1. 40-0046
Sn{Co{NH3}4CO3}6.49 H1.51{PO4}2*1.51H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
11.9000 11.8662 .0338 0 1 0
9.1200 9.0898 .0302 1 0 0
5.9300 5.9331 -.0031 0 2 0
4.2300 4.2307 -.0007 -2 0 1
3.7300 3.7297 .0003 2 1 1
3.0300 3.0299 .0001 3 0 0
2.4900 2.4899 .0001 0 4 2
1.6300 1.6300 .0000 -5 0 3
1.4400 1.4400 .0000 2 4 5
a=9.13 b=11.866 c= 9.20 beta= 95.3
da=.01 db= 4.994 dc=.01 dbeta=.1
V= 992
2. 40-0047
Sn{Co{NH3}6}0.5H0.5{PO4}2*3H2O
Rombik
Groupa 26,28,51
romb.
Dexp. Dcal. d(D) h k l
11.6000 11.5982 .0018 1 0 0
9.1200 9.1041 .0159 0 1 0
4.2600 4.2374 .0226 1 2 0
4.2100 4.2374 -.0274 1 2 0
3.7100 3.7188 -.0088 2 0 1
2.4900 2.4882 .0018 4 0 1
1.6300 1.6301 -.0001 7 1 0
1.4400 1.4400 .0000 4 4 2
a=11.598 b= 9.104 c= 4.846
da= .002 db= .002 dc= .009
V=512
3. 40-0282
{Co2.64{OH}4.28{H2O}0.87Na0.13{Mg2.5Si4O10F2}
geksagon
Groupa 184,192
Dexp. Dcal. d(D) h k l
14.5000 14.6190 -.1190 1 0 0
7.3000 7.3095 -.0095 2 0 0
4.8600 4.8730 -.0130 3 0 0
3.6500 3.6547 -.0047 4 0 0
2.9500 2.9529 -.0029 2 0 2
2.1000 2.0990 .0010 4 2 2
a= 16.88 c= 6.456
da=.02 dc=.004
V=1594
4. 40-0554
C6H4BaCoNO12*3H2O
Mononklin
Grupa 3
Dexp Dcal d(D) h k l
8.5800 8.5722 .0078 1 1 0
6.8560 6.8571 -.0011 0 1 1
5.0340 5.0346 -.0006 -2 1 1
4.2060 4.2059 .0001 -1 0 2
3.7350 3.7351 -.0001 -3 1 1
3.6440 3.6440 -.0000 3 1 0
a= 11.9013 b= 13.023 c= 8.430 beta= 106.900
da= .0007 db=.009 dc=.004 dbeta=.007
V= 1250.1
5. 40-0555
C6H4CoNO12Sr*4H2O
Triklin
Dexp Dcal d(D) h k l
8.2610 8.3119 -.0509 0 0 1
6.2310 6.2401 -.0091 1 2 0
5.5690 5.5615 .0075 1 -2 1
5.4530 5.4567 -.0037 1 2 1
5.2720 5.2529 .0191 -1 -1 1
5.2110 5.2086 .0024 2 0 1
4.8860 4.8866 -.0006 -1 1 1
4.7910 4.7825 .0085 2 1 0
4.6420 4.6323 .0097 1 3 0
4.2870 4.2827 .0043 2 2 0
4.1990 4.2079 -.0089 2 -2 1
4.1480 4.1523 -.0043 -1 2 1
A= 10.665 DA= .002
B= 15.115 DB= .006
C= 9.066 DC= .001
GAMMA= 86.65 DGAMMA= .04
BETA = 67.111 DBETA = .006
ALPHA= 93.86 DALPHA= .05
V=1336
6. 40-0556
C6H4CaCoNO12*4H2O
Tetragon
Groupa 85,118,129
Dexp. Dcal. d(D) h k l
8.0360 8.0404 -.0044 0 0 1
6.1030 6.0831 .0199 1 0 1
4.6660 4.6513 .0147 2 0 0
4.0360 4.0261 .0099 2 0 1
3.6890 3.6903 -.0013 1 0 2
2.7600 2.7626 -.0026 3 1 1
a= 9.30 c= 8.040
da= .03 dc= .006
v= 696
Rombik
Groupa 26,28,51
Dexp. Dcal. d(D) h k l
8.0360 8.0340 .0020 1 0 0
6.1030 6.0893 .0137 1 0 1
4.6660 4.6674 -.0015 0 0 2
4.0360 4.0358 .0002 1 0 2
4.0360 4.0170 .0190 2 0 0
3.6890 3.6899 -.0009 2 0 1
2.7600 2.7600 .0000 0 1 0
a= 8.034 b= 2.7600 c= 9.335
da= .001 db= .00002 dc= .001
V= 206.99
7. 40-0592
RbCoF3*0.5H2O
Rombik
Groupa 32,55
Dexp. Dcal. d(D) h k l
2.9100 2.9070 .0030 0 0 1
2.0600 2.0601 -.0001 2 1 0
1.6800 1.6808 -.0008 2 1 1
1.4800 1.4800 .0000 1 3 0
1.3000 1.3000 .0000 3 1 1
a= 4.586 b= 4.691 c= 2.907
da= .001 db= .004 dc= .001
V= 62.54
8. 40-0598
CoF2*0.5H2O
Triklin
Dexp Dcal d(D) h k l
4.8200 4.8219 -.0019 1 0 0
4.0700 4.0726 -.0026 -1 0 1
3.1500 3.1483 .0017 -1 -1 1
2.9700 2.9696 .0004 1 -1 1
2.7500 2.7485 .0015 1 1 1
2.5900 2.5880 .0020 -1 1 2
2.5500 2.5497 .0003 -2 1 1
2.4400 2.4378 .0022 -2 0 1
2.2000 2.1993 .0007 0 3 1
2.1600 2.1615 -.0015 0 2 2
2.0300 2.0301 -.0001 -2 2 2
1.9900 1.9901 -.0001 2 0 1
1.9500 1.9494 .0006 1 1 2
1.7900 1.7901 -.0001 1 -2 2
A= 5.208 DA= .001
B= 7.3223 DB= .0002
C= 5.367 DC= .002
GAMMA=106.56 DGAMMA= .03
BETA =107.07 DBETA = .03
ALPHA= 80.188 DALPHA= .007
V= 186.7
9. 40-0627
CoF2*4H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
4.8700 4.8701 -.0001 -1 1 1
4.1000 4.1000 .0000 -2 1 1
3.1600 3.1603 -.0003 4 1 0
2.9900 2.9900 .0000 -3 0 2
2.7600 2.7597 .0003 4 1 2
2.5700 2.5699 .0001 -4 0 2
2.1600 2.1600 .0000 2 3 0
2.0300 2.0300 -.0000 3 1 4
a= 14.4715 b= 6.799 c=8.886 beta= 80.594
da=.000204 db=.001 dc=.001 dbeta=.0007
V= 862.5
10. 40-0722
BaCoO2
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
3.2522 3.2485 .0037 0 1 2
2.8376 2.8340 .0036 1 0 3
2.4211 2.4236 -.0025 2 1 2
2.1994 2.1997 -.0003 1 0 4
2.1444 2.1434 .0010 3 1 0
1.9835 1.9823 .0012 1 1 4
1.7112 1.7118 -.0006 0 1 5
1.6379 1.6388 -.0009 2 2 3
1.4238 1.4239 -.0001 4 2 0
a= 7.279 b= 4.573 c= 9.230
da= .006 db= .006 dc= .002
V= 307.3
11. 40-0723
BaCoTi0.07O2.14
Rombik
Groupa 31,59
Dexp. Dcal. d(D) h k l
4.0367 4.0278 .0089 1 0 2
3.0659 3.0693 -.0034 1 0 3
2.9760 2.9744 .0016 2 0 1
2.8115 2.8115 .0000 0 3 1
2.5265 2.5286 -.0021 2 2 0
2.3628 2.3619 .0009 1 3 2
2.2466 2.2489 -.0023 0 3 3
2.1157 2.1140 .0017 1 3 3
2.0650 2.0659 -.0009 3 0 0
1.8225 1.8231 -.0006 1 2 5
1.6681 1.6677 .0004 1 1 6
1.6653 1.6648 .0005 3 3 1
1.6273 1.6275 -.0002 1 4 4
a= 6.1978 b= 8.7477 c=10.599
da= .0008 db= .0007 dc= .003
V= 574.6
Triklin
Dexp Dcal d(D) h k l
4.0367 4.0381 -.0014 1 0 1
3.0659 3.0644 .0015 -1 1 1
2.9760 2.9751 .0009 1 -1 1
2.8115 2.8110 .0005 1 0 2
2.5265 2.5265 .0000 1 1 1
2.3628 2.3646 -.0018 2 0 1
2.2466 2.2490 -.0024 -2 1 1
2.1157 2.1173 -.0016 -1 -1 2
2.0650 2.0652 -.0002 1 0 3
1.8225 1.8224 .0001 -1 2 1
1.6681 1.6679 .0002 -2 1 3
1.6653 1.6648 .0005 -2 -1 2
1.6273 1.6268 .0005 3 -1 1
A= 5.2127 DA= .0006
B= 3.7863 DB= .0008
C= 6.851 DC= .001
GAMMA=102.96 DGAMMA= .08
BETA = 91.59 DBETA = .02
ALPHA= 88.22 DALPHA= .01
V= 131.7
12. 40-0724
BaCoTi0.148O2.296
Triklin
Dexp Dcal d(D) h k l
3.5090 3.5067 .0023 -1 2 0
3.4305 3.4270 .0035 1 2 0
3.1727 3.1717 .0010 1 -3 1
2.7361 2.7330 .0031 0 4 0
2.5265 2.5252 .0013 -1 -3 1
2.4024 2.4009 .0015 2 -1 1
2.3598 2.3582 .0016 -1 4 0
2.2493 2.2511 -.0018 2 -1 2
2.1542 2.1546 -.0004 -1 -2 2
2.1251 2.1248 .0003 1 -3 3
2.0786 2.0794 -.0008 1 -5 2
1.9918 1.9916 .0002 0 -3 3
A= 4.8196 DA= .0001
B= 11.4557 DB= .0005
C= 6.680 DC= .001
GAMMA= 97.48 DGAMMA= .01
BETA = 68.49 DBETA = .01
ALPHA=107.35 DALPHA= .01
V=327.9
13. 40-0725
BaCoTi0.235O2.47
Triklin
Dexp Dcal d(D) h k l
3.7509 3.7504 .0005 0 1 1
3.4176 3.4176 -.0000 0 -1 1
3.1078 3.1097 -.0019 1 1 1
2.8201 2.8205 -.0004 0 2 1
2.5196 2.5192 .0004 1 2 0
2.3539 2.3543 -.0004 1 -2 1
2.2413 2.2415 -.0002 -1 -1 1
2.1299 2.1297 .0002 1 0 2
2.0740 2.0740 .0000 -1 2 1
1.8294 1.8294 .0000 -2 1 0
1.6353 1.6353 .0000 2 2 0
1.4161 1.4161 -.0000 -1 -2 2
A= 3.9674 DA= .0001
B= 7.0027 DB= .0002
C= 4.4115 DC= .0002
GAMMA= 89.74 DGAMMA= .02
BETA = 71.566 DBETA = .005
ALPHA= 84.19 DALPHA= .01
V= 115.6
14. 40-1146
CoSbF12
Monoklin
Dexp Dcal d(D) h k l
4.9800 4.9505 .0295 1 0 1
3.7000 3.6996 .0004 -2 1 1
3.5400 3.5406 -.0006 0 2 0
2.8800 2.8798 .0002 1 2 1
2.2500 2.2498 .0002 -4 0 1
2.0500 2.0501 -.0001 4 1 0
1.7800 1.7800 .0000 -3 3 2
1.6800 1.6802 -.0002 1 1 4
1.6000 1.6004 -.0004 -5 2 1
1.5200 1.5201 -.0001 -5 0 4
1.4600 1.4601 -.0001 -4 0 5
1.4000 1.3997 .0003 6 1 0
1.3500 1.3498 .0002 -4 2 5
a= 9.002 b= 7.08111 c= 7.9064 beta= 107.865
da=.001 db=.00002 dc=.0007 dbeta=.002
V= 479.6
Triklin
Dexp Dcal d(D) h k l
4.9800 4.9869 -.0069 0 1 1
3.7000 3.7042 -.0042 0 -1 1
3.5400 3.5394 .0006 1 0 0
2.8800 2.8793 .0007 1 1 0
2.2500 2.2500 -.0000 0 0 3
2.0500 2.0502 -.0002 0 2 3
1.7800 1.7797 .0003 -1 2 3
1.6800 1.6806 -.0006 -2 1 1
1.6000 1.5999 .0001 -1 -2 2
1.5200 1.5199 .0001 -2 2 0
1.4600 1.4599 .0001 -2 2 2
1.4000 1.4000 -.0000 0 4 1
1.3500 1.3500 -.0000 0 0 5
A= 3.5466 DA= .0002
B= 5.6359 DB= .0006
C= 7.0699 DC= .0005
GAMMA= 92.81 DGAMMA= .03
BETA = 88.57 DBETA = .01
ALPHA= 72.864 DALPHA= .007
V= 134.76
15. 40-1230
Al80Cr13Co7
Rombik
Groupa 33,49,62
Dexp. Dcal. d(D) h k l
3.8584 3.8581 .0003 0 2 0
2.1733 2.1756 -.0023 2 1 0
2.0635 2.0635 .0000 0 0 2
1.4838 1.4835 .0003 3 1 0
1.2758 1.2758 .0000 2 5 0
a= 4.535 b= 7.716 c= 4.127
da= .001 db= .006 dc= .001
V= 144.4
16. 40-1784
C10H10Cl2CoN6O2*2H2O
Triklin
Dexp Dcal d(D) h k l
8.1900 8.1771 .0129 1 0 0
6.6800 6.7096 -.0296 1 1 0
5.9900 5.9874 .0026 -1 0 1
5.3900 5.3862 .0038 -1 1 1
4.9600 4.9593 .0007 0 -1 1
4.7800 4.7798 .0002 0 2 1
4.0900 4.0885 .0015 2 0 0
3.7900 3.7906 -.0006 -2 0 1
3.7000 3.7000 .0000 -1 0 2
3.4700 3.4695 .0005 -2 -1 1
3.3200 3.3186 .0014 0 -2 1
3.1500 3.1507 -.0007 0 -1 2
2.9000 2.8999 .0001 2 2 2
2.7400 2.7405 -.0005 -2 2 0
A= 8.3480 DA= .0004
B= 9.84 DB= .02
C= 8.639 DC= .008
GAMMA= 79.96 DGAMMA= .06
BETA = 91.29 DBETA = .07
ALPHA= 66.47 DALPHA= .05
V= 637.4
17. 40-1786
C12H16Cl2CoN4O4
Triklin
Dexp Dcal d(D) h k l
7.8600 7.8606 -.0006 1 1 1
6.1900 6.1992 -.0092 -1 1 0
5.8100 5.8088 .0012 1 -1 1
5.5200 5.5209 -.0009 0 2 0
5.4000 5.3983 .0017 1 1 2
5.2900 5.2910 -.0010 0 -1 2
5.0400 5.0437 -.0037 0 -2 1
4.7600 4.7623 -.0023 2 0 1
4.2000 4.2016 -.0016 -2 0 1
3.9800 3.9824 -.0024 0 0 3
3.8300 3.8277 .0023 -1 2 1
3.5900 3.5879 .0021 -2 -1 2
A= 10.5241 DA= .0003
B= 11.9031 DB= .0007
C= 12.1640 DC= .0001
GAMMA= 68.094 DGAMMA= .003
BETA = 79.2149 DBETA = .0009
ALPHA= 86.869 DALPHA= .001
V=1389.5
18. 40-1793
C8H12Br2CoN4O4
Triklin
Dexp Dcal d(D) h k l
6.9700 6.9718 -.0018 1 0 0
6.4600 6.4691 -.0091 1 1 0
5.2900 5.2898 .0002 -1 0 1
4.6900 4.6882 .0018 0 -1 1
4.1100 4.1093 .0007 -1 1 0
3.9500 3.9501 -.0001 -1 1 1
3.5500 3.5502 -.0002 -1 0 2
3.4700 3.4709 -.0009 1 2 2
3.2500 3.2508 -.0008 2 0 1
3.0500 3.0497 .0003 2 2 2
A= 7.828 DA= .007
B= 8.12 DB= .01
C= 8.928 DC= .008
GAMMA= 63.00 DGAMMA= .07
BETA = 79.73 DBETA = .07
ALPHA= 69.99 DALPHA= .08
V= 474.7
19. 40-1794
C8H8CoN6O8
Triklin
Dexp Dcal d(D) h k l
9.8300 9.8209 .0091 1 0 0
6.7600 6.7787 -.0187 0 1 1
5.5000 5.4944 .0056 0 -1 1
4.9300 4.9247 .0053 -1 2 0
4.8600 4.8554 .0046 1 2 0
4.6200 4.6199 .0001 1 -1 1
4.5300 4.5294 .0006 -2 1 0
4.3100 4.3136 -.0036 -2 0 1
3.8400 3.8382 .0018 -2 -1 1
3.7100 3.7100 -.0000 -2 2 1
3.6300 3.6314 -.0014 1 -2 1
3.4900 3.4914 -.0014 1 3 0
3.3900 3.3893 .0007 0 2 2
3.3400 3.3400 -.0000 2 2 1
A= 9.9139 DA= .0008
B= 11.597 DB= .007
C= 7.410 DC= .004
GAMMA= 92.72 DGAMMA= .01
BETA = 97.80 DBETA = .03
ALPHA= 76.53 DALPHA= .02
V= 820.7
20. 40-1803
C12H12CoN2O6*2H2O
Triklin
Dexp Dcal d(D) h k l
8.1900 8.1743 .0157 1 0 0
7.6600 7.6590 .0010 0 1 0
7.2500 7.2570 -.0070 0 -1 1
6.7800 6.7640 .0160 1 1 0
5.4500 5.4535 -.0035 -1 0 1
5.1400 5.1343 .0057 1 -1 1
4.9800 4.9956 -.0156 0 1 1
4.6600 4.6679 -.0079 0 -1 2
4.3600 4.3625 -.0025 1 0 2
4.0800 4.0827 -.0027 2 0 1
3.8300 3.8295 .0005 0 2 0
3.6000 3.5980 .0020 -1 0 2
A= 8.690 DA= .007
B= 8.507 DB= .002
C= 9.676 DC= .004
GAMMA= 74.93 DGAMMA= .03
BETA = 82.79 DBETA = .04
ALPHA=108.27 DALPHA= .07
V= 638.9
21. 40-1799
C10H10CoN4O6*2H2o
Triklin
Dexp Dcal d(D) h k l
9.5100 9.5036 .0064 1 0 0
6.8900 6.8872 .0028 0 1 0
6.1900 6.1933 -.0033 -1 -1 1
4.9000 4.8987 .0013 -1 1 0
4.7500 4.7518 -.0018 2 0 0
4.5100 4.5082 .0018 0 1 2
4.2900 4.2898 .0002 1 -1 1
3.6000 3.5999 .0001 -1 -1 3
3.3900 3.3901 -.0001 -2 -1 3
3.1500 3.1500 -.0000 1 1 3
3.0000 3.0003 -.0003 0 2 2
A= 10.357 DA= .004
B= 7.259 DB= .001
C= 12.068 DC= .007
GAMMA= 71.64 DGAMMA= .01
BETA =105.08 DBETA = .08
ALPHA= 93.27 DALPHA= .07
V= 831.2
22. 40-1803
C12H12CoN2O6*2H2O
Triklin
Dexp Dcal d(D) h k l
8.1900 8.1743 .0157 1 0 0
7.6600 7.6590 .0010 0 1 0
7.2500 7.2570 -.0070 0 -1 1
6.7800 6.7640 .0160 1 1 0
5.4500 5.4535 -.0035 -1 0 1
5.1400 5.1343 .0057 1 -1 1
4.9800 4.9956 -.0156 0 1 1
4.6600 4.6679 -.0079 0 -1 2
4.3600 4.3625 -.0025 1 0 2
4.0800 4.0827 -.0027 2 0 1
3.8300 3.8295 .0005 0 2 0
3.6000 3.5980 .0020 -1 0 2
A= 8.690 DA= .007
B= 8.507 DB= .002
C= 9.676 DC= .004
GAMMA= 74.93 DGAMMA= .03
BETA = 82.79 DBETA = .04
ALPHA=108.27 DALPHA= .07
V= 638.9
23. 40-1830
C12H8CoK2N12O12*4H2O
Triklin
Dexp Dcal d(D) h k l
8.6400 8.6573 -.0173 0 1 1
7.8500 7.8303 .0197 0 -1 1
6.2700 6.2591 .0109 1 1 0
6.1600 6.1635 -.0035 -1 0 1
5.2200 5.2149 .0051 1 1 1
4.8800 4.8834 -.0034 0 1 2
3.9700 3.9678 .0022 -1 2 2
3.4440 3.4451 -.0011 2 1 0
3.3640 3.3649 -.0009 -2 2 0
3.1660 3.1663 -.0003 -1 1 3
3.1210 3.1203 .0007 1 4 0
3.0500 3.0487 .0013 1 -4 1
A= 7.327 DA= .002
B= 14.591 DB= .004
C= 10.1049 DC= .0005
GAMMA= 95.846 DGAMMA= .002
BETA = 96.244 DBETA = .009
ALPHA= 83.29880 DALPHA= .00001
V= 1062.3