1. 19-0349
Mn-Co-Si
Triklin
Dexp Dcal d(D) h k l
2.3500 2.3517 -.0017 1 2 0
2.2100 2.2080 .0020 0 2 1
2.1600 2.1591 .0009 0 -2 1
2.1200 2.1200 .0000 1 -2 1
2.0700 2.0699 .0001 1 0 2
2.0500 2.0504 -.0004 0 0 2
1.9900 1.9915 -.0015 -2 2 0
1.9590 1.9582 .0008 -1 -2 1
1.9400 1.9406 -.0006 2 2 0
1.9020 1.9011 .0009 -3 1 0
1.8740 1.8741 -.0001 2 -2 1
1.8360 1.8363 -.0003 -1 0 2
A= 6.1941 DA= .0002
B= 5.16083 DB= .00007
C= 4.18334 DC= .00001
GAMMA= 91.253 DGAMMA= .001
BETA = 78.6986 DBETA = .0004
ALPHA= 88.8543 DALPHA= .0005
V=130.94
2. 19-0350
CoMnSi
Triklin
Dexp Dcal d(D) h k l
3.8400 3.8479 -.0079 0 1 1
3.3600 3.3587 .0013 -1 -1 1
3.3100 3.3036 .0064 0 -1 1
3.2400 3.2376 .0024 0 2 0
3.0500 3.0541 -.0041 1 2 0
2.3140 2.3144 -.0004 2 1 1
2.2570 2.2531 .0039 -3 0 1
2.2160 2.2170 -.0010 -2 -2 1
2.2090 2.2078 .0012 -1 0 2
2.1540 2.1584 -.0044 0 3 0
2.1310 2.1264 .0046 1 3 0
2.1210 2.1179 .0031 0 0 2
A= 6.9884 DA= .0008
B= 6.582 DB= .003
C= 4.462 DC= .003
GAMMA= 85.91 DGAMMA= .01
BETA =105.72 DBETA = .03
ALPHA= 82.00 DALPHA= .08
V=194.5
3. 19-0351
Co{PO3}2
Triklin
Dexp Dcal d(D) h k l
6.1300 6.1312 -.0012 -1 0 1
4.6700 4.6707 -.0007 0 1 1
4.5700 4.5670 .0030 0 -1 1
4.2300 4.2298 .0002 -1 0 2
3.5300 3.5278 .0022 -2 1 1
3.5100 3.5093 .0007 -1 -1 1
3.3700 3.3738 -.0038 -2 0 1
3.2300 3.2277 .0023 2 0 0
3.1800 3.1807 -.0007 1 0 2
2.9900 2.9898 .0002 -1 0 3
2.8600 2.8600 .0000 -1 1 3
2.5800 2.5804 -.0004 -2 2 0
A= 7.308 DA= .004
B= 5.897 DB= .001
C= 9.174 DC= .001
GAMMA=112.18 DGAMMA= .01
BETA =109.28 DBETA = .01
ALPHA= 81.592 DALPHA= .007
V= 345.5
4. 19-0357
Co{NO3}2*6H2O
Triklin
Dexp Dcal d(D) h k l
5.8200 5.8161 .0039 -1 0 1
5.5700 5.5772 -.0072 0 1 1
5.4200 5.4154 .0046 0 -1 1
5.0600 5.0564 .0036 -1 1 0
3.8600 3.8605 -.0005 0 2 0
3.7100 3.7230 -.0130 1 1 1
3.2800 3.2766 .0034 -2 0 1
3.1500 3.1508 -.0008 2 0 0
2.9100 2.9081 .0019 -2 0 2
2.7700 2.7692 .0008 1 -1 2
2.7080 2.7077 .0003 0 -2 2
2.6110 2.6090 .0020 -2 2 1
A= 6.617 DA= .004
B= 7.7501 DB= .0008
C= 8.19618 DC= .00045
GAMMA= 94.684 DGAMMA= .001
BETA =107.3358 DBETA = .0006
ALPHA= 87.01 DALPHA= .01
V= 399.7
5. 19-0363
Co4S3
Triklin
Dexp Dcal d(D) h k l
4.0800 4.0800 .0000 1 0 0
1.9840 1.9840 .0000 2 1 0
1.8070 1.8072 -.0002 1 -4 1
1.5880 1.5881 -.0001 0 -5 1
1.4630 1.4631 -.0001 2 -4 1
1.3580 1.3579 .0001 0 4 3
1.2810 1.2808 .0002 -1 5 2
1.2450 1.2451 -.0001 3 -3 1
1.1010 1.1011 -.0001 3 0 4
1.0890 1.0890 -.0000 0 -7 2
1.0480 1.0479 .0001 4 0 1
1.0360 1.0360 -.0000 1 3 5
A= 4.1967 DA= .0002
B= 8.2686 DB= .0003
C= 5.618 DC= .001
GAMMA= 89.74 DGAMMA= .01
BETA = 76.467 DBETA = .006
ALPHA= 90.64 DALPHA= .01
V= 189.5
6. 19-0546
CoNHBeOCO*10H2O
Triklin
Dexp Dcal d(D) h k l
10.1000 10.0961 .0039 1 0 0
9.4200 9.4370 -.0170 0 1 0
9.1100 9.1262 -.0162 -1 0 1
7.7200 7.7153 .0047 1 0 1
6.0500 6.0611 -.0111 1 1 0
5.5700 5.5677 .0023 -1 1 2
5.4100 5.4077 .0023 1 -1 2
5.1200 5.1226 -.0026 -2 1 0
4.8600 4.8586 .0014 -1 2 0
4.6200 4.6213 -.0013 0 -1 3
4.4400 4.4404 -.0004 -2 1 2
4.0600 4.0582 .0018 -2 -1 1
A= 10.68063 DA= .00005
B= 9.9113 DB= .0003
C= 15.053 DC= .002
GAMMA=106.124 DGAMMA= .004
BETA = 98.46 DBETA = .01
ALPHA= 94.92 DALPHA= .01
V=1500.9
7. 19-0650
C38H46CoN4O8
Triklin
Dexp Dcal d(D) h k l
7.8600 7.8622 -.0022 0 1 1
7.4400 7.4388 .0012 0 -1 1
6.5600 6.5599 .0001 1 0 1
6.3400 6.3391 .0009 1 -1 1
5.4600 5.4600 .0000 1 -2 1
4.8600 4.8603 -.0003 0 3 1
4.3500 4.3497 .0003 -1 2 1
4.1900 4.1899 .0001 1 1 2
4.0700 4.0699 .0001 1 3 1
3.9300 3.9301 -.0001 1 -2 2
3.4800 3.4801 -.0001 -2 1 0
A= 7.3910 DA= .0006
B= 17.1187 DB= .0004
C= 9.113 DC= .001
GAMMA= 98.562 DGAMMA= .001
BETA = 70.482 DBETA = .009
ALPHA= 89.196 DALPHA= .003
V= 1072.1
8. 19-1778
C12H30CoI2N4
Tetragon
Groupa 77,84,93
Dexp. Dcal. d(D) h k l
7.1300 7.0174 .1126 1 0 2
6.2600 6.1977 .0623 1 1 2
5.6300 5.5661 .0639 2 1 1
5.1400 5.1649 -.0249 2 0 2
4.4000 4.4049 -.0049 3 0 0
4.1600 4.1789 -.0189 3 1 0
3.9500 3.9513 -.0013 1 0 4
3.7400 3.7308 .0092 3 1 2
3.3600 3.3516 .0084 3 2 2
3.0500 3.0535 -.0035 3 2 3
2.8900 2.8896 .0004 2 1 5
2.7400 2.7445 -.0045 3 2 4
a= 13.215 c= 16.56
da= .001 dc= .07
V=2892
Triklin
Dexp Dcal d(D) h k l
7.1300 7.1309 -.0009 1 1 0
6.2600 6.2515 .0085 0 1 1
5.6300 5.6305 -.0005 0 -1 1
5.1400 5.1377 .0023 -1 0 1
4.4000 4.3996 .0004 2 1 1
4.1600 4.1550 .0050 -1 1 1
3.9500 3.9544 -.0044 0 2 1
3.7400 3.7386 .0014 2 2 1
3.3600 3.3573 .0027 -1 2 0
3.0500 3.0531 -.0031 -1 1 2
2.8900 2.8881 .0019 1 1 3
A= 9.0534 DA= .0006
B= 9.192 DB= .005
C= 8.723 DC= .007
GAMMA= 68.73 DGAMMA= .02
BETA = 71.44 DBETA = .03
ALPHA= 78.02 DALPHA= .06
V= 637.7
9. 19-01847
C22H28CoN2O6
Triklin
Dexp Dcal d(D) h k l
9.2600 9.2558 .0042 1 0 0
7.3500 7.3551 -.0051 0 1 0
6.6000 6.5928 .0072 -1 0 1
6.3100 6.3025 .0075 1 1 0
4.4600 4.4578 .0022 0 -1 1
3.8900 3.8911 -.0011 -2 -1 1
3.5800 3.5803 -.0003 -1 0 2
3.3700 3.3701 -.0001 2 1 1
3.0300 3.0299 .0001 -3 -1 1
2.6000 2.6001 -.0001 1 -2 1
2.1900 2.1900 .0000 -4 1 2
A= 9.846 DA= .001
B= 7.629 DB= .002
C= 7.326 DC= .001
GAMMA= 84.50 DGAMMA= .02
BETA =107.49 DBETA = .01
ALPHA= 78.027 DALPHA= .005
V= 506.0
10. 19-1855
C20H24CoN2O4
Triklin
Dexp Dcal d(D) h k l
7.8600 7.8672 -.0072 1 0 0
7.4400 7.4199 .0201 1 1 0
6.5600 6.5350 .0250 0 0 1
6.3400 6.3310 .0090 0 1 1
5.4600 5.4681 -.0081 1 0 1
4.8600 4.8463 .0137 -1 1 0
4.3500 4.3475 .0025 2 1 1
4.1900 4.1940 -.0040 0 2 0
4.0700 4.0693 .0007 -1 -1 1
3.9300 3.9336 -.0036 2 0 0
3.4800 3.4812 -.0012 0 1 2
A= 9.163 DA= .003
B= 10.289 DB= .004
C= 7.430 DC= .001
GAMMA= 60.40 DGAMMA= .02
BETA = 69.72 DBETA = .03
ALPHA= 62.96 DALPHA= .03
V=536.0
11. 19-1895
C28H44CoNS4
Rombik
Groupa 29,57
Dexp. Dcal. d(D) h k l
9.3800 9.6016 -.2216 2 0 0
8.3000 8.2873 .0127 0 1 0
7.7400 7.6090 .1310 1 1 0
6.8000 6.8032 -.0032 2 0 1
6.2400 6.2736 -.0336 2 1 0
5.2700 5.2583 .0117 2 1 1
4.8200 4.8205 -.0005 0 0 2
4.2900 4.2975 -.0075 4 0 1
4.0500 4.0504 -.0004 1 2 0
3.8000 3.8045 -.0045 2 2 0
3.5400 3.5389 .0011 2 2 1
a=19.20 b= 8.29 c= 9.6
da= .06 db= .02 dc= .1
v=1534
Triklin
Dexp Dcal d(D) h k l
9.3800 9.3649 .0151 1 0 0
8.3000 8.2666 .0334 0 1 0
7.7400 7.7355 .0045 1 0 1
6.8000 6.8125 -.0125 1 1 0
6.2400 6.2371 .0029 0 1 1
5.2700 5.2717 -.0017 -1 0 1
4.8200 4.8187 .0013 2 1 1
4.2900 4.2909 -.0009 1 1 2
4.0500 4.0503 -.0003 1 2 0
3.8000 3.8009 -.0009 -2 1 0
3.5400 3.5394 .0006 -2 0 1
A= 10.382 DA= .003
B= 8.592 DB= .003
C= 9.01 DC= .01
GAMMA= 76.06 DGAMMA= .03
BETA = 66.34 DBETA = .05
ALPHA= 77.70 DALPHA= .08
V=708.9
12. 19-1896
C38H36Cl8CoNS8
Rombik
Groupa 17
Dexp. Dcal. d(D) h k l
11.4000 11.5136 -.1136 0 0 1
10.4000 10.3527 .0473 0 1 0
9.4900 9.5083 -.0183 2 0 0
7.7000 7.6983 .0017 0 1 1
5.7700 5.7568 .0132 0 0 2
4.5500 4.5463 .0037 2 2 0
3.7700 3.7726 -.0026 1 2 2
3.5700 3.5700 -.0000 5 1 0
3.2900 3.2901 -.0001 3 2 2
a=19.016 b=10.35 c=11.51
da= .002 db= .01 dc= .02
V=2267
13. 19-1898
C36H60CoNS4
Triklin
Dexp Dcal d(D) h k l
12.6000 12.6653 -.0653 1 0 0
11.8000 11.7898 .0102 0 1 0
8.7000 8.6709 .0291 0 0 1
8.0100 7.9755 .0345 0 -1 1
7.6200 7.5858 .0342 -1 -1 1
7.2600 7.2769 -.0169 -1 1 0
6.1400 6.1392 .0008 1 -1 1
5.6200 5.6341 -.0141 -2 -1 1
5.2400 5.2357 .0043 2 0 1
5.1600 5.1616 -.0016 2 1 1
4.4300 4.4346 -.0046 0 -1 2
4.1500 4.1489 .0011 -3 -1 1
3.9300 3.9299 .0001 0 3 0
3.5000 3.4995 .0005 -2 0 2
3.2300 3.2298 .0002 -3 -1 2
A= 13.891 DA= .001
B= 13.3186 DB= .0003
C= 8.9561 DC= .0005
GAMMA= 65.901 DGAMMA= .004
BETA = 93.3174 DBETA = .0002
ALPHA=104.246 DALPHA= .003
V=1464
14. 19-1901
C3H52CoNS4
Triklin
Dexp Dcal d(D) h k l
11.3000 11.3009 -.0009 1 0 0
8.3700 8.3646 .0054 0 1 0
7.7600 7.7603 -.0003 1 0 1
7.0500 7.0506 -.0006 0 0 2
6.6200 6.6223 -.0023 1 1 0
6.1500 6.1502 -.0002 -1 1 1
4.8900 4.8893 .0007 0 1 2
4.7000 4.7004 -.0004 0 0 3
4.3000 4.2991 .0009 -2 0 3
4.1300 4.1301 -.0001 -2 -1 3
3.8700 3.8689 .0011 1 -1 3
3.5300 3.5305 -.0005 -3 1 1
3.1300 3.1304 -.0004 1 -1 4
A= 11.848 DA= .003
B= 8.578 DB= .003
C= 15.14 DC= .03
GAMMA= 87.9621 DGAMMA= .0001
BETA =107.4 DBETA = .1
ALPHA=102.68 DALPHA= .04
V= 1432
15. 19-1931
C22H38CoO4
Triklin
Dexp Dcal d(D) h k l
10.6000 10.6014 -.0014 1 0 0
9.5500 9.5406 .0094 -1 1 0
8.6000 8.6065 -.0065 0 1 1
6.1700 6.1718 -.0018 -1 1 1
5.3500 5.3472 .0028 2 0 1
4.8400 4.8430 -.0030 -1 -1 1
4.6100 4.6096 .0004 2 1 0
4.4000 4.4023 -.0023 -1 3 1
3.9600 3.9600 .0000 -2 3 0
3.7800 3.7809 -.0009 0 3 2
3.5400 3.5390 .0010 -1 4 0
3.1800 3.1802 -.0002 -3 3 0
2.7300 2.7297 .0003 -1 2 3
2.5600 2.5601 -.0001 2 -2 3
2.4300 2.4300 .0000 -4 2 1
A= 11.313 DA= .002
B= 14.690 DB= .006
C= 9.435 DC= .007
GAMMA= 98.44 DGAMMA= .03
BETA = 74.32 DBETA = .03
ALPHA= 75.57 DALPHA= .03
V= 1422.9
16. 19-1936
C36H20AsCl8CoS4
Triklin
Dexp Dcal d(D) h k l
13.9000 13.9269 -.0269 1 0 0
12.5000 12.5083 -.0083 0 1 0
11.2000 11.1767 .0233 -1 0 1
8.5100 8.5200 -.0100 1 1 0
8.2400 8.2470 -.0070 1 0 1
7.7300 7.6930 .0370 -1 -1 1
6.5500 6.5581 -.0081 -1 0 2
5.5600 5.5635 -.0035 0 -2 1
4.7300 4.7286 .0014 1 1 2
4.4600 4.4604 -.0004 -3 1 2
4.1000 4.1003 -.0003 3 1 0
3.9700 3.9696 .0004 -2 3 1
A= 14.914 DA= .001
B= 12.7964 DB= .0001
C= 13.35 DC= .01
GAMMA=102.13 DGAMMA= .01
BETA =107.84 DBETA = .03
ALPHA= 85.16532 DALPHA= .00008
V=2369
17. 19-1959
C12H36CoCl2N4O12
Rombik
Groupa 31,59
Dexp. Dcal. d(D) h k l
7.6400 7.6797 -.0397 2 0 1
6.5900 6.6182 -.0282 3 0 0
6.0100 6.0596 -.0496 0 0 2
5.4600 5.4712 -.0112 2 1 0
5.0000 4.9866 .0134 2 1 1
4.4900 4.4693 .0207 3 0 2
3.9700 3.9709 -.0009 5 0 0
3.7600 3.7621 -.0021 4 1 1
a=19.85 b= 6.56 c=12.12
da= .03 db= .02 dc= .09
V=1578
Monoklin
GRUPA 4,11
Dexp. Dcal. d(D) h k l
7.6400 7.6425 -.0025 1 1 0
6.5900 6.5050 .0850 1 0 2
6.0100 6.0020 .0080 2 0 1
5.4600 5.4542 .0058 1 1 2
5.0000 5.0040 -.0040 0 2 0
4.4900 4.4920 -.0020 1 2 1
3.9700 3.9663 .0037 1 2 2
3.7600 3.7600 .0000 2 1 3
a= 12.243 b= 10.0080 c= 13.627 beta= 75.2
da=.003 db=.0005 dc=.001 dbet=.001
V=1613
Triklin
Dexp Dcal d(D) h k l
7.6400 7.6416 -.0016 1 0 0
6.5900 6.5921 -.0021 0 1 0
6.0100 6.0102 -.0002 0 1 1
5.4600 5.4616 -.0016 -1 0 1
5.0000 4.9999 .0001 1 1 1
4.4900 4.4894 .0006 -1 1 1
3.9700 3.9697 .0003 -1 -1 1
3.7600 3.7600 .0000 1 2 1
A= 8.353 DA= .001
B= 7.814 DB= .001
C= 6.8112 DC= .0005
GAMMA= 70.97 DGAMMA= .01
BETA = 95.15 DBETA = .02
ALPHA= 66.70 DALPHA= .01
V= 373.52
18. 20-0331
LiCoBO3
Rombik
Groupa 31,59
Dexp. Dcal. d(D) h k l
4.3900 4.3889 .0011 2 1 1
4.0400 4.0389 .0011 3 0 1
3.3700 3.3752 -.0052 1 2 1
3.3000 3.3013 -.0013 2 1 2
3.1800 3.1838 -.0038 4 0 1
2.9200 2.9212 -.0012 3 2 0
2.7100 2.7036 .0064 0 1 3
2.5800 2.5761 .0039 5 1 0
2.5300 2.5336 -.0036 4 1 2
2.4400 2.4411 -.0011 4 2 1
2.3200 2.3155 .0045 5 0 2
2.2700 2.2703 -.0003 1 2 3
a=13.690 b= 7.605 c= 8.678
da= .002 db= .005 dc= .007
V= 903.4
Triklin
Dexp Dcal d(D) h k l
4.3900 4.3923 -.0023 -2 1 0
4.0400 4.0386 .0014 0 1 2
3.3700 3.3712 -.0012 0 -1 2
3.3000 3.2986 .0014 0 2 0
3.1800 3.1773 .0027 -2 2 0
2.9200 2.9248 -.0048 0 2 2
2.7100 2.7115 -.0015 -4 2 2
2.5800 2.5786 .0014 2 0 2
2.5300 2.5312 -.0012 -2 2 4
2.4400 2.4386 .0014 0 2 3
2.3200 2.3194 .0006 2 2 0
2.2700 2.2695 .0005 -4 3 2
A= 11.446 DA= .006
B= 7.634 DB= .001
C= 10.940 DC= .003
GAMMA=118.26 DGAMMA= .02
BETA =124.95 DBETA = .02
ALPHA= 65.75 DALPHA= .01
V=677.6
19. 20-0337
KCoPO4
Rombik
Groupa 32,55
Dexp. Dcal. d(D) h k l
4.8700 4.8580 .0120 2 2 0
4.5200 4.5324 -.0124 3 1 0
3.7000 3.7056 -.0056 0 0 1
3.4900 3.4920 -.0020 4 1 0
3.3000 3.2992 .0008 2 0 1
3.2700 3.2736 -.0036 0 4 0
3.2400 3.2387 .0013 3 3 0
3.2000 3.1993 .0007 2 1 1
3.1500 3.1479 .0021 1 2 1
2.7900 2.7879 .0021 4 3 0
2.6500 2.6505 -.0005 5 2 0
a=14.49 b=13.09 c= 3.706
da= .01 db= .02 dc= .001
V=703.2
20. 20-0338
KCoPO4*H2O
Monoklin
grupa 3
Dexp Dcal d(D) h k l
10.3000 10.2990 .0010 0 1 0
4.1100 4.0945 .0155 2 1 0
3.3100 3.3115 -.0015 0 1 1
2.7800 2.7790 .0010 -2 0 1
2.7400 2.7392 .0008 1 2 1
2.7200 2.7269 -.0069 2 0 1
2.7200 2.7209 -.0009 2 3 0
2.4500 2.4456 .0044 -2 2 1
2.4500 2.4499 .0001 0 3 1
2.3700 2.3708 -.0008 -1 3 1
2.1800 2.1806 -.0006 4 1 0
2.0600 2.0575 .0025 3 2 1
2.0600 2.0598 .0002 0 5 0
a= 8.93 b= 10.299 c= 3.498 beta= 91.11
da=.02 db= .005 dc=.003 dbeta=.01
V= 321.5
Triklin
Dexp Dcal d(D) h k l
10.3000 10.3000 -.0000 1 0 0
4.1100 4.1099 .0001 1 0 1
3.3100 3.3102 -.0002 1 -2 1
2.7800 2.7799 .0001 3 -1 1
2.7400 2.7400 .0000 2 2 0
2.7200 2.7200 .0000 -4 1 0
2.4500 2.4500 .0000 -4 1 1
2.3700 2.3700 -.0000 0 0 2
2.1800 2.1800 .0000 -2 -1 2
2.0600 2.0600 .0000 5 0 0
A= 10.92026 DA= .00003
B= 8.4152 DB= .0003
C= 4.81214 DC= .00008
GAMMA=107.9986 DGAMMA= .0003
BETA = 94.9278 DBETA = .0004
ALPHA= 96.655 DALPHA= .004
V= 414.3
21. 20-1093
Na2Co{SO4}2
Triklin
Dexp Dcal d(D) h k l
7.2200 7.2484 -.0284 0 1 1
6.3500 6.3374 .0126 0 -1 1
5.6800 5.6875 -.0075 1 0 1
4.9100 4.8974 .0126 1 -1 1
4.5000 4.5003 -.0003 -1 0 1
4.3500 4.3539 -.0039 1 2 1
4.2300 4.2421 -.0121 -1 2 0
3.8900 3.8960 -.0060 1 0 2
3.7200 3.7260 -.0060 0 -1 2
3.6300 3.6242 .0058 0 2 2
3.5420 3.5445 -.0025 1 -1 2
3.1700 3.1687 .0013 0 -2 2
A= 6.471 DA= .005
B= 11.90 DB= .01
C= 8.583 DC= .006
GAMMA= 86.64 DGAMMA= .08
BETA = 75.87 DBETA = .03
ALPHA= 81.27 DALPHA= .02
V= 633.2
22. 20-1094
Na2Co{SO4}2
Triklin
Dexp Dcal d(D) h k l
7.4600 7.4540 .0060 1 0 0
6.1200 6.1163 .0037 -1 1 0
5.1400 5.1371 .0029 -1 0 1
4.5400 4.5340 .0060 -1 -1 1
4.4300 4.4301 -.0001 -1 1 1
4.3000 4.3083 -.0083 1 -1 1
3.9400 3.9329 .0071 0 -2 1
3.8100 3.8106 -.0006 1 1 1
3.7200 3.7270 -.0070 2 0 0
3.3300 3.3289 .0011 2 1 0
3.1200 3.1200 .0000 0 0 2
2.8500 2.8480 .0020 0 1 2
A= 7.555 DA= .001
B= 9.276 DB= .008
C= 6.336 DC= .002
GAMMA= 95.36 DGAMMA= .05
BETA = 97.063 DBETA = .005
ALPHA= 96.366 DALPHA= .001
V= 435.4
23. 20-1095
Na2Co{SO4}2*0.5H2O
Rombik
Groupa 54
Dexp. Dcal. d(D) h k l
6.0800 6.0659 .0141 2 1 0
4.4300 4.4254 .0046 2 0 2
3.9100 3.9066 .0034 2 2 1
3.8100 3.8107 -.0007 4 0 0
3.7100 3.7118 -.0018 3 0 2
3.3400 3.3398 .0002 0 3 0
3.1200 3.1203 -.0003 4 0 2
2.8430 2.8456 -.0026 0 3 2
2.8000 2.7972 .0028 1 3 2
2.7190 2.7178 .0012 0 0 4
2.6650 2.6658 -.0008 2 3 2
2.5660 2.5700 -.0040 5 1 2
2.4650 2.4625 .0025 6 1 0
a=15.24 b=10.0194 c=10.871
da= .01 db= .0002 dc= .002
V=1660
Triklin
Dexp Dcal d(D) h k l
6.0800 6.0775 .0025 1 0 0
4.4300 4.4344 -.0044 -1 1 1
3.9100 3.9118 -.0018 -1 -1 1
3.8100 3.8090 .0010 1 -1 1
3.7100 3.7086 .0014 0 -1 2
3.3400 3.3416 -.0016 1 1 1
3.1200 3.1230 -.0031 0 0 3
2.8430 2.8408 .0022 -1 1 3
2.8000 2.8028 -.0028 -2 1 2
2.7190 2.7188 .0002 0 2 1
2.6650 2.6648 .0002 2 0 1
2.5660 2.5655 .0005 2 -1 1
2.4650 2.4644 .0006 -2 1 3
A= 6.444 DA= .001
B= 5.8229 DB= .0007
C= 9.82 DC= .01
GAMMA= 98.524 DGAMMA= .001
BETA =107.37 DBETA = .09
ALPHA= 89.710 DALPHA= .009
V= 347.7
24. 20-1096
Na2Co{SO4}*H2O
Rombik
Groupa 52
Dexp. Dcal. d(D) h k l
6.5800 6.5020 .0780 2 0 0
5.0900 5.0317 .0583 2 1 1
4.7700 4.7600 .0100 1 0 3
4.5900 4.6430 -.0530 0 2 0
4.4000 4.3753 .0247 2 1 2
4.3600 4.3753 -.0153 2 1 2
3.8000 3.7990 .0010 1 2 2
3.4000 3.3898 .0102 2 2 2
3.3200 3.3237 -.0037 1 2 3
3.3000 3.3040 -.0040 2 0 4
3.1000 3.1030 -.0030 3 2 1
3.0600 3.0684 -.0084 4 1 0
a=13.00 b= 9.29 c=15.34
da= .04 db= .03 dc= .01
V=1853
Triklin
Dexp Dcal d(D) h k l
6.5800 6.5769 .0031 0 1 1
5.0900 5.0903 -.0003 -1 1 0
4.7700 4.7688 .0012 0 -1 1
4.5900 4.5971 -.0071 -1 0 2
4.4000 4.4071 -.0071 0 0 2
4.3600 4.3710 -.0110 -2 0 1
3.8000 3.7977 .0023 -2 1 1
3.4000 3.3972 .0028 -1 2 1
3.3200 3.3242 -.0042 1 2 0
3.3000 3.2993 .0007 1 2 1
3.1000 3.1010 -.0010 -1 2 0
3.1000 3.1010 -.0010 -1 2 0
A= 8.8240 DA= .0005
B= 7.341 DB= .0011
C= 9.8526 DC= .0003
GAMMA= 90.779 DGAMMA= .004
BETA =109.253 DBETA = .007
ALPHA= 72.18 DALPHA= .01
V=569.8
25. 20-1591
C8H20ClCoN2S
Triklin
Dexp Dcal d(D) h k l
8.0000 8.0007 -.0007 1 0 0
7.2300 7.2150 .0150 0 -1 1
6.6700 6.6764 -.0064 1 0 1
5.8400 5.8405 -.0005 0 -1 2
4.9900 4.9882 .0018 1 1 0
4.6800 4.6781 .0019 0 1 2
4.4200 4.4211 -.0011 -1 1 2
4.0000 4.0004 -.0004 2 0 0
3.4400 3.4375 .0025 1 -2 2
3.3700 3.3685 .0015 2 -1 2
3.0700 3.0709 -.0009 2 1 1
2.9800 2.9776 .0024 -2 2 0
A= 8.1577 DA= .0009
B= 7.611 DB= .006
C= 14.95 DC= .01
GAMMA= 98.89246 DGAMMA= .00001
BETA = 94.93 DBETA = .03
ALPHA=101.643 DALPHA= .004
V= 891.6
26. 20-1592
C12H30Cl3CoN6O12
Triklin
Dexp Dcal d(D) h k l
10.7000 10.6882 .0118 1 0 0
7.2200 7.1981 .0219 -1 1 0
6.5500 6.5669 -.0169 -1 0 1
6.0700 6.0626 .0074 1 1 0
5.3100 5.3007 .0093 1 -1 1
5.2100 5.1960 .0140 1 0 1
4.5700 4.5712 -.0012 0 1 1
4.1500 4.1523 -.0023 0 2 0
3.7700 3.7736 -.0036 2 0 1
3.5500 3.5496 .0004 -3 0 1
3.0800 3.0839 -.0039 3 1 0
2.6500 2.6503 -.0003 2 -2 2
A= 11.102 DA= .006
B= 8.88 DB= .02
C= 7.44 DC= .02
GAMMA= 95.63 DGAMMA= .09
BETA =102.07 DBETA = .04
ALPHA=108.14 DALPHA= .02602
V=670.5
27. 20-1593
C11H23CoN5S2
Rombik
Groupa 16
Dexp. Dcal. d(D) h k l
7.5700 7.5675 .0025 2 0 0
6.8300 6.8404 -.0104 0 0 1
6.2200 6.2334 -.0134 1 0 1
5.0500 5.0450 .0050 3 0 0
4.0300 4.0287 .0013 1 1 1
3.6500 3.6475 .0025 3 1 0
3.4200 3.4202 -.0002 0 0 2
3.0700 3.0755 -.0055 4 1 0
2.7700 2.7681 .0019 5 0 1
2.6400 2.6398 .0002 0 2 0
a=15.135 b= 5.280 c= 6.840
da= .004 db= .002 dc= .001
V= 546.6
28. 20-1594
C8H20Br2CoNO
Groupa 16
Dexp. Dcal. d(D) h k l
7.9500 7.9573 -.0073 0 1 1
7.0000 7.0775 -.0775 1 0 0
6.3700 6.3592 .0108 1 0 1
5.6600 5.6804 -.0204 1 1 0
4.8400 4.8290 .0110 0 0 3
3.3900 3.3904 -.0004 0 2 3
2.7900 2.7871 .0029 2 2 1
2.6900 2.6892 .0008 1 3 2
2.5300 2.5311 -.0011 2 0 4
2.3800 2.3806 -.0006 0 4 0
a= 7.078 b= 9.522 c=14.487
da= .005 db= .003 dc= .002
V= 976.4
29. 20-1595
C8H20Cl2CoN2O
Groupa 19
Dexp. Dcal. d(D) h k l
6.8700 6.8237 .0463 0 0 2
6.1900 6.2485 -.0585 1 0 1
4.9300 4.9244 .0056 0 1 2
3.5200 3.5142 .0058 2 0 0
3.3600 3.3648 -.0048 1 1 3
3.1500 3.1508 -.0008 2 1 0
2.8600 2.8605 -.0005 2 1 2
2.7300 2.7295 .0005 0 0 5
2.5000 2.4999 .0001 2 2 0
2.2400 2.2399 .0001 0 3 2
a= 7.0285 b= 7.114 c=13.647
da= .0005 db= .004 dc= .001
V= 682.4
30. 20-1597
C10H18CoIN10Ni
Triklin
Dexp Dcal d(D) h k l
7.7200 7.7145 .0055 1 0 0
6.8800 6.8864 -.0064 0 1 0
6.4300 6.4463 -.0163 0 1 1
4.4000 4.4043 -.0043 -1 0 1
4.2400 4.2359 .0041 0 -1 1
3.7400 3.7400 .0000 0 2 1
3.5600 3.5599 .0001 1 2 1
3.3000 3.3014 -.0014 -1 -1 1
3.0200 3.0199 .0001 1 -1 2
2.8600 2.8604 -.0004 3 0 1
2.7300 2.7299 .0001 1 2 3
2.5200 2.5199 .0001 -2 2 1
2.3000 2.2997 .0003 -2 1 2
1.9800 1.9799 .0001 3 3 2
A= 8.684 DA= .001
B= 7.552 DB= .006
C= 8.910 DC= .007
GAMMA= 83.62 DGAMMA= .03
BETA = 63.10 DBETA = .02
ALPHA= 66.26 DALPHA= .05
V= 475.2
31. 20-1598
C22H42Br4Co2N6O6
Rombik
Groupa 33,49,62
romb.
Dexp. Dcal. d(D) h k l
8.2600 8.2249 .0351 0 1 1
7.0000 7.0060 -.0060 1 1 0
6.3200 6.3492 -.0292 0 0 2
6.1200 6.1343 -.0143 1 1 1
4.6500 4.6567 -.0067 1 2 0
4.3200 4.3286 -.0086 2 0 1
4.0300 4.0177 .0123 2 1 1
3.7600 3.7550 .0050 1 2 2
3.5000 3.5030 -.0030 2 2 0
a= 9.208687 b=10.795480 c=12.698380
da= .009786 db= .023798 dc= .026418
V=1262
32. 20-1599
C24H42Cl4Co2N6O6
Triklin
Dexp Dcal d(D) h k l
8.1200 8.1418 -.0218 1 0 0
7.0000 7.0241 -.0241 1 1 0
6.4600 6.4629 -.0029 0 1 1
6.1200 6.1169 .0031 -1 0 1
4.6500 4.6555 -.0055 -1 1 1
4.5000 4.4929 .0071 -1 1 0
4.4300 4.4329 -.0029 2 1 0
4.0300 4.0261 .0039 1 2 1
3.9400 3.9387 .0013 -2 0 1
3.8800 3.8810 -.0010 0 1 2
3.7800 3.7784 .0016 -2 -1 1
3.5500 3.5517 -.0017 0 2 0
A= 9.01 DA= .01
B= 8.308 DB= .005
C= 7.849 DC= .007
GAMMA= 67.95 DGAMMA= .06
BETA = 94.0 DBETA = .1
ALPHA= 70.69 DALPHA= .09
V= 501.0
33. 20-1600
C30H54Cl2CoN6O14
Triklin
Dexp Dcal d(D) h k l
9.1000 9.1386 -.0386 -1 1 0
7.6700 7.6515 .0185 1 1 0
6.2000 6.1954 .0046 0 1 1
5.3000 5.3038 -.0038 0 -1 1
4.7800 4.7802 -.0002 -2 1 1
4.2800 4.2772 .0028 -1 3 0
3.7800 3.7802 -.0002 1 3 0
2.5800 2.5800 -.0000 2 4 0
3.2600 3.2605 -.0005 -1 4 1
3.0800 3.0800 .0000 -2 2 2
A= 11.31645 DA= .00402
B= 13.53890 DB= .00001
C= 6.66333 DC= .00088
GAMMA=103.02770 DGAMMA= .00873
BETA =103.81630 DBETA = .00214
ALPHA= 76.22549 DALPHA= .00131
V=946.9
34. 20-1601
C15H11Br2CoN3
Triklin
Dexp Dcal d(D) h k l
7.3700 7.3749 -.0049 1 0 0
7.1100 7.1083 .0017 0 1 1
6.7500 6.7346 .0154 0 -1 1
6.2900 6.3017 -.0117 1 0 1
5.7400 5.7387 .0013 -1 0 1
5.1600 5.1607 -.0007 0 0 2
4.4300 4.4389 -.0089 1 0 2
4.1500 4.1603 -.0103 0 -2 1
4.0400 4.0450 -.0050 -1 0 2
3.4900 3.4900 -.0000 -2 -1 1
3.2600 3.2587 .0013 1 3 0
3.2000 3.2013 -.0013 1 3 1
A= 7.845 DA= .005
B= 9.87 DB= .01
C= 10.42 DC= .01
GAMMA= 70.85 DGAMMA= .02
BETA = 82.96 DBETA = .05
ALPHA= 84.78 DALPHA= .09
V= 755.1
35. 20-1602
C15H11Cl2CoN3
Triklin
Dexp Dcal d(D) h k l
10.8000 10.7969 .0031 1 0 0
9.2900 9.2808 .0092 -1 1 0
7.9800 7.9771 .0029 0 -1 1
7.3400 7.3472 -.0072 1 1 0
6.7300 6.7289 .0011 -1 -1 1
6.1900 6.2069 -.0169 0 2 0
4.4600 4.4547 .0053 0 -1 2
4.2700 4.2704 -.0004 -2 2 1
4.0600 4.0613 -.0013 0 -3 1
3.8200 3.8209 -.0009 -2 -2 1
3.6800 3.6782 .0018 -1 -3 1
3.5100 3.5095 .0005 -1 2 2
A= 11.4252 DA= .0004
B= 12.89 DB= .01
C= 9.299 DC= .001
GAMMA=100.96 DGAMMA= .03
BETA =103.7317 DBETA = .0008
ALPHA= 97.973 DALPHA= .005
V= 1281.2
36. 20-1603
C15H11CoI2N3
Triklin
Dexp Dcal d(D) h k l
7.7100 7.7116 -.0016 1 0 0
7.2500 7.2424 .0076 -1 1 0
6.7200 6.7187 .0013 0 0 1
4.8100 4.8288 -.0188 -1 2 1
4.5000 4.5013 -.0013 1 0 1
4.1500 4.1557 -.0057 -2 1 1
3.5400 3.5301 .0099 -1 3 1
3.4400 3.4370 .0030 -1 0 2
3.3200 3.3218 -.0018 0 3 0
3.2500 3.2473 .0027 -1 -2 1
3.1200 3.1211 -.0011 -2 2 2
3.0400 3.0398 .0002 0 2 2
A= 8.6032 DA= .0001
B= 10.87 DB= .01
C= 7.2586 DC= .0009
GAMMA=111.467 DGAMMA= .008
BETA =109.99 DBETA = .01
ALPHA= 73.97 DALPHA= .06
V= 584.8
37. 20-1604
C6H18CoHgI5N6
Triklin
Dexp Dcal d(D) h k l
7.3400 7.3440 -.0040 1 0 0
6.6300 6.6288 .0012 -1 1 0
6.0000 6.0037 -.0037 -1 0 1
5.3500 5.3514 -.0014 1 -1 1
4.8300 4.8278 .0022 -1 -1 1
4.4900 4.4896 .0004 -1 2 0
4.2400 4.2392 .0008 1 1 1
4.0300 4.0301 -.0001 -1 0 2
3.5800 3.5801 -.0001 1 2 0
A= 7.595 DA= .009
B= 9.76 DB= .01
C= 9.123 DC= .009
GAMMA=103.56 DGAMMA= .09
BETA = 94.13 DBETA = .06
ALPHA= 96.7 DALPHA= .1
V= 649.6
38. 21-0021
{NH42CoCl4*2H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.5000 5.5002 -.0002 0 1 1
3.9800 3.9830 -.0030 -1 0 1
3.2000 3.1995 .0005 0 0 2
3.1200 3.1227 -.0027 1 3 0
2.7500 2.7501 -.0001 0 2 2
2.6900 2.6905 -.0005 0 4 0
2.5700 2.5706 -.0006 -2 0 1
2.5100 2.5102 -.0002 -1 1 2
2.4000 2.3998 .0002 1 4 1
2.2300 2.2295 .0005 -1 4 1
2.0900 2.0895 .0005 -2 3 1
2.0400 2.0401 -.0001 0 5 1
a=6.607 b=10.762 c= 6.6646 beta= 73.76
da=.007 db=.002 dc=.0004 dbeta=.02
V= 455.0
Triklin
Dexp Dcal d(D) h k l
5.5000 5.4999 .0001 -1 0 1
3.9800 3.9792 .0008 -1 -1 1
3.2000 3.1996 .0004 1 -2 1
3.1200 3.1195 .0005 -2 2 0
2.7500 2.7499 .0001 -2 0 2
2.6900 2.6895 .0005 -1 -2 1
2.5700 2.5708 -.0008 3 1 0
2.5100 2.5101 -.0001 0 -2 2
2.4000 2.3996 .0004 -4 1 0
2.2300 2.2301 -.0001 1 -3 1
2.0900 2.0894 .0006 -2 0 3
2.0400 2.0396 .0004 4 1 0
A= 9.73 DA= .01
B= 6.912 DB= .001
C= 7.5399 DC= .0005
GAMMA=105.27 DGAMMA= .01
BETA = 82.26 DBETA = .07
ALPHA= 93.045 DALPHA= .006
V= 484.6
39. 21-0138
Ca3Co2O6
Rombik
Groupa 17
Dexp. Dcal. d(D) h k l
4.5400 4.5370 .0030 0 0 1
4.3300 4.3330 -.0030 2 1 0
3.1300 3.1339 -.0039 2 2 0
2.7530 2.7524 .0006 3 0 1
2.6200 2.6201 -.0001 0 3 0
2.4680 2.4656 .0024 4 1 0
2.1650 2.1665 -.0015 4 2 0
2.1330 2.1331 -.0001 1 1 2
2.0090 2.0084 .0006 5 1 0
1.9540 1.9550 -.0010 4 2 1
1.8980 1.8977 .0003 3 3 1
1.7770 1.7766 .0004 1 4 1
a=10.387 b= 7.860 c= 4.537
da= .001 db= .003 dc= .001
V= 370.4
Triklin
Dexp Dcal d(D) h k l
4.5400 4.5379 .0021 0 1 1
4.3300 4.3243 .0057 0 -1 1
3.1300 3.1303 -.0003 1 1 1
2.7530 2.7529 .0001 1 1 2
2.6200 2.6185 .0015 -1 1 0
2.4680 2.4687 -.0007 0 2 1
2.1650 2.1621 .0029 0 -2 2
2.1330 2.1327 .0003 1 2 2
2.0090 2.0089 .0001 0 2 3
1.9540 1.9540 .0000 1 1 4
1.8980 1.8990 -.0010 0 -2 3
1.7770 1.7775 -.0005 -1 -2 3
A= 3.602 DA= .003
B= 5.184 DB= .004
C= 9.279 DC= .001
GAMMA= 76.98 DGAMMA= .07
BETA = 86.66 DBETA = .02
ALPHA= 86.06 DALPHA= .03
V= 168.25
40. 21-0139
Ca9Co12O28
Triklin
Dexp Dcal d(D) h k l
10.7000 10.7029 -.0029 1 0 0
5.3700 5.3702 -.0002 0 1 1
3.5800 3.5787 .0013 -2 -1 1
3.0700 3.0688 .0012 -3 1 3
2.9400 2.9395 .0005 -3 -1 1
2.6830 2.6830 -.0000 -4 1 1
2.5520 2.5530 -.0010 -2 -1 3
2.4690 2.4685 .0005 -3 2 2
2.4310 2.4314 -.0004 0 0 4
2.4070 2.4070 -.0000 -1 -2 1
2.3340 2.3339 .0001 3 1 2
2.2760 2.2765 -.0005 -5 1 2
2.1440 2.1449 -.0009 -1 -2 2
A= 11.7637 DA= .0009
B= 5.6784 DB= .0004
C= 11.088 DC= .001
GAMMA= 99.42 DGAMMA= .01
BETA =114.419 DBETA = .004
ALPHA= 72.007 DALPHA= .004
V= 640.9
41. 21-0252
{Co{NH3}4Cl2}BrO3
Triklin
Dexp Dcal d(D) h k l
5.4800 5.4939 -.0139 0 1 1
4.7700 4.7758 -.0058 0 -1 1
4.4100 4.4042 .0058 1 0 0
4.2500 4.2491 .0009 1 0 1
4.0300 4.0172 .0128 1 -1 1
3.8500 3.8626 -.0126 1 1 1
3.7200 3.7211 -.0011 -1 2 0
3.1000 3.1044 -.0044 1 2 0
2.9100 2.9114 -.0014 1 0 2
2.7000 2.6984 .0016 0 -1 2
2.6300 2.6265 .0035 1 3 1
2.5500 2.5507 -.0007 0 4 1
2.1900 2.1904 -.0004 1 -3 2
A= 4.707 DA= .009
B= 10.7228 DB= .0002
C= 6.216 DC= .004
GAMMA= 97.92 DGAMMA= .06
BETA = 72.09 DBETA = .02
ALPHA= 83.58 DALPHA= .03
V= 291.7
42. 21-0253
{Co{NH3}4Cl2}IO3*2H2O
Monoklin
GRUPA 3
Dexp. Dcal. d(D) h k l
8.4200 8.4335 -.0135 0 1 0
5.7400 5.7527 -.0127 -1 0 2
5.4800 5.5311 -.0511 1 1 1
4.9500 4.9549 -.0049 0 1 2
4.7600 4.7523 .0077 -1 1 2
4.3900 4.3963 -.0063 -2 1 1
4.2200 4.2167 .0033 0 2 0
4.0700 4.0821 -.0121 0 0 3
3.8000 3.7998 .0002 -1 2 1
3.6700 3.6743 -.0043 0 1 3
3.1900 3.1997 -.0097 1 2 2
2.9300 2.9329 -.0029 0 2 3
a= 10.62 b= 8.43345 c= 12.4484 beta= 100.3
da=.04 db=.00008 dc=.0007 dbet=.2
V=1080
Triklin
Dexp Dcal d(D) h k l
8.4200 8.4025 .0175 0 0 1
5.7400 5.7274 .0126 0 -2 1
5.4800 5.4884 -.0084 1 0 0
4.9500 4.9561 -.0061 -1 1 0
4.7600 4.7630 -.0030 1 2 0
4.3900 4.4023 -.0123 0 -3 1
4.2200 4.2189 .0011 -1 0 1
4.0700 4.0817 -.0117 0 -1 2
3.8000 3.8002 -.0002 1 3 1
3.6700 3.6690 .0010 1 1 2
3.1900 3.1883 .0017 0 3 2
2.9300 2.9301 -.0001 -1 -2 2
A= 5.654 DA= .001
B= 15.355 DB= .006
C= 8.582 DC= .003
GAMMA= 82.53 DGAMMA= .01
BETA = 78.398 DBETA = .007
ALPHA= 90.20 DALPHA= .02
V= 723.2
43. 21-0254
Co{BF4}2*6H2O
Triklin
Dexp Dcal d(D) h k l
5.0400 5.0411 -.0011 0 1 1
4.2300 4.2293 .0007 1 0 1
3.9000 3.8964 .0036 0 -1 1
3.4400 3.4396 .0004 -1 0 1
3.1200 3.1210 -.0010 0 2 0
2.8400 2.8396 .0004 -1 2 1
2.6600 2.6558 .0042 -1 -1 1
2.5200 2.5206 -.0006 0 2 2
2.4100 2.4153 -.0053 2 0 1
2.2800 2.2784 .0016 -1 2 2
2.1900 2.1890 .0010 1 2 2
A= 5.058 DA= .006
B= 6.6357 DB= .0002
C= 6.368 DC= .004
GAMMA=103.58 DGAMMA= .02
BETA = 81.34 DBETA = .08
ALPHA= 78.06 DALPHA= .01
V= 198.7
44. 21-0256
CuCoO2
Triklin
Dexp Dcal d(D) h k l
5.5300 5.5299 .0001 1 0 0
2.8010 2.7999 .0011 0 2 0
2.5860 2.5890 -.0030 0 -2 2
2.4200 2.4193 .0007 1 2 2
2.3870 2.3867 .0003 2 1 2
2.3500 2.3482 .0018 0 -2 3
2.2500 2.2497 .0003 2 2 0
2.1300 2.1306 -.0006 -1 2 2
2.0680 2.0657 .0023 -2 -2 3
1.9890 1.9883 .0007 1 -2 3
1.8610 1.8613 -.0003 -3 -1 2
1.6630 1.6629 .0001 -1 0 7
A= 5.7240 DA= .0006
B= 5.7807 DB= .0006
C= 11.944 DC= .002
GAMMA= 76.0023 DGAMMA= .0002
BETA = 96.30 DBETA = .01
ALPHA= 94.67 DALPHA= .01
V=380.4
45. 21-0266
Co{NO3}2*8H2O
Triklin
Dexp Dcal d(D) h k l
7.5200 7.5187 .0013 1 0 0
6.1600 6.2007 -.0407 0 1 0
6.0600 6.0557 .0043 0 -1 1
5.9000 5.9033 -.0033 1 1 0
5.7400 5.7338 .0062 -1 -1 1
5.4400 5.4321 .0079 1 0 1
5.3500 5.3597 -.0097 -1 0 1
4.1600 4.1497 .0103 0 1 1
4.1000 4.0996 .0004 1 -1 1
4.0700 4.0724 -.0024 1 1 1
3.9100 3.9085 .0015 -1 -1 2
3.8700 3.8703 -.0003 2 1 0
A= 8.09770 DA= .00006
B= 7.1874 DB= .0009
C= 8.4137 DC= .0008
GAMMA= 68.22 DGAMMA= .01
BETA = 97.66 DBETA = .01
ALPHA=112.96 DALPHA= .01
V=419.0
46. 21-0492
Li1.2Co3As2
Rombik
Groupa 34,58
Dexp. Dcal. d(D) h k l
8.0000 7.9967 .0033 1 1 0
6.1100 6.1184 -.0084 2 0 0
4.8500 4.8498 .0002 1 2 0
4.0000 3.9984 .0016 2 2 0
3.8000 3.8052 -.0051 3 1 0
3.4600 3.4585 .0015 0 1 1
3.3300 3.3281 .0019 1 1 1
3.0500 3.0521 -.0021 2 3 0
2.7180 2.7242 -.0062 3 0 1
2.6370 2.6379 -.0009 3 1 1
2.4240 2.4249 -.0009 2 4 0
2.3460 2.3441 .0019 2 3 1
2.2910 2.2914 -.0004 4 1 1
a=12.24 b=10.565 c= 3.660
da= .01 db= .004 dc= .001
V= 473.2
47. 21-0862
{CoNH3}6}Cl3
Triklin
Dexp Dcal d(D) h k l
5.8800 5.8820 -.0020 0 1 1
5.2700 5.2623 .0077 -1 1 0
4.9600 4.9569 .0031 0 -1 1
3.6400 3.6470 -.0070 1 1 0
3.5600 3.5537 .0063 -1 2 0
3.4600 3.4611 -.0011 0 2 0
3.1400 3.1407 -.0007 1 -2 1
3.0300 3.0261 .0039 0 -2 1
2.6170 2.6173 -.0003 2 0 1
2.5450 2.5451 -.0001 -1 1 3
2.5450 2.5451 -.0001 -1 1 3
2.4700 2.4698 .0002 0 -1 3
A= 5.7549 DA= .0007
B= 7.5182 DB= .0008
C= 8.60365 DC= .00009
GAMMA=110.813 DGAMMA= .004
BETA = 88.916 DBETA = .003
ALPHA= 81.10 DALPHA= .01
V=342.9
48. 21-864
C20H30B4CoO22
Triklin
Dexp Dcal d(D) h k l
11.0000 11.0055 -.0055 0 0 1
9.4000 9.4194 -.0194 1 0 0
8.7000 8.6622 .0378 0 1 1
7.5000 7.4770 .0230 0 -1 1
5.3000 5.3025 -.0025 1 0 2
3.9000 3.8989 .0011 -2 2 0
3.5000 3.4999 .0001 1 -3 1
3.4200 3.4198 .0002 0 3 2
3.2300 3.2292 .0008 -1 -2 2
3.1400 3.1398 .0002 3 0 0
3.0400 3.0401 -.0001 3 1 1
2.3300 2.3302 -.0002 1 -5 0
1.9300 1.9301 -.0001 -2 -2 4
A= 9.709 DA= .002
B= 11.838 DB= .001
C= 11.385 DC= .007
GAMMA= 95.15 DGAMMA= .03
BETA = 77.73 DBETA = .03
ALPHA= 82.92 DALPHA= .01
V= 1260
49. 21-0870
CoMo2S4
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.7100 5.6962 .0138 -1 0 1
5.1300 5.1300 -.0000 1 1 0
2.9300 2.9287 .0013 1 1 2
2.8500 2.8481 .0019 -2 0 2
2.5700 2.5692 .0008 -1 1 3
2.1000 2.1008 -.0008 0 4 0
2.0400 2.0405 -.0005 -2 2 3
2.0100 2.0102 -.0002 2 2 2
1.9100 1.9094 .0006 1 4 1
1.6800 1.6802 -.0002 2 4 1
1.6270 1.6268 .0002 1 5 0
1.5900 1.5900 -.0000 4 1 0
a= 6.640 b= 8.403 c= 8.25 beta= 102.71
da=.003 db=.002 dc=.01 dbeta=.05
V= 449.2
Triklin
Dexp Dcal d(D) h k l
5.7100 5.7035 .0065 0 0 1
5.1300 5.1321 -.0021 1 1 0
2.9300 2.9318 -.0018 0 -2 1
2.8500 2.8488 .0012 0 2 0
2.5700 2.5716 -.0016 2 0 1
2.1000 2.1006 -.0006 2 1 2
2.0400 2.0395 .0005 1 -2 2
2.0100 2.0105 -.0005 -2 -3 1
1.9100 1.9103 -.0003 1 0 3
1.6800 1.6801 -.0001 3 1 2
1.6270 1.6263 .0007 2 -1 3
1.5900 1.5896 .0004 3 2 2
A= 5.827 DA= .003
B= 6.5485 DB= .0005
C= 6.005 DC= .002
GAMMA= 66.04 DGAMMA= .04
BETA = 85.92 DBETA = .03
ALPHA=104.46 DALPHA= .09
V= 198.9
50. 21-1289
C8H8CoK3N2O8
Rombik
Groupa 31,59
Dexp. Dcal. d(D) h k l
9.7100 9.7017 .0083 1 0 0
3.7900 3.7922 -.0022 1 1 0
3.3400 3.3406 -.0006 0 0 2
3.3000 3.2980 .0020 1 1 1
2.2800 2.2798 .0002 4 0 1
2.0900 2.0901 -.0001 4 1 0
2.0600 2.0600 .0000 0 2 0
a= 9.7017 b= 4.120001 c= 6.68128
da= .0003 db= .000001 dc= .00002
V=267.06
51. 21-1570
C6H16Cl3CoN4
Rombik
Groupa 56
Dexp. Dcal. d(D) h k l
6.2900 6.2781 .0119 1 1 0
5.8700 5.8798 -.0098 0 1 2
4.9800 4.9802 -.0002 1 0 2
4.4800 4.4770 .0030 0 2 2
4.3900 4.3928 -.0028 1 2 1
3.0700 3.0696 .0004 1 0 4
2.4900 2.4901 -.0001 2 0 4
a= 7.376 b=11.96 c=13.504
da= .001 db= .01 dc= .003
V=1191
52. 21-1571
C6H30Cl4CoN4
Rombik
Groupa 30,53
Dexp. Dcal. d(D) h k l
9.8900 9.8991 -.0091 1 0 0
5.7500 5.7477 .0023 0 1 1
5.5900 5.6175 -.0275 0 2 0
4.9800 4.9706 .0094 1 1 1
4.5300 4.5295 .0005 2 1 0
3.9400 3.9454 -.0054 1 2 1
2.8100 2.8088 .0012 0 4 0
a= 9.8991 b=11.235 c= 6.69
da= .0001 db= .004 dc= .05
V= 744
53. 21-1572
C20H20Cl2CoN4O8
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
8.2900 8.2583 .0317 2 0 0
7.4300 7.3995 .0305 1 1 0
7.1100 7.0962 .0138 0 0 1
5.8500 5.8459 .0041 2 1 0
5.4000 5.3872 .0128 0 1 1
4.5900 4.5840 .0060 3 1 0
4.3400 4.3499 -.0099 3 0 1
4.1300 4.1292 .0008 4 0 0
4.0100 4.0142 -.0042 1 2 0
3.7000 3.6997 .0003 2 2 0
a=16.52 b= 8.28 c= 7.10
da= .01 db= .02 dc= .02
V= 970
Triklin
Dexp Dcal d(D) h k l p
8.2900 8.2639 .0261 1 0 0 0
7.4300 7.4455 -.0156 0 1 0 0
7.1100 7.1214 -.0114 0 0 1 0
5.8500 5.8619 -.0119 -1 -1 1 0
5.4000 5.3959 .0041 0 -1 1 0
4.5900 4.5887 .0013 1 0 1 0
4.3400 4.3378 .0022 -2 -1 1 0
4.1300 4.1319 -.0019 2 0 0 0
4.0100 4.0100 -.0000 1 1 1 0
3.7000 3.6999 .0001 -1 -2 1 0
A= 9.290 DA= .003
B= 7.752 DB= .005
C= 7.863 DC= .002
GAMMA= 74.68 DGAMMA= .05
BETA =114.59 DBETA = .09
ALPHA=100.92 DALPHA= .04
V= 495
54. 21-1573
C3H3CoO4*2H2O
Triklin
Dexp Dcal d(D) h k l
6.1500 6.1525 -.0025 0 1 1
5.8500 5.8561 -.0061 0 -1 1
5.5600 5.5642 -.0042 -1 0 1
5.2000 5.2007 -.0007 1 -1 1
3.8900 3.8886 .0014 0 -1 2
3.7100 3.7059 .0041 0 2 1
3.6600 3.6565 .0035 2 0 1
3.3800 3.3839 -.0039 -2 0 1
3.2700 3.2670 .0030 1 2 0
3.2000 3.1973 .0027 2 1 0
3.1300 3.1304 -.0004 2 1 1
3.0600 3.0599 .0001 0 0 3
A= 7.787 DA= .009
B= 8.078 DB= .004
C= 9.239 DC= .003
GAMMA=100.80 DGAMMA= .06
BETA = 84.16 DBETA = .06
ALPHA= 88.31 DALPHA= .02
V= 567.2
55. 21-1574
C4H16CoN10O10
Triklin
Dexp Dcal d(D) h k l
9.3100 9.3077 .0023 0 1 1
8.6900 8.6910 -.0010 1 1 0
8.0400 8.0315 .0085 0 -1 1
7.5000 7.5023 -.0023 -1 1 1
7.2200 7.2103 .0097 1 -1 1
6.9300 6.9201 .0099 -1 2 0
6.5700 6.6055 -.0355 0 2 1
6.2600 6.2579 .0021 -1 -1 1
5.5300 5.5328 -.0028 1 -2 1
5.0500 5.0576 -.0076 -2 0 1
4.9700 4.9757 -.0057 2 1 1
4.8300 4.8350 -.0050 -1 -2 1
A= 12.2535 DA= .0002
B= 15.37611 DB= .00006
C= 10.6448 DC= .0008
GAMMA= 99.34258 DGAMMA= .0006
BETA = 86.941 DBETA = .001
ALPHA= 81.679 DALPHA= .002
V=1952
56. 21-1575
CH4CoN4O7
Triklin
Dexp Dcal d(D) h k l
9.1800 9.2220 -.0420 1 0 1
8.7000 8.7100 -.0100 0 1 1
8.3400 8.3400 -.0000 0 -1 1
7.7900 7.8141 -.0241 -1 0 1
7.4000 7.3829 .0171 1 1 1
6.9300 6.9421 -.0121 1 0 2
6.6100 6.5739 .0361 -1 1 0
6.4600 6.4705 -.0105 0 1 2
6.1400 6.1153 .0247 1 1 2
5.8000 5.7747 .0253 -1 0 2
5.3600 5.3618 -.0018 1 -1 2
4.9800 4.9782 .0018 2 0 1
A= 10.1429 DA= .0003
B= 10.1218 DB= .0001
C= 16.62900 DC= .00007
GAMMA= 81.323 DGAMMA= .001
BETA = 78.8042 DBETA = .0005
ALPHA= 85.618 DALPHA= .001
V=1653
57. 21-1576
C12H12CoN2S2
Triklin
Dexp Dcal d(D) h k l
5.4800 5.4817 -.0017 0 1 1
5.3100 5.3095 .0005 1 0 0
4.6300 4.6371 -.0071 1 1 1
4.5000 4.5007 -.0007 1 1 0
3.8200 3.8176 .0024 1 2 1
3.5400 3.5481 -.0081 0 3 1
3.0400 3.0422 -.0022 1 0 2
2.8400 2.8387 .0013 1 2 2
2.6200 2.6192 .0008 -2 2 0
2.5600 2.5596 .0004 -1 -2 1
2.3000 2.3005 -.0005 -1 5 0
2.2200 2.2199 .0001 -1 -3 1
A= 5.9035 DA= .0005
B= 11.965 DB= .005
C= 6.188 DC= .001
GAMMA= 97.05 DGAMMA= .03
BETA = 66.605 DBETA = .004
ALPHA= 81.60 DALPHA= .02
V= 388.86
58. 21-1577
C84h60CoN6P3S6
Triklin
Dexp Dcal d(D) h k l
11.8000 11.6102 .1898 0 0 1
10.9000 10.9106 -.0106 0 1 0
10.1000 10.1053 -.0053 -1 0 1
9.3500 9.3772 -.0272 1 0 1
7.8900 7.8828 .0072 -1 1 1
7.3600 7.3531 .0069 -2 0 1
7.0100 7.0198 -.0098 -1 -1 1
6.4900 6.4712 .0188 1 1 1
6.0600 6.0563 .0037 2 1 0
5.7000 5.7204 -.0204 -1 2 0
5.4400 5.4357 .0043 2 -2 0
5.1800 5.1802 -.0002 2 1 1
A= 18.6824 DA= .0001
B= 11.4507 DB= .0001
C= 11.65880 DC= .00001
GAMMA=107.3088 DGAMMA= .0002
BETA = 93.7657 DBETA = .0002
ALPHA= 92.3589 DALPHA= .0001
V=2374
59. 21-1580
C6H24CoN12O10S
Triklin
Dexp Dcal d(D) h k l
10.8000 10.8288 -.0288 0 1 1
9.9200 9.9297 -.0097 0 -1 1
8.6600 8.6532 .0068 1 0 0
7.9800 7.9963 -.0163 0 2 0
7.6400 7.6428 -.0028 -1 1 1
7.2100 7.1703 .0397 0 2 1
6.9700 6.9855 -.0155 1 0 1
6.7300 6.7178 .0122 1 -1 1
6.4500 6.4555 -.0055 0 1 2
6.3200 6.3257 -.0057 -1 2 1
6.1200 6.1261 -.0061 1 1 1
5.4100 5.4144 -.0044 0 2 2
A= 8.91963 DA= .00001
B= 16.46479 DB= .00004
C= 13.73225 DC= .00003
GAMMA=102.82740 DGAMMA= .00001
BETA = 97.03247 DBETA = .00008
ALPHA= 83.57929 DALPHA= .00001
V=1944
60. 21-1581
C2H8CoN4O6S*6H2O
Triklin
Dexp Dcal d(D) h k l
9.2400 9.2388 .0012 0 1 1
7.4200 7.4203 -.0003 0 -1 1
7.2100 7.2411 -.0311 -1 -1 1
6.7500 6.7501 -.0001 1 0 1
6.3100 6.3224 -.0124 -1 1 1
5.9900 5.9783 .0117 0 2 1
5.4400 5.4416 -.0016 0 0 2
5.1400 5.1393 .0007 1 -1 1
4.9700 4.9634 .0066 -2 -1 1
4.7500 4.7495 .0005 1 1 2
4.6200 4.6194 .0006 0 2 2
4.2200 4.2235 -.0035 2 0 1
A= 10.695 DA= .001
B= 13.5974 DB= .0001
C= 11.2050 DC= .0002
GAMMA= 69.215 DGAMMA= .007
BETA = 95.67 DBETA = .01
ALPHA= 80.37 DALPHA= .01
V=1478
61. 21-1582
C4H16CoN10O6S4
Triklin
Dexp Dcal d(D) h k l
7.2300 7.2358 -.0058 0 1 1
6.4900 6.4883 .0017 -1 1 0
6.1000 6.0788 .0212 0 -1 1
5.6000 5.5885 .0115 1 -1 1
4.9100 4.9109 -.0009 0 2 0
4.8200 4.8235 -.0035 1 2 0
4.5000 4.5017 -.0017 2 1 2
4.2700 4.2696 .0004 2 0 2
4.0500 4.0471 .0029 1 2 2
3.9000 3.9010 -.0010 1 -1 2
3.7200 3.7192 .0008 3 0 1
3.6000 3.6003 -.0003 -1 0 2
3.5100 3.5115 -.0015 2 -1 2
3.4600 3.4604 -.0004 -1 1 2
3.2600 3.2605 -.0005 0 3 1
A= 11.672 DA= .005
B= 10.433 DB= .005
C= 10.00 DC= .01
GAMMA= 72.93 DGAMMA= .03
BETA = 64.22 DBETA = .05
ALPHA= 73.93 DALPHA= .05
V= 1032.3
62. 21-1583
C4H16CoN10O6S4
Triklin
Dexp Dcal d(D) h k l
11.1000 11.0771 .0229 1 0 0
6.4500 6.4500 .0000 0 1 1
5.7100 5.7100 -.0000 0 -1 1
4.7900 4.7888 .0012 2 2 1
4.4400 4.4370 .0030 0 2 1
4.0800 4.0788 .0012 3 1 0
3.9400 3.9387 .0013 3 2 1
3.5900 3.5915 -.0015 3 0 1
3.5300 3.5313 -.0013 2 2 2
3.2200 3.2194 .0006 3 1 2
3.1000 3.1004 -.0004 -3 -2 1
3.0400 3.0405 -.0005 2 3 2
2.9600 2.9600 -.0000 3 -1 1
2.6100 2.6098 .0002 2 1 3
2.4300 2.4300 .0000 -2 3 0
A= 12.721 DA= .007
B= 11.3634 DB= .0001
C= 7.944 DC= .004
GAMMA= 62.37 DGAMMA= .01
BETA = 74.57 DBETA = .04
ALPHA= 76.66 DALPHA= .04
V= 972.9
63. 21-1584
C4H16CoN10O6S4
Triklin
Dexp Dcal d(D) h k l
8.7500 8.7377 .0123 0 1 1
8.5800 8.5769 .0031 0 -1 1
6.4800 6.4905 -.0105 1 1 0
5.1300 5.1328 -.0028 -1 1 1
5.0100 5.0095 .0005 1 1 2
4.0900 4.0926 -.0026 -1 0 2
4.0500 4.0491 .0009 1 -2 2
3.9000 3.8995 .0005 -1 1 2
3.7200 3.7209 -.0009 2 1 1
3.4500 3.4495 .0005 -1 -2 2
3.3900 3.3900 .0000 -1 3 1
3.2600 3.2605 -.0005 2 -2 1
3.2000 3.1996 .0004 -2 -1 1
2.9200 2.9204 -.0004 -1 4 0
2.5900 2.5896 .0004 -2 3 1
A= 7.718 DA= .001
B= 12.8379 DB= .0005
C= 12.190 DC= .002
GAMMA= 88.348 DGAMMA= .001
BETA = 74.21 DBETA = .01
ALPHA= 88.527 DALPHA= .004
V= 1161.4
64. 21-1586
C12H30Cl2CoN2
Triklin
Dexp Dcal d(D) h k l
8.5000 8.5130 -.0130 0 0 1
6.1300 6.1258 .0042 1 0 0
5.8000 5.8037 -.0037 -1 0 1
5.2700 5.2691 .0009 1 1 0
5.2300 5.2326 -.0026 -1 2 0
4.4800 4.4822 -.0022 1 -1 1
4.1900 4.1971 -.0071 0 -1 2
4.0000 4.0105 -.0105 1 1 1
3.8400 3.8382 .0018 0 -2 2
3.6100 3.6134 -.0034 -1 2 2
3.4400 3.4392 .0008 -1 4 0
3.3600 3.3609 -.0009 0 -3 2
A= 6.49382 DA= .00009
B= 14.8064 DB= .0002
C= 8.8777 DC= .0001
GAMMA=100.6518 DGAMMA= .0009
BETA =105.5133 DBETA = .0001
ALPHA= 92.521 DALPHA= .001
V=804.4
65. 21-1587
C12H30CoN4O12
Triklin
Dexp Dcal d(D) h k l
7.9700 7.9807 -.0107 1 0 0
7.2400 7.2527 -.0127 0 1 0
5.5700 5.5813 -.0113 0 0 1
5.2100 5.2171 -.0071 0 -1 1
4.3900 4.3914 -.0014 -1 -1 1
3.9100 3.9078 .0022 0 1 1
3.7300 3.7302 -.0002 2 1 0
3.5500 3.5489 .0011 0 -2 1
3.4100 3.4074 .0026 2 0 1
3.1500 3.1511 -.0011 2 -1 1
3.0200 3.0211 -.0011 2 1 1
2.7900 2.7906 -.0006 0 0 2
A= 8.079 DA= .001
B= 7.637 DB= .002
C= 5.844 DC= .001
GAMMA= 83.040 DGAMMA= .008
BETA = 86.62 DBETA = .01
ALPHA=106.33 DALPHA= .01
V= 341.8