240 22-0507
{NH4}4{ZnH6Mo6O24}*5H2O
Triklin
Dexp Dcal d(D) h k l
11.0000 11.0006 -.0006 1 0 0
7.9900 7.9889 .0011 0 1 0
7.2200 7.2215 -.0015 1 0 1
5.7500 5.7498 .0002 1 1 0
5.4800 5.4786 .0014 -1 -1 1
5.1200 5.1212 -.0012 -2 0 1
4.9900 4.9854 .0046 -1 0 2
3.7500 3.7505 -.0005 -3 1 0
3.1300 3.1300 -.0000 -2 0 3
3.0400 3.0399 .0001 0 1 3
2.7800 2.7800 -.0000 1 -3 1
2.7100 2.7099 .0001 -2 3 0
2.6400 2.6403 -.0003 0 0 4
1.8600 1.8600 -.0000 4 1 3
A= 11.4789 DA= .0001
B= 8.4004 DB= .0002
C= 10.7376 DC= .0005
GAMMA=105.319 DGAMMA= .002
BETA = 94.04910 DBETA = .00006
ALPHA= 98.156 DALPHA= .005
V= 982.2
241. 22-0874
K2Zn{NH2}4
Triklin
Dexp Dcal d(D) h k l
7.6200 7.6193 .0007 -2 0 1
6.4600 6.4562 .0038 0 1 0
5.8200 5.8230 -.0030 0 1 1
5.2400 5.2376 .0024 -2 1 1
4.8500 4.8449 .0051 -2 0 2
4.6300 4.6374 -.0074 2 1 1
4.3500 4.3538 -.0038 -3 0 2
4.1800 4.1789 .0011 -2 1 2
3.8100 3.8097 .0003 -4 0 2
3.6900 3.6910 -.0010 0 -1 2
3.6000 3.5967 .0033 -4 -1 1
3.5100 3.5109 -.0009 1 -1 2
A= 18.741 DA= .002
B= 6.53210 DB= .00005
C= 10.3356 DC= .0005
GAMMA= 92.267 DGAMMA= .004
BETA =102.895 DBETA = .006
ALPHA= 81.2669 DALPHA= .0005
V=1219.2
242. 22-1015
ZnP4
Triklin
Dexp Dcal d(D) h k l
3.4800 3.4799 .0001 -2 0 1
3.1800 3.1804 -.0004 -2 1 0
2.9360 2.9370 -.0010 0 -1 2
2.8610 2.8607 .0003 -1 -1 2
2.5320 2.5311 .0009 -2 -1 2
2.2100 2.2089 .0011 2 -2 1
2.0610 2.0611 -.0001 -3 0 2
1.9970 1.9978 -.0008 -1 -1 3
1.9140 1.9135 .0005 -1 0 3
1.8960 1.8949 .0011 1 0 3
1.7700 1.7694 .0006 -2 -2 3
1.7550 1.7551 -.0001 -2 -3 2
1.6240 1.6245 -.0005 5 0 1
1.5730 1.5731 -.0001 0 -3 3
1.5460 1.5467 -.0007 -4 1 2
A= 8.605 DA= .009
B= 5.8559 DB= .0008
C= 6.0929 DC= .0004
GAMMA= 81.50 DGAMMA= .01
BETA = 93.54 DBETA = .04
ALPHA=105.82 DALPHA= .01
V= 292.1
243. 22-1016
ZnP2
Trikln
Dexp Dcal d(D) h k l
4.2100 4.2099 .0001 -1 0 2
3.7200 3.7201 -.0001 0 2 1
3.4100 3.4099 .0001 -1 1 3
3.2100 3.2101 -.0001 -1 -1 2
3.0700 3.0696 .0004 2 0 1
2.9500 2.9501 -.0001 -1 2 3
2.4880 2.4882 -.0002 2 0 3
2.4360 2.4360 .0000 0 3 2
2.3960 2.3974 -.0014 1 -3 1
2.2920 2.2905 .0015 -2 3 0
2.2010 2.2013 -.0003 -3 1 0
2.0530 2.0518 .0012 3 -2 1
A= 6.6067 DA= .0001
B= 7.845 DB= .001
C= 11.887 DC= .002
GAMMA=107.227 DGAMMA= .007
BETA = 91.592 DBETA = .003
ALPHA= 78.608 DALPHA= .003
V= 576.5
244. 22-1018
ZnSO4*xH2O
Rombik
Groupa 16,25,47
Dexp. Dcal. d(D) h k l
4.8700 4.8494 .0206 3 0 0
3.8200 3.8212 -.0012 3 0 2
3.5000 3.4903 .0097 4 0 1
3.1400 3.1379 .0021 4 0 2
2.9200 2.9240 -.0040 0 1 1
2.7100 2.7073 .0027 0 1 2
2.5600 2.5566 .0034 3 1 0
2.3600 2.3606 -.0006 4 0 4
2.2100 2.2098 .0002 3 0 5
2.0900 2.0916 -.0016 5 1 0
1.9900 1.9898 .0002 2 0 6
1.9100 1.9106 -.0006 6 0 4
a=14.55 b= 3.009 c=12.412
da= .01 db= .004 dc= .009
V= 543.3
245. 22-1019
ZnSO4*7H2O
Rombik
Groupa 16, 25, 47
Dexp. Dcal. d(D) h k l
4.4600 4.4505 .0095 3 0 0
4.2300 4.2397 -.0097 0 1 0
4.1100 4.0994 .0106 0 0 3
3.4900 3.4904 -.0004 0 1 2
3.4400 3.4364 .0036 2 1 1
3.0900 3.0932 -.0032 2 1 2
2.9800 2.9783 .0017 3 1 1
2.8800 2.8778 .0022 1 1 3
2.7900 2.7926 -.0026 2 0 4
2.6700 2.6703 -.0003 5 0 0
a=13.351 b= 4.2397 c=12.30
da= .006 db= .0006 dc= .021031
V= 696.1
246. 22-1628
C40H32Clo8Cr2N8Zn
Triklin
Dexp Dcal d(D) h k l
9.5000 9.4733 .0267 0 1 0
8.8400 8.8288 .0112 -1 1 0
7.5600 7.5618 -.0018 1 1 0
6.8600 6.8593 .0007 2 0 1
6.6600 6.6598 .0002 -2 1 0
6.4200 6.4201 -.0001 0 1 1
5.8300 5.8300 .0000 -1 1 1
5.2600 5.2601 -.0001 3 0 0
4.7700 4.7712 -.0012 -1 2 0
4.4400 4.4401 -.0001 2 0 2
A= 16.5975 DA= .0004
B= 9.6590 DB= .0002
C= 9.409 DC= .001
GAMMA=101.005 DGAMMA= .002
BETA = 74.917 DBETA = .006
ALPHA= 95.146 DALPHA= .007
V=1430
247. 23-0622
Rb2Zn{NH2}2{NH}
Triklin
Dexp Dcal d(D) h k l
8.0500 8.0348 .0152 -1 1 0
7.5100 7.5310 -.0210 0 0 1
6.0800 6.0375 .0425 -1 0 1
4.3200 4.3212 -.0012 0 -2 1
4.0000 3.9980 .0020 -2 0 1
3.7800 3.7822 -.0022 -1 2 1
3.6700 3.6760 -.0060 2 0 1
3.5500 3.5541 -.0041 1 -1 2
3.3900 3.3905 -.0005 -2 -1 1
3.2800 3.2815 -.0015 -1 1 2
3.1900 3.1911 -.0011 -3 1 0
3.0600 3.0617 -.0017 -3 2 0
A= 9.58811 DA= .00001
B= 9.987 DB= .003
C= 7.712 DC= .004
GAMMA=111.40 DGAMMA= .09
BETA = 90.96 DBETA = .01
ALPHA=101.20 DALPHA= .07
V= 671.5
248. 23-0741
Zn2ClN
Triklin
Dexp Dcal d(D) h k l
4.6300 4.6379 -.0079 0 0 1
3.6900 3.6905 -.0005 -2 0 1
3.1600 3.1589 .0011 -2 2 0
2.9600 2.9661 -.0061 0 -2 1
2.8300 2.8328 -.0028 -3 -1 1
2.7900 2.7900 -.0000 -3 1 1
2.7200 2.7191 .0009 3 1 1
2.5100 2.5097 .0003 4 0 1
2.3600 2.3613 -.0013 -3 -2 1
2.3200 2.3189 .0011 0 0 2
2.2800 2.2803 -.0003 4 2 0
2.1900 2.1877 .0023 1 -3 1
A= 12.0258 DA= .0001
B= 7.2990 DB= .0001
C= 4.64961 DC= .00002
GAMMA= 91.8556 DGAMMA= .0002
BETA = 90.48045 DBETA = .00008
ALPHA= 94.0358 DALPHA= .0009
V=406.9
249. 23-0742
ZnHPO4*3H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
10.8000 10.8897 -.0897 0 1 0
6.3200 6.3165 .0035 1 1 0
5.4400 5.4448 -.0048 0 2 0
4.2900 4.2896 .0004 -1 1 1
3.6300 3.6299 .0001 0 3 0
3.3200 3.3134 .0066 0 0 2
3.1700 3.1699 .0001 0 1 2
3.0200 3.0150 .0050 2 2 1
2.7900 2.7904 -.0004 1 2 2
2.7500 2.7569 -.0069 2 0 2
2.6700 2.6726 -.0026 2 1 2
2.5700 2.5687 .0013 1 4 0
a= 7.865 b= 10.890 c= 6.721 beta= 80.36
da= .001 db= .003 dc=.008 dbeta=.03
V= 567.6
250. 23-0743
ZnHPO4*H2O
Triklin
Dexp Dcal d(D) h k l
12.2000 12.2025 -.0025 0 1 0
7.5500 7.5457 .0043 2 1 0
5.9000 5.9023 -.0023 2 1 1
5.3700 5.3747 -.0047 0 2 1
3.9500 3.9440 .0060 2 3 0
3.7100 3.7100 .0000 4 2 1
3.5900 3.5910 -.0010 2 -2 1
3.4900 3.4895 .0005 -1 1 2
3.3000 3.2987 .0013 -1 2 2
3.1900 3.1901 -.0001 -4 2 0
3.1300 3.1299 .0001 2 3 2
3.0300 3.0312 -.0012 -2 2 2
A= 17.1199 DA= .0001
B= 12.92558 DB= .00004
C= 7.4153 DC= .0005
GAMMA= 78.0587 DGAMMA= .0009
BETA = 82.379 DBETA = .001
ALPHA= 73.631 DALPHA= .002
V=1534.7
251. 23-0744
Zn{H2PO4}2*2H2O
Triklin
Dexp Dcal d(D) h k l
15.8000 15.8413 -.0413 1 0 0
7.7000 7.6855 .0145 1 1 0
6.5500 6.5482 .0018 0 0 1
6.0200 6.0168 .0032 -1 0 1
5.7200 5.7200 .0000 0 -1 1
5.1000 5.1046 -.0046 0 1 1
5.0100 5.0066 .0034 -2 0 1
4.7400 4.7352 .0048 0 2 0
4.3800 4.3780 .0020 1 2 0
3.8400 3.8425 -.0025 -4 1 0
3.7900 3.7880 .0020 -3 2 0
3.7100 3.7072 .0028 -3 -1 1
A= 15.996 DA= .007
B= 9.632 DB= .004
C= 6.600 DC= .002
GAMMA= 97.92 DGAMMA= .02
BETA = 88.109 DBETA = .04
ALPHA= 97.16 DALPHA= .02
V= 999.3
252. 23-0745
Zn2IN
Triklin
Dexp Dcal d(D) h k l
3.8800 3.8854 -.0054 1 0 2
3.3700 3.3688 .0012 0 1 1
3.1700 3.1687 .0013 0 -1 1
3.1100 3.1106 -.0006 1 1 0
2.9800 2.9803 -.0003 1 1 1
2.9400 2.9394 .0006 0 1 2
2.8200 2.8205 -.0005 1 0 3
2.6400 2.6346 .0054 1 1 2
2.4900 2.4906 -.0006 -2 -1 1
2.4600 2.4607 -.0007 2 1 1
2.3000 2.2972 .0028 -3 1 0
2.1400 2.1422 -.0022 3 -1 1
A= 8.593 DA= .008
B= 3.515 DB= .001
C= 9.657 DC= .003
GAMMA= 96.48 DGAMMA= .07
BETA = 99.49 DBETA = .07
ALPHA= 83.618 DALPHA= .006
V= 284.6
253. 23-0751
C4H4O6Zn*2H2O
Triklin
Dexp Dcal d(D) h k l
5.0300 5.0323 -.0023 0 1 1
4.9800 4.9793 .0007 1 1 0
4.7700 4.7717 -.0017 0 -1 1
4.0700 4.0689 .0011 -1 1 1
2.6300 2.6299 .0001 1 3 0
2.6200 2.6201 -.0001 2 -3 1
2.4800 2.4801 -.0001 -2 -1 1
2.3700 2.3700 -.0000 1 2 2
1.8600 1.8600 -.0000 -2 -3 1
1.8100 1.8100 .0000 2 -1 3
1.7400 1.7400 .0000 2 4 1
1.7100 1.7100 .0000 3 2 2
A= 7.40188 DA= .00005
B= 10.0758 DB= .0008
C= 5.7855 DC= .0002
GAMMA=106.988 DGAMMA= .001
BETA = 80.1230 DBETA = .0002
ALPHA= 89.605 DALPHA= .002
V= 405.8
254. 23-0919
CsZn{NH2}NH
Triklin
Dexp Dcal d(D) h k l
4.5400 4.5464 -.0064 -1 1 1
4.2900 4.2941 -.0041 1 -1 1
4.1300 4.1290 .0010 1 0 2
3.9700 3.9692 .0008 1 1 2
3.8400 3.8452 -.0052 0 0 2
3.7100 3.7077 .0023 2 -1 1
3.5000 3.5014 -.0014 3 0 1
3.2700 3.2660 .0040 3 0 0
3.1700 3.1662 .0038 0 2 1
3.0600 3.0635 -.0035 1 2 1
2.9950 2.9928 .0022 -3 1 0
2.8450 2.8433 .0017 -2 -1 1
A= 10.528 DA= .005
B= 6.368 DB= .001
C= 8.613 DC= .001
GAMMA= 88.90 DGAMMA= .04
BETA = 69.16 DBETA = .02
ALPHA= 73.58 DALPHA= .01
V=515.4
255. 23-0920
Cs2Zn{NH}2
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
4.4000 4.4000 .0000 -2 1 2
3.9000 3.8976 .0024 2 0 2
3.5100 3.5101 -.0001 1 3 0
3.4300 3.4326 -.0026 -3 0 2
3.1900 3.1901 -.0001 -3 0 3
3.0900 3.0898 .0002 3 1 1
2.9280 2.9285 -.0005 -2 2 4
2.8650 2.8655 -.0005 1 2 4
2.7910 2.7916 -.0006 -3 1 4
2.5930 2.5920 .0010 -1 4 2
2.4610 2.4614 -.0004 2 4 0
2.3460 2.3468 -.0008 2 1 5
a= 10.597 b= 11.195 c= 15.55 beta= 102.55
da= .008 db= .002 dc=.01 dbeta=.07
V= 1801
Triklin
Dexp Dcal d(D) h k l
4.4000 4.3997 .0003 0 0 1
3.9000 3.9001 -.0001 -1 0 1
3.5100 3.5108 -.0008 0 -2 1
3.4300 3.4308 -.0008 -1 2 1
3.1900 3.1907 -.0007 -1 -2 1
3.0900 3.0911 -.0011 -2 0 1
2.9280 2.9253 .0027 2 3 0
2.8650 2.8649 .0001 1 4 0
2.7910 2.7890 .0020 -3 2 0
2.5930 2.5963 -.0033 -2 3 1
2.4610 2.4610 -.0000 2 4 0
2.3460 2.3466 -.0006 -3 2 1
A= 9.010 DA= .003
B= 12.4976 DB= .0009
C= 4.4069 DC= .0003
GAMMA= 94.74 DGAMMA= .04
BETA = 88.353 DBETA = .005
ALPHA= 87.31 DALPHA= .01
V= 493.7
256. 23-1370
K2Zn{NH2}4
Triklin
Dexp Dcal d(D) h k l
7.6200 7.6294 -.0094 0 1 1
6.4600 6.4745 -.0145 1 1 0
5.8200 5.8127 .0073 1 -2 1
5.2400 5.2504 -.0104 -1 3 0
4.8500 4.8545 -.0045 -1 0 1
4.6300 4.6222 .0078 0 4 0
4.3500 4.3540 -.0040 1 3 0
4.1800 4.1784 .0016 1 -1 2
3.8100 3.8097 .0003 2 -2 1
3.6900 3.6896 .0004 -2 2 0
3.6000 3.5964 .0036 -1 4 1
3.5100 3.5103 -.0003 2 1 0
A= 7.922 DA= .001
B= 18.841 DB= .001
C= 8.718 DC= .002
GAMMA=101.06 DGAMMA= .03
BETA = 72.39 DBETA = .01
ALPHA= 92.36 DALPHA= .03
V=1217.1
257. 23-1371
K2Zn{NH2}2NH
Triklin
Dexp Dcal d(D) h k l
9.1600 9.1541 .0059 0 1 1
6.6400 6.6397 .0003 -1 -1 1
6.2100 6.2041 .0059 0 -1 1
5.8200 5.8117 .0083 2 1 0
5.6200 5.6130 .0070 0 2 0
5.2700 5.2759 -.0059 -2 -1 1
4.9600 4.9610 -.0010 -1 0 2
4.8500 4.8490 .0010 -1 2 1
4.2000 4.1956 .0044 0 -2 1
3.9500 3.9503 -.0003 1 0 2
3.8400 3.8387 .0013 -3 0 1
3.7400 3.7420 -.0020 0 3 0
A= 11.99472 DA= .00003
B= 12.57387 DB= .00008
C= 10.49262 DC= .00002
GAMMA= 74.4339 DGAMMA= .0001
BETA =101.6346 DBETA = .0003
ALPHA= 72.5361 DALPHA= .0002
V=1383.7
258. 23-1492
ZnBeF4*6H2O
Triklin
Dexp Dcal d(D) h k l
5.9300 5.9519 -.0219 1 0 0
5.7800 5.7798 .0002 0 1 0
5.5500 5.5405 .0095 -1 0 1
5.4300 5.4120 .0180 0 -1 1
5.0700 5.0722 -.0022 0 1 1
4.9100 4.9118 -.0018 1 1 0
4.8000 4.7984 .0016 -1 -1 1
4.4700 4.4692 .0008 -1 0 2
4.4000 4.4070 -.0070 0 -1 2
4.3600 4.3599 .0001 1 1 1
4.1200 4.1185 .0015 1 0 2
4.0500 4.0507 -.0007 0 1 2
A= 6.253 DA= .003
B= 6.073 DB= .001
C= 12.458 DC= .004
GAMMA= 72.76 DGAMMA= .03
BETA = 96.37 DBETA = .01
ALPHA= 96.488 DALPHA= .005
V=447.1
259. 23-1498
ZnPbO3
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
10.4000 10.3996 .0004 -2 0 1
5.2000 5.1998 .0002 -4 0 2
3.9100 3.9114 -.0014 1 1 3
3.8000 3.7996 .0004 6 0 1
3.7100 3.7131 -.0031 2 1 3
3.5700 3.5715 -.0015 -5 1 2
3.4600 3.4601 -.0001 7 0 0
3.1800 3.1788 .0012 4 0 4
3.0800 3.0760 .0040 -6 0 4
2.7410 2.7408 .0002 -6 1 4
2.7190 2.7188 .0002 -2 0 6
a= 24.4428 b= 6.037 c= 16.378 beta= 97.723
da= .0003 db= .0004 dc=.001 dbeta=.002
V= 2394.8
Triklin
Dexp Dcal d(D) h k l
10.4000 10.3880 .0120 1 0 0
5.2000 5.1992 .0008 -1 1 1
3.9100 3.9154 -.0054 1 -1 1
3.8000 3.8048 -.0048 -1 2 0
3.7100 3.7083 .0017 2 1 0
3.5700 3.5688 .0012 2 0 1
3.4600 3.4627 -.0027 3 0 0
3.1800 3.1813 -.0013 -3 0 1
3.0800 3.0823 -.0023 2 1 1
2.7410 2.7398 .0012 3 -1 1
2.7190 2.7163 .0027 -4 1 1
2.6370 2.6370 .0000 1 0 2
A= 11.220 DA= .003
B= 7.8564 DB= .0008
C= 5.9267 DC= .0004
GAMMA=110.45 DGAMMA= .07
BETA =103.03 DBETA = .02
ALPHA= 75.78 DALPHA= .01
V= 468.9
260. 23-1970
C10H14O4Zn
Triklin
Dexp Dcal d(D) h k l
10.6000 10.5958 .0042 1 0 0
7.8300 7.8317 -.0017 1 1 0
7.2000 7.2053 -.0053 -1 0 1
6.0300 6.0396 -.0096 -1 -1 1
5.5000 5.5012 -.0012 1 1 2
4.9000 4.8955 .0045 -1 1 1
4.3900 4.3899 .0001 1 -1 2
4.0400 4.0411 -.0011 0 2 0
3.8700 3.8703 -.0003 -2 1 0
3.6500 3.6497 .0003 3 0 1
3.5300 3.5307 -.0007 -2 1 1
3.0200 3.0198 .0002 -2 -2 2
2.6500 2.6498 .0002 -2 -3 1
2.4700 2.4700 -.0000 -4 -2 1
A= 11.744 DA= .005
B= 8.6710 DB= .0009
C= 12.95 DC= .02
GAMMA= 68.88 DGAMMA= .01
BETA = 73.53 DBETA = .04
ALPHA= 82.18 DALPHA= .02
V= 1178.7
261. 23-1972
C8H16N4O2*ZnCl2
Triklin
Dexp Dcal d(D) h k l
9.0200 9.0305 -.0105 0 1 1
7.6200 7.6202 -.0002 0 -1 1
7.0200 7.0079 .0121 1 1 0
6.1900 6.2019 -.0119 0 0 2
6.0600 6.0582 .0018 1 1 1
5.8200 5.8439 -.0239 0 1 2
4.9000 4.9146 -.0146 1 2 0
4.8200 4.8199 .0001 -1 1 2
4.4800 4.4723 .0077 -1 -2 1
4.2700 4.2709 -.0009 -1 2 1
4.1100 4.1065 .0035 0 1 3
3.9800 3.9774 .0026 1 2 2
A= 8.116 DA= .008
B= 11.289 DB= .009
C= 12.67 DC= .01
GAMMA= 81.90 DGAMMA= .09
BETA = 96.73 DBETA = .01
ALPHA= 81.378 DALPHA= .004
V= 1125.1
262. 23-1976
C8H12F2N4O6S2Zn
Triklin
Dexp Dcal d(D) h k l
9.0600 9.0352 .0248 1 1 0
8.1800 8.1814 -.0014 0 1 1
7.4300 7.4385 -.0085 0 -1 1
6.8600 6.8495 .0105 1 0 1
6.2800 6.2731 .0069 1 -1 1
5.9400 5.9353 .0047 -1 0 1
5.6900 5.6840 .0060 -1 3 0
5.3700 5.3756 -.0056 -1 2 1
4.2100 4.2086 .0014 0 1 2
3.8500 3.8508 -.0008 -1 -4 1
3.6500 3.6513 -.0013 -1 0 2
3.5500 3.5497 .0003 -2 4 0
A= 9.886 DA= .004
B= 21.851 DB= .004
C= 8.527 DC= .001
GAMMA= 86.441 DGAMMA= .002
BETA = 81.297 DBETA = .006
ALPHA= 81.458 DALPHA= .005
V= 1799.1
263. 23-1977
C82H77N19Zn2
Triklin
Dexp Dcal d(D) h k l
12.3000 12.2972 .0028 1 0 0
11.9000 11.8758 .0242 -1 1 0
9.7800 9.7779 .0021 -1 1 1
8.7500 8.7503 -.0003 -1 -1 1
8.2200 8.2252 -.0052 -1 2 1
7.5900 7.5929 -.0029 0 2 1
7.0800 7.0741 .0059 -1 -2 1
6.1900 6.1993 -.0093 1 1 1
6.0100 6.0118 -.0018 1 3 0
5.7100 5.7116 -.0016 -1 -3 1
5.5800 5.5801 -.0001 -2 3 1
5.5000 5.4936 .0064 1 2 1
A= 13.724 DA= .009
B= 23.64 DB= .01
C= 11.132 DC= .002
GAMMA=102.21 DGAMMA= .06
BETA =113.92 DBETA = .06
ALPHA= 85.67 DALPHA= .02
V=3225.4
264. 23-1979
C22H38O4Zn
Triklin
Dexp Dcal d(D) h k l
9.6100 9.6101 -.0001 -1 1 0
6.2500 6.2488 .0012 -1 1 1
5.3400 5.3396 .0004 -1 -1 1
4.8200 4.8196 .0004 -1 2 1
4.6800 4.6794 .0006 2 -2 1
4.4500 4.4499 .0001 -2 1 1
4.0100 4.0085 .0015 -2 2 1
3.5900 3.5894 .0006 -3 2 0
3.2400 3.2405 -.0005 2 2 1
2.9500 2.9497 .0003 0 3 2
2.8800 2.8806 -.0006 -3 3 1
2.7600 2.7601 -.0001 2 -4 2
2.6300 2.6299 .0001 2 3 1
2.5800 2.5800 .0000 1 4 0
2.4900 2.4901 -.0001 -1 4 2
A= 11.3616 DA= .0004
B= 12.493 DB= .003
C= 9.893 DC= .009
GAMMA=111.18 DGAMMA= .02
BETA = 78.95 DBETA = .01
ALPHA= 96.876 DALPHA= .002
V= 1283.1
265. 23-1980
C5H5NO8Re2Zn
Monoklin
GRUPA 3
Dexp. Dcal. d(D) h k l
9.8000 9.8364 -.0364 0 1 0
8.0000 8.0099 -.0099 0 1 1
7.3000 7.2902 .0098 1 1 1
6.6000 6.6055 -.0055 2 0 1
4.2500 4.2476 .0024 2 0 3
4.1700 4.1669 .0031 0 1 3
3.9600 3.9603 -.0003 2 2 0
3.8500 3.8482 .0018 3 1 2
3.6200 3.6197 .0003 3 0 3
3.4500 3.4501 -.0001 0 0 4
3.3400 3.3395 .0005 4 0 0
3.1300 3.1310 -.0010 4 1 2
a= 13.690 b= 9.84 c= 14.143 beta= 77.35
da=.001 db= .03 dc=.003 dbet=.01
V=1858.5
266. 23-1981
C15H11Cl2N3Zn
Triklin
Dexp Dcal d(D) h k l
11.0000 10.9477 .0523 0 1 1
8.1100 8.1006 .0094 0 -1 1
7.3700 7.3804 -.0104 1 0 0
7.0200 7.0041 .0159 -1 1 1
6.7000 6.7100 -.0100 -1 0 1
6.2600 6.2628 -.0028 1 0 1
5.7200 5.7198 .0002 1 -1 1
5.4700 5.4738 -.0038 0 2 2
5.1600 5.1586 .0014 0 -2 1
4.3400 4.3381 .0019 1 2 1
4.2000 4.2006 -.0006 0 3 0
4.2000 4.2006 -.0006 0 3 0
A= 7.655 DA= .001
B= 13.625 DB= .001
C= 14.285 DC= .004
GAMMA=104.68 DGAMMA= .01
BETA = 98.977 DBETA = .007
ALPHA= 71.370 DALPHA= .002
V=1362.1
267. 24-0676
Li1.6Zn1.2SiO4
Triklin
Dexp Dcal d(D) h k l
8.2000 8.2234 -.0234 1 0 0
6.4500 6.4333 .0167 0 1 1
5.6000 5.6066 -.0066 0 -1 1
5.5000 5.4950 .0050 -1 0 1
5.3000 5.3004 -.0004 1 0 2
4.6000 4.6064 -.0064 -1 1 1
4.4300 4.4184 .0116 2 0 1
4.1200 4.1117 .0083 2 0 0
4.0600 4.0462 .0138 1 -1 2
4.0000 4.0016 -.0016 2 0 2
3.7600 3.7634 -.0034 -1 0 2
3.7100 3.7188 -.0088 2 -1 1
A= 8.84965 DA= .00001
B= 7.4534 DB= .0001
C= 11.11026 DC= .00003
GAMMA= 87.790 DGAMMA= .001
BETA = 68.3435 DBETA = .0003
ALPHA= 81.4922 DALPHA= .0007
V=673.5
268. 24-0677
Li2ZnSiO4
Triklin
Dexp Dcal d(D) h k l
5.4500 5.4539 -.0039 2 1 1
5.4000 5.4043 -.0043 2 -1 1
4.6000 4.6029 -.0029 -2 1 1
4.0900 4.0866 .0034 0 2 0
3.9800 3.9786 .0014 2 1 3
3.9700 3.9675 .0025 -2 -1 1
3.7100 3.7097 .0003 0 2 2
3.6900 3.6908 -.0008 -2 0 2
3.1750 3.1734 .0016 2 2 3
3.1700 3.1700 .0000 2 -2 2
3.0900 3.0909 -.0009 3 0 4
2.9000 2.8997 .0003 0 0 4
A= 14.7576 DA= .0008
B= 8.346 DB= .004
C= 12.954 DC= .007
GAMMA= 91.54 DGAMMA= .09
BETA = 66.07 DBETA = .04
ALPHA= 80.07 DALPHA= .05
V=1427.8
269. 24-0682
Li2ZnSiO4
Triklin
Dexp Dcal d(D) h k l
5.4500 5.4600 -.0100 2 0 0
4.1200 4.1219 -.0019 -2 1 1
3.9600 3.9607 -.0007 -2 -1 1
3.9300 3.9217 .0083 -2 2 0
3.6800 3.6817 -.0017 2 0 1
3.1800 3.1793 .0007 -3 2 0
3.1700 3.1722 -.0022 3 1 0
2.7200 2.7192 .0008 0 1 2
2.6800 2.6793 .0007 -4 1 1
2.5000 2.5015 -.0015 1 1 2
2.4700 2.4698 .0002 -3 -1 2
2.3900 2.3892 .0008 -2 2 2
A= 11.31834 DA= .00004
B= 9.43179 DB= .00004
C= 6.13376 DC= .00001
GAMMA=100.1467 DGAMMA= .0002
BETA = 99.98737 DBETA = .00003
ALPHA= 96.75024 DALPHA= .00001
V=627.4
270. 24-0684
Li3.6Zn0.2SiO4
Triklin
Dexp Dcal d(D) h k l
7.5000 7.4848 .0152 0 1 1
5.8000 5.8045 -.0045 0 -1 1
5.3500 5.3430 .0070 1 1 0
5.2500 5.2441 .0059 1 1 1
4.0300 4.0281 .0019 1 1 2
3.9700 3.9793 -.0093 -2 1 0
3.8800 3.8737 .0063 -1 1 2
3.7100 3.7069 .0031 1 2 1
3.6900 3.6861 .0039 -1 0 2
3.4600 3.4652 -.0052 -1 2 2
3.4000 3.3980 .0020 -2 0 1
3.1800 3.1773 .0027 2 -2 1
A= 8.141 DA= .009
B= 9.739 DB= .009
C= 9.500 DC= .002
GAMMA=102.57 DGAMMA= .09
BETA = 83.475 DBETA = .004
ALPHA= 77.49 DALPHA= .08
V= 707.4
271. 24-0684
Li3.6Zn0.2SiO4
Triklin
Dexp Dcal d(D) h k l
7.5000 7.4848 .0152 0 1 1
5.8000 5.8045 -.0045 0 -1 1
5.3500 5.3430 .0070 1 1 0
5.2500 5.2441 .0059 1 1 1
4.0300 4.0281 .0019 1 1 2
3.9700 3.9793 -.0093 -2 1 0
3.8800 3.8737 .0063 -1 1 2
3.7100 3.7069 .0031 1 2 1
3.6900 3.6861 .0039 -1 0 2
3.4600 3.4652 -.0052 -1 2 2
3.4000 3.3980 .0020 -2 0 1
3.1800 3.1773 .0027 2 -2 1
A= 8.141 DA= .009
B= 9.739 DB= .009
C= 9.500 DC= .002
GAMMA=102.57 DGAMMA= .09
BETA = 83.475 DBETA = .004
ALPHA= 77.49 DALPHA= .08
V= 707.4
272. 24-0687
Li3.82Zn0.009SiO4
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.3000 5.3056 -.0056 -2 0 1
5.3000 5.2892 .0108 1 1 1
5.2000 5.2027 -.0027 2 1 0
4.0400 4.0334 .0066 -1 0 2
3.9800 3.9739 .0061 0 0 2
3.7000 3.7048 -.0048 3 1 0
3.6800 3.6783 .0017 0 3 0
3.1700 3.1659 .0041 -3 2 1
3.0600 3.0595 .0005 -2 2 2
2.6850 2.6863 -.0013 1 4 0
2.6500 2.6493 .0007 0 0 3
2.5800 2.5793 .0007 -4 1 2
a= 12.073 b= 11.035 c= 8.132 beta= 102.23
da= .001 db=.001 dc=.008 dbeta=.06
V= 1058.9
Triklin
Dexp Dcal d(D) h k l
5.3000 5.3001 -.0001 1 0 1
5.2000 5.2019 -.0019 -1 1 0
4.0400 4.0441 -.0041 1 -1 2
3.9800 3.9825 -.0025 1 1 0
3.7000 3.7009 -.0009 1 1 1
3.6800 3.6814 -.0014 0 1 2
3.1700 3.1687 .0013 0 2 1
3.0600 3.0585 .0015 1 -1 3
2.6850 2.6885 -.0035 2 -2 1
2.6500 2.6500 -.0000 2 0 2
2.5800 2.5814 -.0014 1 2 1
2.5600 2.5565 .0035 0 -2 3
A= 6.1062 DA= .0001
B= 7.528 DB= .005
C= 9.766 DC= .002
GAMMA=107.34 DGAMMA= .03
BETA = 77.992 DBETA = .001
ALPHA=101.79 DALPHA= .01
V= 414.3
273. 24-1166
Na2Zn{NH}2
Triklin
Dexp Dcal d(D) h k l
8.3800 8.3754 .0046 -1 0 1
6.2800 6.2783 .0017 0 1 0
5.2100 5.2152 -.0052 -1 1 0
4.4200 4.4182 .0018 -1 -1 2
4.1000 4.1004 -.0004 0 -1 2
3.9500 3.9489 .0011 -2 -1 2
3.1900 3.1915 -.0015 -3 -1 2
3.1400 3.1392 .0008 0 2 0
3.0100 3.0096 .0004 1 2 0
2.9600 2.9601 -.0001 0 0 3
2.9000 2.8992 .0008 0 -2 2
2.8130 2.8141 -.0011 -3 -1 3
A= 10.642 DA= .003
B= 6.5077 DB= .0005
C= 9.987 DC= .002
GAMMA= 82.63 DGAMMA= .02
BETA =113.93 DBETA = .01
ALPHA=105.20 DALPHA= .06
V= 609.9
274. 24-1171
gamma-Na2Zn{SO4}2
Triklin
Dexp Dcal d(D) h k l
8.4900 8.4841 .0059 1 0 0
8.3000 8.3012 -.0012 0 1 0
6.0700 6.0774 -.0074 -1 0 1
5.1500 5.1505 -.0005 0 0 2
4.4500 4.4468 .0032 1 2 0
4.4100 4.4034 .0066 0 1 2
4.3500 4.3501 -.0001 0 -1 2
3.8900 3.8933 -.0033 -2 -1 1
3.8400 3.8318 .0082 0 -2 1
3.7600 3.7597 .0003 2 1 2
3.3800 3.3818 -.0018 1 0 3
3.3300 3.3276 .0024 1 1 3
A= 9.314 DA= .004
B= 8.990 DB= .005
C= 10.48 DC= .01
GAMMA= 67.44 DGAMMA= .01
BETA = 79.47 DBETA = .05
ALPHA= 85.28 DALPHA= .03
V= 796.5
275. 24-1454
In16S41Zn17
Triklin
Dexp Dcal d(D) h k l
6.2200 6.2098 .0102 1 0 0
3.7300 3.7311 -.0011 1 1 1
3.3300 3.3294 .0006 1 1 2
3.2000 3.1973 .0027 0 1 3
3.0800 3.0807 -.0007 1 0 3
3.0150 3.0151 -.0001 -2 1 1
2.8650 2.8637 .0013 -2 0 1
2.7920 2.7917 .0003 2 0 2
2.6650 2.6662 -.0012 2 -1 2
2.4150 2.4175 -.0025 2 0 3
2.3850 2.3862 -.0012 2 -2 1
2.3650 2.3637 .0013 1 -2 2
A= 6.533 DA= .001
B= 6.129 DB= .002
C= 10.207 DC= .002
GAMMA=106.69 DGAMMA= .05
BETA = 86.69 DBETA = .03
ALPHA= 78.30 DALPHA= .08
V= 380.4
276. 26-1994
C6H8O4S2Zn
Triklin
Dexp Dcal d(D) h k l
6.0200 6.0185 .0015 0 1 1
5.0600 5.0576 .0024 0 -1 1
4.7700 4.7711 -.0011 -1 0 1
4.1100 4.1134 -.0034 0 0 2
3.5600 3.5586 .0014 1 1 1
3.4200 3.4234 -.0034 -1 0 2
3.2100 3.2102 -.0002 1 0 2
3.1200 3.1178 .0022 1 -2 1
2.9600 2.9591 .0009 -2 1 0
2.6600 2.6606 -.0006 -1 1 3
2.5300 2.5296 .0004 -1 0 3
2.3500 2.3501 -.0001 1 2 2
A= 5.9799 DA= .0005
B= 7.962 DB= .001
C= 8.430 DC= .001
GAMMA=110.659 DGAMMA= .004
BETA = 97.766 DBETA = .002
ALPHA= 77.98 DALPHA= .01
V= 366.5
277. 26-1995
C6H12O4S3Zn
Triklin
Dexp Dcal d(D) h k l
6.9100 6.9153 -.0053 0 -1 1
4.5300 4.5349 -.0049 1 0 0
4.1500 4.1544 -.0044 0 -3 1
3.9000 3.9001 -.0001 -1 2 0
3.5900 3.5869 .0031 -1 -2 1
3.4000 3.4014 -.0014 -1 2 1
3.2500 3.2503 -.0003 0 -4 1
3.0400 3.0403 -.0003 -1 0 2
2.9000 2.8995 .0005 -1 3 1
2.7600 2.7587 .0013 -1 4 0
2.5500 2.5495 .0005 1 0 2
2.3800 2.3801 -.0001 0 -5 2
2.2300 2.2302 -.0002 0 5 1
2.0500 2.0501 -.0001 2 0 1
1.9500 1.9501 -.0001 -2 4 0
A= 4.6189 DA= .0003
B= 13.310 DB= .002
C= 7.3044 DC= .0005
GAMMA= 93.488 DGAMMA= .008
BETA = 99.20 DBETA = .04
ALPHA=104.12 DALPHA= .04
V= 427.6
278. 26-1996
C3H9N5O4Zn
Triklin
Dexp Dcal d(D) h k l
6.9400 6.9393 .0007 1 0 0
5.7500 5.7590 -.0090 -1 1 1
5.1500 5.1520 -.0020 1 0 1
4.9300 4.9243 .0057 -1 -1 1
4.5600 4.5559 .0041 0 0 2
4.3400 4.3405 -.0005 1 1 1
4.1000 4.1093 -.0093 -1 0 2
3.7900 3.7870 .0030 0 3 0
3.5100 3.5086 .0014 -1 2 2
3.2900 3.2926 -.0026 1 -2 2
3.1900 3.1890 .0010 2 -1 1
3.0800 3.0820 -.0020 -2 -1 1
A= 7.2632 DA= .0002
B= 11.768 DB= .004
C= 9.2226 DC= .0004
GAMMA=104.79 DGAMMA= .04
BETA = 98.33 DBETA = .01
ALPHA= 90.89 DALPHA= .01
V= 753.0
279. 26-1997
C36H24Cl2N6O11Zn
Monoklin
GRUPA 3
Dexp. Dcal. d(D) h k l
11.8000 11.6857 .1143 0 0 2
9.9300 10.0689 -.1389 1 0 1
6.3200 6.3171 .0029 1 1 1
5.3300 5.3230 .0070 -1 1 2
4.2900 4.2777 .0123 2 1 2
3.9500 3.9402 .0098 -2 0 3
3.8300 3.8319 -.0019 0 2 2
3.6800 3.6809 -.0009 -1 2 1
3.5000 3.5086 -.0086 1 1 6
3.4000 3.3997 .0003 3 0 0
2.8400 2.8401 -.0001 3 0 6
2.8100 2.8081 .0019 1 2 6
2.7700 2.7699 .0001 2 0 8
2.5100 2.5088 .0012 1 1 9
a= 10.38 b= 8.112 c= 23.797 beta= 79.1
da= .04 db=.005 dc=.002 dbet= .4
V=1958
Triklin
Dexp Dcal d(D) h k l
11.8000 12.0853 -.2853 0 0 1
9.9300 9.9004 .0296 -1 0 1
6.3200 6.3271 -.0071 0 1 1
5.3300 5.3330 -.0030 0 -1 1
4.2900 4.2959 -.0059 -1 0 3
4.2100 4.2093 .0007 -2 1 2
3.9500 3.9450 .0050 -2 0 3
3.8300 3.8297 .0003 2 1 1
3.6800 3.6818 -.0018 -3 0 2
3.5000 3.5002 -.0002 1 -1 2
3.4000 3.3990 .0010 1 0 3
2.8400 2.8401 -.0001 0 2 3
2.8100 2.8099 .0001 1 -2 1
2.7700 2.7702 -.0002 -3 1 4
2.5100 2.5099 .0001 -2 2 4
A= 11.4096 DA= .0006
B= 6.702 DB= .001
C= 13.1557 DC= .0005
GAMMA= 91.56 DGAMMA= .02
BETA =110.300 DBETA = .08
ALPHA= 78.5476 DALPHA= .0003
V= 923.8
280. 26-1998
C30H30B2F8N6O6Zn
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
9.5400 9.5675 -.0275 1 0 1
7.2100 7.1996 .0104 1 1 0
6.2800 6.2784 .0016 1 1 1
4.6900 4.6896 .0004 1 1 2
4.4200 4.4198 .0002 -2 0 2
4.0000 3.9960 .0040 1 2 0
3.7600 3.7589 .0011 -1 0 3
3.6000 3.5998 .0002 2 2 0
3.1200 3.1192 .0008 -4 1 1
2.9700 2.9708 -.0008 1 0 4
2.8500 2.8521 -.0021 1 2 3
2.8000 2.7999 .0001 -4 1 2
2.5300 2.5311 -.0011 3 2 3
2.4500 2.4516 -.0016 -4 1 3
2.3500 2.3493 .0007 -2 3 2
2.2500 2.2492 .0008 5 2 2
2.2100 2.2099 .0001 -4 0 4
2.0800 2.0802 -.0002 0 4 0
1.9900 1.9900 -.0000 7 0 2
1.8800 1.8795 .0005 -2 0 6
a= 14.4081 b= 8.321 c= 11.980 beta= 85.39
da= .0004 db=.002 dc=.003 dbeta=.01
V= 1431.6
281. 26-1999
C10H10Cl2N2S2Zn
Triklin
Dexp Dcal d(D) h k l
13.5000 13.4531 .0469 1 0 0
12.4000 12.4178 -.0178 0 1 0
10.8000 10.8015 -.0015 0 0 1
10.0000 10.0029 -.0029 0 -1 1
8.2700 8.2484 .0216 -1 -1 1
7.0000 7.0503 -.0503 0 1 1
6.6800 6.7266 -.0466 2 0 0
6.3500 6.3310 .0190 2 1 0
6.0600 6.0553 .0047 -1 -2 1
5.7300 5.7304 -.0004 -2 -1 1
5.4000 5.4007 -.0007 0 0 2
4.9200 4.9261 -.0061 -2 -2 1
A= 13.61 DA= .01
B= 13.325 DB= .005
C= 11.486 DC= .001
GAMMA= 82.21 DGAMMA= .02
BETA = 88.72 DBETA = .03
ALPHA=109.47 DALPHA= .03
V= 1941.4