1. 38-0315
{NH4}{Ni,Co}PO4*0.67H2O
Triklin
Dexp Dcal d(D) h k l
8.7500 8.7501 -.0001 1 0 0
4.6790 4.6781 .0009 -1 2 0
4.3500 4.3509 -.0009 -1 -1 1
4.1580 4.1581 -.0001 1 0 1
3.6080 3.6084 -.0004 0 -2 1
3.3300 3.3340 -.0040 -2 2 0
2.7730 2.7754 -.0024 3 2 0
2.6460 2.6456 .0004 0 1 2
2.4820 2.4819 .0001 -1 -1 2
2.3660 2.3657 .0003 0 5 1
2.3130 2.3140 -.0010 1 5 1
2.2680 2.2678 .0002 1 3 2
A= 8.937 DA= .003
B= 12.344 DB= .005
C= 5.3569 DC= .0001
GAMMA= 84.03 DGAMMA= .01
BETA = 98.88 DBETA = .01
ALPHA= 80.120 DALPHA= .005
V= 570.0
2. 38-0316
{NH}4{Ni,Co}PO4*4H2O
Rombik
Groupa 31,59
Dexp. Dcal. d(D) h k l
5.8820 5.9126 -.0306 0 1 1
5.5520 5.5673 -.0153 1 1 1
5.3200 5.2943 .0257 2 0 2
4.4240 4.4280 -.0040 1 0 3
4.1200 4.1162 .0038 2 1 2
4.0090 4.0168 -.0078 2 0 3
3.4500 3.4470 .0030 0 0 4
3.3790 3.3744 .0046 1 0 4
3.2120 3.2102 .0018 1 2 0
3.1240 3.1266 -.0026 1 2 1
2.8860 2.8859 .0001 5 1 1
2.8640 2.8613 .0027 2 1 4
a=16.532 b= 6.545 c=13.788
da= .005 db= .005 dc= .004
v=1492
Triklin
Dexp Dcal d(D) h k l
5.8820 5.8814 .0006 0 1 1
5.5520 5.5380 .0140 0 -1 1
5.3200 5.3252 -.0052 -1 0 1
4.4240 4.4272 -.0032 -1 1 1
4.1200 4.1156 .0044 0 2 1
4.0090 4.0138 -.0048 1 1 1
3.4500 3.4470 .0030 -1 2 0
3.3790 3.3834 -.0044 0 1 2
3.2120 3.2109 .0011 -1 1 2
3.1240 3.1200 .0040 1 3 0
2.8860 2.8816 .0044 1 -2 1
2.8640 2.8680 -.0040 0 -3 1
A= 6.357 DA= .003
B= 9.89 DB= .01
C= 7.315 DC= .005
GAMMA= 78.89 DGAMMA= .01
BETA =104.94 DBETA = .02
ALPHA= 89.42 DALPHA= .03
V= 435.2
3. 38-0518
CsFe0.5Co0.5Cl3*2H2O
Triklin
Dexp Dcal d(D) h k l
5.6400 5.6430 -.0030 1 1 0
4.8200 4.8216 -.0016 0 1 1
4.7000 4.7060 -.0060 0 -1 1
4.4100 4.4183 -.0083 1 0 1
4.2600 4.2581 .0019 -1 2 0
3.9200 3.9137 .0063 0 -2 1
3.7400 3.7431 -.0031 1 2 1
3.5600 3.5555 .0045 1 3 0
3.1600 3.1543 .0057 1 3 1
3.0200 3.0195 .0005 2 1 0
2.8600 2.8628 -.0028 1 4 0
2.7900 2.7897 .0003 2 -1 1
A= 6.2804 DA= .0001
B= 12.5830 DB= .0001
C= 5.2682 DC= .0004
GAMMA= 86.062 DGAMMA= .003
BETA = 77.908 DBETA = .002
ALPHA= 87.247 DALPHA= .003
V=405.9
4. 38-0547
Co{CO3}0.35Cl0.2{OH}1.1*1.74H2O
Triklin
Dexp Dcal d(D) h k l
8.7100 8.7058 .0042 1 0 0
5.0800 5.0824 -.0024 0 1 1
3.3600 3.3634 -.0034 -2 -1 1
3.0900 3.0915 -.0015 1 2 0
2.9440 2.9436 .0004 -3 0 1
2.6680 2.6678 .0002 0 -1 2
2.5560 2.5561 -.0001 -1 2 2
2.4640 2.4640 -.0000 2 2 1
2.3000 2.3009 -.0009 2 1 2
1.9820 1.9819 .0001 1 1 3
1.9390 1.9392 -.0002 1 -2 2
1.7110 1.7108 .0002 -3 -3 1
A= 9.010 DA= .001
B= 6.619 DB= .002
C= 6.742 DC= .001
GAMMA= 90.06 DGAMMA= .02
BETA =104.68 DBETA = .02
ALPHA= 79.02 DALPHA= .01
V= 381.4
5. 38-0592
Co{ClO4}2
Triklin
Dexp Dcal d(D) h k l
7.3500 7.3505 -.0005 1 0 0
4.7500 4.7498 .0002 -1 1 0
4.1300 4.1287 .0013 0 0 1
3.9100 3.9107 -.0007 2 1 0
3.3300 3.3306 -.0006 -1 -1 1
3.1200 3.1197 .0003 2 1 1
3.0100 3.0102 -.0002 2 0 1
2.4200 2.4204 -.0004 -1 2 1
2.2900 2.2898 .0002 0 3 1
2.0200 2.0200 -.0000 -3 -2 1
1.4500 1.4500 .0000 3 6 0
1.3900 1.3900 .0000 -5 -2 1
A= 7.9776 DA= .0004
B= 8.937 DB= .001
C= 4.194 DC= .001
GAMMA= 69.22 DGAMMA= .01
BETA = 79.96 DBETA = .02
ALPHA= 87.40 DALPHA= .03
V= 275.2
6. 38-0597
SnCo{PO4}2*6H2O
Rombik
Groupa 32,55
Dexp. Dcal. d(D) h k l
16.3000 16.3141 -.0141 0 0 1
8.4000 8.3554 .0446 2 0 0
4.2900 4.2863 .0037 1 1 1
3.6700 3.6652 .0048 2 0 4
2.4800 2.4789 .0011 6 0 3
2.1300 2.1292 .0008 3 2 0
1.6200 1.6203 -.0003 4 2 6
1.4400 1.4401 -.0001 9 2 1
a=16.71 b= 4.61 c=16.31
da= .04 db= .01 dc= .02
V=1256
7. 38-0656
Co{HPO3NH2}2*3H2O
Triklin
Dexp Dcal d(D) h k l
6.6000 6.6270 -.0270 1 0 0
6.5300 6.5114 .0186 0 1 0
6.4600 6.4430 .0170 0 1 1
5.5200 5.5277 -.0077 -1 1 1
4.7000 4.6994 .0006 1 0 1
4.1000 4.1033 -.0033 0 -1 1
3.3800 3.3790 .0010 -1 -1 1
3.2400 3.2425 -.0025 -2 1 0
3.2200 3.2215 -.0015 0 2 2
2.7300 2.7295 .0005 2 1 0
2.4900 2.4898 .0002 -2 -1 1
2.3500 2.3497 .0003 2 0 2
A= 6.955 DA= .004
B= 7.51136 DB= .00005
C= 8.417 DC= .007
GAMMA=106.59 DGAMMA= .03
BETA =102.89 DBETA = .04
ALPHA= 62.482 DALPHA= .004
V=372.4
8. 38-0675
{Co{NH3}6}{Nd{SO4}3}*5H2O
Triklin
Dexp Dcal d(D) h k l
10.8000 10.7657 .0343 1 0 0
9.4100 9.3951 .0149 1 1 0
7.0800 7.0771 .0029 0 1 1
6.3300 6.3210 .0090 1 2 0
6.1900 6.1934 -.0034 1 1 1
5.4700 5.4726 -.0026 -1 -2 1
5.4000 5.3904 .0096 2 1 0
4.9000 4.8963 .0037 1 2 1
4.7400 4.7433 -.0033 -2 -1 1
4.5800 4.5843 -.0043 2 0 1
4.4800 4.4845 -.0045 1 3 0
4.3700 4.3703 -.0003 -1 2 1
A= 11.0028 DA= .0003
B= 13.8765 DB= .0008
C= 9.0045 DC= .0005
GAMMA= 78.113 DGAMMA= .001
BETA = 92.185 DBETA = .003
ALPHA= 97.035 DALPHA= .001
V=1337
9. 38-0676
{Co{NH3}6}{Nd{SO4}3}*4H2O
Triklin
Dexp Dcal d(D) h k l
11.0000 10.9743 .0257 1 0 0
7.7600 7.7704 -.0104 1 -1 0
7.2500 7.2337 .0163 1 -1 1
6.0700 6.0732 -.0032 -1 0 1
5.8700 5.8547 .0153 2 0 1
5.5400 5.5344 .0056 1 1 0
5.4700 5.4694 .0006 -2 1 0
4.7700 4.7649 .0051 1 -1 2
4.6700 4.6788 -.0088 2 -1 2
4.1700 4.1730 -.0030 -1 2 0
4.0800 4.0773 .0027 2 -2 1
4.0000 3.9971 .0029 2 1 1
A= 12.990 DA= .009
B= 8.523 DB= .003
C= 10.507 DC= .007
GAMMA=113.14 DGAMMA= .03
BETA = 64.20 DBETA = .03
ALPHA=101.69 DALPHA= .04
V=963.2
10. 38-0989
Co2As2Se5
Triklin
Dexp Dcal d(D) h k l
4.2584 4.2622 -.0038 -1 -1 1
3.5413 3.5454 -.0041 1 -1 1
3.3130 3.3133 -.0003 1 1 3
2.9850 2.9807 .0043 0 2 2
2.8687 2.8671 .0016 2 0 2
2.7742 2.7731 .0011 -1 1 3
2.5609 2.5615 -.0006 0 0 4
2.3655 2.3673 -.0018 0 -2 2
2.1801 2.1782 .0019 -2 -1 3
2.1419 2.1438 -.0019 -2 1 3
2.0911 2.0909 .0002 2 0 4
2.0682 2.0687 -.0005 3 1 3
A= 6.9997 DA= .0003
B= 6.64711 DB= .00006
C= 10.7174 DC= .0002
GAMMA= 71.844 DGAMMA= .001
BETA = 81.6432 DBETA = .0009
ALPHA= 73.3036 DALPHA= .0004
V=453.4
11. 38-0990
CoSb2Se4
Triklin
Dexp Dcal d(D) h k l
5.8990 5.8998 -.0008 1 1 0
5.2771 5.2665 .0106 0 1 1
4.1291 4.1312 -.0021 0 -1 1
3.7200 3.7158 .0042 1 1 2
3.2433 3.2425 .0008 1 2 0
3.1317 3.1362 -.0045 0 2 0
2.9308 2.9327 -.0019 1 2 2
2.8613 2.8607 .0006 -1 0 2
2.7748 2.7745 .0003 -2 1 1
2.6984 2.6993 -.0009 1 -1 2
2.6173 2.6161 .0012 0 -2 1
2.5177 2.5192 -.0015 2 1 3
A= 9.89 DA= .01
B= 6.9647 DB= .0001
C= 7.6110 DC= .0006
GAMMA= 68.04 DGAMMA= .02
BETA = 66.09 DBETA = .02
ALPHA= 69.27 DALPHA= .01
V=431.9
12. 38-1165
CoSb2F8*6H2O
Triklin
Dexp Dcal d(D) h k l
9.1100 9.1231 -.0131 0 1 0
6.4770 6.4789 -.0019 -1 -1 1
5.2600 5.2589 .0011 0 -1 2
4.7800 4.7803 -.0003 1 -1 2
4.4810 4.4810 -.0000 1 2 0
4.3610 4.3663 -.0053 -1 -1 2
4.0260 4.0253 .0007 1 -2 2
3.8150 3.8144 .0006 -1 0 2
3.6870 3.6877 -.0007 -2 -2 1
3.6410 3.6408 .0002 2 2 0
3.4120 3.4121 -.0001 0 -3 2
3.2410 3.2395 .0015 -2 -2 2
A= 9.422 DA= .007
B= 10.53806 DB= .00003
C= 10.586 DC= .002
GAMMA= 82.20 DGAMMA= .04
BETA = 83.610 DBETA = .005
ALPHA=117.63 DALPHA= .04
V= 904.2
13. 38-1659
C4H12Cl2CoO8*2H2O
Triklin
Dexp Dcal d(D) h k l
9.3100 9.3233 -.0133 0 1 0
6.6550 6.6533 .0017 -1 -1 1
4.5980 4.5996 -.0016 0 -1 2
3.5610 3.5613 -.0003 -1 -1 3
3.1530 3.1528 .0002 1 0 3
2.9980 2.9981 -.0001 -1 -2 3
2.7970 2.7971 -.0001 -3 -1 2
2.7800 2.7801 -.0001 3 2 0
2.7715 2.7719 -.0004 0 -2 3
2.4620 2.4619 .0001 1 4 1
2.3440 2.3440 .0000 0 4 1
2.0360 2.0360 .0000 -4 -2 3
1.7492 1.7492 .0000 -2 3 5
A= 8.756 DA= .008
B= 9.977 DB= .004
C= 11.731 DC= .001
GAMMA= 70.46 DGAMMA= .02
BETA =101.89 DBETA = .01
ALPHA= 87.10 DALPHA= .01
V= 937.1
14. 38-1844
C8H25Cl5CoN5Zn
Triklin
Dexp Dcal d(D) h k l
7.2484 7.2524 -.0040 -1 1 0
6.5532 6.5755 -.0223 -1 1 1
5.7118 5.7073 .0045 -1 -1 1
5.3040 5.3136 -.0096 1 -1 1
5.1509 5.1442 .0067 1 0 1
4.5715 4.5756 -.0041 -1 1 2
4.4577 4.4585 -.0008 1 -2 1
4.1678 4.1731 -.0053 1 1 1
4.0367 4.0445 -.0078 0 -2 2
3.8634 3.8609 .0025 1 2 0
3.7509 3.7502 .0007 2 0 0
3.6012 3.6011 .0001 0 -3 1
A= 8.3079 DA= .0002
B= 11.329 DB= .002
C= 10.634 DC= .002
GAMMA=104.514 DGAMMA= .004
BETA =108.937 DBETA = .002
ALPHA= 95.42 DALPHA= .01
V=899.2
15. 38-1990
C22H22Cl2CoC4O14*2H2O
Triklin
Dexp Dcal d(D) h k l
5.2800 5.2863 -.0063 0 1 1
4.6200 4.6145 .0055 -1 1 1
4.4300 4.4320 -.0020 0 -1 1
4.0000 4.0044 -.0044 1 -1 1
3.7000 3.7004 -.0004 1 1 0
3.3700 3.3731 -.0031 0 2 0
3.1100 3.1101 -.0001 -1 1 2
2.8800 2.8806 -.0006 -2 1 1
2.7400 2.7405 -.0005 -2 2 0
2.5100 2.5093 .0007 1 2 0
2.4300 2.4302 -.0002 -1 3 0
2.1600 2.1600 .0000 1 2 2
2.0100 2.0096 .0004 2 -3 1
A= 6.138 DA= .001
B= 7.427 DB= .001
C= 6.966 DC= .003
GAMMA=112.71 DGAMMA= .09
BETA = 94.34 DBETA = .02
ALPHA= 79.07 DALPHA= .01
V= 287.7