.4
32. 50-2165
C4H18CoN6O6
Triklin
Dexp Dcal d(D) h k l
7.0300 7.0196 .0104 1 0 0
6.3400 6.3410 -.0010 -1 1 0
5.5700 5.5659 .0041 -1 1 1
4.0600 4.0665 -.0065 1 -1 1
3.9300 3.9297 .0003 -2 1 1
3.5600 3.5595 .0005 -1 2 1
3.4800 3.4774 .0026 -1 1 2
3.3400 3.3502 -.0102 1 1 1
2.8600 2.8596 .0004 2 0 1
2.7800 2.7829 -.0029 -2 2 2
2.6800 2.6814 -.0014 1 -1 2
2.5800 2.5799 .0001 1 2 0
A= 8.164 DA= .003
B= 7.4602 DB= .0007
C= 7.198 DC= .003
GAMMA=117.82 DGAMMA= .06
BETA =107.87 DBETA = .03
ALPHA= 77.06 DALPHA= .02
V= 367.3
33. 50-2211
C1.3H1.3C00.13Na0.19S2Ta*H2O
Groupa 50
Dexp. Dcal. d(D) h k l
11.4200 11.5097 -.0897 0 0 1
5.7460 5.7548 -.0088 0 0 2
3.8340 3.8366 -.0026 0 0 3
2.8770 2.8774 -.0004 0 0 4
2.3030 2.3038 -.0008 1 1 1
1.9190 1.9189 .0001 0 2 2
1.6450 1.6452 -.0002 1 2 1
1.4400 1.4403 -.0003 2 0 0
1.2802 1.2800 .0002 2 1 3
1.1519 1.1519 .0000 2 2 2
a= 2.881 b= 4.071 c=11.51
da= .001 db= .001 dc= .01
v= 135.0